Evaluacion de la variable temperatura y fraccion acido acetico en solvente del del ejercicio 10.

43 Separation Pr

F,S Lb/h Variable

P psia Contante
T °C/F
Flujo Lb/h
Temperatura Acido Acetico en solvente (Ys) F
20/68 0 32060
40/104 0 32060
50/122 0 32060
60/140 0 32060

Temperatura %Recuperacion. Concentracion Extracto. (Fraccion)

20/68 92.7194539 0.0777789
40/104 90.3077628 0.0762058
50/122 89.0975231 0.0754317
60/140 87.940288 0.0746811

F,S Lb/h Variable

P psia Contante
T °C/F
Flujo Lb/h
Temperatura Acido Acetico en solvente (Ys) F
40/104 0.05 32060
40/105 0.1 32060
40/106 0.15 32060
40/107 0.20 32060

Temperatura Acido Acetico en solvente (Ys) %Recuperacion.

40/104 0.05 126.329212
40/105 0.1 165.02147
40/106 0.15 210.015572
40/107 0.20 284.19889
en solvente del del ejercicio 10.43 Separation Process Principles Seader and E.J. Henley, Operado en dos etapas.

T
(Ys,F,S,P)

S P
71100 15
71100 15
71100 15
71100 15

Concentracion Extracto. (Fraccion) Flujo del refinado. Conc. A la alimentacion. (Frac)

0.0777789 484.892 0.220096
0.0762058 645.513 0.220096
0.0754317 726.112 0.220096
0.0746811 805.603 0.220096

(Ys)
(T,F,S,P)

S P
71100 15
71100 15
71100 15
71100 15

Concentracion Extracto. (Fraccion) Flujo del refinado.

0.106322 22226.9
0.137333 21331.8
0.16953 18854.5
0.204689 8889
Operado en dos etapas.

Flujo del Extracto Concentracion Refinado

6175.13 0.0220745
6014.51 0.0287726
5933.91 0.0319965
5854.42 0.0350761

Conc. alimentacion. (Frac) Flujo del Extracto Concentracion Refinado

0.220096 79132.7 0.081051
0.220096 80027.8 0.1303
0.220096 82505 0.177036
0.220096 92470.5 0.219632
Temperatura Acido Acetico en solvente (Ys) F S P
20 0 32060 71100 15

Stream Alimentaci Solvente Extracto Refinado

F
Stage 1 2 1 2 S
Pressure (psia) 14.6959 14.6959 15 15 E
Light phase frac 0 1 0 0 R
Temperature (F) 68 68 68 68
Xf
Total molar flo 0.179031 0.115589 0.150771 0.143849 Y1
Total mass flow 30259.6 71099.9 79393.4 21966.2
Light liquid std.vol.flow ( 0.00987315 %Recuperacion.
Liquid std.vol. 0.00377956 0.0108638 0.00278894
%Recuperacion.
Mole flows (kmol/s)
Ethyl acetate 0 0.0981039 0.0961994 0.00190451
Water 0.165057 0.0174849 0.041615 0.140927
Acetic acid 0.0139737 0 0.0129563 0.00101737

Mole fractions (-)

Ethyl acetate 0 0.848732 0.638051 0.0132397
Water 0.921948 0.151268 0.276015 0.979688
Acetic acid 0.078052 0 0.085934 0.00707252

Mass flows (lb/h)

Ethyl acetate 0 68599.9 67268.2 1331.74
Water 23599.6 2499.97 5950.05 20149.5
Acetic acid 6660.02 0 6175.13 484.892

Mass fractions (-)

Ethyl acetate 0 0.964839 0.847277 0.060627
Water 0.779904 0.0351613 0.0749439 0.917298
Acetic acid 0.220096 0 0.0777789 0.0220745

Combined feed fractions (-)

Ethyl acetate 0 1 0.980587 0.0194132
Water 0.904214 0.0957857 0.227975 0.772025
Acetic acid 1 0 0.927194 0.0728064

Light liquid:
Mole weight (kg/kmol) 77.5028
Density (kg/m3) 902.649
Std.density (kg/m3) 907.354
Viscosity (N/m2.s) 0.00046799
Heat capacity (J/kmol/K) 156949
Thermal cond. (J/s/m/K) 0.210704

Liquid:
Mole weight (k 21.2963 20.5687 19.2406
Density (kg/m3) 1018.81 1011.45 1010.33
Std.density (kg 1008.76 920.804 992.38
Viscosity (N/m2.0.00105165 0.00095894 0.00096723
Heat capacity 79228.9 78749.3 77144.9
Thermal cond. 0.556862 0.569705 0.581569
Surface tension* 0.00317079 0.00498356
 30259.6
71099.9
79393.4
21966.2

