Datos Obtenidos de la Experiencia

% BARRIDOS
Fase organica 10
fase acuosa 15

PULSACIONES REFINADO EXTRACTO TITULACION DE REFINADO (Agua :50 ml)

V refinado (mt refinado (s)V extracto (mt extracto (s) V refinado (mV NaOH (ml)
0 31 37 35 37 10 8.005
26 25 31.5 25 10 8.04
10 25.5 23 21 23 10 7.39
26 21 20 21 10 7.13
15 25.5 17 13 17 10 7.005
25 21 23.5 21 10 7.06

% BARRIDOS
Fase organica 15
fase acuosa 15

PULSACIONES REFINADO EXTRACTO TITULACION DE REFINADO (Agua :50 ml)

V refinado (mt refinado (s)V extracto (mt extracto (s) V refinado (mV NaOH (ml)
0 26.5 23 30 23 10 7.9
25 17.81 18.5 17.81 10 8.86
10 24 24.56 33 24.56 10 8.19
27 19 22 19 10 7.335
15 26.5 20 23 20 10 7.09
25.5 20 23 20 10 7.185

% BARRIDOS
Fase organica 15
fase acuosa 10

PULSACIONES REFINADO EXTRACTO TITULACION DE REFINADO (Agua :50 ml)

V refinado (mt refinado (s)V extracto (mt extracto (s) V refinado (mV NaOH (ml)
0 26.5 39 48 39 10 6.735
25.5 38 47 38 10 7.285
10 26 34 33 34 10 6.42
25.5 33 40 33 10 6.4
15 25.5 31 30 31 10 6.775
25.5 32 39 32 10 6.8
 Tratamiento de Datos Experimentales

% BARRIDOS
Fase organica 10
fase acuosa 15

(Agua :50 ml) PULSACIONEREFINADO EXTRACTO TITULACION DE REFINADO (Agua

Q (ml/s) Q prom (ml/sQ (ml/s) Q prom (ml/sV NaOH prom
0 0.83783784 0.93891892 0.94594595 1.10297297 8.0225
1.04 1.26
10 1.10869565 1.17339545 0.91304348 0.93271222 7.26
1.23809524 0.95238095
15 1.5 1.3452381 0.76470588 0.94187675 7.0325
1.19047619 1.11904762

% BARRIDOS
Fase organica 15
fase acuosa 15

(Agua :50 ml) PULSACIONEREFINADO EXTRACTO TITULACION DE REFINADO (Agua

Q (ml/s) Q prom (ml/sQ (ml/s) Q prom (ml/sV NaOH prom
0 1.15217391 1.27793985 1.30434783 1.17154505 8.38
1.40370578 1.03874228
10 0.9771987 1.19912566 1.34364821 1.25077147 7.7625
1.42105263 1.15789474
15 1.325 1.3 1.15 1.15 7.1375
1.275 1.15

% BARRIDOS
Fase organica 15
fase acuosa 10

PULSACIONEREFINADO EXTRACTO TITULACION DE REFINADO (Agua

(Agua :50 ml) Q (ml/s) Q prom (ml/sQ (ml/s) Q prom (ml/sV NaOH prom
0 0.67948718 0.67526991 1.23076923 1.23380567 7.01
0.67105263 1.23684211
10 0.76470588 0.76871658 0.97058824 1.09135472 6.41
0.77272727 1.21212121
15 0.82258065 0.80972782 0.96774194 1.09324597 6.7875
0.796875 1.21875
ITULACION DE REFINADO (Agua :50 ml) NORMALIZACION DEL NaOH
[ac ben] (N) [ac ben] (g/l)X (g ac ben/gX´ (gac ben/g agua)
0.00737362 0.90046664 0.00090047 0.00090128 V HCL (ml)
N HCL (eq/l)
0.00667279 0.81488162 0.00081488 0.00081555 V NaOH (ml)
N NaOH (eq/l
0.00646369 0.78934642 0.00078935 0.00078997

ITULACION DE REFINADO (Agua :50 ml)

[ac ben] (N) [ac ben(g/l)] X (g ac ben/gX´(gac ben/g agua)
0.00770221 0.94059338 0.00094059 0.00094148

0.00713465 0.87128355 0.00087128 0.00087204

0.0065602 0.80113189 0.00080113 0.00080177

ITULACION DE REFINADO (Agua :50 ml)

