STD - Ore - Sevenhundred Paquete Datos

Table 1.
Abbreviations used for OREAS 700
Abbreviation
Std.Dev.
Rel.Std.Dev.
PDM3
NR
<
FA*AAS
FA*OES
INAA
BF*XRF
PF*OES
PSF*XRF
BF*MS
PF*MS
at 1000°C
4A*OES/MS
4A*MS
4A*OES
AR*OES/MS
AR*MS
AR*OES
AR*AAS
AR*OES/AAS
IRC
AD*TITR
DTR-REC
MAG-SUS
Legend:-
Individual
Batch & Limits

Table 1. Abbreviations used for OREAS 700
Explanation
one sigma standard deviation

one sigma relative standard deviation
percent deviation of lab mean from corrected mean of means
not reported
‘less than’
fire assay with AAS finish
fire assay with ICP-OES finish
INAA using a charge weight as deemed appropriate
lithium borate fusion with XRF finish
sodium peroxide fusion with ICP-OES finish
pyro-sulfate fusion with x-ray fluorescence finish
lithium borate fusion with ICP-MS finish
sodium peroxide fusion with ICP-MS finish
loss on ignition at 1000°C
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES or ICP-MS finish as appropriate
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-MS finish
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES finish
aqua regia digest with ICP-OES or ICP-MS finish as appropriate
aqua regia digest with ICP-MS finish
aqua regia digest with ICP-OES finish
aqua regia digest with AAS finish
ore grade aqua regia digest with either AAS or ICP-OES finish as appropriate
infrared combustion furnace
acid digest (non-specific) with Titration finish
Davis Tube Recovery
Magnetic Susceptibility
(for Method Group Tabulated Results omitted in the determination of Certified Values)
- Outlying individual values
- Outlying laboratory batch data sets and superfluous limit values

Table 2. Certified Values, SD's, 95% Confidence and Tolerance Limits for OREAS 700
95% Confidence 95% Tolerance
Certified
Constituent SD Limits Limits
Value Low High Low High
Pb Fire Assay
Au, Gold (ppm) 0.506 0.023 0.493 0.520 0.493 0.520
Borate Fusion XRF
Al2O3, Aluminium(III) oxide (wt.%) 10.62 0.132 10.55 10.69 10.52 10.72
CaO, Calcium oxide (wt.%) 7.86 0.111 7.79 7.92 7.81 7.91
Cl, Chlorine (ppm) 158 22 138 178 IND IND
Cu, Copper (wt.%) 0.204 0.009 0.198 0.209 0.186 0.221
Fe, Iron (wt.%) 16.06 0.175 15.95 16.16 15.97 16.15
K2O, Potassium oxide (wt.%) 1.89 0.028 1.87 1.91 1.87 1.90
MgO, Magnesium oxide (wt.%) 1.74 0.038 1.71 1.76 1.72 1.76
MnO, Manganese oxide (wt.%) 0.415 0.010 0.407 0.422 0.410 0.419
Na2O, Sodium oxide (wt.%) 1.65 0.030 1.63 1.67 1.63 1.68
Ni, Nickel (ppm) < 50 IND IND IND IND IND
P, Phosphorus (wt.%) 0.353 0.008 0.348 0.357 0.349 0.356
Pb, Lead (ppm) < 10 IND IND IND IND IND
S, Sulphur (wt.%) 0.304 0.014 0.295 0.313 0.288 0.320
SiO2, Silicon dioxide (wt.%) 47.30 0.511 47.03 47.58 47.06 47.54
Sn, Tin (ppm) 182 34 156 208 IND IND
TiO2, Titanium dioxide (wt.%) 0.320 0.010 0.314 0.327 0.309 0.331
V2O5, Vanadium(V) oxide (ppm) 110 14 101 120 IND IND
W, Tungsten (wt.%) 1.13 0.025 1.11 1.14 1.12 1.14
WO3, Tungsten oxide (wt.%) 1.42 0.031 1.40 1.44 1.41 1.44
Zn, Zinc (ppm) 231 26 216 245 206 255
Thermogravimetry
LOI, Loss On Ignition @1000°C (wt.%) 1.95 0.20 1.79 2.12 1.86 2.05
4-Acid Digestion
Al, Aluminium (wt.%) 5.57 0.296 5.38 5.76 5.45 5.69
As, Arsenic (ppm) 4.35 0.57 3.90 4.80 4.08 4.63
Ba, Barium (ppm) 158 6 154 162 154 163
Be, Beryllium (ppm) 2.32 0.084 2.27 2.36 2.20 2.44
Ca, Calcium (wt.%) 5.55 0.227 5.41 5.69 5.40 5.69
Co, Cobalt (ppm) 16.8 2.6 15.0 18.5 15.8 17.8
Cr, Chromium (ppm) 47.2 4.8 44.2 50.1 45.0 49.4
Cs, Cesium (ppm) 109 6 102 115 102 115
Cu, Copper (wt.%) 0.202 0.007 0.199 0.206 0.191 0.214
Fe, Iron (wt.%) 15.57 0.920 14.94 16.19 15.28 15.86
Ga, Gallium (ppm) 129 5 125 134 124 134
Hf, Hafnium (ppm) 1.42 0.141 1.26 1.58 1.35 1.48
In, Indium (ppm) 2.10 0.050 2.06 2.14 2.00 2.20
K, Potassium (wt.%) 1.57 0.056 1.53 1.60 1.53 1.61
La, Lanthanum (ppm) 32.5 2.43 30.7 34.3 30.9 34.1
Li, Lithium (ppm) 223 19 205 242 217 230
Lu, Lutetium (ppm) 0.18 0.014 0.16 0.20 0.17 0.19
Mg, Magnesium (wt.%) 0.995 0.025 0.978 1.012 0.978 1.013
Mn, Manganese (wt.%) 0.314 0.013 0.306 0.323 0.307 0.321
Mo, Molybdenum (ppm) 81 7.5 75 86 78 83
Na, Sodium (wt.%) 1.21 0.053 1.18 1.25 1.19 1.24
Ni, Nickel (ppm) 24.1 2.7 22.3 25.9 22.5 25.7
P, Phosphorus (wt.%) 0.347 0.029 0.329 0.366 0.339 0.355
Pb, Lead (ppm) 6.83 1.33 5.98 7.67 6.43 7.22
Rb, Rubidium (ppm) 444 34 416 473 429 459
S, Sulphur (wt.%) 0.295 0.015 0.289 0.301 0.277 0.312
Sb, Antimony (ppm) 0.70 0.059 0.65 0.74 0.64 0.76
Sc, Scandium (ppm) 9.55 0.878 8.80 10.30 9.12 9.98
Sn, Tin (ppm) 133 9 125 140 128 138
Sr, Strontium (ppm) 124 7 119 129 121 127
Th, Thorium (ppm) 7.75 0.751 7.01 8.49 7.59 7.91
Ti, Titanium (wt.%) 0.179 0.014 0.168 0.190 0.172 0.185
Tl, Thallium (ppm) 2.54 0.43 2.12 2.96 2.45 2.63
U, Uranium (ppm) 4.73 0.49 4.25 5.20 4.58 4.87
V, Vanadium (ppm) 62 2.0 61 63 60 64
W, Tungsten (wt.%) 0.989 0.081 0.910 1.068 0.896 1.081
Y, Yttrium (ppm) 13.5 0.77 12.9 14.1 13.0 14.0
Yb, Ytterbium (ppm) 1.26 0.13 1.09 1.42 1.20 1.32
Zn, Zinc (ppm) 216 16 205 227 211 221
Zr, Zirconium (ppm) 47.3 4.8 43.4 51.2 44.3 50.2
Aqua Regia Digestion
Ag, Silver (ppm) 0.499 0.075 0.450 0.548 0.438 0.560
Al, Aluminium (wt.%) 3.13 0.143 3.05 3.22 3.04 3.23
As, Arsenic (ppm) 3.88 0.73 3.47 4.29 3.59 4.18
Au, Gold (ppm) 0.505 0.034 0.489 0.520 0.468 0.541
B, Boron (ppm) < 30 IND IND IND IND IND
Ba, Barium (ppm) 81 6.9 76 86 78 84
Be, Beryllium (ppm) 0.73 0.041 0.70 0.76 0.66 0.81
Bi, Bismuth (ppm) 6.89 0.84 6.58 7.19 6.59 7.18
Ca, Calcium (wt.%) 4.45 0.366 4.21 4.68 4.35 4.55
Cd, Cadmium (ppm) < 0.5 IND IND IND IND IND
Ce, Cerium (ppm) 43.9 7.7 36.5 51.3 42.3 45.5
Co, Cobalt (ppm) 15.2 1.21 14.3 16.1 14.5 15.9
Cr, Chromium (ppm) 51 2.6 49 52 49 52
Cu, Copper (wt.%) 0.203 0.008 0.199 0.206 0.192 0.213
Fe, Iron (wt.%) 14.66 0.710 14.22 15.10 14.31 15.00
Ga, Gallium (ppm) 112 10 106 119 109 115
Hf, Hafnium (ppm) 0.81 0.12 0.65 0.98 0.79 0.84
In, Indium (ppm) 1.67 0.109 1.56 1.77 1.58 1.75
K, Potassium (wt.%) 1.24 0.044 1.21 1.26 1.21 1.26
La, Lanthanum (ppm) 20.6 1.71 19.4 21.8 19.9 21.3
Li, Lithium (ppm) 84 6.6 77 91 81 86
Lu, Lutetium (ppm) 0.13 0.011 0.12 0.15 IND IND
Mg, Magnesium (wt.%) 0.948 0.058 0.910 0.987 0.924 0.972
Mn, Manganese (wt.%) 0.237 0.014 0.227 0.246 0.230 0.243
Mo, Molybdenum (ppm) 83 9 77 89 81 86
Na, Sodium (wt.%) 0.164 0.030 0.143 0.185 0.158 0.170
Nb, Niobium (ppm) 10.4 2.0 8.3 12.5 9.2 11.6
Ni, Nickel (ppm) 24.5 2.6 22.8 26.2 23.5 25.5
P, Phosphorus (wt.%) 0.340 0.012 0.331 0.348 0.330 0.349
Pb, Lead (ppm) 5.10 1.01 4.33 5.87 4.59 5.61
S, Sulphur (wt.%) 0.297 0.017 0.289 0.306 0.281 0.313
Sc, Scandium (ppm) 8.77 1.35 7.83 9.71 8.33 9.22
Se, Selenium (ppm) 2.01 0.151 1.85 2.16 IND IND
Sn, Tin (ppm) 110 7 104 116 106 113
Sr, Strontium (ppm) 46.1 4.07 43.2 49.1 44.2 48.0
Te, Tellurium (ppm) 0.19 0.03 0.16 0.21 0.16 0.22
Ti, Titanium (wt.%) 0.097 0.005 0.093 0.100 0.093 0.100
V, Vanadium (ppm) 56 2.3 55 58 55 58
Y, Yttrium (ppm) 11.5 1.2 10.6 12.5 11.0 12.0
Zn, Zinc (ppm) 207 11 199 214 200 213
Zr, Zirconium (ppm) 24.9 1.86 23.2 26.7 23.9 26.0
Acid Digestion Titration
FeO, Iron(II) oxide (wt.%) 12.07 0.398 11.81 12.33 11.79 12.35
Davis Tube Recovery
MassRec, Mass Recovered (wt.%) 11.28 0.240 11.11 11.45 10.86 11.70
Satmagan 135
Fe3O4, Iron(II,III) oxide (wt.%) 10.91 0.196 10.76 11.07 10.76 11.07
Table 3. Indicative Values for OREAS 700
Constituent Unit Value Constituent Unit Value Constituent Unit Value
Pb Fire Assay
Pd ppb 5 Pt ppb <5
Borate Fusion XRF
As ppm 33.3 Cr2O3 ppm 79 Zr ppm 53
BaO ppm 135 Mo ppm 118
Co ppm 17.2 Sr ppm 47.5
4-Acid Digestion
Ag ppm 0.525 Gd ppm 4.17 Re ppm 0.17
Bi ppm 6.75 Ge ppm 3.43 Se ppm 2.09
Cd ppm 0.37 Hg ppm < 10 Sm ppm 5.26
Ce ppm 66 Ho ppm 0.56 Ta ppm 0.65
Dy ppm 2.68 Nb ppm 16.1 Tb ppm 0.50
Er ppm 1.38 Nd ppm 26.3 Te ppm 0.16
Eu ppm 0.86 Pr ppm 7.84 Tm ppm 0.19
Cs ppm 45.0 Pd ppb < 10 Tb ppm 0.45
Dy ppm 2.27 Pr ppm 4.69 Th ppm 7.19
Er ppm 1.07 Pt ppb <1 Tl ppm 2.31
Eu ppm 0.63 Rb ppm 361 Tm ppm 0.15
Gd ppm 3.18 Re ppm 0.045 U ppm 4.46
Ge ppm 2.82 Sb ppm 0.35 W wt.% 0.440
Hg ppm 0.89 Si wt.% 0.139 Yb ppm 0.95
Ho ppm 0.41 Sm ppm 3.86
Nd ppm 19.9 Ta ppm 0.21
Infrared Combustion
S wt.% 0.325
Table 4. Pooled-Lab Performance Gates for OREAS 700
Certified Absolute Standard Deviations Relative Standard Deviations 5% window

Constituent
Value 1SD 2SD Low 2SD High 3SD Low 3SD High 1RSD 2RSD 3RSD Low
Pb Fire Assay
Au, ppm 0.506 0.023 0.461 0.552 0.439 0.574 4.45% 8.90% 13.35% 0.481
Borate Fusion XRF
Al2O3, wt.% 10.62 0.132 10.36 10.89 10.23 11.02 1.24% 2.49% 3.73% 10.09
CaO, wt.% 7.86 0.111 7.63 8.08 7.52 8.19 1.42% 2.84% 4.25% 7.46
Cl, ppm 158 22 114 203 91 225 14.11% 28.23% 42.34% 150
Cu, wt.% 0.204 0.009 0.186 0.221 0.177 0.230 4.37% 8.74% 13.12% 0.193
Fe, wt.% 16.06 0.175 15.71 16.41 15.53 16.58 1.09% 2.18% 3.26% 15.25
K2O, wt.% 1.89 0.028 1.83 1.94 1.80 1.97 1.49% 2.98% 4.46% 1.79
MgO, wt.% 1.74 0.038 1.66 1.81 1.63 1.85 2.17% 4.35% 6.52% 1.65
MnO, wt.% 0.415 0.010 0.394 0.435 0.384 0.445 2.47% 4.93% 7.40% 0.394
Na2O, wt.% 1.65 0.030 1.59 1.71 1.56 1.74 1.84% 3.67% 5.51% 1.57
Ni, ppm < 50 IND IND IND IND IND IND IND IND IND
P, wt.% 0.353 0.008 0.337 0.369 0.329 0.377 2.27% 4.54% 6.81% 0.335
Pb, ppm < 10 IND IND IND IND IND IND IND IND IND
S, wt.% 0.304 0.014 0.275 0.333 0.261 0.347 4.73% 9.46% 14.19% 0.289
SiO2, wt.% 47.30 0.511 46.28 48.32 45.77 48.84 1.08% 2.16% 3.24% 44.94
Sn, ppm 182 34 114 250 80 285 18.73% 37.46% 56.19% 173
TiO2, wt.% 0.320 0.010 0.301 0.339 0.292 0.349 2.98% 5.96% 8.94% 0.304
V2O5, ppm 110 14 82 139 67 153 12.98% 25.97% 38.95% 105
W, wt.% 1.13 0.025 1.08 1.18 1.05 1.20 2.19% 4.37% 6.56% 1.07
WO3, (wt.%) 1.42 0.03 1.36 1.48 1.33 1.52 2.19% 4.37% 6.56% 1.35
Zn, ppm 231 26 178 283 152 309 11.37% 22.74% 34.11% 219
Thermogravimetry
LOI, wt.% 1.95 0.20 1.55 2.36 1.34 2.57 10.46% 20.93% 31.39% 1.86
4-Acid Digestion
Al, wt.% 5.57 0.296 4.98 6.16 4.68 6.46 5.31% 10.62% 15.93% 5.29
As, ppm 4.35 0.57 3.20 5.50 2.63 6.07 13.20% 26.40% 39.60% 4.13
Ba, ppm 158 6 146 171 139 177 4.00% 8.01% 12.01% 150
Be, ppm 2.32 0.084 2.15 2.49 2.07 2.57 3.62% 7.24% 10.86% 2.20
Ca, wt.% 5.55 0.227 5.09 6.00 4.86 6.23 4.10% 8.20% 12.29% 5.27
Co, ppm 16.8 2.6 11.6 21.9 9.0 24.5 15.40% 30.79% 46.19% 15.9
Cr, ppm 47.2 4.8 37.7 56.7 32.9 61.4 10.07% 20.13% 30.20% 44.8
Cs, ppm 109 6 97 120 92 125 5.09% 10.17% 15.26% 103
Cu, wt.% 0.202 0.007 0.188 0.217 0.181 0.224 3.49% 6.98% 10.47% 0.192
Fe, wt.% 15.57 0.920 13.73 17.41 12.81 18.33 5.91% 11.82% 17.73% 14.79
Ga, ppm 129 5 119 140 114 145 3.98% 7.96% 11.94% 123
Hf, ppm 1.42 0.141 1.13 1.70 0.99 1.84 9.95% 19.90% 29.86% 1.35
In, ppm 2.10 0.050 2.00 2.20 1.95 2.25 2.38% 4.76% 7.15% 2.00
K, wt.% 1.57 0.056 1.45 1.68 1.40 1.73 3.57% 7.14% 10.71% 1.49
La, ppm 32.5 2.43 27.6 37.3 25.2 39.8 7.48% 14.96% 22.44% 30.9
Li, ppm 223 19 186 261 167 280 8.43% 16.87% 25.30% 212
Lu, ppm 0.18 0.014 0.15 0.21 0.14 0.22 7.69% 15.39% 23.08% 0.17
Mg, wt.% 0.995 0.025 0.945 1.046 0.919 1.072 2.55% 5.10% 7.65% 0.946
Mn, wt.% 0.314 0.013 0.288 0.341 0.274 0.354 4.23% 8.46% 12.70% 0.299
Mo, ppm 81 7.5 66 96 58 103 9.33% 18.66% 27.99% 77
Na, wt.% 1.21 0.053 1.11 1.32 1.06 1.37 4.37% 8.74% 13.11% 1.15
Ni, ppm 24.1 2.7 18.6 29.6 15.9 32.3 11.36% 22.72% 34.08% 22.9
P, wt.% 0.347 0.029 0.290 0.405 0.261 0.434 8.32% 16.65% 24.97% 0.330
Pb, ppm 6.83 1.33 4.16 9.50 2.82 10.83 19.55% 39.11% 58.66% 6.48
Rb, ppm 444 34 377 511 343 545 7.56% 15.11% 22.67% 422
S, wt.% 0.295 0.015 0.265 0.324 0.251 0.339 4.99% 9.97% 14.96% 0.280
Sb, ppm 0.70 0.059 0.58 0.81 0.52 0.87 8.48% 16.96% 25.43% 0.66
Sc, ppm 9.55 0.878 7.80 11.31 6.92 12.19 9.19% 18.38% 27.57% 9.08
Sn, ppm 133 9 115 150 107 159 6.52% 13.04% 19.56% 126
Sr, ppm 124 7 109 139 102 146 5.99% 11.98% 17.98% 118
Th, ppm 7.75 0.751 6.25 9.25 5.50 10.00 9.69% 19.38% 29.08% 7.36
Ti, wt.% 0.179 0.014 0.151 0.206 0.137 0.220 7.74% 15.48% 23.22% 0.170
Tl, ppm 2.54 0.43 1.68 3.40 1.25 3.83 16.89% 33.79% 50.68% 2.41
U, ppm 4.73 0.49 3.74 5.71 3.25 6.20 10.41% 20.83% 31.24% 4.49
V, ppm 62 2.0 58 66 56 68 3.16% 6.32% 9.47% 59
W, wt.% 0.989 0.081 0.826 1.151 0.745 1.232 8.22% 16.43% 24.65% 0.939
Y, ppm 13.5 0.77 12.0 15.1 11.2 15.8 5.72% 11.44% 17.15% 12.8
Yb, ppm 1.26 0.13 1.00 1.51 0.87 1.64 10.18% 20.35% 30.53% 1.19
Zn, ppm 216 16 183 249 167 265 7.55% 15.09% 22.64% 205
Zr, ppm 47.3 4.8 37.8 56.8 33.0 61.6 10.07% 20.13% 30.20% 44.9
Ag, ppm 0.499 0.075 0.350 0.649 0.275 0.724 14.97% 29.94% 44.92% 0.474
Al, wt.% 3.13 0.143 2.85 3.42 2.71 3.56 4.55% 9.11% 13.66% 2.98
As, ppm 3.88 0.73 2.41 5.35 1.68 6.09 18.91% 37.82% 56.74% 3.69
Au, ppm 0.505 0.034 0.437 0.572 0.404 0.605 6.65% 13.30% 19.95% 0.479
B, ppm < 30 IND IND IND IND IND IND IND IND IND
Ba, ppm 81 6.9 67 95 60 102 8.51% 17.02% 25.54% 77
Be, ppm 0.73 0.041 0.65 0.81 0.61 0.85 5.62% 11.25% 16.87% 0.69
Bi, ppm 6.89 0.84 5.21 8.56 4.37 9.40 12.18% 24.37% 36.55% 6.54
Ca, wt.% 4.45 0.366 3.71 5.18 3.35 5.54 8.23% 16.46% 24.69% 4.22
Cd, ppm < 0.5 IND IND IND IND IND IND IND IND IND
Ce, ppm 43.9 7.7 28.5 59.4 20.7 67.1 17.60% 35.19% 52.79% 41.7
Co, ppm 15.2 1.21 12.8 17.6 11.6 18.9 7.98% 15.96% 23.94% 14.5
Cr, ppm 51 2.6 45 56 43 59 5.23% 10.47% 15.70% 48
Cu, wt.% 0.203 0.008 0.187 0.218 0.179 0.226 3.90% 7.80% 11.70% 0.192
Fe, wt.% 14.66 0.710 13.24 16.08 12.53 16.79 4.84% 9.68% 14.52% 13.93
Ga, ppm 112 10 93 132 83 141 8.63% 17.26% 25.89% 107
Hf, ppm 0.81 0.12 0.58 1.05 0.46 1.17 14.57% 29.14% 43.72% 0.77
In, ppm 1.67 0.109 1.45 1.88 1.34 1.99 6.57% 13.14% 19.71% 1.58
K, wt.% 1.24 0.044 1.15 1.32 1.10 1.37 3.57% 7.13% 10.70% 1.17
La, ppm 20.6 1.71 17.2 24.0 15.5 25.7 8.29% 16.59% 24.88% 19.6
Li, ppm 84 6.6 70 97 64 103 7.85% 15.70% 23.55% 79
Lu, ppm 0.13 0.011 0.11 0.16 0.10 0.17 8.35% 16.71% 25.06% 0.13
Mg, wt.% 0.948 0.058 0.832 1.065 0.774 1.123 6.13% 12.26% 18.38% 0.901
Mn, wt.% 0.237 0.014 0.209 0.265 0.195 0.279 5.90% 11.81% 17.71% 0.225
Mo, ppm 83 9 66 101 57 110 10.71% 21.43% 32.14% 79
Na, wt.% 0.164 0.030 0.104 0.225 0.074 0.255 18.34% 36.67% 55.01% 0.156
Nb, ppm 10.4 2.0 6.5 14.3 4.5 16.3 18.78% 37.56% 56.34% 9.9
Ni, ppm 24.5 2.6 19.3 29.7 16.7 32.3 10.62% 21.24% 31.86% 23.3
P, wt.% 0.340 0.012 0.316 0.364 0.304 0.376 3.54% 7.08% 10.63% 0.323
Pb, ppm 5.10 1.01 3.07 7.13 2.06 8.14 19.86% 39.72% 59.59% 4.84
S, wt.% 0.297 0.017 0.263 0.331 0.246 0.348 5.74% 11.48% 17.23% 0.282
Sc, ppm 8.77 1.35 6.07 11.47 4.72 12.83 15.41% 30.81% 46.22% 8.33
Se, ppm 2.01 0.151 1.71 2.31 1.55 2.46 7.52% 15.03% 22.55% 1.91
Sn, ppm 110 7 97 123 90 130 6.09% 12.17% 18.26% 104
Sr, ppm 46.1 4.07 38.0 54.3 33.9 58.4 8.83% 17.66% 26.49% 43.8
Te, ppm 0.19 0.03 0.13 0.24 0.10 0.27 15.03% 30.05% 45.08% 0.18
Ti, wt.% 0.097 0.005 0.086 0.107 0.081 0.113 5.54% 11.09% 16.63% 0.092
V, ppm 56 2.3 52 61 49 63 4.08% 8.17% 12.25% 53
Y, ppm 11.5 1.2 9.1 14.0 7.9 15.2 10.61% 21.22% 31.84% 11.0
Zn, ppm 207 11 184 230 172 241 5.52% 11.04% 16.56% 196
Zr, ppm 24.9 1.86 21.2 28.7 19.4 30.5 7.46% 14.92% 22.38% 23.7
Acid Digestion Titration
FeO, wt.% 12.07 0.398 11.27 12.87 10.87 13.26 3.30% 6.60% 9.90% 11.47
Davis Tube Recovery
MassRec, wt.% 11.28 0.240 10.80 11.76 10.56 12.00 2.13% 4.26% 6.38% 10.72
Satmagan 135
Fe3O4, wt.% 10.91 0.196 10.52 11.31 10.33 11.50 1.79% 3.59% 5.38% 10.37
5% window
High
0.532
11.15
8.25
166
0.214
16.86
1.98
1.83
0.435
1.74
IND
0.370
IND
0.319
49.67
191
0.336
116
1.18
1.49
242
2.05
5.85
4.57
166
2.43
5.82
17.6
49.6
114
0.213
16.35
136
1.49
2.21
1.64
34.1
235
0.19
1.045
0.330
85
1.28
25.3
0.365
7.17
466
0.309
0.73
10.03
139
130
8.14
0.188
2.67
4.96
65
1.038
14.2
1.32
227
49.7
0.524
3.29
4.08
0.530
IND
85
0.77
7.23
4.67
IND
46.1
16.0
53
0.213
15.39
118
0.85
1.75
1.30
21.6
88
0.14
0.996
0.248
88
0.173
10.9
25.7
0.357
5.35
0.312
9.21
2.11
115
48.4
0.20
0.101
59
12.1
217
26.2
12.67
11.85
11.46
Analytical results for Au in OREAS 700 (Certified Value 0.506 ppm)
Au Round Replicate Lab Lab Lab Lab Lab Lab
No No 00 1.01 1.03 1.04 1.06 1.07
INAA FA*AAS FA*OES FA*OES FA*AAS FA*AAS
1.0g 30g 25g 40g 40g 30g
1 1 0.497 0.496 0.490 0.507 0.550 0.520
1 2 0.495 0.531 0.470 0.539 0.540 0.530
1 3 0.505 0.484 0.460 0.510 0.520 0.610
1 4 0.514 0.505 0.470 0.542 0.520 0.540
1 5 0.500 0.510 0.480 0.516 0.520 0.590
1 6 0.494 0.519 0.480 0.520 0.530 0.540
7 0.466
8 0.439
9 0.498
10 0.499
11 0.502
12 0.465
13 0.540
14 0.512
15 0.503
16 0.499
17 0.493
18 0.463
19 0.477
20 0.496
Mean 0.493 0.508 0.475 0.522 0.530 0.555
Median 0.498 0.508 0.475 0.518 0.525 0.540
Std Dev. 0.022 0.017 0.010 0.015 0.013 0.036
Rel.Std.Dev. 4.44% 3.28% 2.21% 2.84% 2.39% 6.52%
PDM3 -2.69% 0.21% -6.21% 3.14% 4.65% 9.59%
Z-Score (Absolute) NA 0.14 1.39 0.84 1.20 1.32
Analytical results for Pd in OREAS 700 (Indicative Value 5 ppb)