0.220096
0.0777789

Recuperacion. 92.7194539

Recuperacion. E*Y1/F*Xs
Temperatura Acido Acetico en solvente (Ys) F S
40 0 32060 71100

Stream Alimentaci Solvente Extracto Refinado

Stage 1 2 1 2
Pressure (psia) 14.6959 14.6959 15 15
Light phase frac 0 1 0 0
Temperature (F) 104 104 104 104

Total molar flo 0.179031 0.115589 0.151402 0.143218

Total mass flow 30259.6 71099.9 78924.6 22435
Light liquid std.vol.flow ( 0.00987315
Liquid std.vol. 0.00377956 0.0107983 0.00285443

Mole flows (kmol/s)

Ethyl acetate 0 0.0981039 0.0953965 0.00270736
Water 0.165057 0.0174849 0.0433859 0.139156
Acetic acid 0.0139737 0 0.0126193 0.00135438

Mole fractions (-)

Ethyl acetate 0 0.848732 0.630089 0.0189038
Water 0.921948 0.151268 0.286561 0.971639
Acetic acid 0.078052 0 0.0833499 0.00945679

Mass flows (lb/h)

Ethyl acetate 0 68599.9 66706.8 1893.14
Water 23599.6 2499.97 6203.25 19896.3
Acetic acid 6660.02 0 6014.51 645.513

Mass fractions (-)

Ethyl acetate 0 0.964839 0.845197 0.0843834
Water 0.779904 0.0351613 0.0785973 0.886844
Acetic acid 0.220096 0 0.0762058 0.0287726

Combined feed fractions (-)

Ethyl acetate 0 1 0.972403 0.0275968
Water 0.904214 0.0957857 0.237676 0.762324
Acetic acid 1 0 0.903076 0.0969235

Light liquid:
Mole weight (kg/kmol) 77.5028
Density (kg/m3) 878.84
Std.density (kg/m3) 907.354
Viscosity (N/m2.s) 0.00037376
Heat capacity (J/kmol/K) 160909
Thermal cond. (J/s/m/K) 0.208863

Liquid:
Mole weight (k 21.2963 21.3223 19.7378
Density (kg/m3) 1002.4 993.979 993.893
Std.density (kg 1008.76 920.918 990.307
Viscosity (N/m2.0.00070094 0.00062859 0.00062732
Heat capacity 79598.5 80025 77942.7
Thermal cond. 0.582192 0.590011 0.604845
Surface tension* 0.00325869 0.00498496
 P
15

F 30259.6
S 71099.9
E 78924.6
R 22435

Xf 0.220096
Y1 0.0762058

%Recuperacion. 90.30776278

%Recuperacion. E*Y1/F*Xs
Temperatura Acido Acetico en solvente (Ys) F S
50 0 32060 71100

Stream Alimentaci Solvente Extracto Refinado

Stage 1 2 1 2
Pressure (psia) 14.6959 14.6959 15 15
Light phase frac 0 1 0 0
Temperature (F) 122 122 122 122

Total molar flo 0.179031 0.115589 0.151834 0.142785

Total mass flow 30259.6 71099.9 78666 22693.5
Light liquid std.vol.flow ( 0.00987315
Liquid std.vol. 0.00377956 0.0107618 0.00289088

Mole flows (kmol/s)

Ethyl acetate 0 0.0981039 0.0949221 0.00318179
Water 0.165057 0.0174849 0.0444617 0.13808
Acetic acid 0.0139737 0 0.0124502 0.00152349

Mole fractions (-)

Ethyl acetate 0 0.848732 0.62517 0.0222837
Water 0.921948 0.151268 0.292831 0.967046
Acetic acid 0.078052 0 0.0819988 0.0106698

Mass flows (lb/h)

Ethyl acetate 0 68599.9 66375 2224.89
Water 23599.6 2499.97 6357.08 19742.5
Acetic acid 6660.02 0 5933.91 726.112

Mass fractions (-)

Ethyl acetate 0 0.964839 0.843757 0.0980409
Water 0.779904 0.0351613 0.0808109 0.869963
Acetic acid 0.220096 0 0.0754317 0.0319965

Combined feed fractions (-)

Ethyl acetate 0 1 0.967567 0.0324329
Water 0.904214 0.0957857 0.24357 0.75643
Acetic acid 1 0 0.890974 0.109026

Light liquid:
Mole weight (kg/kmol) 77.5028
Density (kg/m3) 866.589
Std.density (kg/m3) 907.354
Viscosity (N/m2.s) 0.00033586
Heat capacity (J/kmol/K) 163066
Thermal cond. (J/s/m/K) 0.207683