[ac ben] (N) [ac ben] (g/l)X (g ac ben/gX´(gac ben/g agua)
0.00644301 0.78682096 0.00078682 0.00078744

0.00589154 0.71947537 0.00071948 0.00071999

0.00623851 0.76184697 0.00076185 0.00076243

NORMALIZACION DEL NaOH

10
0.01
10.88
0.00919118
% BARRIDOS
Fase organica 10
fase acuosa 15

PULSACIONECorrida X´ Y´ (A/B) %RendimientNTU A´(g/cm2. s)

0 1 0.00090128 0.0015058 1.08462035 36.4296369 0.9391 0.04781864
10 2 0.00081555 0.00129772 1.59008402 42.4764672 1.6834 0.0597604
15 3 0.00078997 0.00123692 1.75168804 44.2807122 2.2457 0.06851225
1.62273333

Corrida 1
X Y Xi (1-Xi)
0.0009013 0.0012703 0.0007276
0.0010304 0.0011302 0.0006785 0.9991455
0.0011595 0.0009902 0.0006270 0.9991067
0.0012886 0.0008502 0.0005724 0.9990695
0.0014177 0.0007102 0.0005140 0.9990341
Corrida 2
X Y Xi (1-Xi)
0.0008156 0.0016676 0.0008561
0.0009661 0.0014283 0.0007804 0.9991267
0.0011166 0.0011889 0.0006994 0.9990920
0.0012672 0.0009495 0.0006115 0.9990607
0.0014177 0.0007102 0.0005140 0.9990341
Corrida 3
X Y Xi (1-Xi)
0.0007900 0.0018098 0.0008990
0.0009469 0.0015349 0.0008147 0.9991192
0.0011038 0.0012600 0.0007241 0.9990860
0.0012608 0.0009851 0.0006250 0.9990571
0.0014177 0.0007102 0.0005140 0.9990341

% BARRIDOS
Fase organica 15
fase acuosa 15

PULSACIONECorrida X´ Y´ (A/B) %RendimientNTU

0 4 0.00094148 0.00160483 1.34371505 33.5941933 0.8528
10 5 0.00087204 0.00143422 2.58348133 38.4920342 2.0773
15 6 0.00080177 0.00126488 1.4308422 43.4484178 1.668
1.5327
 Corrida 4
X Y Xi (1-Xi)
0.0009415 0.0013501 0.0007546
0.0010605 0.0011901 0.0006998 0.9991198
0.0011796 0.0010301 0.0006420 0.9990892
0.0012986 0.0008701 0.0005804 0.9990604
0.0014177 0.0007102 0.0005140 0.9990341
Corrida 5
X Y Xi (1-Xi)
0.0008720 0.0021199 0.0009881
0.0010085 0.0017675 0.0008864 0.9990526
0.0011449 0.0014151 0.0007761 0.9990395
0.0012813 0.0010627 0.0006540 0.9990323
0.0014177 0.0007102 0.0005141 0.9990341
Corrida 6
X Y Xi (1-Xi)
0.0008018 0.0015915 0.0008325
0.0009558 0.0013711 0.0007616 0.9991413
0.0011097 0.0011508 0.0006859 0.9991022
0.0012637 0.0009305 0.0006041 0.9990661
0.0014177 0.0007102 0.0005140 0.9990341

% BARRIDOS
Fase organica 15
fase acuosa 10

PULSACIONECorrida X´ Y´ (A/B) %RendimientNTU

0 7 0.00078744 0.00123095 1.29476995 44.4591617 1.6724
10 8 0.00071999 0.00107492 1.36043177 49.2166411 2.7499
15 9 0.00076243 0.00117235 1.5027708 46.2232026 2.4004
2.27423333

Corrida 7
X Y Xi (1-Xi)
0.0007874 0.0015262 0.0008120
0.0009450 0.0013222 0.0007452 0.9991549
0.0011026 0.0011182 0.0006742 0.9991116
0.0012601 0.0009142 0.0005977 0.9990710
0.0014177 0.0007102 0.0005140 0.9990341
Corrida 8
X Y Xi (1-Xi)
0.0007200 0.0016593 0.0008536
0.0008944 0.0014221 0.0007784 0.9991636
0.0010688 0.0011848 0.0006979 0.9991166
 0.0012433 0.0009475 0.0006107 0.9990730
0.0014177 0.0007102 0.0005140 0.9990341
Corrida 9
X Y Xi (1-Xi)
0.0007624 0.0016949 0.0008644
0.0009262 0.0014487 0.0007871 0.9991433
0.0010901 0.0012025 0.0007042 0.9991029
0.0012539 0.0009564 0.0006141 0.9990660
0.0014177 0.0007102 0.0005140 0.9990341