Pd Round Replicate Lab
No No 1.04
FA*OES
40g
1 1 5
1 2 5
1 3 5
1 4 5
1 5 5
1 6 <5
Mean 5
Median 5
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3 9.09%
Z-Score (Absolute) NA
Analytical results for Pt in OREAS 700 (Indicative Value < 5 ppb)

Pt Round Replicate Lab
No No 1.04
FA*OES
40g
1 1 <5
1 2 <5
1 3 <5
1 4 <5
1 5 <5
1 6 <5
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Lab Lab Lab Lab Lab Lab Lab
1.08 1.09 1.10 1.11 1.12 1.14 1.15
FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS
30g 40g 30g 30g 30g 30g 30g
0.530 0.509 0.506 0.493 0.501 0.459 0.492
0.524 0.515 0.497 0.515 0.502 0.491 0.493
0.534 0.530 0.488 0.495 0.482 0.468 0.512
0.524 0.519 0.507 0.513 0.514 0.469 0.495
0.545 0.562 0.493 0.504 0.495 0.464 0.495
0.524 0.503 0.505 0.489 0.506 0.461 0.510
0.530 0.523 0.499 0.502 0.500 0.469 0.500

0.527 0.517 0.501 0.500 0.502 0.466 0.495
0.008 0.021 0.008 0.011 0.011 0.012 0.009
1.58% 4.01% 1.54% 2.17% 2.17% 2.48% 1.80%
4.68% 3.28% -1.41% -0.98% -1.27% -7.46% -1.37%
1.21 0.51 0.24 0.14 0.21 1.89 0.23
Certified
1.00
ppm
3.00
3.00
1.000
#N/A
16.000
0.506
7.000
Indicative
1.00
ppb
0.00
0.00
1
1
16
5
7
Indicative
1.00
ppb
0.00
0.00
1
1
16
<5
7
Analytical results for Al2O3 in OREAS 700 (Certified Value 10.62 wt.%)
Al2O3 Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.08 1.09
BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF
1 1 10.60 10.63 10.70 10.48 10.80 10.82

1 2 10.70 10.64 10.60 10.41 10.80 10.66
1 3 10.60 10.64 10.40 10.44 10.80 10.51
1 4 10.70 10.67 10.50 10.46 10.80 10.43
1 5 10.60 10.73 10.30 10.64 10.70 10.72
1 6 10.60 10.66 10.40 10.58 10.60 10.48
Mean 10.63 10.66 10.48 10.50 10.75 10.60
Median 10.60 10.65 10.45 10.47 10.80 10.58
Std Dev. 0.052 0.037 0.147 0.089 0.084 0.154
Rel.Std.Dev. 0.49% 0.34% 1.40% 0.85% 0.78% 1.45%
PDM3 0.10% 0.37% -1.31% -1.14% 1.20% -0.20%
Z-Score (Absolute) 0.08 0.30 1.06 0.92 1.20 0.16
Analytical results for As in OREAS 700 (Indicative Value 33.3 ppm)

As Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.09 1.11 1.13 1.14 1.15 3.05
1 1 < 100 30.0 30.0 50.0 30.0 < 10

1 2 < 100 30.0 30.0 30.0 40.0 < 10
1 3 < 100 30.0 30.0 40.0 30.0 < 10
1 4 < 100 30.0 40.0 30.0 30.0
1 5 < 100 30.0 40.0 40.0 40.0
1 6 < 100 30.0 30.0 40.0 20.0
Mean 30.0 33.3 38.3 31.7
Median 30.0 30.0 40.0 30.0
Std Dev. 0.0 5.2 7.5 7.5
Rel.Std.Dev. 0.00% 15.49% 19.64% 23.77%
PDM3 -10.00% 0.00% 15.00% -5.00%
Z-Score (Absolute) NA 1.01 0.34 2.36 0.34 NA
Analytical results for BaO in OREAS 700 (Indicative Value 135 ppm)
BaO Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.06 1.11 1.13 1.15 1.16 3.05
1 1 113 150 130 130 170 150

1 2 < 100 150 150 100 180 160
1 3 120 150 100 100 210 130
1 4 190 180 130 100 190
1 5 123 170 90 120 210
1 6 117 150 130 100 210
Mean 133 158 122 108 195 147
Median 120 150 130 100 200 150
Std Dev. 32 13 22 13 18 15
Rel.Std.Dev. 24.36% 8.39% 18.32% 12.27% 9.03% 10.41%
PDM3 -1.70% 17.38% -9.81% -19.69% 44.56% 8.73%
Z-Score (Absolute) 0.47 0.81 0.54 1.77 4.27 0.47
Analytical results for CaO in OREAS 700 (Certified Value 7.86 wt.%)
CaO Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.08 1.09
1 1 8.00 7.96 8.13 7.82 7.74 8.02

1 2 7.97 7.93 8.06 7.75 7.75 7.89
1 3 7.97 7.94 7.97 7.75 7.78 7.88
1 4 7.98 7.95 8.01 7.71 7.73 7.82
1 5 7.99 7.95 7.86 7.79 7.88 7.95
1 6 7.94 7.96 7.90 7.85 7.86 7.89
Mean 7.98 7.95 7.99 7.78 7.79 7.91
Median 7.98 7.95 7.99 7.77 7.77 7.89
Std Dev. 0.021 0.012 0.100 0.052 0.064 0.069
Rel.Std.Dev. 0.26% 0.15% 1.26% 0.66% 0.83% 0.88%
PDM3 1.50% 1.16% 1.67% -1.00% -0.86% 0.63%
Z-Score (Absolute) 0.67 0.48 0.77 0.76 0.67 0.18
Analytical results for Cl in OREAS 700 (Certified Value 158 ppm)

Cl Round Replicate Lab Lab Lab Lab Lab
No No 1.11 1.13 1.14 1.15 3.05
BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF
1 1 220 180 120 160 140

1 2 210 160 180 150 130
1 3 160 170 160 150 140
1 4 160 170 190 140
1 5 160 160 160 140
1 6 150 180 150 150
Mean 177 170 160 148 137
Median 160 170 160 150 140
Std Dev. 30 9 24 8 6
Rel.Std.Dev. 17.04% 5.26% 15.31% 5.07% 4.22%
PDM3 11.58% 7.37% 1.05% -6.32% -13.68%
Z-Score (Absolute) 0.96 0.58 0.00 0.67 1.35
Analytical results for Co in OREAS 700 (Indicative Value 17.2 ppm)

Co Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.06 1.11 1.13 1.14 1.15 3.05
1 1 < 100 20.0 20.0 < 10 10.0 < 10

1 2 < 100 20.0 10.0 20.0 10.0 < 10
1 3 < 100 20.0 10.0 20.0 20.0 < 10
1 4 < 100 20.0 20.0 30.0 10.0
1 5 < 100 30.0 10.0 20.0 10.0
1 6 < 100 30.0 10.0 20.0 10.0
Mean 23.3 13.3 22.0 11.7
Median 20.0 10.0 20.0 10.0
Std Dev. 5.2 5.2 4.5 4.1
Rel.Std.Dev. 22.13% 38.73% 20.33% 34.99%
PDM3 35.92% -22.33% 28.16% -32.04%
Z-Score (Absolute) NA 0.76 0.58 0.58 1.03 NA
Analytical results for Cr2O3 in OREAS 700 (Indicative Value 79 ppm)

Cr2O3 Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.05 1.06 1.11 1.13 1.14 1.15
1 1 < 100 < 100 85 60 51 70

1 2 < 100 < 100 78 67 103 66
1 3 < 100 < 100 78 61 88 74
1 4 < 100 < 100 85 119 110 68
1 5 < 100 < 100 86 62 96 69
1 6 < 100 < 100 81 65 82 93
Mean 82 72 88 73
Median 83 64 92 70
Std Dev. 4 23 21 10
Rel.Std.Dev. 4.45% 31.81% 23.62% 13.63%
PDM3 4.03% -8.42% 11.84% -7.15%
Z-Score (Absolute) NA NA 0.00 1.31 0.42 0.88
Analytical results for Cu in OREAS 700 (Certified Value 0.204 wt.%)

Cu Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.04 1.06 1.11 1.13 1.14 1.15
1 1 0.212 0.200 0.204 0.192 0.192 0.224

1 2 0.205 0.210 0.196 0.208 0.198 0.215
1 3 0.210 0.230 0.202 0.213 0.208 0.202
1 4 0.205 0.260 0.220 0.190 0.207 0.208
1 5 0.210 0.210 0.202 0.195 0.195 0.220
1 6 0.212 0.240 0.211 0.201 0.190 0.237
Mean 0.209 0.225 0.206 0.200 0.198 0.218
Median 0.210 0.220 0.203 0.198 0.197 0.218
Std Dev. 0.003 0.023 0.008 0.009 0.008 0.012
Rel.Std.Dev. 1.54% 10.04% 4.10% 4.60% 3.84% 5.68%
PDM3 2.68% 10.54% 1.13% -1.82% -2.56% 6.94%
Z-Score (Absolute) 0.86 3.13 0.41 0.44 0.65 1.54
Analytical results for Fe in OREAS 700 (Certified Value 16.06 wt.%)
Fe Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.07 1.08
1 1 16.40 16.20 17.00 16.76 16.18 16.00

1 2 16.30 16.20 16.90 16.99 16.13 15.90
1 3 16.40 16.20 16.70 16.95 16.17 15.90
1 4 16.40 16.20 16.90 16.92 16.10 15.90
1 5 16.40 16.20 16.60 16.99 16.06 16.00
1 6 16.20 16.20 16.50 17.00 16.16 16.00
Mean 16.35 16.20 16.77 16.94 16.13 15.95
Median 16.40 16.20 16.80 16.97 16.15 15.95
Std Dev. 0.084 0.000 0.197 0.091 0.046 0.055
Rel.Std.Dev. 0.51% 0.00% 1.17% 0.54% 0.29% 0.34%
PDM3 1.83% 0.89% 4.42% 5.47% 0.48% -0.66%
Z-Score (Absolute) 1.56 0.73 3.80 4.71 0.35 0.48
Analytical results for K2O in OREAS 700 (Certified Value 1.89 wt.%)
K2O Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.08 1.09
1 1 1.95 1.92 1.91 1.87 1.89 1.77

1 2 1.91 1.91 1.91 1.86 1.88 1.74
1 3 1.92 1.92 1.86 1.84 1.88 1.75
1 4 1.91 1.92 1.89 1.86 1.86 1.74
1 5 1.91 1.93 1.85 1.89 1.90 1.74
1 6 1.90 1.93 1.84 1.85 1.89 1.74
Mean 1.92 1.92 1.88 1.86 1.88 1.75
Median 1.91 1.92 1.88 1.86 1.89 1.74
Std Dev. 0.018 0.006 0.031 0.017 0.014 0.012
Rel.Std.Dev. 0.91% 0.31% 1.64% 0.93% 0.73% 0.67%
PDM3 1.48% 1.74% -0.63% -1.43% -0.28% -7.56%
Z-Score (Absolute) 1.31 1.82 0.15 0.80 0.15 6.06
Analytical results for MgO in OREAS 700 (Certified Value 1.74 wt.%)
MgO Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.08 1.09
1 1 1.72 1.75 1.65 1.68 1.70 1.78

1 2 1.73 1.74 1.64 1.69 1.76 1.74
1 3 1.72 1.74 1.67 1.63 1.77 1.76
1 4 1.74 1.75 1.65 1.65 1.75 1.73
1 5 1.70 1.74 1.62 1.67 1.77 1.76
1 6 1.71 1.75 1.62 1.68 1.78 1.73
Mean 1.72 1.75 1.64 1.67 1.76 1.75
Median 1.72 1.75 1.65 1.68 1.77 1.75
Std Dev. 0.014 0.005 0.019 0.023 0.029 0.019
Rel.Std.Dev. 0.82% 0.31% 1.18% 1.35% 1.64% 1.07%
PDM3 -1.11% 0.33% -5.61% -4.18% 0.90% 0.64%
Z-Score (Absolute) 0.63 0.02 2.53 1.92 0.49 0.11
Analytical results for MnO in OREAS 700 (Certified Value 0.415 wt.%)
MnO Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.06 1.08 1.09 1.11
1 1 0.410 0.430 0.370 0.400 0.381 0.412

1 2 0.420 0.430 0.370 0.400 0.376 0.412
1 3 0.420 0.410 0.370 0.400 0.374 0.414
1 4 0.410 0.410 0.370 0.400 0.369 0.411
1 5 0.400 0.430 0.370 0.400 0.375 0.414
1 6 0.390 0.430 0.380 0.410 0.374 0.411
Mean 0.408 0.423 0.372 0.402 0.375 0.412
Median 0.410 0.430 0.370 0.400 0.375 0.412
Std Dev. 0.012 0.010 0.004 0.004 0.004 0.001
Rel.Std.Dev. 2.86% 2.44% 1.10% 1.02% 1.10% 0.33%
PDM3 -1.53% 2.09% -10.37% -3.14% -9.63% -0.56%
Z-Score (Absolute) 0.17 0.67 2.57 0.69 2.27 0.08
Analytical results for Mo in OREAS 700 (Indicative Value 118 ppm)

Mo Round Replicate Lab
No No 1.05
BF*XRF
1 1 120
1 2 120
1 3 110
1 4 120
1 5 120
1 6 120
Mean 118
Median 120
Std Dev. 4
Rel.Std.Dev. 3.45%
PDM3 0.00%
Analytical results for Na2O in OREAS 700 (Certified Value 1.65 wt.%)
Na2O Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.05 1.06 1.08 1.09 1.11
1 1 1.66 1.73 1.49 1.57 1.60 1.66

1 2 1.67 1.69 1.42 1.59 1.56 1.66
1 3 1.61 1.66 1.42 1.60 1.59 1.68
1 4 1.65 1.69 1.39 1.63 1.55 1.67
1 5 1.64 1.64 1.43 1.61 1.57 1.66
1 6 1.63 1.68 1.44 1.68 1.56 1.65
Mean 1.64 1.68 1.43 1.61 1.57 1.66
Median 1.65 1.69 1.43 1.61 1.57 1.66
Std Dev. 0.022 0.031 0.033 0.038 0.021 0.010
Rel.Std.Dev. 1.31% 1.82% 2.31% 2.37% 1.34% 0.62%
PDM3 -0.62% 1.69% -13.42% -2.44% -4.90% 0.49%
Z-Score (Absolute) 0.11 1.02 6.68 0.99 2.19 0.43
Analytical results for Ni in OREAS 700 (Certified Value < 50 ppm)

Ni Round Replicate Lab Lab Lab Lab Lab
No No 1.11 1.13 1.14 1.15 3.05
1 1 60 20 < 10 20 30
1 2 30 30 30 20 60
1 3 40 30 20 20 30
1 4 40 20 40 40
1 5 40 30 30 20
1 6 30 40 10 60
Mean 40 28 26 30 40
Median 40 30 30 20 30
Std Dev. 11 8 11 17 17
Rel.Std.Dev. 27.39% 26.57% 43.85% 55.78% 43.30%
PDM3
Z-Score (Absolute) 1.35 0.00 0.67 0.50 1.35
Analytical results for P in OREAS 700 (Certified Value 0.353 wt.%)

P Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.08 1.09
1 1 0.360 0.356 0.353 0.340 0.359 0.348

1 2 0.360 0.359 0.345 0.340 0.359 0.342
1 3 0.350 0.354 0.343 0.340 0.360 0.337
1 4 0.360 0.358 0.347 0.340 0.364 0.332
1 5 0.340 0.356 0.342 0.340 0.360 0.342
1 6 0.360 0.360 0.340 0.340 0.366 0.340
Mean 0.355 0.357 0.345 0.340 0.361 0.340
Median 0.360 0.357 0.344 0.340 0.360 0.341
Std Dev. 0.008 0.002 0.005 0.000 0.003 0.005
Rel.Std.Dev. 2.36% 0.62% 1.33% 0.00% 0.81% 1.55%
PDM3 0.68% 1.29% -2.16% -3.57% 2.48% -3.55%
Z-Score (Absolute) 0.65 0.69 1.17 1.34 1.33 1.93
Analytical results for Pb in OREAS 700 (Certified Value < 10 ppm)
Pb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.06 1.11 1.13 1.14 1.15 3.05
1 1 < 100 < 10 < 10 < 10 < 10 20.0

1 2 < 100 < 10 < 10 < 10 < 10 30.0
1 3 < 100 < 10 < 10 < 10 < 10 10.0
1 4 < 100 < 10 < 10 < 10 < 10
1 5 < 100 < 10 < 10 < 10 < 10
1 6 < 100 < 10 < 10 < 10 < 10
Mean 20.0
Median 20.0
Std Dev. 10.0
Rel.Std.Dev. 50.00%
PDM3
Z-Score (Absolute) NA NA NA NA NA NA
Analytical results for S in OREAS 700 (Certified Value 0.304 wt.%)

S Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.04 1.05 1.06 1.09 1.11 1.13
1 1 0.320 0.320 0.200 0.301 0.300 0.304

1 2 0.310 0.330 0.190 0.302 0.292 0.322
1 3 0.310 0.330 0.210 0.304 0.295 0.325
1 4 0.320 0.360 0.100 0.273 0.319 0.302
1 5 0.310 0.290 0.100 0.306 0.295 0.303
1 6 0.330 0.360 0.090 0.310 0.308 0.308
Mean 0.317 0.332 0.148 0.299 0.302 0.311
Median 0.315 0.330 0.145 0.303 0.298 0.306
Std Dev. 0.008 0.026 0.057 0.013 0.010 0.010
Rel.Std.Dev. 2.58% 7.96% 38.47% 4.43% 3.40% 3.28%
PDM3 4.19% 9.12% -51.20% -1.51% -0.80% 2.21%
Z-Score (Absolute) 1.34 1.43 18.44 0.00 0.35 0.67
Analytical results for SiO2 in OREAS 700 (Certified Value 47.3 wt.%)
SiO2 Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.07 1.08
1 1 47.30 47.50 47.30 47.36 47.88 47.10

1 2 46.90 47.50 47.00 47.31 48.21 47.20
1 3 47.00 47.50 46.40 47.30 48.20 47.50
1 4 47.10 47.50 46.80 47.20 47.88 47.10
1 5 47.00 47.60 45.90 47.45 47.79 48.00
1 6 47.10 47.60 46.00 47.37 48.05 47.90
Mean 47.07 47.53 46.57 47.33 48.00 47.47
Median 47.05 47.50 46.60 47.34 47.97 47.35
Std Dev. 0.137 0.052 0.561 0.084 0.179 0.403
Rel.Std.Dev. 0.29% 0.11% 1.20% 0.18% 0.37% 0.85%
PDM3 -0.50% 0.49% -1.55% 0.06% 1.48% 0.35%
Z-Score (Absolute) 0.67 0.37 1.80 0.08 1.43 0.22
Analytical results for Sn in OREAS 700 (Certified Value 182 ppm)

Sn Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.09 1.11 1.13 1.14
PSF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF
1 1 150 230 58 200 170 150

1 2 130 210 39 220 170 170
1 3 150 190 80 200 170 170
1 4 130 200 10 220 190 190
1 5 140 200 83 200 180 170
1 6 130 210 < 10 220 190 150
Mean 138 207 54 210 178 167
Median 135 205 58 210 175 170
Std Dev. 10 14 30 11 10 15
Rel.Std.Dev. 7.11% 6.61% 56.28% 5.22% 5.51% 9.03%
PDM3 -24.09% 13.41% -70.37% 15.24% -2.14% -8.54%
Z-Score (Absolute) 0.67 0.71 2.38 0.78 0.13 0.10
Analytical results for Sr in OREAS 700 (Indicative Value 47.5 ppm)

Sr Round Replicate Lab Lab Lab Lab Lab
No No 1.11 1.13 1.14 1.15 3.05
1 1 100.0 60.0 < 10 30.0 50.0

1 2 100.0 50.0 30.0 30.0 50.0
1 3 100.0 50.0 10.0 30.0 40.0
1 4 100.0 50.0 60.0 30.0
1 5 100.0 40.0 < 10 30.0
1 6 100.0 50.0 < 10 40.0
Mean 100.0 50.0 33.3 31.7 46.7
Median 100.0 50.0 30.0 30.0 50.0
Std Dev. 0.0 6.3 25.2 4.1 5.8
Rel.Std.Dev. 0.00% 12.65% 75.50% 12.89% 12.37%
PDM3 110.38% 5.19% -29.87% -33.38% -1.82%
Z-Score (Absolute) 2.16 0.13 1.44 0.67 0.00
Analytical results for TiO2 in OREAS 700 (Certified Value 0.32 wt.%)
TiO2 Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.04 1.05 1.06 1.08 1.09
1 1 0.330 0.330 0.290 0.430 0.340 0.317