Liquid:
Mole weight (k 21.2963 21.7412 20.0257
Density (kg/m3) 994.02 984.636 985.215
Std.density (kg 1008.76 921.011 989.087
Viscosity (N/m2.0.00059019 0.00052667 0.00052343
Heat capacity 79814.1 80794.8 78444.3
Thermal cond. 0.592767 0.597471 0.613813
Surface tension* 0.00328462 0.00497128
 P
15

F 30259.6
S 71099.9
E 78666
R 22693.5

Xf 0.220096
Y1 0.0754317

%Recuperacion. 89.09752306

%Recuperacion. E*Y1/F*Xs
Temperatura Acido Acetico en solvente (Ys) F S
60 0 32060 71100

Stream Alimentaci Solvente Extracto Refinado

Stage 1 2 1 2
Pressure (psia) 14.6959 14.6959 15 15
Light phase frac 0 1 0 0
Temperature (F) 140 140 140 140

Total molar flo 0.179031 0.115589 0.152354 0.142266

Total mass flow 30259.6 71099.9 78392.3 22967.3
Light liquid std.vol.flow ( 0.00987315
Liquid std.vol. 0.00377956 0.010723 0.00292973

Mole flows (kmol/s)

Ethyl acetate 0 0.0981039 0.0943965 0.00370744
Water 0.165057 0.0174849 0.0456738 0.136868
Acetic acid 0.0139737 0 0.0122834 0.00169027

Mole fractions (-)

Ethyl acetate 0 0.848732 0.619587 0.0260599
Water 0.921948 0.151268 0.299788 0.962059
Acetic acid 0.078052 0 0.0806244 0.0118811

Mass flows (lb/h)

Ethyl acetate 0 68599.9 66007.5 2592.46
Water 23599.6 2499.97 6530.38 19569.2
Acetic acid 6660.02 0 5854.42 805.603

Mass fractions (-)

Ethyl acetate 0 0.964839 0.842015 0.112876
Water 0.779904 0.0351613 0.0833039 0.852048
Acetic acid 0.220096 0 0.0746811 0.0350761

Combined feed fractions (-)

Ethyl acetate 0 1 0.962209 0.0377909
Water 0.904214 0.0957857 0.25021 0.74979
Acetic acid 1 0 0.879039 0.120961

Light liquid:
Mole weight (kg/kmol) 77.5028
Density (kg/m3) 854.073
Std.density (kg/m3) 907.354
Viscosity (N/m2.s) 0.00030282
Heat capacity (J/kmol/K) 165317
Thermal cond. (J/s/m/K) 0.206349

Liquid:
Mole weight (k 21.2963 22.1905 20.3413
Density (kg/m3) 985.506 974.838 976.177
Std.density (kg 1008.76 921.131 987.745
Viscosity (N/m2.0.00050554 0.00044946 0.00044525
Heat capacity 80052.1 81666.1 79027.8
Thermal cond. 0.60201 0.603199 0.62106
Surface tension* 0.00329754 0.00494726
 P
15

F 30259.6
S 71099.9
E 78392.3
R 22967.3

Xf 0.220096
Y1 0.0746811

%Recuperacion. 87.90402884

%Recuperacion. E*Y1/F*Xs
Temperatura Acido Acetico en solvente (Ys) F S P
40/104 0.05 32060 71100 15

Stream Alimentaci Solvente Extracto Refinado

F
Stage 1 2 1 2 S
Pressure (psia) 14.6959 14.6959 15 15 E
Light phase fr 0 1 0 0 R
Temperature (F) 104 104 104 104
Xf
Total molar f 0.179031 0.117964 0.16397 0.133024 Y1
Total mass flo 30259.6 71099.9 79132.7 22226.9
Light liquid std.vol.flow ( 0.00980407 %Recuperacion.
Liquid std.vo 0.00377956 0.0107557 0.0028279
%Recuperacion.
Mole flows (kmol/s)
Ethyl acetate 0 0.0930199 0.0895213 0.00349858
Water 0.165057 0.0174849 0.0567962 0.125746
Acetic acid 0.0139737 0.00745891 0.0176528 0.00377983

Mole fractions (-)

Ethyl acetate 0 0.788547 0.54596 0.0263004
Water 0.921948 0.148223 0.346381 0.945285
Acetic acid 0.078052 0.0632305 0.107658 0.0284146

Mass flows (lb/h)

Ethyl acetate 0 65044.9 62598.5 2446.41
Water 23599.6 2499.97 8120.65 17978.9
Acetic acid 6660.02 3555 8413.51 1801.51