Nota NTU 1.8098889

 Refinado Extracto
Kya (g/s*m3) Vprom (ml) t prom (s) m ref (g/cm2.V prom (ml) t prom (s) m ext (g/cm2A
0.0002993765 28.5 31 0.04682225 33.25 31 0.04315451 0.04678009
0.000670671 25.75 22 0.05961062 20.5 22 0.03749103 0.05955694
0.0010257198 25.25 19 0.06768258 18.25 19 0.03864608 0.06762163

Área
transversal
(cm^2)
ida 1
f(X) Integral
0.9391
2842.7795933
1878.4502892 h
1396.7725053 0.0001291
1107.1206225
ida 2
f(X) Integral
1.6834
5386.1005831
2397.1949768 h
1525.5906788 0.0001505
1107.0955385
ida 3
f(X) Integral
2.2457
7565.1517425
2633.7406707 h
1573.4988998 0.0001569
1107.1013232

Refinado Extracto
A´(g/cm2. s) Kya (g/s*m3)Vprom (ml) t prom (s) m ref (g/cm2.V prom (ml) t prom (s) m ext (g/cm2
0.0650847899 0.00037003 25.75 20.405 0.06427021 24.25 20.405 0.04781579
0.0610708256 0.00084575 25.5 21.78 0.05962816 12.5 21.78 0.0230913
0.0650847899 0.00072374 26 20 0.0662083 23 20 0.04626942
ida 4
f(X) Integral
0.8528
2772.5974784
1860.5098697 h
1392.7260827 0.0001191
1107.0867196
ida 5
f(X) Integral
2.0773
8193.3954177
2712.1773191 h
1594.6901921 0.0001364
1107.1310981
ida 6
f(X) Integral
1.6680
5151.0183393
2359.9314836 h
1516.5342865 0.0001540
1107.0898384

Refinado Extracto
A´(g/cm2. s) Kya (g/s*m3)Vprom (ml) t prom (s) m ref (g/cm2.V prom (ml) t prom (s) m ext (g/cm2
0.0343911337 0.00038344 25.75 20.405 0.06427021 47.5 38.5 0.04963969
0.0391503224 0.00071773 25.5 21.78 0.05962816 36.5 33.5 0.04383734
0.0412390028 0.00065993 26 20 0.0662083 34.5 31.5 0.04406611

ida 7
f(X) Integral
1.6724
5006.1330525
2334.9974620 h
1510.1875208 0.0001576
1107.0849676
ida 8
f(X) Integral
2.7499
8617.8161096
2696.4737226 h
 1581.2481182 0.0001744
1107.0873180
ida 9
f(X) Integral
2.4004
7185.0421852
2591.8153369 h
1563.4809979 0.0001638
1107.0924131
 Cálculo de Ys

Conc ac. Ben 0.56055636

m alimenta Ac refinad Ac extraido B den fas organ 790
0.04682225 4.2162E-05 0.000024127 0.043130378 Ys 0.00070957
0.05960552 4.8576E-05 3.58116E-05 0.037455218 Ys´ 0.00071007
0.06767505 5.3425E-05 4.238641E-05 0.038603694
Cálculo de Zf

Conc ac. Ben 0.01159319

19.635 PE(eq/L) 122.12

Conc ac. Ben 1.41576036
dens fas. Ac ( 1000
Zf 0.00141576
Zf´ 0.00141777

A m alimenta Ac refinad Ac extraido B

0.06420976 0.06427021 6.045192E-05 3.053928E-05 0.04778525
0.05957207 0.05962402 5.195282E-05 3.246048E-05 0.02305884
0.06614603 0.06619906 5.304146E-05 4.068053E-05 0.04622874
A m alimenta Ac refinad Ac extraido B
0.06421964 0.06427021 5.056909E-05 4.042211E-05 0.04959927
0.05958124 0.05962414 4.290127E-05 4.15122E-05 0.04379583
0.06615621 0.06620665 5.044079E-05 4.329193E-05 0.04402282
Corrida 1
X Y
0.00090128 0.00071017
0.00103038 0.00085019 FRACCIONES
0.007 MASICAS DE AC. BENZOICO LIBRE DE S
0.00115948 0.00099021
0.006
f(x) = 931447582483.08x^5 - 4023438616.50801x^4 + 6362896.31110943x^3 - 3078.4803
0.00128858 0.00113024
R² = 0.9999868746
0.00141768 0.00127026 0.005