1 2 0.320 0.320 0.300 0.350 0.340 0.315
1 3 0.320 0.330 0.280 0.350 0.340 0.311
1 4 0.320 0.330 0.290 0.350 0.340 0.310
1 5 0.320 0.330 0.280 0.380 0.340 0.313
1 6 0.330 0.330 0.280 0.390 0.330 0.309
Mean 0.323 0.328 0.287 0.375 0.338 0.312
Median 0.320 0.330 0.285 0.365 0.340 0.312
Std Dev. 0.005 0.004 0.008 0.032 0.004 0.003
Rel.Std.Dev. 1.60% 1.24% 2.85% 8.56% 1.21% 0.98%
PDM3 0.97% 2.53% -10.48% 17.10% 5.65% -2.42%
Z-Score (Absolute) 0.20 0.71 2.62 4.18 1.35 0.64
Analytical results for V2O5 in OREAS 700 (Certified Value 110 ppm)
V2O5 Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.06 1.11 1.13 1.14 1.15 3.05
1 1 < 100 120 110 70 110 110

1 2 < 100 120 110 140 120 110
1 3 < 100 120 110 110 110 90
1 4 < 100 120 110 120 110
1 5 < 100 120 110 120 110
1 6 < 100 110 110 90 110
Mean 118 110 108 112 103
Median 120 110 115 110 110
Std Dev. 4 0 25 4 12
Rel.Std.Dev. 3.45% 0.00% 22.92% 3.66% 11.17%
PDM3 7.49% -0.08% -1.59% 1.43% -6.14%
Z-Score (Absolute) NA 2.70 0.67 0.00 0.00 2.02
Analytical results for W in OREAS 700 (Certified Value 1.13 wt.%)

W Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.07 1.08 1.09
PSF*XRF PF*MS BF*XRF BF*XRF BF*XRF BF*XRF
1 1 1.14 1.25 1.14 1.15 1.14 0.96

1 2 1.14 1.13 1.13 1.15 1.16 0.97
1 3 1.14 1.11 1.13 1.15 1.16 0.93
1 4 1.14 1.08 1.14 1.16 1.15 0.79
1 5 1.14 1.13 1.13 1.15 1.16 0.93
1 6 1.14 1.14 1.14 1.15 1.17 0.96
Mean 1.14 1.14 1.14 1.15 1.16 0.92
Median 1.14 1.13 1.14 1.15 1.16 0.94
Std Dev. 0.000 0.056 0.005 0.004 0.010 0.068
Rel.Std.Dev. 0.00% 4.93% 0.48% 0.35% 0.89% 7.38%
PDM3 1.06% 1.07% 0.61% 2.09% 2.53% -18.07%
Z-Score (Absolute) 0.73 0.02 0.56 1.12 1.29 5.63
Analytical results for Zn in OREAS 700 (Certified Value 231 ppm)
Zn Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.06 1.11 1.13 1.14 1.15 3.05
1 1 200 240 220 210 220 240

1 2 200 240 210 230 220 240
1 3 200 240 220 220 220 230
1 4 300 240 210 250 220
1 5 300 250 210 220 220
1 6 300 240 220 220 220
Mean 250 242 215 225 220 237
Median 250 240 215 220 220 240
Std Dev. 55 4 5 14 0 6
Rel.Std.Dev. 21.91% 1.69% 2.55% 6.13% 0.00% 2.44%
PDM3 8.43% 4.82% -6.75% -2.41% -4.58% 2.65%
Z-Score (Absolute) 1.35 0.83 0.83 0.52 0.52 0.52
Analytical results for Zr in OREAS 700 (Indicative Value 53 ppm)

Zr Round Replicate Lab Lab Lab Lab Lab
No No 1.11 1.13 1.14 1.15 3.05
1 1 70 40 < 10 40 50
1 2 70 50 140 40 60
1 3 70 50 120 40 50
1 4 80 40 180 40
1 5 70 40 110 40
1 6 70 60 100 40
Mean 72 47 130 40 53
Median 70 45 120 40 50
Std Dev. 4 8 32 0 6
Rel.Std.Dev. 5.70% 17.50% 24.33% 0.00% 10.83%
PDM3 36.51% -11.11% 147.62% -23.81% 1.59%
Z-Score (Absolute) 0.84 0.34 2.82 0.67 0.00
Lab Lab Lab Lab Lab Lab
1.11 1.13 1.14 1.15 1.16 3.05
10.65 10.55 10.70 10.50 10.64 10.75

10.65 10.35 10.85 10.50 10.65 10.80
10.65 10.45 10.70 10.55 10.60 10.75
10.60 10.50 10.90 10.65 10.60
10.70 10.35 10.85 10.50 10.59
10.60 10.50 10.65 10.70 10.60
10.64 10.45 10.78 10.57 10.61 10.77
10.65 10.48 10.78 10.53 10.60 10.75
0.038 0.084 0.104 0.088 0.025 0.029
0.35% 0.80% 0.96% 0.83% 0.24% 0.27%
0.18% -1.63% 1.43% -0.53% -0.10% 1.35%
0.15 1.32 1.16 0.43 0.08 1.10
1.11 1.13 1.14 1.15 1.16 3.05
7.86 7.70 7.85 7.72 7.91 7.77

7.87 7.66 7.97 7.71 7.97 7.79
7.87 7.66 7.88 7.75 7.95 7.77
7.83 7.70 8.00 7.78 7.92
7.88 7.61 7.96 7.73 7.95
7.84 7.69 7.86 7.72 7.94
7.86 7.67 7.92 7.74 7.94 7.78
7.87 7.68 7.92 7.73 7.94 7.77
0.019 0.035 0.064 0.026 0.019 0.012
0.25% 0.45% 0.81% 0.33% 0.24% 0.15%
0.01% -2.38% 0.80% -1.56% 1.06% -1.03%
0.18 1.55 0.27 1.07 0.42 0.77
Lab
3.05
BF*XRF
90
99
87
92
90
6
6.79%
16.49%
0.67
Lab Lab
3.04 3.05
BF*XRF BF*XRF
0.200 0.208
0.200 0.192
0.200 0.194
0.200 0.198
0.200 0.194
0.000 0.009
0.00% 4.40%
-1.74% -2.72%
0.41 0.70
Lab Lab Lab Lab Lab Lab Lab Lab
1.09 1.11 1.13 1.14 1.15 1.16 3.04 3.05
BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF
16.15 15.94 15.91 15.84 15.78 16.19 16.00 16.02

16.15 15.97 15.77 16.10 15.73 16.23 16.00 16.02
16.20 16.00 15.83 15.89 15.82 16.24 16.00 15.98
16.23 15.94 15.78 16.17 15.84 16.20
16.14 16.03 15.77 16.08 15.78 16.21
16.24 15.92 15.87 15.90 15.94 16.22
16.18 15.97 15.82 16.00 15.82 16.21 16.00 16.01
16.18 15.96 15.81 15.99 15.80 16.21 16.00 16.02
0.043 0.042 0.059 0.136 0.072 0.018 0.000 0.023
0.26% 0.26% 0.37% 0.85% 0.46% 0.11% 0.00% 0.14%
0.79% -0.56% -1.46% -0.37% -1.51% 0.98% -0.35% -0.31%
0.62 0.56 1.35 0.40 1.39 0.79 0.38 0.35

1.11 1.13 1.14 1.15 1.16 3.05
1.87 1.90 1.92 1.87 1.94 1.88

1.88 1.87 1.95 1.87 1.94 1.88
1.88 1.89 1.93 1.88 1.95 1.88
1.86 1.89 1.96 1.87 1.93
1.88 1.87 1.95 1.87 1.94
1.86 1.89 1.93 1.88 1.95
1.87 1.88 1.94 1.87 1.94 1.88
1.87 1.89 1.94 1.87 1.94 1.88
0.009 0.014 0.017 0.006 0.006 0.003
0.47% 0.75% 0.87% 0.34% 0.30% 0.15%
-1.12% -0.37% 2.50% -0.99% 2.87% -0.55%
0.55 0.07 2.44 0.44 2.75 0.07

1.11 1.13 1.14 1.15 1.16 3.05
1.76 1.72 1.78 1.70 1.75 1.78

1.74 1.69 1.82 1.69 1.76 1.78
1.76 1.72 1.78 1.70 1.74 1.77
1.74 1.72 1.82 1.71 1.75
1.76 1.70 1.80 1.68 1.74
1.74 1.72 1.78 1.71 1.75
1.75 1.71 1.80 1.70 1.75 1.78
1.75 1.72 1.79 1.70 1.75 1.78
0.011 0.013 0.020 0.012 0.007 0.006
0.63% 0.78% 1.09% 0.69% 0.40% 0.32%
0.62% -1.59% 3.30% -2.35% 0.41% 2.15%
0.10 0.72 1.24 1.15 0.02 0.75
Lab Lab Lab Lab Lab

1.13 1.14 1.15 1.16 3.05
0.416 0.424 0.412 0.427 0.411

0.405 0.433 0.412 0.429 0.412
0.411 0.425 0.414 0.430 0.411
0.411 0.434 0.409 0.427
0.405 0.433 0.410 0.430
0.412 0.425 0.414 0.429
0.410 0.429 0.412 0.429 0.411
0.411 0.429 0.412 0.429 0.411
0.004 0.005 0.002 0.001 0.001
1.05% 1.11% 0.50% 0.32% 0.14%
-1.13% 3.46% -0.68% 3.38% -0.80%
0.07 1.11 0.09 1.02 0.00
Lab Lab Lab Lab

1.13 1.14 1.15 3.05
BF*XRF BF*XRF BF*XRF BF*XRF
1.71 1.62 1.65 1.64

1.65 1.66 1.66 1.64
1.68 1.64 1.67 1.64
1.70 1.68 1.67
1.66 1.66 1.65
1.68 1.65 1.68
1.68 1.65 1.66 1.64
1.68 1.65 1.66 1.64
0.023 0.020 0.012 0.003
1.37% 1.22% 0.73% 0.18%
1.49% -0.17% 0.49% -0.93%
0.92 0.11 0.43 0.26

1.11 1.13 1.14 1.15 1.16 3.05
0.350 0.352 0.364 0.355 0.351 0.354

0.351 0.345 0.368 0.354 0.352 0.355
0.350 0.349 0.364 0.356 0.350 0.353
0.350 0.349 0.370 0.359 0.351
0.351 0.346 0.370 0.354 0.351
0.350 0.349 0.363 0.360 0.353
0.350 0.348 0.367 0.356 0.351 0.354
0.350 0.349 0.366 0.356 0.351 0.354
0.001 0.003 0.003 0.003 0.001 0.001
0.15% 0.72% 0.88% 0.72% 0.29% 0.28%
-0.64% -1.21% 3.94% 1.06% -0.36% 0.40%
0.36 0.66 2.11 0.56 0.20 0.20
Lab Lab Lab Lab Lab
1.14 1.15 1.16 3.04 3.05
0.275 0.311 0.301 0.350 0.317

0.277 0.302 0.301 0.350 0.296
0.300 0.284 0.302 0.350 0.301
0.287 0.289 0.312
0.274 0.304 0.343
0.275 0.313 0.293
0.281 0.301 0.309 0.350 0.305
0.276 0.303 0.302 0.350 0.301
0.010 0.012 0.018 0.000 0.011
3.67% 3.90% 5.79% 0.00% 3.60%
-7.44% -1.13% 1.55% 15.15% 0.24%
3.00 0.46 0.31 5.05 0.01
Lab Lab Lab Lab Lab Lab Lab Lab Lab

1.09 1.10 1.11 1.13 1.14 1.15 1.16 3.04 3.05
BF*XRF PF*OES BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF
47.56 49.21 47.30 46.30 47.00 46.60 47.40 48.00 47.60

47.32 49.05 47.50 46.30 47.70 46.60 47.28 48.00 47.70
46.68 48.63 47.40 46.70 47.00 46.80 47.29 48.00 47.70
47.11 49.34 47.30 46.10 47.80 46.80 47.34
47.66 48.34 47.50 46.40 47.80 46.60 47.21
47.22 48.91 47.20 46.80 47.70 47.00 47.29
47.26 48.91 47.37 46.43 47.50 46.73 47.30 48.00 47.67
47.27 48.98 47.35 46.35 47.70 46.70 47.29 48.00 47.70
0.349 0.375 0.121 0.266 0.390 0.163 0.064 0.000 0.058
0.74% 0.77% 0.26% 0.57% 0.82% 0.35% 0.14% 0.00% 0.12%
-0.09% 3.41% 0.14% -1.84% 0.42% -1.20% 0.00% 1.48% 0.77%
0.24 3.48 0.00 2.10 0.30 1.42 0.15 1.42 0.67
Lab Lab Lab

1.15 1.16 1.20
BF*XRF BF*XRF BF*MS
160 220 230

170 160 232
170 140 227
180 120 236
170 100 227
180 190 235
172 155 231
170 150 231
8 45 4
4.39% 28.78% 1.67%
-5.80% -14.94% 26.85%
0.00 0.34 1.20

1.11 1.13 1.14 1.15 1.16 3.05
0.320 0.320 0.320 0.310 0.322 0.320

0.310 0.310 0.330 0.310 0.319 0.320
0.320 0.310 0.320 0.310 0.320 0.320
0.310 0.310 0.330 0.310 0.320
0.310 0.310 0.320 0.310 0.325
0.310 0.310 0.320 0.310 0.323
0.313 0.312 0.323 0.310 0.322 0.320
0.310 0.310 0.320 0.310 0.321 0.320
0.005 0.004 0.005 0.000 0.002 0.000
1.65% 1.31% 1.60% 0.00% 0.70% 0.00%
-2.15% -2.67% 0.97% -3.20% 0.40% -0.07%
0.57 0.83 0.20 0.83 0.06 0.06
Lab Lab Lab Lab Lab Lab Lab Lab

1.10 1.11 1.13 1.14 1.16 1.17 1.20 3.04
PF*OES BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF BF*XRF
1.11 1.09 1.12 1.10 1.11 1.16 1.16 1.10

1.13 1.08 1.11 1.12 1.11 1.15 1.17 1.10
1.11 1.09 1.11 1.11 1.11 1.16 1.16 1.10
1.12 1.09 1.12 1.13 1.11 1.15 1.17
1.12 1.09 1.11 1.13 1.11 1.16 1.17
1.15 1.10 1.12 1.10 1.11 1.15 1.16
1.12 1.09 1.12 1.11 1.11 1.16 1.17 1.10
1.12 1.09 1.12 1.11 1.11 1.16 1.17 1.10
0.012 0.006 0.005 0.014 0.003 0.005 0.005 0.000
1.11% 0.58% 0.49% 1.24% 0.27% 0.47% 0.47% 0.00%
-0.50% -3.38% -1.16% -1.60% -1.62% 2.39% 3.27% -2.49%
0.02 0.96 0.12 0.29 0.29 1.23 1.57 0.62
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
10.62
9.00
Indicative
1.00
ppm
1.00
1.00
1.0
3.0
16.0
33.3
9.0
Indicative
1.00
ppm
0.00
0.00
1
4
16
135
10
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
7.86
10.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
158
11
Indicative
1.00
ppm
1.00
1.00
1.0
5.0
16.0
17.2
11.0
Indicative
1.00
ppm
0.00
0.00
1
3
16
79
9
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.204
12.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
16.06
13.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.89
14.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.74
15.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.415
16.000
Indicative
1.00
ppm
0.00
0.00
1
4
16
118
10
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.65
17.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
< 50
18
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.353
19.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
< 10
20.0
Certified
1.00
wt.%
3.00
3.00
1.000
25.000
16.000
0.304
21.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
47.30
22.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
182
23
Indicative
1.00
ppm
1.00
1.00
1.0
5.0
16.0
47.5
11.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.320
24.000
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
110
25
Certified
1.00
wt.%
2.00
3.00
1.00
20.00
16.00
1.13
26.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
231
27
Indicative
1.00
ppm
0.00
0.00
1
3
16
53
9
Analytical results for LOI in OREAS 700 (Certified Value 1.95 wt.%)
LOI Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.06 1.08 1.09 1.11 1.13
BF*XRF BF*XRF at 1000°C BF*XRF at 1000°C at 1000°C
1 1 2.44 1.54 2.07 2.09 2.01 1.89

1 2 2.47 1.52 2.07 1.98 2.02 1.83
1 3 2.43 1.44 1.87 1.98 1.91 1.87
1 4 2.45 1.77 1.99 1.96 2.02 1.88
1 5 2.44 1.72 2.08 2.01 1.90 1.89
1 6 2.53 1.75 1.73 1.47 1.91 1.88
Mean 2.46 1.62 1.97 1.91 1.96 1.87
Median 2.45 1.63 2.03 1.98 1.96 1.88
Std Dev. 0.037 0.140 0.141 0.223 0.060 0.023
Rel.Std.Dev. 1.50% 8.63% 7.19% 11.69% 3.08% 1.20%
PDM3 25.85% -16.95% 0.70% -2.17% 0.36% -4.16%
Z-Score (Absolute) 3.28 2.27 0.02 0.24 0.02 0.61
Lab Lab Lab Lab
1.14 1.15 1.16 3.05
at 1000°C at 1000°C at 1000°C at 1000°C
2.13 2.32 1.48 1.94

2.02 2.34 1.48 1.84
2.04 2.28 1.52 1.78
2.29 1.67 1.54
1.92 2.32 1.55
1.91 2.26 1.54
2.05 2.20 1.52 1.85
2.03 2.30 1.53 1.84
0.142 0.260 0.031 0.081
6.94% 11.85% 2.06% 4.36%
4.96% 12.47% -22.32% -5.18%
0.57 2.25 2.96 0.74
Certified
1.00
wt.%
2.00
2.00
1.00
#N/A
16.00
1.95
29.00
Analytical results for Ag in OREAS 700 (Indicative Value 0.525 ppm)
Ag Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*MS
1 1 0.510 0.520 0.500 1.090 1.330 < 0.5

1 2 0.520 0.530 < 0.5 1.030 1.180 < 0.5
1 3 0.540 0.560 0.500 1.080 1.030 < 0.5
1 4 0.500 0.490 < 0.5 1.000 0.920 0.581
1 5 0.510 0.590 < 0.5 1.100 1.230 < 0.5
1 6 0.530 0.530 0.500 1.060 1.120 0.951
Mean 0.518 0.537 0.500 1.060 1.135 0.766
Median 0.515 0.530 0.500 1.070 1.150 0.766
Std Dev. 0.015 0.034 0.000 0.038 0.146 0.262
Rel.Std.Dev. 2.84% 6.42% 0.00% 3.63% 12.86% 34.18%
PDM3 -1.27% 2.22% -4.76% 101.90% 116.19% 45.81%
Z-Score (Absolute) 0.10 0.20 0.67 3.02 3.43 0.99
Analytical results for Al in OREAS 700 (Certified Value 5.57 wt.%)

Al Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
4A*OES/MS 4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*OES
1 1 5.57 5.54 5.43 6.03 4.85 5.58

1 2 5.43 5.55 5.52 6.05 5.16 5.62
1 3 5.52 5.53 5.58 6.03 5.18 5.58
1 4 5.19 5.51 5.63 5.71 4.94 5.76
1 5 5.48 5.49 5.60 6.08 5.01 5.66
1 6 5.36 5.46 5.55 5.93 4.94 5.77
Mean 5.42 5.51 5.55 5.97 5.01 5.66
Median 5.45 5.52 5.57 6.03 4.98 5.64
Std Dev. 0.136 0.033 0.071 0.138 0.132 0.085
Rel.Std.Dev. 2.51% 0.60% 1.28% 2.31% 2.63% 1.50%
PDM3 -2.63% -1.04% -0.33% 7.21% -10.00% 1.67%
Z-Score (Absolute) 0.67 0.32 0.17 1.71 2.30 0.28
Analytical results for As in OREAS 700 (Certified Value 4.35 ppm)

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 3.61 4.30 4.00 5.00 11.00 4.00

1 2 4.24 4.30 4.00 4.00 4.00 3.86
1 3 3.56 4.20 5.00 5.00 6.00 3.07
1 4 4.20 4.20 4.00 4.00 5.00 3.76
1 5 1.99 4.20 4.00 5.00 10.00 3.40
1 6 3.00 4.00 5.00 5.00 3.00 3.09
Mean 3.43 4.20 4.33 4.67 6.50 3.53
Median 3.58 4.20 4.00 5.00 5.50 3.58
Std Dev. 0.845 0.110 0.516 0.516 3.271 0.401
Rel.Std.Dev. 24.63% 2.61% 11.92% 11.07% 50.32% 11.38%
PDM3 -21.15% -3.47% -0.40% 7.26% 49.39% -18.92%
Z-Score (Absolute) 1.50 0.67 0.53 0.00 2.90 1.80
Analytical results for Ba in OREAS 700 (Certified Value 158 ppm)

Ba Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES
1 1 140 163 158 111 163 158

1 2 139 161 148 108 165 157
1 3 142 158 146 109 170 160
1 4 132 160 160 109 167 162
1 5 138 163 158 108 157 159
1 6 135 157 159 108 157 165
Mean 138 160 155 109 163 160
Median 138 160 158 109 164 159
Std Dev. 4 2 6 1 5 3
Rel.Std.Dev. 2.66% 1.48% 3.97% 1.07% 3.25% 1.93%
PDM3 -13.02% 1.26% -2.14% -31.21% 3.13% 1.26%
Z-Score (Absolute) 3.21 0.44 0.43 7.84 0.91 0.44
Analytical results for Be in OREAS 700 (Certified Value 2.32 ppm)

Be Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 2.12 2.46 2.40 <5 3.50 2.30

1 2 2.12 2.40 2.50 <5 3.50 2.29
1 3 2.13 2.35 2.30 <5 3.90 2.29
1 4 2.12 2.23 2.50 <5 2.90 2.35
1 5 2.15 2.47 2.20 <5 3.20 2.27
1 6 2.10 2.35 2.40 <5 3.60 2.20
Mean 2.12 2.38 2.38 3.43 2.28
Median 2.12 2.38 2.40 3.50 2.29
Std Dev. 0.016 0.088 0.117 0.344 0.048
Rel.Std.Dev. 0.77% 3.72% 4.91% 10.03% 2.11%
PDM3 -8.41% 2.52% 2.81% 48.10% -1.55%
Z-Score (Absolute) 2.83 0.58 0.67 NA 14.83 0.46
Analytical results for Bi in OREAS 700 (Indicative Value 6.75 ppm)

Bi Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 6.08 6.66 7.70 9.00 5.40 6.46

1 2 6.10 6.30 7.90 10.00 5.46 6.25
1 3 6.23 6.63 7.60 9.00 5.42 6.32
1 4 6.21 6.63 7.90 9.00 5.31 6.43
1 5 6.26 6.73 7.80 11.00 5.42 6.61
1 6 6.24 6.11 8.10 13.00 5.41 6.38
Mean 6.19 6.51 7.83 10.17 5.40 6.41
Median 6.22 6.63 7.85 9.50 5.42 6.41
Std Dev. 0.078 0.246 0.175 1.602 0.050 0.124
Rel.Std.Dev. 1.27% 3.79% 2.24% 15.76% 0.93% 1.94%
PDM3 -8.32% -3.51% 16.11% 50.69% -19.91% -4.99%
Z-Score (Absolute) 0.26 0.00 0.81 1.95 0.77 0.12
Analytical results for Ca in OREAS 700 (Certified Value 5.55 wt.%)

Ca Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 5.08 5.34 5.70 5.45 5.39 5.41

1 2 5.22 5.38 5.84 5.40 5.55 5.49
1 3 5.36 5.34 5.83 5.43 5.49 5.53
1 4 4.93 5.33 5.88 5.32 5.62 5.61
1 5 5.24 5.42 5.76 5.41 5.41 5.46
1 6 5.18 5.34 5.70 5.33 5.32 5.61
Mean 5.17 5.36 5.79 5.39 5.46 5.52
Median 5.20 5.34 5.80 5.41 5.45 5.51
Std Dev. 0.149 0.036 0.076 0.053 0.111 0.081
Rel.Std.Dev. 2.88% 0.67% 1.32% 0.99% 2.03% 1.46%
PDM3 -6.79% -3.35% 4.29% -2.83% -1.50% -0.48%
Z-Score (Absolute) 1.48 0.60 1.34 0.47 0.13 0.13
Analytical results for Cd in OREAS 700 (Indicative Value 0.37 ppm)

