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FTM9 ‘loop’ tack measurement

scope test conditions


This test method describes a means of assessing probably 23°C ± 2°C and 50% RH ± 5% RH.
the most important and yet the hardest to measure
property of pressure sensitive materials, the tack. The The test sample or test strips should be conditioned for not
method described should allow the end user to compare less than 4 hours before testing.
the “initial grab” or “application tack” of different laminates
and can be extremely useful to those working with
automatic labelling equipment where this property is of
particular importance.

definition
The ‘loop’ tack value of a pressure sensitive material is
expressed as the force required to separate, at a specified
speed, a loop of material (adhesive outermost) which
has been brought into contact with a specified area of a
standard surface.

test equipment
A tensile tester or similar machine with reversing facility procedure
and a vertical jaw separation rate of 300mm per minute
with an accuracy of ± 2%. It should also have a capability Remove the backing
of measuring direct loads up to at least 20 Newton with an material from each strip
accuracy of ±2%. immediately prior to
the test being carried
A flat plate made of float glass or equivalent plate glass out. Hold the two ends
measuring 25 ± 0.5 mm x 30 ± 2.0 mm x minimum of the adhesive coated
thickness 3.0 mm. A metal peg is attached at the centre of facing material strip and
one face of the plate. The dimensions of the peg should be from the strip into a
such that the peg can be clamped in the lower jaw of the loop, adhesive surface
tensometer. outermost, by bringing
the two ends together.
Clamp the ends of the
test pieces loop for a distance of
10 mm into the top
These should be strips taken from a representative sample jaw of the ensile tester
of material. The strips should be 25 mm wide and have a leaving the loop hanging
minimum length of 175 mm in the machine direction. The vertically downwards.
cuts should be clean and straight. At least five strips should The sides of the jaw
be taken from each sample. should be protected from the adhesive coating.

FINAT TECHNICAL HANDBOOK 2014 |

Clamp the glass plate in the lower jaw with the longer axis
of the plate positioned at right angles to the long axis of
the strip. Start the machine and bring the loop into contact
with the glass plate at a speed of 300 mm per minute.
When full contact over the glass plate has been achieved
(25 mm x 25 mm) immediately reverse the direction of the
machine and allow separation to take place at a speed of
300 mm per minute. It is important that delay in reversing
direction is kept to an absolute minimum.

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If the force exceeds the strength of a paper facing material,
the result quoted should be the maximum reached before
the paper tears and this result should be followed by the
postscript PT (paper tear)

If adhesive transfer occurs, this should be indicated by the


letters AT, and the approximate extend of transfer quoted
as percentage.

notes
1. The rigidity of the sample affects the results and must
be considered when comparing different adhesives on
different facing materials.
2. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:

• Diacetone alcohol non-residual,


technical grade or better
• Methyl Ethyl Ketone (MEK)
• Acetone
• Methanol 95%
• n-Heptane
• Ethyl Acetate

The cleaning material must be absorbent, e.g. surgical


gauze, cotton wool or tissue. To be suitable, materials must
be lint-free during use, absorbent, contain no additives
that are soluble in the solvents listed above, and made
exclusively from virgin materials.

Dispense one of the solvents listed above on to the panel,


wiping it to dryness with fresh absorbent cleaning material.
Repeat for a total of three washes with the solvent. Final
wipe shall be with MEK or acetone.

Alternative methods which remove contamination properly
can be adopted, e.g. ultrasonic cleaning.

Prior to use, the cleaned plates should be left for 4 hours
under standard test conditions. Care should be taken to
handle clean plates by the edge only.
FINAT TECHNICAL HANDBOOK 2014 |


Record the maximum force necessary to completely 3. Conversion 1 kgf- = 9.81 Newton.
separate each loop from the glass plate.
Issued October 1985
Revised March 1999
results Revised May 2001
Added pictures January 20
‘Loop’ tack is expressed as the average value (ignoring the
initial peak) and range for the five strips tested in Newton.

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