Mass fractions (-)

Ethyl acetate 0 0.914839 0.791058 0.110066
Water 0.779904 0.0351613 0.102621 0.808884
Acetic acid 0.220096 0.0500001 0.106322 0.081051

Combined feed fractions (-)

Ethyl acetate 0 1 0.962389 0.0376111
Water 0.904214 0.0957857 0.311141 0.688859
Acetic acid 0.651983 0.348017 0.823641 0.176359

Light liquid:
Mole weight (kg/kmol) 75.9424
Density (kg/m3) 888.202
Std.density (kg/m3) 913.746
Viscosity (N/m2.s) 0.00039102
Heat capacity (J/kmol/K) 158135
Thermal cond. (J/s/m/K) 0.208611

Liquid:
Mole weight 21.2963 22.3894 21.0531
Density (kg/m3 1002.4 993.452 994.043
Std.density ( 1008.76 926.999 990.324
Viscosity (N/m0.00070094 0.00062718 0.00062869
Heat capacit 79598.5 81440.5 79669.6
Thermal cond 0.582192 0.580289 0.592496
Surface tens* 0.00254187 0.00348468
 30259.6
71099.9
79132.7
22226.9

0.220096
0.106322

Recuperacion. 126.329212

Recuperacion. E*Y1/F*Xs
Temperatura Acido Acetico en solvente (Ys) F S P
40/104 0.1 32060 71100 15

Stream Alimentaci Solvente Extracto Refinado

F
Stage 1 2 1 2 S
Pressure (psia) 14.6959 14.6959 15 15 E
Light phase fra 0 1 0 0 R
Temperature (F) 104 104 104 104
Xf
Total molar fl 0.179031 0.120339 0.180839 0.11853 Y1
Total mass flow 30259.6 71099.9 80027.8 21331.8
Light liquid std.vol.flow ( 0.009735 %Recuperacion.
Liquid std.vol 0.00377956 0.010798 0.0027166
%Recuperacion.
Mole flows (kmol/s)
Ethyl acetate 0 0.087936 0.0835519 0.0043841
Water 0.165057 0.0174849 0.0742275 0.108314
Acetic acid 0.0139737 0.0149178 0.0230596 0.00583186

Mole fractions (-)

Ethyl acetate 0 0.730738 0.462024 0.0369871
Water 0.921948 0.145297 0.410462 0.913811
Acetic acid 0.078052 0.123965 0.127515 0.0492014

Mass flows (lb/h)

Ethyl acetate 0 61489.9 58424.3 3065.61
Water 23599.6 2499.97 10612.9 15486.6
Acetic acid 6660.02 7109.99 10990.5 2779.53

Mass fractions (-)

Ethyl acetate 0 0.864839 0.730051 0.143711
Water 0.779904 0.0351613 0.132616 0.725989
Acetic acid 0.220096 0.1 0.137333 0.1303

Combined feed fractions (-)

Ethyl acetate 0 1 0.950145 0.0498555
Water 0.904214 0.0957857 0.406633 0.593367
Acetic acid 0.483661 0.516339 0.798146 0.201854

Light liquid:
Mole weight (kg/kmol) 74.4436
Density (kg/m3) 897.402
Std.density (kg/m3) 920.23
Viscosity (N/m2.s) 0.00040907
Heat capacity (J/kmol/K) 155470
Thermal cond. (J/s/m/K) 0.208369

Liquid:
Mole weight ( 21.2963 23.7088 22.676
Density (kg/m3) 1002.4 992.283 993.243
Std.density (k 1008.76 933.818 989.384
Viscosity (N/m20.00070094 0.00062351 0.00062654
Heat capacity 79598.5 83204.1 81822.3
Thermal cond. 0.582192 0.568545 0.577713
Surface tensi* 0.00192483 0.00238742
 30259.6
71099.9
80027.8
21331.8

0.220096
0.137333

Recuperacion. 165.0214705

Recuperacion. E*Y1/F*Xs
Temperatura Acido Acetico en solvente (Ys) F S P
40/104 0.15 32060 71100 15

Stream Alimentaci Solvente Extracto Refinado

F
Stage 1 2 1 2 S
Pressure (psia) 14.6959 14.6959 15 15 E
Light phase fra 0 1 0 0 R
Temperature (F) 104 104 104 104
Xf
Total molar fl 0.179031 0.122714 0.206298 0.0954458 Y1
Total mass flow 30259.6 71099.9 82505 18854.5
Light liquid std.vol.flow ( 0.00966592 %Recuperacion.
Liquid std.vol 0.00377956 0.0110383 0.00240715
%Recuperacion.
Mole flows (kmol/s)
Ethyl acetate 0 0.082852 0.0776905 0.00516148
Water 0.165057 0.0174849 0.099261 0.0832809
Acetic acid 0.0139737 0.0223767 0.0293469 0.00700347