Cd Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.18 0.29 < 0.5 < 0.5 < 0.02 < 0.5
1 2 0.20 0.26 < 0.5 < 0.5 < 0.02 < 0.5
1 3 0.15 0.42 < 0.5 < 0.5 < 0.02 < 0.5
1 4 0.11 0.23 < 0.5 < 0.5 < 0.02 < 0.5
1 5 0.18 0.36 < 0.5 < 0.5 < 0.02 < 0.5
1 6 0.20 0.28 < 0.5 < 0.5 < 0.02 < 0.5
Mean 0.17 0.31
Median 0.18 0.29
Std Dev. 0.032 0.070
Rel.Std.Dev. 18.79% 22.93%
PDM3 -54.03% -16.82%
Z-Score (Absolute) 0.67 0.12 NA NA NA NA
Analytical results for Ce in OREAS 700 (Indicative Value 66 ppm)
Ce Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
4A*OES/MS 4A*MS 4A*MS 4A*OES/MS 4A*MS 4A*MS
1 1 57 59 62 79 58 71
1 2 58 59 63 81 60 71
1 3 57 60 63 81 59 73
1 4 60 61 64 86 62 73
1 5 59 62 65 81 61 71
1 6 59 61 63 79 61 72
Mean 58 60 63 81 60 72
Median 58 61 63 81 60 72
Std Dev. 1 1 1 2 2 1
Rel.Std.Dev. 1.65% 1.89% 1.46% 2.98% 2.60% 1.22%
PDM3 -11.30% -8.14% -3.85% 23.24% -8.71% 9.07%
Z-Score (Absolute) 0.78 0.53 0.19 1.82 0.57 0.82
Analytical results for Co in OREAS 700 (Certified Value 16.8 ppm)

No No 1.01 1.03 1.04 1.06 1.08 1.09
4A*OES/MS 4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*MS
1 1 14.8 17.0 15.0 13.0 17.9 15.4

1 2 15.1 16.7 20.0 12.0 18.4 15.4
1 3 16.1 16.5 15.0 12.0 17.9 15.2
1 4 15.5 16.6 15.0 13.0 17.6 15.5
1 5 15.7 16.6 15.0 12.0 18.2 14.9
1 6 15.2 16.4 20.0 12.0 18.2 14.6
Mean 15.4 16.6 16.7 12.3 18.0 15.2
Median 15.4 16.6 15.0 12.0 18.1 15.3
Std Dev. 0.5 0.2 2.6 0.5 0.3 0.4
Rel.Std.Dev. 2.97% 1.24% 15.49% 4.19% 1.59% 2.41%
PDM3 -8.24% -0.86% -0.66% -26.49% 7.49% -9.67%
Z-Score (Absolute) 0.59 0.01 0.01 2.02 0.65 0.70
Analytical results for Cr in OREAS 700 (Certified Value 47.2 ppm)

Cr Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 46.1 42.0 50.0 53.9 38.0 53.1

1 2 45.1 42.0 40.0 48.6 35.0 54.8
1 3 45.8 45.0 50.0 54.8 42.0 54.7
1 4 44.2 42.0 50.0 52.0 39.0 54.4
1 5 46.3 44.0 50.0 50.7 41.0 54.3
1 6 44.8 41.0 40.0 50.0 45.0 54.9
Mean 45.4 42.7 46.7 51.7 40.0 54.4
Median 45.5 42.0 50.0 51.3 40.0 54.6
Std Dev. 0.8 1.5 5.2 2.3 3.5 0.6
Rel.Std.Dev. 1.80% 3.53% 11.07% 4.55% 8.66% 1.19%
PDM3 -3.81% -9.59% -1.12% 9.45% -15.24% 15.17%
Z-Score (Absolute) 0.26 0.81 0.00 1.01 1.35 1.56
Analytical results for Cs in OREAS 700 (Certified Value 109 ppm)

Cs Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.13
1 1 100 116 108 156 107 109

1 2 101 114 105 169 110 106
1 3 105 114 105 169 111 109
1 4 101 117 116 163 119 105
1 5 108 117 109 161 112 104
1 6 96 111 108 165 114 109
Mean 102 115 109 164 112 107
Median 101 115 108 164 111 107
Std Dev. 4 2 4 5 4 2
Rel.Std.Dev. 4.03% 1.98% 3.72% 3.05% 3.71% 2.11%
PDM3 -6.18% 5.91% -0.01% 50.98% 3.21% -1.55%
Z-Score (Absolute) 1.28 0.90 0.42 9.05 0.42 0.44

No No 1.01 1.03 1.04 1.06 1.07 1.08
4A*OES 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS
1 1 0.192 0.206 0.197 0.214 0.199 0.188

1 2 0.204 0.209 0.197 0.212 0.205 0.253
1 3 0.199 0.218 0.209 0.212 0.206 0.197
1 4 0.213 0.194 0.199 0.208 0.197 0.192
1 5 0.208 0.210 0.208 0.223 0.196 0.236
1 6 0.202 0.195 0.199 0.209 0.205 0.187
Mean 0.203 0.205 0.202 0.213 0.201 0.209
Median 0.203 0.207 0.199 0.212 0.202 0.194
Std Dev. 0.007 0.009 0.006 0.005 0.005 0.028
Rel.Std.Dev. 3.58% 4.53% 2.73% 2.56% 2.26% 13.61%
PDM3 0.28% 1.44% -0.46% 5.13% -0.58% 3.21%
Z-Score (Absolute) 0.10 0.83 0.36 2.53 0.44 3.62
Analytical results for Dy in OREAS 700 (Indicative Value 2.68 ppm)

Dy Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
4A*MS 4A*MS 4A*MS 4A*MS
1 1 2.64 3.15 2.71 2.46

1 2 2.55 2.80 2.69 2.46
1 3 2.58 3.15 2.67 2.49
1 4 2.79 2.75 2.88 2.42
1 5 2.69 2.90 2.71 2.46
1 6 2.72 2.75 2.72 2.47
Mean 2.66 2.92 2.73 2.46
Median 2.67 2.85 2.71 2.46
Std Dev. 0.090 0.189 0.074 0.023
Rel.Std.Dev. 3.37% 6.48% 2.72% 0.92%
PDM3 -0.86% 8.64% 1.67% -8.36%
Z-Score (Absolute) 0.11 1.32 0.11 1.24
Analytical results for Er in OREAS 700 (Indicative Value 1.38 ppm)

Er Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 1.34 1.50 1.32 1.36

1 2 1.36 1.65 1.37 1.40
1 3 1.36 1.50 1.40 1.39
1 4 1.37 1.65 1.46 1.42
1 5 1.40 1.75 1.37 1.35
1 6 1.42 1.60 1.37 1.39
Mean 1.38 1.61 1.38 1.39
Median 1.37 1.63 1.37 1.39
Std Dev. 0.029 0.097 0.047 0.027
Rel.Std.Dev. 2.15% 6.03% 3.37% 1.98%
PDM3 -0.43% 16.47% 0.05% 0.38%
Z-Score (Absolute) 1.07 26.94 0.28 0.28
Analytical results for Eu in OREAS 700 (Indicative Value 0.86 ppm)

Eu Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 0.83 0.85 0.81 1.16

1 2 0.85 0.90 0.86 1.18
1 3 0.80 0.85 0.86 1.13
1 4 0.81 0.95 0.89 1.17
1 5 0.87 0.95 0.84 1.16
1 6 0.84 0.80 0.89 1.11
Mean 0.83 0.88 0.86 1.15
Median 0.84 0.88 0.86 1.16
Std Dev. 0.026 0.061 0.029 0.029
Rel.Std.Dev. 3.10% 6.86% 3.40% 2.56%
PDM3 -2.95% 2.87% 0.08% 34.10%
Z-Score (Absolute) 1.03 0.32 0.32 7.56
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 13.81 16.69 16.50 15.56 > 15 15.96

1 2 14.10 16.57 16.60 15.70 > 15 16.08
1 3 14.25 16.66 16.60 15.60 > 15 16.13
1 4 13.08 16.49 16.70 15.33 > 15 16.68
1 5 14.08 16.38 16.80 15.70 > 15 16.07
1 6 13.71 16.38 16.70 15.24 > 15 16.54
Mean 13.84 16.53 16.65 15.52 16.24
Median 13.94 16.53 16.65 15.58 16.11
Std Dev. 0.419 0.135 0.105 0.194 0.292
Rel.Std.Dev. 3.03% 0.81% 0.63% 1.25% 1.80%
PDM3 -11.11% 6.17% 6.95% -0.30% 4.33%
Z-Score (Absolute) 1.65 0.97 1.09 0.01 NA 0.69
Analytical results for Ga in OREAS 700 (Certified Value 129 ppm)

Ga Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 118 130 118 106 126 141

1 2 119 132 114 109 131 140
1 3 121 131 112 108 133 139
1 4 120 130 114 106 132 141
1 5 125 131 114 109 128 137
1 6 122 129 107 104 124 135
Mean 121 130 113 107 129 139
Median 120 131 114 107 130 140
Std Dev. 3 1 4 2 4 2
Rel.Std.Dev. 2.14% 0.86% 3.18% 1.87% 2.74% 1.78%
PDM3 -6.47% 0.92% -12.43% -17.21% -0.22% 7.36%
Z-Score (Absolute) 1.34 0.24 2.42 3.65 0.00 1.63
Analytical results for Gd in OREAS 700 (Indicative Value 4.17 ppm)

Gd Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 3.55 3.80 3.67 5.46

1 2 3.54 4.00 3.59 5.39
1 3 3.65 3.80 3.77 5.35
1 4 3.56 4.00 3.85 5.39
1 5 3.62 4.00 3.82 5.37
1 6 3.74 4.00 3.90 5.37
Mean 3.61 3.93 3.77 5.39
Median 3.59 4.00 3.79 5.38
Std Dev. 0.077 0.103 0.114 0.037
Rel.Std.Dev. 2.13% 2.63% 3.03% 0.69%
PDM3 -13.53% -5.79% -9.76% 29.08%
Z-Score (Absolute) 1.00 0.35 0.35 6.42
Analytical results for Ge in OREAS 700 (Indicative Value 3.43 ppm)

Ge Round Replicate Lab Lab Lab
No No 1.03 1.08 1.13
4A*MS 4A*OES/MS 4A*MS
1 1 5.44 2.90 0.21

1 2 7.64 2.30 0.28
1 3 6.75 0.30 0.24
1 4 6.51 2.50 0.38
1 5 7.83 4.80 0.29
1 6 8.11 4.90 0.28
Mean 7.05 2.95 0.28
Median 7.20 2.70 0.28
Std Dev. 1.005 1.725 0.058
Rel.Std.Dev. 14.27% 58.47% 20.58%
PDM3 105.71% -13.88% -91.83%
Z-Score (Absolute) 1.03 0.00 0.67
Analytical results for Hf in OREAS 700 (Certified Value 1.42 ppm)

Hf Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 1.20 1.42 1.60 1.02 1.40 1.89

1 2 1.40 1.41 1.40 0.86 1.42 1.84
1 3 1.34 1.38 1.60 0.70 1.25 1.88
1 4 1.30 1.42 1.60 0.63 1.32 1.87
1 5 1.30 1.41 1.80 0.71 1.26 1.86
1 6 1.36 1.33 1.80 0.96 1.30 1.85
Mean 1.32 1.40 1.63 0.81 1.33 1.87
Median 1.32 1.41 1.60 0.79 1.31 1.87
Std Dev. 0.069 0.035 0.151 0.157 0.072 0.017
Rel.Std.Dev. 5.21% 2.51% 9.22% 19.33% 5.41% 0.93%
PDM3 -7.07% -1.54% 15.28% -42.59% -6.41% 31.69%
Z-Score (Absolute) 0.67 0.06 1.89 4.75 0.60 3.77
Analytical results for Hg in OREAS 700 (Indicative Value < 10 ppm)

Hg Round Replicate Lab
No No 1.12
4A*OES
1 1 < 10
1 2 < 10
1 3 < 10
1 4 < 10
1 5 < 10
1 6 < 10
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Ho in OREAS 700 (Indicative Value 0.56 ppm)

Ho Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 0.49 0.56 0.50 0.68

1 2 0.50 0.56 0.50 0.69
1 3 0.50 0.54 0.51 0.68
1 4 0.52 0.52 0.53 0.68
1 5 0.50 0.58 0.51 0.70
1 6 0.51 0.58 0.50 0.66
Mean 0.50 0.56 0.51 0.68
Median 0.50 0.56 0.50 0.68
Std Dev. 0.010 0.023 0.014 0.014
Rel.Std.Dev. 2.05% 4.20% 2.66% 2.05%
PDM3 -10.28% -0.77% -9.31% 21.27%
Z-Score (Absolute) 0.68 0.67 0.67 3.80
Analytical results for In in OREAS 700 (Certified Value 2.1 ppm)

In Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 2.07 2.12 2.14 2.49 2.09 2.55

1 2 2.14 2.11 2.06 2.49 2.20 2.63
1 3 2.11 2.02 2.10 2.50 2.14 2.53
1 4 2.13 2.04 2.20 2.41 2.14 2.62
1 5 2.13 2.07 2.16 2.43 2.14 2.67
1 6 2.14 2.04 2.02 2.51 1.99 2.62
Mean 2.12 2.07 2.11 2.47 2.12 2.60
Median 2.13 2.06 2.12 2.49 2.14 2.62
Std Dev. 0.026 0.040 0.067 0.041 0.073 0.055
Rel.Std.Dev. 1.25% 1.94% 3.15% 1.67% 3.47% 2.10%
PDM3 0.78% -1.75% 0.52% 17.56% 0.67% 23.84%
Z-Score (Absolute) 0.00 0.76 0.08 5.04 0.34 6.93
Analytical results for K in OREAS 700 (Certified Value 1.57 wt.%)
K Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 1.61 1.58 1.56 1.41 1.80 1.53

1 2 1.59 1.58 1.61 1.41 1.85 1.57
1 3 1.63 1.58 1.59 1.40 1.79 1.55
1 4 1.52 1.57 1.61 1.37 2.00 1.61
1 5 1.59 1.56 1.60 1.39 1.82 1.58
1 6 1.57 1.56 1.58 1.37 1.75 1.62
Mean 1.59 1.57 1.59 1.39 1.84 1.57
Median 1.59 1.57 1.60 1.40 1.81 1.57
Std Dev. 0.037 0.011 0.019 0.018 0.087 0.033
Rel.Std.Dev. 2.33% 0.69% 1.22% 1.32% 4.76% 2.09%
PDM3 1.22% 0.25% 1.63% -11.14% 17.16% 0.54%
Z-Score (Absolute) 0.10 0.18 0.22 3.52 4.16 0.10
Analytical results for La in OREAS 700 (Certified Value 32.5 ppm)

La Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 31.1 33.8 33.3 22.0 40.8 33.6

1 2 31.8 33.8 34.4 22.0 42.5 33.3
1 3 30.9 34.3 34.1 22.0 42.8 32.5
1 4 32.2 34.7 34.8 22.0 45.3 35.1
1 5 32.3 35.6 35.4 22.0 42.6 35.1
1 6 32.1 34.8 33.7 22.0 41.7 34.4
Mean 31.7 34.5 34.3 22.0 42.6 34.0
Median 31.9 34.5 34.3 22.0 42.6 34.0
Std Dev. 0.586 0.710 0.757 0.000 1.509 1.047
Rel.Std.Dev. 1.85% 2.06% 2.21% 0.00% 3.54% 3.08%
PDM3 -2.29% 6.22% 5.57% -32.26% 31.23% 4.68%
Z-Score (Absolute) 0.18 0.62 0.56 2.98 2.96 0.48
Analytical results for Li in OREAS 700 (Certified Value 223 ppm)

Li Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 235 229 207 194 295 210

1 2 228 231 218 191 303 214
1 3 233 228 214 194 300 211
1 4 220 228 217 188 355 215
1 5 231 227 208 191 298 215
1 6 227 226 204 186 288 218
Mean 229 228 211 191 307 214
Median 229 228 211 191 299 214
Std Dev. 5 2 6 3 24 3
Rel.Std.Dev. 2.38% 0.82% 2.74% 1.68% 7.93% 1.42%
PDM3 2.52% 2.10% -5.38% -14.63% 37.23% -4.30%
Z-Score (Absolute) 0.00 0.04 0.67 1.46 2.59 0.58
Analytical results for Lu in OREAS 700 (Certified Value 0.18 ppm)

Lu Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 0.17 0.15 0.20 0.19 0.18 0.25

1 2 0.17 0.17 0.18 0.20 0.20 0.24
1 3 0.17 0.15 0.18 0.20 0.17 0.26
1 4 0.17 0.17 0.20 0.19 0.17 0.24
1 5 0.18 0.17 0.20 0.19 0.18 0.24
1 6 0.17 0.17 0.18 0.20 0.17 0.24
Mean 0.17 0.16 0.19 0.20 0.18 0.24
Median 0.17 0.17 0.19 0.20 0.17 0.24
Std Dev. 0.003 0.009 0.011 0.005 0.010 0.007
Rel.Std.Dev. 1.69% 5.37% 5.77% 2.81% 5.80% 2.89%
PDM3 -4.65% -7.91% 6.26% 9.05% -0.54% 36.32%
Z-Score (Absolute) 0.63 0.95 0.44 0.72 0.44 3.40
Analytical results for Mg in OREAS 700 (Certified Value 0.995 wt.%)

Mg Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.989 1.013 1.010 0.910 0.980 0.989

1 2 0.999 1.014 1.030 0.890 1.030 1.000
1 3 1.010 1.003 1.030 0.910 1.020 0.997
1 4 0.945 0.999 1.050 0.880 1.020 1.021
1 5 0.989 0.998 1.040 0.900 1.000 1.012
1 6 0.974 1.005 1.020 0.890 0.980 1.018
Mean 0.984 1.005 1.030 0.897 1.005 1.006
Median 0.989 1.004 1.030 0.895 1.010 1.006
Std Dev. 0.023 0.007 0.014 0.012 0.022 0.013
Rel.Std.Dev. 2.30% 0.68% 1.37% 1.35% 2.16% 1.27%
PDM3 -1.11% 0.98% 3.47% -9.92% 0.96% 1.06%
Z-Score (Absolute) 0.54 0.18 1.04 3.57 0.17 0.21
Analytical results for Mn in OREAS 700 (Certified Value 0.314 wt.%)

Mn Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.298 0.313 0.322 0.248 0.300 0.307

1 2 0.292 0.314 0.332 0.245 0.310 0.309
1 3 0.300 0.312 0.332 0.250 0.310 0.309
1 4 0.278 0.309 0.332 0.246 0.310 0.318
1 5 0.292 0.311 0.336 0.246 0.300 0.314
1 6 0.289 0.310 0.327 0.246 0.300 0.321
Mean 0.292 0.312 0.330 0.247 0.305 0.313
Median 0.292 0.312 0.332 0.246 0.305 0.312
Std Dev. 0.008 0.002 0.005 0.002 0.005 0.006
Rel.Std.Dev. 2.67% 0.56% 1.49% 0.74% 1.80% 1.77%
PDM3 -7.16% -0.84% 5.06% -21.48% -2.95% -0.41%
Z-Score (Absolute) 1.50 0.04 1.59 4.97 0.47 0.14
Analytical results for Mo in OREAS 700 (Certified Value 81 ppm)

Mo Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 75 89 96 59 100 74
1 2 75 88 88 56 101 81
1 3 76 86 92 57 97 78
1 4 75 87 92 58 98 80
1 5 76 88 90 59 101 74
1 6 77 83 95 59 100 75
Mean 76 87 92 58 100 77
Median 76 88 92 59 100 77
Std Dev. 0.8 2.0 3.0 1.3 1.5 3.1
Rel.Std.Dev. 1.09% 2.26% 3.22% 2.18% 1.52% 4.03%
PDM3 -5.96% 7.86% 14.03% -27.98% 23.55% -4.22%
Z-Score (Absolute) 0.59 0.79 1.41 2.79 2.36 0.42
Analytical results for Na in OREAS 700 (Certified Value 1.21 wt.%)

Na Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 1.22 1.28 1.27 1.17 N.A. 1.22

1 2 1.21 1.28 1.29 1.17 N.A. 1.23
1 3 1.22 1.28 1.28 1.17 N.A. 1.22
1 4 1.15 1.27 1.28 1.14 N.A. 1.25
1 5 1.23 1.26 1.28 1.16 N.A. 1.24
1 6 1.20 1.26 1.29 1.14 N.A. 1.25
Mean 1.20 1.27 1.28 1.16 1.23
Median 1.21 1.28 1.28 1.17 1.23
Std Dev. 0.028 0.010 0.008 0.015 0.014
Rel.Std.Dev. 2.32% 0.78% 0.59% 1.27% 1.17%
PDM3 -0.81% 4.79% 5.53% -4.62% 1.67%
Analytical results for Nb in OREAS 700 (Indicative Value 16.1 ppm)
Nb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.03 1.04 1.06 1.08 1.09 1.12
4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*MS 4A*OES
1 1 17.7 10.5 <5 35.5 15.3 19.0

1 2 11.3 11.0 <5 36.9 15.2 20.0
1 3 12.4 11.0 <5 20.7 14.7 21.0
1 4 11.9 12.5 <5 25.8 15.1 20.0
1 5 9.6 13.0 <5 36.5 15.3 21.0
1 6 7.0 13.0 <5 35.9 13.1 20.0
Mean 11.6 11.8 31.9 14.8 20.2
Median 11.6 11.8 35.7 15.1 20.0
Std Dev. 3.5 1.1 6.9 0.8 0.8
Rel.Std.Dev. 30.47% 9.51% 21.63% 5.74% 3.73%
PDM3 -27.67% -26.50% 98.04% -8.26% 25.26%
Z-Score (Absolute) 0.81 0.79 NA 2.24 0.34 0.34
Analytical results for Nd in OREAS 700 (Indicative Value 26.3 ppm)

Nd Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 26.0 26.2 27.4 24.5

1 2 26.0 26.8 27.2 24.0
1 3 26.5 25.6 27.1 24.2
1 4 26.7 27.1 28.5 24.1
1 5 27.2 27.4 28.4 24.9
1 6 26.5 26.1 28.7 24.5
Mean 26.5 26.5 27.9 24.4
Median 26.5 26.5 27.9 24.3
Std Dev. 0.4 0.7 0.7 0.3
Rel.Std.Dev. 1.66% 2.56% 2.62% 1.35%
PDM3 0.65% 0.84% 5.90% -7.39%
Z-Score (Absolute) 0.02 0.02 1.33 2.09
Analytical results for Ni in OREAS 700 (Certified Value 24.1 ppm)

Ni Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 24.8 20.9 30.0 20.0 33.1 24.9

1 2 21.8 22.2 30.0 22.0 33.8 25.9
1 3 23.2 21.6 25.0 21.0 34.2 26.0
1 4 21.7 21.3 25.0 19.0 32.7 25.7
1 5 24.1 21.3 30.0 19.0 32.9 25.2
1 6 24.0 21.5 25.0 21.0 37.0 26.1
Mean 23.3 21.5 27.5 20.3 34.0 25.6
Median 23.6 21.4 27.5 20.5 33.5 25.8
Std Dev. 1.3 0.4 2.7 1.2 1.6 0.5
Rel.Std.Dev. 5.57% 2.01% 9.96% 5.96% 4.71% 1.84%
PDM3 -3.40% -10.93% 14.10% -15.63% 40.87% 6.40%
Z-Score (Absolute) 0.16 0.67 1.04 1.00 2.71 0.52

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.293 0.342 0.335 0.299 0.356 0.326

1 2 0.297 0.348 0.340 0.292 0.376 0.334
1 3 0.303 0.340 0.340 0.296 0.337 0.339
1 4 0.280 0.341 0.350 0.294 0.348 0.342
1 5 0.288 0.343 0.350 0.296 0.353 0.329
1 6 0.294 0.343 0.345 0.295 0.361 0.342
Mean 0.292 0.343 0.343 0.295 0.355 0.336
Median 0.293 0.342 0.343 0.295 0.354 0.337
Std Dev. 0.008 0.003 0.006 0.002 0.013 0.007
Rel.Std.Dev. 2.70% 0.78% 1.76% 0.73% 3.72% 2.04%
PDM3 -15.85% -1.31% -1.15% -15.00% 2.24% -3.39%
Z-Score (Absolute) 2.01 0.23 0.21 1.90 0.21 0.48
Analytical results for Pb in OREAS 700 (Certified Value 6.83 ppm)

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 7.70 7.10 8.00 26.00 5.30 6.73