Corrida 2 0.004 Curva

X Y Polyn
Equil

Y'
0.00081555 0.00071017 0.003
Corri
0.00096609 0.00094954 Corri
0.002 Corri
0.00111663 0.00118891
0.00126716 0.00142828 0.001
0.0014177 0.00166765
0
0 0.0002 0.0004 0.0006 0.0008 0.001 0.0012 0.0014 0.001
Corrida 3
X'
X Y
0.00078997 0.00071017
0.0009469 0.00098508
0.00110384 0.00125998
0.00126077 0.00153488
0.0014177 0.00180977

Corrida 4
X Y
0.00094148 0.00071017
0.00106054 0.00087014
0.00117959 0.00103011
0.00129865 0.00119009 FRACCIONES
0.007 MASICAS DE AC. BENZOICO LIBRE DE
0.0014177 0.00135006
0.006
f(x) = 931447582483.08x^5 - 4023438616.50801x^4 + 6362896.31110943x^3 - 3078.480
R² = 0.9999868746
Corrida 5 0.005
X Y
0.00087204 0.00071017 0.004 Curv
Poly
0.00100846 0.00106267 Equ
Y'

0.00114487 0.00141509 0.003

Corr
0.00128129 0.00176752 Corr
0.002 Corr
0.0014177 0.00211995
0.001
Corrida 6
X Y 0
0 0.0002 0.0004 0.0006 0.0008 0.001 0.0012 0.0014 0.00
0.00080177 0.00071017
X'
0.00095575 0.00093049
0.00110974 0.00115081
0.00126372 0.00137114
0.0014177 0.00159146

Corrida 7
X Y
0.00078744 0.00071018
0.00094501 0.00091417
0.00110257 0.00111818 FRACCIONES
0.007 MASICAS DE AC. BENZOICO LIBRE DE
0.00126014 0.00132219
0.006
0.0014177 0.0015262 f(x) = 931447582483.08x^5 - 4023438616.50801x^4 + 6362896.31110943x^3 - 3078.48
R² = 0.9999868746
0.005
Corrida 8
X Y 0.004 Cur
0.00071999 0.00071017 Pol
Equ

Y'
0.00089442 0.00094746 0.003
Cor
0.00106885 0.00118475 Cor
0.002 Cor
0.00124327 0.00142205
0.0014177 0.00165935 0.001

Corrida 9 0
0 0.0002 0.0004 0.0006 0.0008 0.001 0.0012 0.0014 0.00
X Y
X'
0.00076243 0.00071017
0.00092625 0.00095635
0.00109007 0.00120253
0.00125388 0.00144871
0.0014177 0.00169489
AS DE AC. BENZOICO LIBRE DE SOLUTO

16.50801x^4 + 6362896.31110943x^3 - 3078.4803033335x^2 + 2.1279764919x - 0.0001983239

Curva de Equilibrio
Polynomial (Curva de
Equilibrio)
Corrida1
Corrida 2
Corrida 3

0006 0.0008 0.001 0.0012 0.0014 0.0016 0.0018 0.002

X'

CAS DE AC. BENZOICO LIBRE DE SOLUTO

616.50801x^4 + 6362896.31110943x^3 - 3078.4803033335x^2 + 2.1279764919x - 0.0001983239

Curva de Equilibrio
Polynomial (Curva de
Equilibrio)
Corrida4
Corrida 5
Corrida 6

0.0006 0.0008 0.001 0.0012 0.0014 0.0016 0.0018 0.002

X'
CAS DE AC. BENZOICO LIBRE DE SOLUTO

8616.50801x^4 + 6362896.31110943x^3 - 3078.4803033335x^2 + 2.1279764919x - 0.0001983239

Curva de Equilibrio
Polynomial (Curva de
Equilibrio)
Corrida7
Corrida 8
Corrida9

0.0006 0.0008 0.001 0.0012 0.0014 0.0016 0.0018 0.002

X'