Mole fractions (-)

Ethyl acetate 0 0.675166 0.376593 0.0540776
Water 0.921948 0.142485 0.481152 0.872546
Acetic acid 0.078052 0.182349 0.142255 0.0733763

Mass flows (lb/h)

Ethyl acetate 0 57934.9 54325.7 3609.21
Water 23599.6 2499.97 14192.2 11907.4
Acetic acid 6660.02 10665 13987.1 3337.93

Mass fractions (-)

Ethyl acetate 0 0.814839 0.658454 0.191424
Water 0.779904 0.0351613 0.172016 0.63154
Acetic acid 0.220096 0.15 0.16953 0.177036

Combined feed fractions (-)

Ethyl acetate 0 1 0.937702 0.0622976
Water 0.904214 0.0957857 0.543771 0.456229
Acetic acid 0.384417 0.615583 0.807335 0.192665

Light liquid:
Mole weight (kg/kmol) 73.0029
Density (kg/m3) 906.445
Std.density (kg/m3) 926.806
Viscosity (N/m2.s) 0.00042796
Heat capacity (J/kmol/K) 152909
Thermal cond. (J/s/m/K) 0.208136

Liquid:
Mole weight ( 21.2963 25.4682 24.8901
Density (kg/m3) 1002.4 990.017 990.839
Std.density (k 1008.76 941.76 986.905
Viscosity (N/m20.00070094 0.00061619 0.00061885
Heat capacity 79598.5 85577 84794.6
Thermal cond. 0.582192 0.553321 0.558272
Surface tensi* 0.00980432 0.00152506
 30259.6
71099.9
82505
18854.5

0.220096
0.16953

Recuperacion. 210.0155723

Recuperacion. E*Y1/F*Xs
Temperatura Acido Acetico en solvente (Ys) F S P
40/104 0.2 32060 71100 15

Stream Alimentaci Solvente Extracto Refinado

F
Stage 1 2 1 2 S
Pressure (psia) 14.6959 14.6959 15 15 E
Light phase fra 0 1 0 0 R
Temperature (F) 104 104 104 104
Xf
Total molar fl 0.179031 0.125089 0.264959 0.0391602 Y1
Total mass flow 30259.6 71099.9 92470.5 8889
Light liquid std.vol.flow ( 0.00959685 %Recuperacion.
Liquid std.vol 0.00377956 0.0122347 0.00114173
%Recuperacion.
Mole flows (kmol/s)
Ethyl acetate 0 0.077768 0.0743106 0.00345741
Water 0.165057 0.0174849 0.150935 0.0316066
Acetic acid 0.0139737 0.0298357 0.0397132 0.00409624

Mole fractions (-)

Ethyl acetate 0 0.621703 0.280461 0.0882889
Water 0.921948 0.13978 0.569655 0.807109
Acetic acid 0.078052 0.238517 0.149884 0.104602

Mass flows (lb/h)

Ethyl acetate 0 54379.9 51962.3 2417.62
Water 23599.6 2499.97 21580.5 4519.06
Acetic acid 6660.02 14220 18927.7 1952.31

Mass fractions (-)

Ethyl acetate 0 0.764838 0.561933 0.271979
Water 0.779904 0.0351613 0.233377 0.508388
Acetic acid 0.220096 0.200001 0.204689 0.219632

Combined feed fractions (-)

Ethyl acetate 0 1 0.955542 0.044458
Water 0.904214 0.0957857 0.826853 0.173147
Acetic acid 0.318966 0.681034 0.906499 0.0935013

Light liquid:
Mole weight (kg/kmol) 71.6168
Density (kg/m3) 915.336
Std.density (kg/m3) 933.476
Viscosity (N/m2.s) 0.00044772
Heat capacity (J/kmol/K) 150444
Thermal cond. (J/s/m/K) 0.207912

Liquid:
Mole weight ( 21.2963 28.3173 28.6006
Density (kg/m3) 1002.4 985.119 984.57
Std.density (k 1008.76 952.301 980.962
Viscosity (N/m20.00070094 0.00060066 0.00059896
Heat capacity 79598.5 89465.1 89854.5
Thermal cond. 0.582192 0.529606 0.527305
Surface tensi* 0.00980432 0.00073162
 30259.6
71099.9
92470.5
8889

0.220096
0.204689

Recuperacion. 284.1988901

Recuperacion. E*Y1/F*Xs