1 2 7.10 7.00 7.00 25.00 5.60 6.58
1 3 7.70 7.20 8.00 26.00 5.30 6.75
1 4 9.40 7.10 8.00 26.00 5.30 7.17
1 5 7.60 7.30 7.00 25.00 5.50 6.79
1 6 8.24 7.00 8.00 26.00 5.30 6.67
Mean 7.96 7.12 7.67 25.67 5.38 6.78
Median 7.70 7.10 8.00 26.00 5.30 6.74
Std Dev. 0.794 0.117 0.516 0.516 0.133 0.202
Rel.Std.Dev. 9.98% 1.64% 6.74% 2.01% 2.47% 2.98%
PDM3 16.56% 4.26% 12.32% 276.03% -21.13% -0.66%
Z-Score (Absolute) 0.24 0.08 0.24 10.80 1.09 0.28
Analytical results for Pr in OREAS 700 (Indicative Value 7.84 ppm)

Pr Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 6.91 7.46 6.99 9.58

1 2 6.81 7.54 7.46 9.66
1 3 6.91 7.40 6.98 9.63
1 4 7.02 7.54 7.60 9.63
1 5 7.06 7.66 7.58 9.84
1 6 6.99 7.36 7.07 9.50
Mean 6.95 7.49 7.28 9.64
Median 6.95 7.50 7.27 9.63
Std Dev. 0.092 0.109 0.296 0.112
Rel.Std.Dev. 1.33% 1.46% 4.07% 1.16%
PDM3 -11.37% -4.42% -7.14% 22.93%
Z-Score (Absolute) 1.08 0.26 0.26 5.57
Analytical results for Rb in OREAS 700 (Certified Value 444 ppm)

Rb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 425 440 438 444 402 494

1 2 402 447 448 503 389 494
1 3 408 436 441 502 393 500
1 4 401 443 466 478 397 484
1 5 397 444 432 480 390 483
1 6 403 435 431 488 384 472
Mean 406 441 443 482 393 488
Median 402 441 440 484 392 489
Std Dev. 10 5 13 22 6 10
Rel.Std.Dev. 2.44% 1.07% 2.94% 4.46% 1.61% 2.09%
PDM3 -8.61% -0.73% -0.34% 8.59% -11.61% 9.87%
Z-Score (Absolute) 0.88 0.02 0.01 0.89 1.09 1.01
Analytical results for Re in OREAS 700 (Indicative Value 0.17 ppm)

Re Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.13
1 1 0.20 0.30 0.12 0.06

1 2 0.20 0.30 0.16 0.06
1 3 0.21 0.30 0.12 0.06
1 4 0.20 0.30 0.13 0.06
1 5 0.19 0.30 0.12 0.07
1 6 0.17 0.30 0.12 0.06
Mean 0.19 0.30 0.13 0.06
Median 0.20 0.30 0.12 0.06
Std Dev. 0.012 0.000 0.016 0.003
Rel.Std.Dev. 6.24% 0.00% 12.49% 4.91%
PDM3 14.42% 78.00% -25.10% -63.61%
Z-Score (Absolute) 0.37 1.47 0.37 0.98
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.289 0.302 0.310 0.310 0.270 0.281

1 2 0.321 0.304 0.300 0.300 0.360 0.286
1 3 0.284 0.315 0.320 0.290 0.270 0.293
1 4 0.292 0.286 0.310 0.290 0.280 0.346
1 5 0.305 0.309 0.300 0.340 0.330 0.289
1 6 0.280 0.284 0.300 0.300 0.260 0.290
Mean 0.295 0.300 0.307 0.305 0.295 0.297
Median 0.291 0.303 0.305 0.300 0.275 0.290
Std Dev. 0.015 0.012 0.008 0.019 0.040 0.024
Rel.Std.Dev. 5.18% 4.14% 2.66% 6.13% 13.69% 8.12%
PDM3 0.19% 1.84% 4.10% 3.53% 0.14% 0.96%
Z-Score (Absolute) 0.00 0.40 0.95 0.81 1.09 0.61
Analytical results for Sb in OREAS 700 (Certified Value 0.7 ppm)

Sb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.13
1 1 0.64 0.77 0.80 1.16 0.65 0.73

1 2 0.65 0.73 0.60 0.98 0.71 0.71
1 3 0.65 0.68 0.60 0.93 0.66 0.72
1 4 0.66 0.71 0.80 0.95 0.68 0.72
1 5 0.65 0.75 0.80 0.85 0.64 0.68
1 6 0.62 0.71 0.80 0.87 0.65 0.72
Mean 0.64 0.73 0.73 0.96 0.67 0.71
Median 0.65 0.72 0.80 0.94 0.66 0.72
Std Dev. 0.013 0.032 0.103 0.111 0.026 0.018
Rel.Std.Dev. 2.02% 4.43% 14.08% 11.60% 3.93% 2.45%
PDM3 -7.55% 4.11% 5.31% 37.38% -4.31% 2.43%
Z-Score (Absolute) 1.52 0.12 0.29 4.79 1.06 0.12
Analytical results for Sc in OREAS 700 (Certified Value 9.55 ppm)

Sc Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
4A*OES/MS 4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES
1 1 8.62 10.40 15.00 8.00 16.90 14.44

1 2 8.66 10.30 15.00 8.00 17.40 14.77
1 3 8.63 9.90 15.00 8.00 17.10 15.31
1 4 8.75 10.00 15.00 8.00 15.20 15.61
1 5 8.85 10.20 16.00 8.00 16.20 14.85
1 6 8.63 9.90 15.00 8.00 19.10 15.89
Mean 8.69 10.12 15.17 8.00 16.98 15.15
Median 8.64 10.10 15.00 8.00 17.00 15.08
Std Dev. 0.093 0.214 0.408 0.000 1.301 0.551
Rel.Std.Dev. 1.07% 2.11% 2.69% 0.00% 7.66% 3.64%
PDM3 -9.04% 5.90% 58.77% -16.26% 77.78% 58.54%
Z-Score (Absolute) 0.76 0.00 2.68 1.12 3.64 2.67
Analytical results for Se in OREAS 700 (Indicative Value 2.09 ppm)

Se Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.12
4A*OES/MS 4A*MS 4A*MS 4A*OES/MS 4A*MS 4A*OES
1 1 <2 1.30 5.00 2.00 <5 10.00

1 2 <2 1.90 <5 2.00 <5 10.00
1 3 <2 1.80 <5 2.00 <5 10.00
1 4 <2 1.80 <5 <2 <5 10.00
1 5 <2 2.00 <5 2.00 <5 20.00
1 6 <2 1.40 <5 2.00 <5 10.00
Mean 1.70 5.00 2.00 11.67
Median 1.80 5.00 2.00 10.00
Std Dev. 0.283 0.000 4.082
Rel.Std.Dev. 16.64% 0.00% 34.99%
PDM3 -18.73% 139.04% -4.38% 457.77%
Z-Score (Absolute) NA 0.85 0.22 0.67 NA 10.34
Analytical results for Sm in OREAS 700 (Indicative Value 5.26 ppm)

Sm Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 4.59 5.30 4.82 6.38

1 2 4.67 5.10 4.83 6.41
1 3 4.50 5.05 4.82 6.48
1 4 4.61 5.25 5.00 6.23
1 5 4.76 5.25 4.89 6.41
1 6 4.66 4.95 5.01 6.20
Mean 4.63 5.15 4.89 6.35
Median 4.64 5.18 4.86 6.39
Std Dev. 0.088 0.138 0.089 0.113
Rel.Std.Dev. 1.89% 2.68% 1.83% 1.77%
PDM3 -11.90% -2.04% -6.90% 20.83%
Z-Score (Absolute) 1.02 0.33 0.33 3.46

No No 1.01 1.03 1.04 1.06 1.07 1.08
4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES/MS
1 1 110 140 140 38 141 194

1 2 122 140 134 36 144 193
1 3 120 136 146 38 141 193
1 4 123 139 148 38 134 190
1 5 124 139 138 37 143 189
1 6 122 134 136 37 129 195
Mean 120 138 140 37 139 192
Median 122 139 139 38 141 193
Std Dev. 5 2 6 1 6 2
Rel.Std.Dev. 4.33% 1.81% 3.97% 2.19% 4.25% 1.19%
PDM3 -9.49% 3.86% 5.67% -71.89% 4.41% 44.69%
Z-Score (Absolute) 0.86 0.00 0.13 5.50 0.04 2.96
Analytical results for Sr in OREAS 700 (Certified Value 124 ppm)

Sr Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 114 130 125 200 111 122

1 2 120 130 119 200 115 127
1 3 117 129 120 200 114 123
1 4 108 130 122 200 111 127
1 5 115 130 116 200 113 122
1 6 112 128 122 200 110 124
Mean 115 129 121 200 113 124
Median 115 130 121 200 112 124
Std Dev. 4 1 3 0 2 2
Rel.Std.Dev. 3.61% 0.69% 2.55% 0.00% 1.82% 1.70%
PDM3 -7.74% 4.30% -2.79% 61.11% -9.35% 0.10%
Z-Score (Absolute) 0.85 0.45 0.32 6.55 1.02 0.00
Analytical results for Ta in OREAS 700 (Indicative Value 0.65 ppm)

Ta Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 < 0.05 0.54 0.40 <5 12.59 0.64

1 2 < 0.05 1.08 0.40 <5 14.52 0.75
1 3 < 0.05 0.89 0.50 <5 9.11 0.51
1 4 < 0.05 0.87 0.50 <5 8.78 0.58
1 5 < 0.05 0.66 0.60 <5 11.73 0.56
1 6 < 0.05 0.50 0.60 <5 9.56 0.50
Mean 0.76 0.50 11.05 0.59
Median 0.77 0.50 10.65 0.57
Std Dev. 0.227 0.089 2.281 0.092
Rel.Std.Dev. 29.98% 17.89% 20.64% 15.56%
PDM3 16.87% -22.77% 1606.49% -8.71%
Z-Score (Absolute) NA 0.02 0.82 NA 34.07 0.52
Analytical results for Tb in OREAS 700 (Indicative Value 0.5 ppm)
Tb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 0.50 0.49 0.54 0.67 0.46 1.37

1 2 0.50 0.49 0.54 0.71 0.47 1.33
1 3 0.50 0.49 0.50 0.71 0.47 1.32
1 4 0.51 0.47 0.52 0.68 0.49 1.29
1 5 0.51 0.50 0.54 0.71 0.50 1.33
1 6 0.51 0.48 0.52 0.70 0.48 1.28
Mean 0.51 0.49 0.53 0.70 0.48 1.32
Median 0.51 0.49 0.53 0.71 0.48 1.33
Std Dev. 0.007 0.010 0.016 0.018 0.015 0.032
Rel.Std.Dev. 1.36% 2.14% 3.10% 2.51% 3.08% 2.45%
PDM3 1.15% -2.36% 5.49% 39.54% -4.28% 164.80%
Z-Score (Absolute) 0.22 0.58 0.22 3.68 0.77 16.41
Analytical results for Te in OREAS 700 (Indicative Value 0.16 ppm)

Te Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.12
4A*OES/MS 4A*MS 4A*MS 4A*OES/MS 4A*MS 4A*OES
1 1 0.08 0.22 0.20 0.85 0.27 < 10

1 2 0.10 0.16 < 0.2 0.60 0.27 < 10
1 3 0.16 0.20 < 0.2 0.49 0.25 < 10
1 4 0.11 0.11 < 0.2 0.39 0.22 < 10
1 5 0.10 0.14 < 0.2 0.44 0.20 < 10
1 6 0.10 0.22 0.20 0.40 < 0.2 < 10
Mean 0.11 0.18 0.20 0.53 0.24
Median 0.10 0.18 0.20 0.47 0.25
Std Dev. 0.027 0.045 0.000 0.175 0.030
Rel.Std.Dev. 25.14% 26.00% 0.00% 33.16% 12.31%
PDM3 -33.31% 7.56% 22.93% 224.74% 48.80%
Z-Score (Absolute) 1.32 0.11 0.77 4.48 0.58 NA
Analytical results for Th in OREAS 700 (Certified Value 7.75 ppm)

Th Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 7.77 7.87 7.90 6.90 6.88 7.42

1 2 7.72 7.94 7.70 6.60 6.82 7.42
1 3 8.09 7.99 7.80 6.60 6.99 7.49
1 4 8.07 8.02 8.30 7.00 6.93 7.53
1 5 8.23 7.98 8.30 6.50 7.28 7.43
1 6 8.02 8.03 8.70 6.30 7.09 7.45
Mean 7.98 7.97 8.12 6.65 7.00 7.46
Median 8.04 7.99 8.10 6.60 6.96 7.44
Std Dev. 0.196 0.059 0.382 0.259 0.165 0.046
Rel.Std.Dev. 2.46% 0.74% 4.70% 3.89% 2.36% 0.61%
PDM3 3.02% 2.89% 4.76% -14.17% -9.67% -3.76%
Z-Score (Absolute) 0.01 0.00 0.19 1.73 1.27 0.67
Analytical results for Ti in OREAS 700 (Certified Value 0.179 wt.%)

Ti Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.10
1 1 0.127 0.180 0.190 0.100 0.160 0.201

1 2 0.125 0.180 0.200 0.100 0.160 0.203
1 3 0.128 0.178 0.190 0.100 0.150 0.207
1 4 0.119 0.178 0.200 0.100 0.150 0.201
1 5 0.127 0.177 0.200 0.100 0.160 0.200
1 6 0.124 0.176 0.190 0.100 0.160 0.203
Mean 0.125 0.178 0.195 0.100 0.157 0.202
Median 0.126 0.178 0.195 0.100 0.160 0.202
Std Dev. 0.003 0.002 0.005 0.000 0.005 0.002
Rel.Std.Dev. 2.63% 0.92% 2.81% 0.00% 3.30% 1.21%
PDM3 -30.05% -0.26% 9.12% -44.04% -12.33% 13.24%
Z-Score (Absolute) 2.65 0.00 0.85 3.99 1.10 1.23
Analytical results for Tl in OREAS 700 (Certified Value 2.54 ppm)

Tl Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 2.63 2.49 2.80 2.22 2.46 1.89

1 2 2.66 2.53 2.80 2.19 2.42 1.84
1 3 2.70 2.56 2.80 2.18 2.43 1.93
1 4 2.75 2.55 2.80 2.15 2.43 1.83
1 5 2.74 2.46 2.90 2.17 2.51 1.83
1 6 2.72 2.49 2.80 2.15 2.43 1.78
Mean 2.70 2.51 2.82 2.18 2.45 1.85
Median 2.71 2.51 2.80 2.18 2.43 1.84
Std Dev. 0.046 0.039 0.041 0.027 0.034 0.054
Rel.Std.Dev. 1.70% 1.56% 1.45% 1.22% 1.37% 2.94%
PDM3 6.34% -1.00% 10.95% -14.26% -3.56% -27.14%
Z-Score (Absolute) 0.07 0.30 0.07 0.72 0.38 1.12
Analytical results for Tm in OREAS 700 (Indicative Value 0.19 ppm)

Tm Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 0.18 0.20 0.18 0.19

1 2 0.18 0.22 0.20 0.18
1 3 0.19 0.20 0.17 0.18
1 4 0.20 0.22 0.23 0.19
1 5 0.19 0.22 0.18 0.17
1 6 0.19 0.22 0.18 0.19
Mean 0.19 0.21 0.19 0.18
Median 0.19 0.22 0.18 0.18
Std Dev. 0.008 0.010 0.022 0.008
Rel.Std.Dev. 4.00% 4.84% 11.49% 4.64%
PDM3 -1.65% 11.41% -0.99% -4.63%
Z-Score (Absolute) 0.58 5.63 0.77 0.58
Analytical results for U in OREAS 700 (Certified Value 4.73 ppm)

U Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 5.27 4.85 4.70 3.80 4.39 4.39

1 2 5.32 4.86 4.70 3.90 4.45 4.33
1 3 5.32 4.93 4.90 3.80 4.50 4.34
1 4 5.38 4.93 4.90 4.00 4.73 4.33
1 5 5.42 5.01 5.00 3.90 4.63 4.37
1 6 5.45 5.03 4.90 3.80 4.36 4.39
Mean 5.36 4.94 4.85 3.87 4.51 4.36
Median 5.35 4.93 4.90 3.85 4.47 4.35
Std Dev. 0.069 0.074 0.122 0.082 0.144 0.028
Rel.Std.Dev. 1.29% 1.50% 2.53% 2.11% 3.20% 0.64%
PDM3 13.45% 4.43% 2.63% -18.18% -4.59% -7.79%
Z-Score (Absolute) 0.98 0.16 0.00 1.89 0.66 0.95
Analytical results for V in OREAS 700 (Certified Value 62 ppm)

V Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.10
1 1 61 65 60 49 59 64
1 2 62 65 60 48 61 63
1 3 62 65 60 50 60 64
1 4 60 65 60 49 60 64
1 5 63 64 65 49 59 62
1 6 60 64 60 49 58 64
Mean 61 65 61 49 60 64
Median 61 65 60 49 60 64
Std Dev. 1.2 0.5 2.0 0.6 1.0 0.8
Rel.Std.Dev. 1.91% 0.80% 3.36% 1.29% 1.76% 1.23%
PDM3 -0.94% 4.21% -1.97% -21.03% -4.11% 2.42%
Z-Score (Absolute) 0.00 1.27 0.58 4.95 0.78 0.83
Analytical results for W in OREAS 700 (Certified Value 0.989 wt.%)
No No 1.03 1.04 1.08 1.09 1.11 1.12
4A*MS 4A*MS 4A*OES/MS 4A*MS 4A*OES 4A*OES
1 1 > 2000 0.839 0.489 1.057 > 10000 0.924

1 2 > 2000 0.928 0.375 1.052 > 10000 0.975
1 3 > 2000 0.966 0.287 1.171 > 10000 0.967
1 4 > 2000 0.947 0.330 1.067 > 10000 0.924
1 5 > 2000 1.130 0.479 1.111 > 10000 > 10000
1 6 > 2000 1.010 0.554 1.141 > 10000 0.925
Mean 0.970 0.419 1.100 0.943
Median 0.957 0.427 1.089 0.925
Std Dev. 0.097 0.104 0.049 0.026
Rel.Std.Dev. 9.96% 24.80% 4.45% 2.73%
PDM3 -1.88% -57.61% 11.25% -4.61%
Z-Score (Absolute) NA 0.34 21.13 5.40 NA 0.71
Analytical results for Y in OREAS 700 (Certified Value 13.5 ppm)

Y Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 13.5 13.6 14.6 12.0 12.9 13.8

1 2 13.8 13.6 14.2 12.0 13.9 14.0
1 3 13.6 13.3 14.6 12.0 14.4 13.5
1 4 13.7 13.4 15.0 12.0 14.2 13.8
1 5 14.0 13.7 13.5 12.0 13.5 13.1
1 6 13.9 13.3 13.3 12.0 14.2 13.4
Mean 13.7 13.5 14.2 12.0 13.9 13.6
Median 13.7 13.5 14.4 12.0 14.1 13.6
Std Dev. 0.178 0.184 0.672 0.000 0.561 0.335
Rel.Std.Dev. 1.29% 1.37% 4.73% 0.00% 4.05% 2.46%
PDM3 1.69% -0.32% 5.12% -11.17% 2.53% 0.62%
Z-Score (Absolute) 0.16 0.14 0.67 1.77 0.29 0.00
Analytical results for Yb in OREAS 700 (Certified Value 1.26 ppm)

Yb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 1.15 1.14 1.30 1.40 1.16 1.74

1 2 1.15 1.08 1.30 1.50 1.29 1.74
1 3 1.13 1.13 1.25 1.50 1.19 1.76
1 4 1.19 1.17 1.30 1.40 1.29 1.73
1 5 1.16 1.12 1.40 1.50 1.23 1.72
1 6 1.18 1.16 1.30 1.50 1.24 1.77
Mean 1.16 1.13 1.31 1.47 1.23 1.74
Median 1.16 1.14 1.30 1.50 1.23 1.74
Std Dev. 0.023 0.032 0.049 0.052 0.053 0.020
Rel.Std.Dev. 1.99% 2.83% 3.76% 3.52% 4.32% 1.15%
PDM3 -7.64% -9.80% 4.12% 16.72% -1.94% 38.76%
Z-Score (Absolute) 0.59 0.75 0.17 1.21 0.17 2.85

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 189 210 225 191 208 214

1 2 189 212 225 189 210 216
1 3 197 209 220 192 203 217
1 4 179 208 225 190 204 229
1 5 187 210 225 191 199 216
1 6 184 209 225 190 197 225
Mean 187 210 224 191 204 219
Median 188 210 225 191 204 217
Std Dev. 6 1 2 1 5 6
Rel.Std.Dev. 3.15% 0.65% 0.91% 0.55% 2.46% 2.70%
PDM3 -13.22% -2.93% 3.78% -11.80% -5.79% 1.59%
Z-Score (Absolute) 2.29 0.70 0.34 2.08 1.14 0.00
Analytical results for Zr in OREAS 700 (Certified Value 47.3 ppm)

Zr Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 41.9 46.7 41.0 27.0 56.0 48.7

1 2 45.4 45.5 39.0 28.0 59.4 48.9
1 3 40.6 45.4 44.0 27.0 50.9 51.3
1 4 44.3 45.5 47.0 26.0 56.2 53.4
1 5 42.6 46.4 49.0 26.0 52.8 50.2
1 6 44.9 44.5 48.0 27.0 65.6 53.1
Mean 43.3 45.7 44.7 26.8 56.8 50.9
Median 43.5 45.5 45.5 27.0 56.1 50.7
Std Dev. 1.9 0.8 4.0 0.8 5.2 2.0
Rel.Std.Dev. 4.36% 1.72% 9.03% 2.81% 9.18% 3.99%
PDM3 -8.49% -3.45% -5.56% -43.27% 20.13% 7.66%
Z-Score (Absolute) 0.39 0.00 0.16 3.05 1.52 0.85
Lab Lab Lab Lab Lab
1.11 1.12 1.13 1.14 1.15
4A*OES 4A*OES 4A*MS 4A*OES 4A*OES
< 0.5 0.500 0.540 < 0.5 < 0.5

< 0.5 < 0.5 0.530 < 0.5 0.500
0.500 < 0.5 0.490 0.500 < 0.5
0.700 < 0.5 0.560 0.500 0.700
0.500 0.500 0.500 < 0.5 0.600
< 0.5 < 0.5 0.500 < 0.5 0.700
0.567 0.500 0.520 0.500 0.625
0.500 0.500 0.515 0.500 0.650
0.115 0.000 0.028 0.000 0.096
20.38% 0.00% 5.30% 0.00% 15.32%
7.94% -4.76% -0.95% -4.76% 19.05%
0.49 0.90 0.11 0.90 0.00

1.10 1.11 1.12 1.13 1.14 1.15
4A*OES 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES
5.87 5.57 5.36 5.75 5.20 5.74

5.85 5.56 5.58 5.69 5.03 5.78
5.86 5.67 5.58 5.76 5.01 5.68
5.92 5.52 5.42 5.78 5.14 5.85
5.91 5.79 5.63 5.79 5.00 5.80
5.95 5.70 5.53 5.81 5.07 5.79
5.89 5.64 5.52 5.76 5.08 5.77
5.89 5.62 5.56 5.77 5.05 5.79
0.038 0.103 0.105 0.042 0.080 0.058
0.64% 1.82% 1.90% 0.73% 1.57% 1.00%
5.77% 1.16% -0.96% 3.47% -8.89% 3.65%
1.18 0.17 0.30 0.67 2.06 0.71
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
5.00 7.00 4.30 7.00 <5

<5 5.00 4.30 8.00 9.00
<5 <5 4.40 <5 9.00
<5 <5 3.00 <5 <5
<5 <5 4.40 <5 10.00
<5 <5 4.20 <5 7.00
5.00 6.00 4.10 7.50 8.75
5.00 6.00 4.30 7.50 9.00
1.414 0.544 0.707 1.258
23.57% 13.27% 9.43% 14.38%
14.92% 37.90% -5.77% 72.38% 101.11%
0.53 0.53 0.55 4.48 6.45

1.10 1.11 1.12 1.13 1.14 1.15
169 160 150 160 160 150

169 160 160 160 150 150
170 160 160 160 150 150
169 160 150 160 150 150
168 160 160 160 150 150
168 160 150 160 150 150
169 160 155 160 152 150
169 160 155 160 150 150
1 0 5 0 4 0
0.49% 0.00% 3.53% 0.00% 2.69% 0.00%
6.65% 1.13% -2.03% 1.13% -4.14% -5.19%
1.81 0.40 0.40 0.40 1.21 1.21

1.10 1.11 1.12 1.13 1.14 1.15
4A*MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES
3.58 2.30 2.20 2.42 2.30 2.40

3.54 2.30 2.30 2.23 2.20 2.40
3.63 2.30 2.30 2.32 2.20 2.30
3.74 2.30 2.20 2.22 2.30 2.40
3.54 2.40 2.30 2.22 2.20 2.30
3.96 2.40 2.20 2.31 2.30 2.40
3.67 2.33 2.25 2.29 2.25 2.37
3.60 2.30 2.25 2.27 2.25 2.40
0.163 0.052 0.055 0.079 0.055 0.052
4.45% 2.21% 2.43% 3.47% 2.43% 2.18%
58.12% 0.65% -2.94% -1.36% -2.94% 2.09%
17.17 0.00 1.12 0.63 1.12 0.45
Lab Lab Lab Lab Lab

1.10 1.11 1.12 1.13 1.15
4A*MS 4A*OES 4A*OES 4A*MS 4A*OES
7.97 3.00 10.00 6.76 <2

7.58 <2 8.00 6.70 5.00
7.75 4.00 6.00 6.79 <2
7.47 9.00 8.00 6.84 4.00
7.22 3.00 9.00 6.88 4.00
7.78 9.00 8.00 6.80 3.00
7.63 5.60 8.17 6.80 4.00
7.66 4.00 8.00 6.80 4.00
0.265 3.130 1.329 0.063 0.816
3.47% 55.90% 16.28% 0.92% 20.41%
13.08% -17.00% 21.05% 0.72% -40.71%
0.67 0.64 1.02 0.13 1.68

1.10 1.11 1.12 1.13 1.14 1.15
5.84 5.59 5.36 5.58 5.47 5.75

5.86 5.60 5.60 5.59 5.28 5.94
5.95 5.68 5.44 5.66 5.39 5.70
6.02 5.60 5.28 5.72 5.40 5.88
5.90 5.77 5.51 5.72 5.31 5.70
5.93 5.69 5.36 5.72 5.61 5.82
5.92 5.66 5.43 5.67 5.41 5.80
5.92 5.64 5.40 5.69 5.40 5.79
0.066 0.071 0.116 0.066 0.119 0.099
1.12% 1.26% 2.14% 1.17% 2.20% 1.71%
6.70% 1.95% -2.20% 2.13% -2.47% 4.54%
1.96 0.75 0.31 0.79 0.38 1.41

1.10 1.11 1.12 1.13 1.14 1.15
0.69 < 0.5 0.50 < 0.02 < 0.5 1.10

0.62 < 0.5 < 0.5 < 0.02 < 0.5 1.50
0.67 < 0.5 < 0.5 < 0.02 < 0.5 1.30
0.62 < 0.5 0.50 < 0.02 < 0.5 1.60
0.64 < 0.5 < 0.5 < 0.02 < 0.5 1.50
0.69 < 0.5 < 0.5 < 0.02 < 0.5 1.90
0.65 0.50 1.48
0.65 0.50 1.50
0.031 0.000 0.271
4.77% 0.00% 18.30%
77.37% 35.61% 302.32%
1.42 NA 0.00 NA NA 5.08
Lab Lab
1.12 1.13
4A*OES 4A*MS
90 69
90 66
90 68
90 62
100 66
90 68
92 66
90 67
4 2
4.45% 3.70%
39.38% 1.09%
2.99 0.19

1.10 1.11 1.12 1.13 1.14 1.15
16.2 20.0 25.0 16.5 22.0 38.0

16.6 19.0 26.0 16.4 21.0 35.0
15.9 18.0 27.0 16.6 20.0 36.0
15.5 24.0 27.0 15.0 20.0 37.0
16.5 20.0 29.0 17.8 19.0 40.0
16.6 23.0 27.0 16.8 19.0 33.0
16.2 20.7 26.8 16.5 20.2 36.5
16.3 20.0 27.0 16.6 20.0 36.5
0.4 2.3 1.3 0.9 1.2 2.4
2.73% 11.31% 4.95% 5.45% 5.80% 6.65%
-3.42% 23.18% 59.94% -1.55% 20.20% 117.56%
0.21 1.88 4.77 0.06 1.65 9.30
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
40.0 49.0 49.0 51.0 49.0

45.0 51.0 50.0 48.0 50.0
44.0 52.0 50.0 44.0 50.0
47.0 50.0 49.0 43.0 51.0
43.0 51.0 51.0 43.0 49.0
43.0 50.0 51.0 44.0 50.0
43.7 50.5 50.0 45.5 49.8
43.5 50.5 50.0 44.0 50.0
2.3 1.0 0.9 3.3 0.8
5.35% 2.08% 1.79% 7.19% 1.51%
-7.47% 7.00% 5.95% -3.59% 5.59%
0.61 0.78 0.67 0.46 0.64
Lab Lab Lab Lab Lab Lab Lab

1.09 1.10 1.11 1.12 1.13 1.14 1.15
4A*OES 4A*OES 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES
0.192 0.204 0.205 0.206 0.212 0.202 0.204

0.189 0.190 0.196 0.209 0.209 0.200 0.202
0.191 0.197 0.200 0.201 0.203 0.213 0.202
0.237 0.197 0.212 0.198 0.216 0.199 0.205
0.196 0.192 0.209 0.206 0.201 0.195 0.212
0.195 0.208 0.198 0.196 0.207 0.194 0.198
0.200 0.198 0.203 0.203 0.208 0.201 0.204
0.193 0.197 0.202 0.204 0.208 0.200 0.203
0.018 0.007 0.007 0.005 0.006 0.007 0.005
9.16% 3.54% 3.21% 2.53% 2.69% 3.41% 2.29%
-1.18% -2.15% 0.36% 0.12% 2.75% -0.95% 0.69%
3.12 1.43 0.16 0.00 1.66 0.67 0.36
1.10 1.11 1.12 1.13 1.14 1.15
16.17 15.45 14.65 15.20 14.45 16.10

16.04 15.40 15.20 15.05 14.10 16.30
16.18 15.65 15.15 15.30 14.05 16.15
16.15 15.15 14.75 15.90 14.30 16.40
16.20 15.90 15.30 15.60 13.90 16.15
16.02 15.65 15.10 15.50 14.00 16.25
16.13 15.53 15.03 15.43 14.13 16.23
16.16 15.55 15.13 15.40 14.08 16.20
0.076 0.258 0.262 0.306 0.204 0.113
0.47% 1.66% 1.75% 1.98% 1.44% 0.70%
3.60% -0.22% -3.49% -0.92% -9.22% 4.22%
0.58 0.00 0.50 0.11 1.36 0.67
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
130 130 125 120 130

130 130 124 120 130
130 130 125 110 130
130 130 116 110 130
130 130 125 110 130
130 130 128 110 130
130 130 123 113 130
130 130 125 110 130
0 0 4 5 0
0.00% 0.00% 3.30% 4.56% 0.00%
0.59% 0.59% -4.57% -12.31% 0.59%
0.17 0.17 0.67 2.60 0.17
Lab
1.13
4A*MS
1.40
1.40
1.40
1.40
1.40
1.40
1.40
1.40
0.000
0.00%
-1.19%
0.00
Lab
1.13
4A*MS
2.11
2.08
2.06
2.01
2.09
2.08
2.07
2.08
0.034
1.66%
-1.46%
0.67
1.10 1.11 1.12 1.13 1.14 1.15
1.63 1.58 1.43 1.54 1.52 1.62

1.64 1.57 1.51 1.52 1.45 1.59
1.62 1.61 1.48 1.52 1.49 1.59
1.65 1.52 1.43 1.63 1.51 1.62
1.64 1.63 1.51 1.55 1.46 1.62
1.65 1.60 1.45 1.56 1.57 1.62
1.64 1.59 1.47 1.55 1.50 1.61
1.64 1.59 1.47 1.55 1.50 1.62
0.013 0.038 0.037 0.041 0.044 0.015
0.77% 2.42% 2.53% 2.63% 2.92% 0.96%
4.64% 1.20% -6.25% -0.82% -4.23% 2.80%
1.11 0.10 2.09 0.78 1.49 0.57

1.10 1.11 1.12 1.13 1.14 1.15
32.0 30.0 30.0 37.7 30.0 30.0

33.9 30.0 30.0 36.7 30.0 30.0
33.8 30.0 30.0 37.4 30.0 30.0
32.5 30.0 30.0 33.9 30.0 30.0
32.5 30.0 30.0 36.8 30.0 30.0
33.1 30.0 30.0 37.9 30.0 30.0
33.0 30.0 30.0 36.7 30.0 30.0
32.8 30.0 30.0 37.1 30.0 30.0
0.755 0.000 0.000 1.468 0.000 0.000
2.29% 0.00% 0.00% 4.00% 0.00% 0.00%
1.47% -7.62% -7.62% 13.11% -7.62% -7.62%
0.18 0.67 0.67 1.43 0.67 0.67
Lab Lab Lab

1.10 1.12 1.13
4A*OES 4A*OES 4A*MS
311 240 250

312 250 245
310 250 242
311 240 224
314 250 237
319 250 246
313 247 241
311 250 244
3 5 9
1.06% 2.09% 3.84%
40.03% 10.44% 7.75%
3.20 0.68 0.57

1.10 1.11 1.12 1.13 1.14 1.15
1.109 0.990 0.930 0.970 0.910 1.000

1.102 0.990 0.970 0.960 0.890 1.000
1.104 1.010 0.960 0.980 0.880 1.000
1.104 0.980 0.930 0.990 0.900 1.010
1.099 1.020 0.970 0.980 0.880 0.990
1.109 1.010 0.950 0.980 0.880 1.000
1.104 1.000 0.952 0.977 0.890 1.000
1.104 1.000 0.955 0.980 0.885 1.000
0.004 0.015 0.018 0.010 0.013 0.006
0.37% 1.55% 1.93% 1.06% 1.42% 0.63%
10.94% 0.46% -4.40% -1.88% -10.59% 0.46%
3.61 0.00 1.67 0.81 3.80 0.00

1.10 1.11 1.12 1.13 1.14 1.15
0.334 0.325 0.306 0.301 0.310 0.324

0.333 0.317 0.319 0.302 0.299 0.332
0.340 0.321 0.313 0.305 0.306 0.321
0.335 0.317 0.303 0.317 0.306 0.329
0.332 0.327 0.317 0.305 0.300 0.321
0.336 0.323 0.306 0.308 0.320 0.326
0.335 0.322 0.311 0.306 0.307 0.326
0.334 0.322 0.310 0.305 0.306 0.325
0.003 0.004 0.007 0.006 0.008 0.004
0.81% 1.28% 2.12% 1.89% 2.49% 1.36%
6.59% 2.35% -1.15% -2.53% -2.37% 3.57%
1.84 0.81 0.04 0.54 0.33 1.11

1.10 1.11 1.12 1.13 1.14 1.15
64 86 79 84 79 80
64 86 80 82 76 83
65 85 80 84 78 80
64 76 78 82 80 84
65 89 81 88 76 80
64 87 81 84 77 80
64 85 80 84 78 81
64 86 80 84 78 80
0.5 4.5 1.2 2.3 1.6 1.8
0.80% 5.35% 1.46% 2.69% 2.10% 2.26%
-20.02% 5.33% -0.87% 4.44% -3.56% 0.78%
2.00 0.76 0.08 0.45 0.35 0.08

1.10 1.11 1.12 1.13 1.14 1.15
1.12 1.25 1.17 1.25 1.17 1.20

1.12 1.25 1.23 1.24 1.16 1.21
1.13 1.27 1.22 1.24 1.13 1.18
1.12 1.19 1.19 1.26 1.16 1.23
1.12 1.29 1.23 1.25 1.12 1.22
1.14 1.28 1.21 1.27 1.14 1.22
1.12 1.26 1.21 1.25 1.15 1.21
1.12 1.26 1.22 1.25 1.15 1.22
0.007 0.036 0.024 0.012 0.020 0.018
0.59% 2.84% 1.99% 0.93% 1.71% 1.48%
-7.38% 3.34% -0.50% 3.06% -5.58% -0.37%
1.53 0.67 0.12 0.62 1.16 0.09
Lab
1.13
4A*MS
21.8
21.3
22.7
21.8
20.8
22.1
21.8
21.8
0.7
3.00%
35.10%
0.56
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
26.0 23.0 26.4 25.0 21.0

25.0 23.0 25.7 22.0 21.0
28.0 22.0 26.4 22.0 22.0
30.0 22.0 25.2 27.0 25.0
27.0 23.0 26.4 23.0 24.0
27.0 21.0 27.6 24.0 26.0
27.2 22.3 26.3 23.8 23.2
27.0 22.5 26.4 23.5 23.0
1.7 0.8 0.8 1.9 2.1
6.34% 3.66% 3.09% 8.14% 9.22%
12.72% -7.33% 9.06% -1.11% -3.88%
0.95 0.43 0.70 0.00 0.19

1.10 1.11 1.12 1.13 1.14 1.15
0.373 0.364 0.366 0.361 0.343 0.376

0.370 0.369 0.382 0.359 0.340 0.385
0.374 0.372 0.378 0.364 0.335 0.374
0.376 0.364 0.370 0.380 0.344 0.380
0.375 0.377 0.382 0.265 0.335 0.378
0.371 0.377 0.376 0.367 0.339 0.379
0.373 0.371 0.376 0.349 0.339 0.379
0.374 0.371 0.377 0.363 0.340 0.379
0.002 0.006 0.007 0.042 0.004 0.004
0.65% 1.59% 1.73% 12.02% 1.13% 1.00%
7.48% 6.67% 8.16% 0.58% -2.30% 9.02%
0.85 0.75 0.93 0.60 0.35 1.04
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
5.00 9.00 7.30 12.00 <2

7.00 14.00 7.20 14.00 6.00
4.00 9.00 7.30 13.00 <2
7.00 9.00 7.40 15.00 <2
5.00 5.00 6.90 12.00 <2
3.00 10.00 7.40 11.00 <2
5.17 9.33 7.25 12.83 6.00
5.00 9.00 7.30 12.50 6.00
1.602 2.875 0.187 1.472
31.01% 30.81% 2.58% 11.47%
-24.31% 36.74% 6.22% 88.01% -12.10%
1.22 0.67 0.00 3.27 0.73
Lab Lab
1.12 1.13
4A*OES 4A*MS
450 440
470 440
470 440
460 438
470 440
460 450
463 441
465 440
8 4
1.76% 0.98%
4.32% -0.64%
0.47 0.01
Lab Lab Lab Lab Lab
1.11 1.12 1.13 1.14 1.15
0.300 0.290 0.310 0.290 0.330

0.290 0.290 0.300 0.280 0.290
0.300 0.290 0.290 0.390 0.280
0.300 0.280 0.320 0.280 0.310
0.310 0.290 0.300 0.280 0.290
0.300 0.280 0.300 0.280 0.290
0.300 0.287 0.303 0.300 0.298
0.300 0.290 0.300 0.280 0.290
0.006 0.005 0.010 0.044 0.018
2.11% 1.80% 3.40% 14.76% 6.15%
1.83% -2.69% 2.97% 1.83% 1.27%
0.40 0.70 0.67 1.09 0.26
Lab
1.15
4A*OES
<5
<5
<5
<5
<5
<5
NA

1.10 1.11 1.12 1.13 1.14 1.15
15.14 10.00 10.00 10.10 9.00 10.00

15.10 10.00 11.00 10.00 9.00 10.00
15.52 10.00 11.00 10.20 9.00 10.00
15.46 10.00 10.00 10.00 9.00 10.00
15.81 10.00 11.00 10.10 9.00 9.00
15.55 10.00 11.00 10.30 9.00 10.00
15.43 10.00 10.67 10.12 9.00 9.83
15.49 10.00 11.00 10.10 9.00 10.00
0.267 0.000 0.516 0.117 0.000 0.408
1.73% 0.00% 4.84% 1.16% 0.00% 4.15%
61.51% 4.68% 11.66% 5.90% -5.79% 2.94%
2.82 0.06 0.29 0.00 0.59 0.15
Lab
1.13
4A*MS
2.00
2.00
2.00
3.00
3.00
2.00
2.33
2.00
0.516
22.13%
11.55%
0.00
Lab Lab Lab

1.09 1.12 1.13
4A*MS 4A*OES 4A*MS
132 120 127

152 130 124
137 130 126
142 120 118
136 130 125
140 120 127
140 125 124
139 125 126
7 5 4
4.87% 4.38% 2.84%
5.28% -5.88% -6.44%
0.10 0.71 0.67

1.10 1.11 1.12 1.13 1.14 1.15
124 133 129 132 119 125

124 131 134 131 114 125
126 134 134 132 116 121
123 132 130 132 119 127
126 137 135 134 115 124
123 135 133 135 118 124
124 134 133 132 117 124
124 134 134 132 117 125
2 2 2 1 2 2
1.22% 1.62% 1.83% 1.00% 1.83% 1.58%
0.12% 7.68% 6.74% 6.67% -5.88% 0.16%
0.00 0.81 0.71 0.70 0.65 0.00
Lab Lab
1.12 1.13
4A*OES 4A*MS
10.00 0.72
< 10 0.73
10.00 0.79
10.00 0.74
10.00 0.63
< 10 0.73
10.00 0.72
10.00 0.73
0.000 0.052
0.00% 7.19%
1444.57% 11.72%
25.09 0.02
Lab
1.13
4A*MS
0.20
0.20
0.17
0.18
0.20
0.18
0.19
0.19
0.013
7.06%
15.76%
0.11
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
< 20 < 20 9.00 < 20 < 20

< 20 < 20 9.00 < 20 < 20
< 20 < 20 9.10 < 20 < 20
< 20 < 20 8.30 < 20 < 20
< 20 < 20 9.10 < 20 < 20
< 20 < 20 9.10 < 20 < 20
8.93
9.05
0.314
3.52%
15.30%
NA NA 1.43 NA NA
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
0.180 0.160 0.179 0.180 0.180

0.180 0.170 0.178 0.170 0.180
0.180 0.170 0.181 0.170 0.180
0.180 0.160 0.187 0.170 0.180
0.180 0.170 0.180 0.170 0.180
0.180 0.160 0.181 0.170 0.180
0.180 0.165 0.181 0.172 0.180
0.180 0.165 0.181 0.170 0.180
0.000 0.005 0.003 0.004 0.000
0.00% 3.32% 1.75% 2.38% 0.00%
0.73% -7.66% 1.29% -3.93% 0.73%
0.09 0.67 0.14 0.42 0.09
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
10.00 < 10 3.25 < 10 < 10

10.00 < 10 3.21 < 10 < 10
< 10 10.00 3.30 < 10 10.00
10.00 < 10 3.30 < 10 < 10
< 10 < 10 3.26 < 10 < 10
10.00 10.00 3.28 < 10 < 10
10.00 10.00 3.27 10.00
10.00 10.00 3.27 10.00
0.000 0.000 0.034
0.00% 0.00% 1.05%
293.89% 293.89% 28.67% 293.89%
8.96 8.96 0.63 NA 8.96
Lab Lab Lab Lab
1.11 1.13 1.14 1.15
4A*OES 4A*MS 4A*OES 4A*OES
< 10 5.20 < 10 < 10

< 10 5.20 < 10 < 10
< 10 5.20 < 10 < 10
< 10 5.20 < 10 < 10
< 10 5.00 < 10 < 10
< 10 5.20 < 10 < 10
5.17
5.20
0.082
1.58%
9.33%
NA 0.67 NA NA
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
64 61 62 62 62
64 62 61 59 64
65 60 62 61 63
62 59 63 62 64
66 63 60 60 63
65 61 62 63 63
64 61 62 61 63
65 61 62 62 63
1.4 1.4 1.0 1.5 0.8
2.12% 2.32% 1.67% 2.41% 1.19%
3.68% -1.70% -0.62% -1.43% 1.80%
1.14 0.19 0.08 0.12 0.67
Lab Lab Lab
1.13 1.14 1.15
4A*MS 4A*OES 4A*OES
> 10000 > 10000 0.959

> 10000 0.932 1.000
> 10000 > 10000 0.991
> 10000 > 10000 0.957
> 10000 0.973 > 10000
> 10000 > 10000 0.981
0.953 0.978
0.953 0.981
0.029 0.019
3.04% 1.96%
-3.65% -1.11%
NA 0.34 0.64
Lab Lab Lab

1.10 1.12 1.13
4A*MS 4A*OES 4A*MS
13.2 10.0 14.3

12.8 10.0 14.0
12.8 10.0 14.3
12.8 10.0 13.2
13.1 10.0 14.3
13.0 10.0 14.5
12.9 10.0 14.1
12.9 10.0 14.3
0.162 0.000 0.469
1.25% 0.00% 3.33%
-4.18% -25.97% 4.38%
0.72 3.99 0.76
Lab Lab Lab Lab Lab
1.11 1.12 1.13 1.14 1.15
228 223 225 221 240

226 233 227 216 241
229 226 227 218 238
237 220 232 217 242
232 230 231 213 238
228 221 231 227 239
230 226 229 219 240
229 225 229 218 240
4 5 3 5 2
1.72% 2.29% 1.25% 2.22% 0.68%
6.48% 4.40% 5.94% 1.24% 10.96%
0.66 0.44 0.67 0.05 1.45
Lab Lab Lab

1.10 1.12 1.13
4A*OES 4A*OES 4A*MS
52.5 41.0 46.1

53.2 42.0 45.1
51.5 42.0 46.1
50.2 40.0 44.6
50.7 43.0 45.4
51.5 41.0 46.8
51.6 41.5 45.7
51.5 41.5 45.8
1.1 1.0 0.8
2.16% 2.53% 1.75%
9.11% -12.26% -3.41%
0.96 0.67 0.00
Indicative
1.00
ppm
3.00
3.00
1.000
7.000
16.000
0.525
13.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
5.57
31.00
Certified
1.00
ppm
2.00
2.00
1.00
3.00
16.00
4.35
32.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
158
33
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.32
34.00
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
6.75
14.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
5.55
35.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
0.37
15.00
Indicative
1.00
ppm
0.00
0.00
1
10
16
66
16
Certified
1.00
ppm
1.00
1.00
1.0
5.0
16.0
16.8
36.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
47.2
37.0
Certified
1.00
ppm
0.00
0.00
1
15
16
109
38
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.202
39.000
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
2.68
17.00
Indicative
1.00
ppm
2.00
2.00
1.00
12.00
16.00
1.38
18.00
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
0.86
19.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
15.57
40.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
129
41
Indicative
1.00
ppm
2.00
2.00
1.00
19.00
16.00
4.17
13.00
Indicative
1.00
ppm
2.00
2.00
1.00
20.00
16.00
3.43
14.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.42
42.00
Indicative
1.00
ppm
1.00
1.00
1.0
21.0
16.0
< 10
15.0
Indicative
1.00
ppm
2.00
2.00
1.00
22.00
16.00
0.56
16.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.10
43.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.57
44.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
32.5
45.0
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
223
46
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.18
47.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.995
48.000
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.314
49.000
Certified
1.00
ppm
0.00
1.00
1
4
16
81
50
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.21
51.00
Indicative
1.00
ppm
1.00
1.00
1.0
11.0
16.0
16.1
17.0
Indicative
1.00
ppm
1.00
1.00
1.0
23.0
16.0
26.3
18.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
24.1
52.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.347
53.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
6.83
54.00
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
7.84
19.00
Certified
1.00
ppm
0.00
0.00
1
18
16
444
55
Indicative
1.00
ppm
2.00
2.00
1.00
19.00
16.00
0.17
13.00
Certified
1.00
wt.%
3.00
3.00
1.000
25.000
16.000
0.295
56.000
Certified
1.00
ppm
2.00
3.00
1.00
20.00
16.00
0.70
57.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
9.55
58.00
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
2.09
14.00
Indicative
1.00
ppm
2.00
2.00
1.00
22.00
16.00
5.26
15.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
133
59
Certified
1.00
ppm
0.00
0.00
1
5
16
124
60
Indicative
1.00
ppm
2.00
2.00
1.00
23.00
16.00
0.65
16.00
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
0.50
17.00
Indicative
1.00
ppm
2.00
2.00
1.00
12.00
16.00
0.16
18.00
Certified
1.00
ppm
2.00
3.00
1.00
16.00
16.00
7.75
61.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.179
62.000
Certified
1.00
ppm
2.00
2.00
1.00
17.00
16.00
2.54
63.00
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
0.19
19.00
Certified
1.00
ppm
2.00
2.00
1.00
19.00
16.00
4.73
64.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
62
65
Certified
1.00
wt.%
3.00
3.00
1.000
20.000
16.000
0.989
66.000
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
13.5
67.0
Certified
1.00
ppm
2.00
2.00
1.00
21.00
16.00
1.26
68.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
216
69
Certified
1.00
ppm
1.00
1.00
1.0
3.0
16.0
47.3
70.0
Analytical results for Ag in OREAS 700 (Certified Value 0.499 ppm)
Ag Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
AR*OES/MS AR*MS AR*MS AR*OES AR*OES/MS AR*MS
1 1 0.473 0.560 0.450 0.810 1.000 0.407

1 2 0.480 0.510 0.500 0.810 1.570 0.517
1 3 0.511 0.670 0.650 0.810 0.970 0.431
1 4 0.490 0.580 0.500 0.800 1.060 0.454
1 5 0.488 0.720 0.500 0.810 1.880 0.424
1 6 0.491 0.530 0.450 0.820 1.200 0.439
Mean 0.489 0.595 0.508 0.810 1.280 0.445
Median 0.489 0.570 0.500 0.810 1.130 0.435
Std Dev. 0.013 0.083 0.074 0.006 0.367 0.039
Rel.Std.Dev. 2.63% 13.89% 14.48% 0.78% 28.67% 8.66%
PDM3 -2.12% 19.14% 1.78% 62.19% 156.30% -10.84%
Z-Score (Absolute) 0.12 0.81 0.20 2.68 6.79 0.50
Analytical results for Al in OREAS 700 (Certified Value 3.13 wt.%)

Al Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
AR*OES/MS AR*OES AR*OES AR*OES AR*OES/MS AR*MS
1 1 3.01 3.25 2.92 3.18 2.59 2.93

1 2 3.04 3.19 2.93 3.18 2.56 3.16
1 3 3.02 3.17 2.93 3.21 2.49 2.91
1 4 2.75 3.24 2.98 3.22 2.47 3.00
1 5 3.05 3.20 2.98 3.18 2.46 3.11
1 6 3.11 3.14 2.99 3.16 2.43 3.06
Mean 3.00 3.20 2.96 3.19 2.50 3.03
Median 3.03 3.19 2.96 3.18 2.48 3.03
Std Dev. 0.126 0.040 0.031 0.022 0.062 0.101
Rel.Std.Dev. 4.20% 1.26% 1.06% 0.70% 2.48% 3.34%
PDM3 -4.43% 2.00% -5.72% 1.72% -20.24% -3.34%
Z-Score (Absolute) 0.05 0.83 0.57 0.78 3.20 0.14
Analytical results for As in OREAS 700 (Certified Value 3.88 ppm)

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 2.32 4.00 3.80 7.00 4.00 2.87

1 2 2.97 4.00 4.00 7.00 2.00 3.38
1 3 2.54 4.00 4.20 7.00 3.00 2.97
1 4 2.29 4.00 3.80 7.00 3.00 3.25
1 5 2.54 5.00 4.00 6.00 4.00 3.07
1 6 2.47 3.00 3.80 7.00 4.00 3.39
Mean 2.52 4.00 3.93 6.83 3.33 3.16
Median 2.50 4.00 3.90 7.00 3.50 3.16
Std Dev. 0.244 0.632 0.163 0.408 0.816 0.218
Rel.Std.Dev. 9.68% 15.81% 4.15% 5.97% 24.49% 6.92%
PDM3 -35.10% 3.02% 1.30% 75.99% -14.15% -18.71%
Z-Score (Absolute) 1.54 0.04 0.04 3.23 0.67 0.86
Analytical results for Au in OREAS 700 (Certified Value 0.505 ppm)

Au Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.03 1.04 1.06 1.08 1.09 1.10
AR*AAS AR*MS AR*AAS AR*AAS AR*MS AR*AAS
1 1 0.500 0.501 0.480 0.521 0.440 0.509

1 2 0.530 0.493 0.490 0.508 0.568 0.532
1 3 0.510 0.537 0.530 0.536 0.445 0.557
1 4 0.500 0.531 0.510 0.506 0.486 0.483
1 5 0.480 0.525 0.480 0.526 0.484 0.558
1 6 0.520 0.531 0.510 0.491 0.482 0.539
Mean 0.507 0.520 0.500 0.515 0.484 0.530
Median 0.505 0.528 0.500 0.515 0.483 0.535
Std Dev. 0.018 0.018 0.020 0.016 0.046 0.029
Rel.Std.Dev. 3.46% 3.49% 4.00% 3.14% 9.45% 5.48%
PDM3 0.41% 2.99% -0.91% 2.00% -4.07% 4.96%
Z-Score (Absolute) 0.16 0.80 0.16 0.55 0.94 1.28
Analytical results for B in OREAS 700 (Certified Value < 30 ppm)

B Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.03 1.06 1.08 1.11 1.12 1.13
AR*OES AR*OES AR*OES/MS AR*OES AR*OES AR*MS
1 1 17.0 35.0 < 10 10.0 10.0 10.0

1 2 26.0 39.0 < 10 10.0 10.0 10.0
1 3 15.0 37.0 < 10 10.0 10.0 10.0
1 4 18.0 38.0 < 10 10.0 10.0 10.0
1 5 10.0 37.0 < 10 10.0 10.0 10.0
1 6 13.0 35.0 < 10 10.0 10.0 10.0
Mean 16.5 36.8 10.0 10.0 10.0
Median 16.0 37.0 10.0 10.0 10.0
Std Dev. 5.5 1.6 0.0 0.0 0.0
Rel.Std.Dev. 33.14% 4.35% 0.00% 0.00% 0.00%
PDM3
Z-Score (Absolute) NA NA NA NA NA NA
Analytical results for Ba in OREAS 700 (Certified Value 81 ppm)

Ba Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.06 1.08 1.09 1.10
AR*OES/MS AR*MS AR*OES AR*OES/MS AR*MS AR*OES
1 1 76 104 89 77 65 89
1 2 79 102 89 79 78 88
1 3 80 104 89 77 70 89
1 4 73 104 89 77 76 89
1 5 80 105 89 77 77 89
1 6 81 102 89 75 74 89
Mean 78 104 89 77 73 89
Median 79 104 89 77 75 89
Std Dev. 3.2 1.2 0.0 1.3 5.1 0.4
Rel.Std.Dev. 4.14% 1.18% 0.00% 1.64% 6.92% 0.49%
PDM3 -3.56% 27.63% 9.75% -5.05% -9.55% 9.66%
Z-Score (Absolute) 0.07 2.38 0.91 0.30 0.67 0.90
Analytical results for Be in OREAS 700 (Certified Value 0.73 ppm)

Be Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.06 1.08 1.10 1.11
AR*OES/MS AR*MS AR*OES AR*OES/MS AR*MS AR*OES
1 1 0.99 0.76 <5 1.00 1.08 0.70

1 2 0.93 0.70 <5 1.00 1.08 0.70
1 3 0.96 0.79 <5 1.00 1.02 0.70
1 4 0.85 0.75 <5 1.00 1.08 0.70
1 5 0.97 0.77 <5 1.00 0.99 0.70
1 6 0.97 0.79 <5 1.00 1.06 0.70
Mean 0.94 0.76 1.00 1.05 0.70
Median 0.97 0.77 1.00 1.07 0.70
Std Dev. 0.051 0.033 0.000 0.038 0.000
Rel.Std.Dev. 5.42% 4.40% 0.00% 3.66% 0.00%
PDM3 29.21% 3.95% 36.78% 43.64% -4.26%
Z-Score (Absolute) 2.29 0.00 NA 2.70 3.26 0.67
Analytical results for Bi in OREAS 700 (Certified Value 6.89 ppm)

Bi Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 6.32 7.80 6.60 8.00 5.37 5.68

1 2 6.44 7.51 6.26 9.00 5.42 6.84
1 3 6.47 7.46 6.64 10.00 5.25 5.99
1 4 6.49 7.54 6.64 7.00 5.71 6.43
1 5 6.54 7.76 6.90 6.00 5.31 6.84
1 6 6.46 7.48 6.80 7.00 5.79 6.48
Mean 6.45 7.59 6.64 7.83 5.48 6.38
Median 6.47 7.53 6.64 7.50 5.40 6.45
Std Dev. 0.074 0.149 0.219 1.472 0.222 0.464
Rel.Std.Dev. 1.14% 1.96% 3.29% 18.79% 4.05% 7.28%
PDM3 -6.29% 10.24% -3.58% 13.74% -20.50% -7.39%
Z-Score (Absolute) 0.51 1.37 0.20 1.77 2.12 0.63
Analytical results for Ca in OREAS 700 (Certified Value 4.45 wt.%)
Ca Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 4.80 5.00 4.69 4.09 3.96 4.58

1 2 4.82 4.92 4.64 4.11 3.97 5.00
1 3 4.90 4.79 4.75 4.14 3.92 4.57
1 4 4.44 4.98 4.69 4.13 3.92 4.75
1 5 4.84 4.94 4.70 4.12 3.90 4.83
1 6 5.10 4.83 4.75 4.09 3.94 4.74
Mean 4.82 4.91 4.70 4.11 3.94 4.75
Median 4.83 4.93 4.70 4.12 3.93 4.75
Std Dev. 0.217 0.083 0.042 0.021 0.027 0.161
Rel.Std.Dev. 4.50% 1.70% 0.89% 0.50% 0.68% 3.38%
PDM3 8.31% 10.43% 5.78% -7.49% -11.50% 6.73%
Z-Score (Absolute) 0.94 0.98 0.56 0.63 0.99 0.64
Analytical results for Cd in OREAS 700 (Certified Value < 0.5 ppm)
Cd Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.24 0.07 0.05 0.52 0.04 0.05

1 2 0.27 0.13 0.10 < 0.5 < 0.01 0.08
1 3 0.20 0.30 0.10 < 0.5 < 0.01 0.06
1 4 0.24 0.12 0.10 < 0.5 < 0.01 0.07
1 5 0.22 0.06 0.05 < 0.5 < 0.01 0.06
1 6 0.28 0.01 0.05 < 0.5 < 0.01 0.07
Mean 0.24 0.12 0.08 0.52 0.04 0.06
Median 0.24 0.10 0.08 0.52 0.04 0.06
Std Dev. 0.030 0.101 0.027 0.011
Rel.Std.Dev. 12.39% 87.43% 36.51% 16.40%
PDM3
Z-Score (Absolute) 0.86 0.10 0.41 0.93 0.94 0.49
Analytical results for Ce in OREAS 700 (Certified Value 43.9 ppm)

Ce Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
AR*OES/MS AR*MS AR*MS AR*OES/MS AR*MS AR*MS
1 1 37.4 58.3 31.6 51.2 34.0 45.4

1 2 39.9 57.8 33.5 51.8 41.9 45.0
1 3 39.8 55.7 31.6 51.5 37.0 45.7
1 4 40.7 57.4 37.2 49.6 38.4 45.2
1 5 41.4 57.4 32.9 50.6 42.5 44.2
1 6 37.6 57.4 34.4 49.9 40.1 44.9
Mean 39.5 57.4 33.5 50.8 39.0 45.0
Median 39.9 57.4 33.2 50.9 39.3 45.1
Std Dev. 1.6 0.9 2.1 0.9 3.2 0.5
Rel.Std.Dev. 4.11% 1.54% 6.27% 1.77% 8.19% 1.15%
PDM3 -10.16% 30.56% -23.66% 15.54% -11.20% 2.54%
Z-Score (Absolute) 0.49 1.57 1.17 0.81 0.54 0.16
Analytical results for Co in OREAS 700 (Certified Value 15.2 ppm)

No No 1.01 1.03 1.04 1.06 1.08 1.09
AR*OES/MS AR*MS AR*OES AR*OES AR*OES/MS AR*MS
1 1 15.8 16.1 14.0 13.0 15.5 13.1

1 2 16.3 15.1 14.0 13.0 15.6 15.4
1 3 15.8 16.6 15.0 13.0 15.4 13.8
1 4 16.0 15.9 14.0 13.0 17.5 14.5
1 5 16.2 16.1 13.0 13.0 15.3 15.3
1 6 16.0 15.2 14.0 13.0 17.4 14.8
Mean 16.0 15.8 14.0 13.0 16.1 14.5
Median 16.0 16.0 14.0 13.0 15.6 14.7
Std Dev. 0.204 0.579 0.632 0.000 1.038 0.879
Rel.Std.Dev. 1.27% 3.65% 4.52% 0.00% 6.44% 6.06%
PDM3 5.28% 4.08% -7.97% -14.55% 5.94% -4.66%
Z-Score (Absolute) 0.00 0.10 1.12 1.68 0.06 0.84
Analytical results for Cr in OREAS 700 (Certified Value 51 ppm)

Cr Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 48 55 50 54 50 51
1 2 48 55 45 54 52 56
1 3 48 53 45 55 53 51
1 4 44 54 45 55 52 53
1 5 49 55 50 54 50 54
1 6 50 53 50 55 52 53
Mean 48 54 48 55 52 53
Median 48 55 48 55 52 53
Std Dev. 2.1 1.0 2.7 0.6 1.2 1.8
Rel.Std.Dev. 4.47% 1.82% 5.77% 1.04% 2.38% 3.45%
PDM3 -5.53% 7.05% -6.13% 8.39% 1.78% 4.56%
Z-Score (Absolute) 0.68 1.33 1.09 1.57 0.36 0.87
Analytical results for Cs in OREAS 700 (Indicative Value 45 ppm)

Cs Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 96.2 115.4 22.3 149.1 36.9 0.8

1 2 96.2 111.2 18.6 146.9 58.1 0.9
1 3 98.7 119.8 16.8 149.3 31.5 0.9
1 4 101.4 114.9 16.8 163.1 9.6 0.8
1 5 100.4 115.6 18.8 145.2 22.5 0.7
1 6 99.3 114.1 22.0 167.6 14.6 0.8
Mean 98.7 115.1 19.2 153.5 28.9 0.8
Median 99.0 115.1 18.7 149.2 27.0 0.8
Std Dev. 2.2 2.8 2.4 9.4 17.6 0.1
Rel.Std.Dev. 2.18% 2.43% 12.64% 6.12% 60.80% 11.03%
PDM3 119.17% 155.71% -57.32% 241.02% -35.89% -98.18%
Z-Score (Absolute) 1.68 2.07 0.23 3.00 0.00 0.67

No No 1.01 1.03 1.04 1.06 1.08 1.09
AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*MS
1 1 0.201 0.203 0.205 0.203 0.216 0.209

1 2 0.198 0.198 0.198 0.213 0.186 0.205
1 3 0.203 0.211 0.194 0.203 0.186 0.200
1 4 0.214 0.199 0.209 0.216 0.204 0.211
1 5 0.199 0.200 0.199 0.225 0.239 0.204
1 6 0.200 0.192 0.204 0.209 0.201 0.209
Mean 0.203 0.201 0.202 0.211 0.205 0.206
Median 0.201 0.200 0.202 0.211 0.202 0.207
Std Dev. 0.006 0.006 0.005 0.009 0.020 0.004
Rel.Std.Dev. 2.91% 3.02% 2.71% 4.04% 9.80% 2.08%
PDM3 -0.04% -0.94% -0.54% 4.36% 1.26% 1.79%
Z-Score (Absolute) 0.16 0.10 0.01 1.28 0.39 0.62
Analytical results for Dy in OREAS 700 (Indicative Value 2.27 ppm)

Dy Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
AR*MS AR*MS AR*MS AR*MS
1 1 2.61 1.82 < 10 2.38

1 2 2.48 1.90 < 10 2.36
1 3 2.48 1.86 < 10 2.38
1 4 2.53 1.84 < 10 2.38
1 5 2.65 1.89 < 10 2.39
1 6 2.57 1.89 < 10 2.38
Mean 2.55 1.87 2.38
Median 2.55 1.88 2.38
Std Dev. 0.069 0.032 0.012
Rel.Std.Dev. 2.72% 1.72% 0.50%
PDM3 12.67% -17.63% 4.96%
Z-Score (Absolute) 0.67 1.98 NA 0.00
Analytical results for Er in OREAS 700 (Indicative Value 1.07 ppm)
Er Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 1.35 0.87 < 10 1.01

1 2 1.28 0.89 < 10 1.03
1 3 1.25 0.89 < 10 1.02
1 4 1.29 0.88 < 10 1.04
1 5 1.34 0.88 < 10 1.03
1 6 1.27 0.90 < 10 1.04
Mean 1.30 0.89 1.03
Median 1.29 0.89 1.03
Std Dev. 0.040 0.010 0.012
Rel.Std.Dev. 3.07% 1.19% 1.16%
PDM3 21.21% -17.27% -3.94%
Analytical results for Eu in OREAS 700 (Indicative Value 0.63 ppm)

Eu Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 0.73 0.48 <2 0.69

1 2 0.72 0.50 <2 0.68
1 3 0.68 0.48 <2 0.68
1 4 0.70 0.48 <2 0.69
1 5 0.74 0.50 <2 0.67
1 6 0.69 0.50 <2 0.68
Mean 0.71 0.49 0.68
Median 0.71 0.49 0.68
Std Dev. 0.024 0.013 0.006
Rel.Std.Dev. 3.33% 2.63% 0.95%
PDM3 13.21% -21.87% 8.66%

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 13.71 16.29 15.20 15.12 14.90 14.20

1 2 13.52 15.89 15.00 15.19 14.69 15.57
1 3 14.01 15.84 15.30 15.21 14.35 14.45
1 4 12.79 16.13 15.40 15.47 14.30 15.00
1 5 14.14 16.18 15.40 15.29 14.38 15.10
1 6 14.10 15.61 15.20 15.17 14.06 15.08
Mean 13.71 15.99 15.25 15.24 14.45 14.90
Median 13.86 16.01 15.25 15.20 14.37 15.04
Std Dev. 0.510 0.254 0.152 0.125 0.300 0.495
Rel.Std.Dev. 3.72% 1.59% 0.99% 0.82% 2.08% 3.32%
PDM3 -6.47% 9.08% 4.03% 3.97% -1.45% 1.65%
Z-Score (Absolute) 1.15 1.76 0.81 0.80 0.21 0.37
Analytical results for Ga in OREAS 700 (Certified Value 112 ppm)

Ga Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 115 124 118 95 106 83

1 2 116 119 126 95 107 101
1 3 118 126 119 95 107 91
1 4 120 123 117 95 105 98
1 5 120 121 122 96 104 102
1 6 119 119 116 95 108 100
Mean 118 122 120 95 106 96
Median 118 122 119 95 106 99
Std Dev. 2 3 4 0 1 8
Rel.Std.Dev. 1.73% 2.23% 3.11% 0.43% 1.26% 8.01%
PDM3 4.97% 8.60% 6.55% -15.26% -5.41% -14.67%
Z-Score (Absolute) 0.51 0.78 0.63 0.97 0.25 0.75
Analytical results for Gd in OREAS 700 (Indicative Value 3.18 ppm)

Gd Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 3.75 2.50 <5 3.41

1 2 3.49 2.54 <5 3.47
1 3 3.49 2.48 <5 3.44
1 4 3.55 2.49 <5 3.43
1 5 3.67 2.61 <5 3.40
1 6 3.56 2.58 <5 3.42
Mean 3.59 2.53 3.43
Median 3.56 2.52 3.42
Std Dev. 0.104 0.053 0.025
Rel.Std.Dev. 2.91% 2.08% 0.73%
PDM3 12.68% -20.38% 7.70%
Analytical results for Ge in OREAS 700 (Indicative Value 2.82 ppm)

Ge Round Replicate Lab Lab Lab
No No 1.01 1.08 1.13
AR*OES/MSAR*OES/MS AR*MS
1 1 3.42 1.90 3.15

1 2 3.42 1.90 3.11
1 3 3.35 2.00 2.94
1 4 3.20 2.10 3.02
1 5 3.60 1.90 2.97
1 6 3.60 2.30 2.90
Mean 3.43 2.02 3.02
Median 3.42 1.95 3.00
Std Dev. 0.153 0.160 0.098
Rel.Std.Dev. 4.46% 7.94% 3.25%
PDM3 21.59% -28.50% 6.90%
Analytical results for Hf in OREAS 700 (Certified Value 0.81 ppm)

Hf Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.10 1.12
AR*OES/MS AR*MS AR*MS AR*OES/MS AR*MS AR*OES
1 1 0.85 0.97 0.60 0.39 0.87 < 10

1 2 0.83 0.98 0.60 0.40 0.89 < 10
1 3 0.83 0.94 0.60 0.41 0.87 < 10
1 4 0.86 0.97 0.60 0.45 0.87 < 10
1 5 0.88 0.93 0.80 0.38 0.87 < 10
1 6 0.84 0.96 0.60 0.44 0.88 < 10
Mean 0.85 0.96 0.63 0.41 0.87
Median 0.85 0.97 0.60 0.41 0.87
Std Dev. 0.021 0.019 0.082 0.028 0.008
Rel.Std.Dev. 2.44% 2.03% 12.89% 6.77% 0.90%
PDM3 4.37% 17.97% -22.04% -49.32% 7.58%
Analytical results for Hg in OREAS 700 (Indicative Value 0.89 ppm)

Hg Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.11
AR*OES/MS AR*MS AR*MS AR*OES AR*OES/MS AR*OES
1 1 <1 0.69 < 0.01 <5 4.84 <1

1 2 <1 0.37 < 0.01 <5 4.61 1.00
1 3 <1 0.51 < 0.01 <5 4.78 1.00
1 4 <1 0.52 < 0.01 <5 4.90 2.00
1 5 <1 0.47 < 0.01 <5 4.65 2.00
1 6 <1 0.43 < 0.01 <5 4.87 <1
Mean 0.50 4.78 1.50
Median 0.49 4.81 1.50
Std Dev. 0.109 0.120 0.577
Rel.Std.Dev. 21.85% 2.51% 38.49%
PDM3 -43.90% 437.52% 68.86%
Z-Score (Absolute) NA 0.67 NA NA 3.64 0.00
Analytical results for Ho in OREAS 700 (Indicative Value 0.41 ppm)
Ho Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 0.50 0.35 <5 0.38

1 2 0.48 0.40 <5 0.40
1 3 0.47 0.35 <5 0.39
1 4 0.47 0.35 <5 0.39
1 5 0.48 0.36 <5 0.40
1 6 0.47 0.35 <5 0.39
Mean 0.48 0.36 0.39
Median 0.48 0.35 0.39
Std Dev. 0.012 0.021 0.005
Rel.Std.Dev. 2.44% 5.73% 1.26%
PDM3 17.36% -11.88% -3.48%
Analytical results for In in OREAS 700 (Certified Value 1.67 ppm)

In Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 1.73 1.87 1.63 <5 1.59 1.38

1 2 1.72 1.79 1.74 <5 1.61 1.64
1 3 1.74 1.88 1.70 <5 1.61 1.51
1 4 1.61 1.79 1.64 <5 1.68 1.64
1 5 1.78 1.78 1.67 <5 1.54 1.72
1 6 1.79 1.81 1.63 <5 1.70 1.67
Mean 1.73 1.82 1.67 1.62 1.59
Median 1.74 1.80 1.66 1.61 1.64
Std Dev. 0.066 0.045 0.044 0.059 0.126
Rel.Std.Dev. 3.84% 2.45% 2.66% 3.65% 7.91%
PDM3 3.77% 9.35% 0.17% -2.64% -4.27%
Analytical results for K in OREAS 700 (Certified Value 1.24 wt.%)

K Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 1.28 1.40 1.28 1.23 1.18 1.20

1 2 1.33 1.37 1.27 1.23 1.18 1.35
1 3 1.28 1.37 1.29 1.24 1.17 1.20
1 4 1.15 1.39 1.30 1.25 1.18 1.23
1 5 1.27 1.38 1.28 1.24 1.17 1.27
1 6 1.31 1.35 1.29 1.23 1.17 1.25
Mean 1.27 1.38 1.29 1.24 1.18 1.25
Median 1.28 1.37 1.29 1.24 1.18 1.24
Std Dev. 0.062 0.019 0.010 0.008 0.005 0.058
Rel.Std.Dev. 4.85% 1.35% 0.82% 0.66% 0.47% 4.65%
PDM3 2.97% 11.35% 3.99% 0.07% -4.92% 1.06%
Z-Score (Absolute) 0.88 2.20 0.70 0.10 1.12 0.10
Analytical results for La in OREAS 700 (Certified Value 20.6 ppm)

La Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 21.4 31.6 17.1 14.0 23.4 19.1

1 2 21.5 31.3 17.5 14.0 23.7 22.7
1 3 21.7 29.8 17.3 14.0 23.7 20.0
1 4 20.3 30.8 17.1 14.0 23.8 21.6
1 5 21.8 31.0 18.1 14.0 23.1 22.6
1 6 22.3 31.1 18.2 14.0 24.0 21.9
Mean 21.5 30.9 17.6 14.0 23.6 21.3
Median 21.6 31.0 17.4 14.0 23.7 21.7
Std Dev. 0.676 0.629 0.489 0.000 0.319 1.465
Rel.Std.Dev. 3.14% 2.03% 2.79% 0.00% 1.35% 6.87%
PDM3 4.35% 50.06% -14.82% -32.05% 14.62% 3.44%
Z-Score (Absolute) 0.77 4.81 1.08 2.64 1.59 0.58
Analytical results for Li in OREAS 700 (Certified Value 84 ppm)

Li Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 72 85 89 66 87 62
1 2 73 82 95 66 86 68
1 3 71 83 92 66 84 60
1 4 65 83 91 67 84 63
1 5 71 82 95 66 83 65
1 6 73 81 95 66 82 63
Mean 71 82 93 66 84 64
Median 72 82 93 66 84 63
Std Dev. 3.0 1.5 2.4 0.4 1.9 2.6
Rel.Std.Dev. 4.29% 1.78% 2.61% 0.62% 2.21% 4.16%
PDM3 -15.24% -1.38% 10.90% -20.87% 0.85% -23.91%
Z-Score (Absolute) 1.38 0.11 1.14 2.10 0.11 2.41
Analytical results for Lu in OREAS 700 (Certified Value 0.13 ppm)

Lu Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 0.14 0.16 0.12 0.13 <5 0.14

1 2 0.13 0.15 0.12 0.13 <5 0.14
1 3 0.13 0.14 0.12 0.13 <5 0.13
1 4 0.12 0.16 0.12 0.13 <5 0.14
1 5 0.14 0.15 0.12 0.13 <5 0.14
1 6 0.14 0.15 0.12 0.13 <5 0.15
Mean 0.13 0.15 0.12 0.13 0.14
Median 0.13 0.15 0.12 0.13 0.14
Std Dev. 0.005 0.007 0.000 0.000 0.006
Rel.Std.Dev. 4.04% 4.44% 0.00% 0.00% 4.17%
PDM3 -1.78% 12.06% -11.05% -3.63% 2.84%
Analytical results for Mg in OREAS 700 (Certified Value 0.948 wt.%)

Mg Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.986 0.970 1.020 0.910 0.920 0.975

1 2 0.996 0.960 1.020 0.920 0.920 1.092
1 3 1.010 0.940 1.030 0.920 0.890 0.981
1 4 0.905 0.970 1.040 0.930 0.890 1.024
1 5 0.983 0.950 1.030 0.920 0.890 1.040
1 6 1.030 0.930 1.020 0.930 0.880 1.022
Mean 0.985 0.953 1.027 0.922 0.898 1.022
Median 0.991 0.955 1.025 0.920 0.890 1.023
Std Dev. 0.043 0.016 0.008 0.008 0.017 0.043
Rel.Std.Dev. 4.35% 1.71% 0.80% 0.82% 1.92% 4.18%
PDM3 3.87% 0.53% 8.26% -2.81% -5.27% 7.81%
Z-Score (Absolute) 0.93 0.24 1.30 0.22 0.55 1.24
Analytical results for Mn in OREAS 700 (Certified Value 0.237 wt.%)

Mn Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.239 0.304 0.245 0.214 0.230 0.238

1 2 0.249 0.304 0.243 0.217 0.220 0.265
1 3 0.243 0.296 0.250 0.220 0.220 0.242
1 4 0.221 0.305 0.246 0.218 0.220 0.245
1 5 0.244 0.302 0.248 0.217 0.220 0.249
1 6 0.251 0.296 0.243 0.218 0.210 0.248
Mean 0.241 0.301 0.246 0.217 0.220 0.248
Median 0.243 0.303 0.246 0.218 0.220 0.246
Std Dev. 0.011 0.004 0.003 0.002 0.006 0.009
Rel.Std.Dev. 4.38% 1.43% 1.13% 0.90% 2.87% 3.71%
PDM3 1.86% 27.26% 3.88% -8.16% -7.04% 4.68%
Z-Score (Absolute) 0.02 2.75 0.06 1.33 1.10 0.15
Analytical results for Mo in OREAS 700 (Certified Value 83 ppm)
Mo Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 88 97 85 56 95 75
1 2 88 92 93 55 94 89
1 3 88 97 91 55 95 78
1 4 87 95 88 56 103 85
1 5 87 96 91 55 96 83
1 6 88 92 92 54 104 86
Mean 88 95 90 55 98 83
Median 88 96 91 55 95 84
Std Dev. 0 2 3 1 4 5
Rel.Std.Dev. 0.49% 2.51% 3.23% 1.36% 4.58% 6.61%
PDM3 4.99% 13.50% 7.95% -33.87% 17.04% -1.02%
Z-Score (Absolute) 0.32 0.86 0.51 2.12 1.08 0.05
Analytical results for Na in OREAS 700 (Certified Value 0.164 wt.%)

Na Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.220 0.140 0.190 0.170 0.130 0.118

1 2 0.226 0.150 0.190 0.180 0.130 0.130
1 3 0.221 0.150 0.210 0.180 0.130 0.116
1 4 0.193 0.140 0.200 0.180 0.130 0.118
1 5 0.220 0.150 0.200 0.180 0.130 0.122
1 6 0.229 0.150 0.190 0.180 0.140 0.120
Mean 0.218 0.147 0.197 0.178 0.132 0.121
Median 0.221 0.150 0.195 0.180 0.130 0.119
Std Dev. 0.013 0.005 0.008 0.004 0.004 0.005
Rel.Std.Dev. 5.89% 3.52% 4.15% 2.29% 3.10% 4.10%
PDM3 32.79% -10.73% 19.70% 8.54% -19.86% -26.53%
Z-Score (Absolute) 1.92 0.29 1.16 0.63 0.72 1.04
Analytical results for Nb in OREAS 700 (Certified Value 10.4 ppm)

Nb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.10
1 1 6.9 1.0 10.6 12.0 20.5 7.8

1 2 7.2 0.4 11.0 12.0 20.6 8.4
1 3 8.5 0.8 12.0 13.0 23.0 8.3
1 4 8.7 0.7 12.4 13.0 21.7 8.4
1 5 8.0 0.6 13.2 13.0 21.6 7.9
1 6 8.5 0.6 13.2 12.0 22.5 8.0
Mean 8.0 0.7 12.1 12.5 21.6 8.1
Median 8.3 0.6 12.2 12.5 21.6 8.1
Std Dev. 0.8 0.2 1.1 0.5 1.0 0.3
Rel.Std.Dev. 9.47% 34.13% 9.06% 4.38% 4.55% 3.21%
PDM3 -23.52% -93.67% 15.99% 20.16% 108.00% -21.86%
Z-Score (Absolute) 0.90 3.15 0.37 0.50 3.32 0.85
Analytical results for Nd in OREAS 700 (Indicative Value 19.9 ppm)

Nd Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 25.5 16.0 16.3 19.2

1 2 25.1 15.9 19.9 19.4
1 3 24.5 16.6 18.2 19.3
1 4 25.3 16.4 18.7 19.4
1 5 25.3 17.0 20.6 19.0
1 6 24.9 17.4 19.3 19.2
Mean 25.1 16.6 18.8 19.3
Median 25.2 16.5 19.0 19.3
Std Dev. 0.3 0.6 1.5 0.1
Rel.Std.Dev. 1.36% 3.50% 8.10% 0.78%
PDM3 25.89% -16.97% -5.52% -3.40%
Z-Score (Absolute) 3.02 1.24 0.11 0.11
Analytical results for Ni in OREAS 700 (Certified Value 24.5 ppm)

Ni Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 21.6 21.5 22.0 21.0 29.9 22.9

1 2 21.3 21.6 22.0 21.0 30.5 25.1
1 3 21.9 21.3 21.0 21.0 30.0 23.5
1 4 19.2 21.8 23.0 21.0 33.0 23.7
1 5 22.0 21.4 22.0 21.0 29.3 24.8
1 6 21.9 21.0 22.0 21.0 36.6 24.4
Mean 21.3 21.4 22.0 21.0 31.6 24.0
Median 21.7 21.5 22.0 21.0 30.3 24.0
Std Dev. 1.1 0.3 0.6 0.0 2.8 0.8
Rel.Std.Dev. 5.03% 1.27% 2.87% 0.00% 8.84% 3.46%
PDM3 -13.00% -12.49% -10.17% -14.26% 28.82% -1.81%
Z-Score (Absolute) 0.78 0.86 0.70 0.99 1.59 0.11

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.342 0.334 0.330 0.298 0.341 0.335

1 2 0.343 0.328 0.318 0.299 0.337 0.342
1 3 0.350 0.326 0.320 0.301 0.352 0.334
1 4 0.314 0.334 0.318 0.302 0.348 0.332
1 5 0.340 0.328 0.320 0.301 0.333 0.332
1 6 0.353 0.320 0.328 0.300 0.357 0.331
Mean 0.340 0.328 0.322 0.300 0.345 0.334
Median 0.342 0.328 0.320 0.301 0.344 0.333
Std Dev. 0.014 0.005 0.005 0.001 0.009 0.004
Rel.Std.Dev. 4.07% 1.57% 1.64% 0.46% 2.72% 1.19%
PDM3 0.13% -3.40% -5.13% -11.68% 1.41% -1.62%
Z-Score (Absolute) 0.57 1.34 1.99 4.46 0.47 0.67
Analytical results for Pb in OREAS 700 (Certified Value 5.1 ppm)

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 4.66 5.40 5.00 15.00 3.80 4.03

1 2 5.07 5.20 4.00 15.00 3.60 4.90
1 3 4.83 5.50 5.00 15.00 4.00 4.20
1 4 4.80 5.40 5.00 16.00 4.30 4.54
1 5 5.20 5.80 5.00 16.00 4.00 4.68
1 6 4.89 5.20 5.00 15.00 3.90 4.53
Mean 4.91 5.42 4.83 15.33 3.93 4.48
Median 4.86 5.40 5.00 15.00 3.95 4.54
Std Dev. 0.199 0.223 0.408 0.516 0.234 0.315
Rel.Std.Dev. 4.05% 4.11% 8.45% 3.37% 5.94% 7.03%
PDM3 -3.76% 6.21% -5.23% 200.66% -22.87% -12.13%
Z-Score (Absolute) 0.37 0.00 0.30 7.15 1.07 0.67
Analytical results for Pd in OREAS 700 (Indicative Value < 10 ppb)

Pd Round Replicate Lab Lab
No No 1.03 1.04
AR*MS AR*MS
1 1 < 10 < 10
1 2 < 10 < 10
1 3 10 < 10
1 4 < 10 < 10
1 5 < 10 < 10
1 6 < 10 < 10
Mean 10
Median 10
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA NA
Analytical results for Pr in OREAS 700 (Indicative Value 4.69 ppm)
Pr Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 6.66 4.14 <5 5.64

1 2 6.57 4.23 <5 5.50
1 3 6.38 4.19 <5 5.27
1 4 6.60 4.05 <5 5.44
1 5 6.58 4.32 5.03 5.42
1 6 6.48 4.53 <5 5.49
Mean 6.55 4.24 5.03 5.46
Median 6.57 4.21 5.03 5.46
Std Dev. 0.100 0.167 0.122
Rel.Std.Dev. 1.53% 3.93% 2.24%
PDM3 39.66% -9.47% 7.40% 16.47%
Z-Score (Absolute) 0.99 0.36 1.38 0.36
Analytical results for Pt in OREAS 700 (Indicative Value < 1 ppb)

Pt Round Replicate Lab Lab
No No 1.03 1.09
AR*MS AR*MS
1 1 <5 <1
1 2 <5 <1
1 3 <5 <1
1 4 <5 <1
1 5 <5 <1
1 6 5 <1
Mean 5
Median 5
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA NA
Analytical results for Rb in OREAS 700 (Indicative Value 361 ppm)

Rb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.12
1 1 388 435 297 401 306 380

1 2 388 414 320 405 358 370
1 3 383 445 306 409 309 360
1 4 400 425 298 424 265 360
1 5 386 429 332 391 321 360
1 6 386 423 330 425 302 380
Mean 388 428 314 409 310 368
Median 387 427 313 407 308 365
Std Dev. 6 11 16 13 30 10
Rel.Std.Dev. 1.51% 2.52% 4.99% 3.23% 9.75% 2.67%
PDM3 7.48% 18.55% -13.17% 13.20% -14.13% 1.91%
Z-Score (Absolute) 0.22 0.74 0.67 0.50 0.72 0.00
Analytical results for Re in OREAS 700 (Indicative Value 0.045 ppm)

Re Round Replicate Lab Lab Lab
No No 1.03 1.08 1.13
AR*MS AR*OES/MS AR*MS
1 1 0.035 < 0.1 0.045

1 2 0.025 < 0.1 0.047
1 3 0.024 0.100 0.047
1 4 0.026 < 0.1 0.045
1 5 0.026 0.100 0.043
1 6 0.023 < 0.1 0.041
Mean 0.027 0.100 0.045
Median 0.026 0.100 0.045
Std Dev. 0.004 0.000 0.002
Rel.Std.Dev. 16.32% 0.00% 5.23%
PDM3 -41.60% 120.37% -1.57%

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.241 0.290 0.310 0.290 0.300 0.314

1 2 0.324 0.286 0.315 0.300 0.260 0.365
1 3 0.263 0.298 0.310 0.300 0.270 0.297
1 4 0.237 0.287 0.315 0.330 0.290 0.317
1 5 0.253 0.280 0.320 0.320 0.330 0.305
1 6 0.261 0.277 0.320 0.290 0.280 0.308
Mean 0.263 0.286 0.315 0.305 0.288 0.318
Median 0.257 0.286 0.315 0.300 0.285 0.311
Std Dev. 0.032 0.007 0.004 0.016 0.025 0.024
Rel.Std.Dev. 12.00% 2.56% 1.42% 5.39% 8.61% 7.67%
PDM3 -11.43% -3.67% 6.02% 2.65% -2.96% 6.93%
Z-Score (Absolute) 2.97 0.59 1.35 0.67 0.45 0.89
Analytical results for Sb in OREAS 700 (Indicative Value 0.35 ppm)

Sb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 0.30 0.38 0.34 0.40 0.27 0.35

1 2 0.31 0.35 0.38 0.37 0.33 0.37
1 3 0.30 0.43 0.38 0.37 0.29 0.36
1 4 0.28 0.34 0.38 0.42 0.32 0.37
1 5 0.33 0.36 0.38 0.37 0.33 0.36
1 6 0.29 0.32 0.36 0.42 0.30 0.38
Mean 0.30 0.36 0.37 0.39 0.31 0.37
Median 0.30 0.36 0.38 0.39 0.31 0.37
Std Dev. 0.018 0.038 0.017 0.025 0.024 0.009
Rel.Std.Dev. 6.07% 10.54% 4.52% 6.34% 7.78% 2.56%
PDM3 -12.52% 5.13% 7.05% 13.32% -10.86% 5.97%
Z-Score (Absolute) 1.45 0.00 0.30 0.67 1.31 0.07
Analytical results for Sc in OREAS 700 (Certified Value 8.77 ppm)

Sc Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
AR*OES/MS AR*MS AR*OES AR*OES AR*OES/MS AR*MS
1 1 9.30 8.40 10.00 5.00 10.10 11.18

1 2 9.30 8.00 11.00 5.00 10.30 12.29
1 3 9.30 8.40 10.00 5.00 10.30 11.08
1 4 9.50 8.40 10.00 5.00 10.70 10.87
1 5 9.60 8.40 10.00 5.00 9.80 11.40
1 6 9.90 8.00 11.00 5.00 10.90 11.23
Mean 9.48 8.27 10.33 5.00 10.35 11.34
Median 9.40 8.40 10.00 5.00 10.30 11.21
Std Dev. 0.240 0.207 0.516 0.000 0.399 0.498
Rel.Std.Dev. 2.53% 2.50% 5.00% 0.00% 3.85% 4.39%
PDM3 8.12% -5.75% 17.81% -42.99% 18.00% 29.30%
Z-Score (Absolute) 0.67 0.07 1.20 2.07 1.21 1.70
Analytical results for Se in OREAS 700 (Certified Value 2.01 ppm)

Se Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.12
1 1 1.87 2.00 2.00 2.00 1.73 < 10

1 2 2.35 2.00 2.00 2.00 2.20 < 10
1 3 1.95 2.00 3.00 2.00 1.80 < 10
1 4 1.82 3.00 2.00 2.00 1.91 < 10
1 5 1.95 3.00 2.00 2.00 1.95 < 10
1 6 1.92 2.00 2.00 2.00 1.94 < 10
Mean 1.98 2.33 2.17 2.00 1.92
Median 1.94 2.00 2.00 2.00 1.92
Std Dev. 0.189 0.516 0.408 0.000 0.161
Rel.Std.Dev. 9.58% 22.13% 18.84% 0.00% 8.38%
PDM3 -1.52% 16.22% 7.92% -0.38% -4.42%
Analytical results for Si in OREAS 700 (Indicative Value 0.139 wt.%)
Si Round Replicate Lab
No No 1.12
AR*OES
1 1 0.139
1 2 0.128
1 3 0.135
1 4 0.132
1 5 0.140
1 6 0.157
Mean 0.139
Median 0.137
Std Dev. 0.010
Rel.Std.Dev. 7.29%
PDM3 0.00%
Analytical results for Sm in OREAS 700 (Indicative Value 3.86 ppm)

Sm Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 4.59 3.10 < 10 3.82

1 2 4.52 3.25 < 10 3.93
1 3 4.41 3.19 < 10 3.88
1 4 4.53 3.10 < 10 3.78
1 5 4.57 3.28 < 10 3.89
1 6 4.40 3.37 < 10 3.87
Mean 4.50 3.22 3.86
Median 4.53 3.22 3.87
Std Dev. 0.080 0.106 0.053
Rel.Std.Dev. 1.79% 3.31% 1.37%
PDM3 16.69% -16.70% 0.01%

No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 111 148 105 121 135 99

1 2 112 141 117 121 136 114
1 3 112 150 110 123 138 101
1 4 113 148 108 122 144 110
1 5 114 146 111 123 133 115
1 6 115 143 106 120 144 108
Mean 113 146 110 122 138 108
Median 113 147 109 122 137 109
Std Dev. 1 3 4 1 5 7
Rel.Std.Dev. 1.25% 2.29% 3.95% 1.00% 3.35% 6.23%
PDM3 2.67% 32.72% -0.39% 10.68% 25.89% -1.85%
Z-Score (Absolute) 0.40 4.62 0.03 1.52 3.66 0.24
Analytical results for Sr in OREAS 700 (Certified Value 46.1 ppm)

Sr Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 50.9 51.3 38.9 73.0 34.0 38.0

1 2 50.7 48.6 43.1 73.0 33.6 43.5
1 3 52.0 51.7 42.1 74.0 32.2 38.4
1 4 45.9 50.3 40.0 74.0 32.1 41.2
1 5 50.7 50.5 41.0 74.0 32.0 44.5
1 6 54.2 49.1 40.8 73.0 31.9 42.2
Mean 50.7 50.2 41.0 73.5 32.6 41.3
Median 50.8 50.4 40.9 73.5 32.2 41.7
Std Dev. 2.703 1.198 1.488 0.548 0.918 2.634
Rel.Std.Dev. 5.33% 2.38% 3.63% 0.75% 2.81% 6.38%
PDM3 9.96% 8.89% -11.17% 59.30% -29.27% -10.48%
Z-Score (Absolute) 0.71 0.62 0.99 4.67 2.44 0.93
Analytical results for Ta in OREAS 700 (Indicative Value 0.21 ppm)

Ta Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.12
1 1 < 0.05 < 0.01 0.12 <5 0.33 < 10

1 2 < 0.05 < 0.01 0.14 <5 0.18 10.00
1 3 < 0.05 < 0.01 0.14 <5 0.17 10.00
1 4 < 0.05 < 0.01 0.15 <5 0.53 10.00
1 5 < 0.05 < 0.01 0.16 <5 0.14 < 10
1 6 < 0.05 < 0.01 0.13 <5 0.32 10.00
Mean 0.14 0.28 10.00
Median 0.14 0.25 10.00
Std Dev. 0.014 0.147 0.000
Rel.Std.Dev. 10.52% 52.87% 0.00%
PDM3 -34.14% 34.14% 4719.28%
Z-Score (Absolute) NA NA 0.67 NA 0.00 38.34
Analytical results for Tb in OREAS 700 (Indicative Value 0.45 ppm)

Tb Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 0.42 0.49 0.34 0.54 <5 0.47

1 2 0.42 0.46 0.36 0.54 <5 0.46
1 3 0.44 0.47 0.35 0.54 <5 0.46
1 4 0.40 0.48 0.34 0.54 <5 0.47
1 5 0.44 0.48 0.36 0.52 <5 0.45
1 6 0.43 0.47 0.36 0.54 <5 0.45
Mean 0.42 0.48 0.35 0.54 0.46
Median 0.43 0.48 0.35 0.54 0.46
Std Dev. 0.014 0.012 0.008 0.008 0.009
Rel.Std.Dev. 3.36% 2.59% 2.39% 1.52% 1.91%
PDM3 -5.79% 5.75% -22.27% 19.19% 2.38%
Analytical results for Te in OREAS 700 (Certified Value 0.19 ppm)

Te Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.15 0.20 0.18 <5 0.30 0.14

1 2 0.17 0.14 0.18 <5 0.26 0.20
1 3 0.17 0.19 0.20 <5 0.26 0.18
1 4 0.14 0.23 0.18 <5 0.37 0.20
1 5 0.14 0.26 0.20 <5 0.27 0.19
1 6 0.16 0.17 0.20 <5 0.35 0.19
Mean 0.15 0.20 0.19 0.30 0.18
Median 0.16 0.20 0.19 0.29 0.19
Std Dev. 0.012 0.043 0.011 0.048 0.022
Rel.Std.Dev. 8.09% 21.49% 5.77% 15.89% 12.11%
PDM3 -17.25% 6.69% 2.21% 62.27% -2.58%
Analytical results for Th in OREAS 700 (Indicative Value 7.19 ppm)

Th Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 7.16 8.23 6.60 6.00 5.77 7.49

1 2 7.14 8.05 6.26 6.10 7.27 7.28
1 3 7.18 7.88 6.56 6.00 6.33 7.26
1 4 6.54 8.02 6.50 6.30 6.85 7.20
1 5 7.15 7.99 6.94 6.00 7.23 7.24
1 6 7.24 7.94 6.82 6.40 7.02 7.11
Mean 7.07 8.02 6.61 6.13 6.74 7.26
Median 7.16 8.01 6.58 6.05 6.93 7.25
Std Dev. 0.262 0.120 0.241 0.175 0.588 0.128
Rel.Std.Dev. 3.71% 1.50% 3.64% 2.86% 8.72% 1.77%
PDM3 -1.70% 11.53% -8.02% -14.69% -6.21% 1.02%
Z-Score (Absolute) 0.00 1.02 0.67 1.25 0.52 0.11
Analytical results for Ti in OREAS 700 (Certified Value 0.097 wt.%)
Ti Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 0.092 0.089 0.095 0.100 0.090 0.103

1 2 0.091 0.090 0.090 0.100 0.090 0.114
1 3 0.093 0.087 0.090 0.100 0.090 0.104
1 4 0.084 0.090 0.095 0.100 0.090 0.107
1 5 0.093 0.089 0.095 0.100 0.090 0.109
1 6 0.092 0.087 0.095 0.100 0.090 0.108
Mean 0.091 0.089 0.093 0.100 0.090 0.108
Median 0.092 0.089 0.095 0.100 0.090 0.108
Std Dev. 0.003 0.001 0.003 0.000 0.000 0.004
Rel.Std.Dev. 3.78% 1.36% 2.77% 0.00% 0.00% 3.82%
PDM3 -5.96% -8.24% -3.37% 3.53% -6.82% 11.31%
Z-Score (Absolute) 1.18 2.03 0.91 0.67 1.71 2.15
Analytical results for Tl in OREAS 700 (Indicative Value 2.31 ppm)

Tl Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 2.37 2.64 2.20 < 10 1.90 1.80

1 2 2.37 2.56 2.17 < 10 1.90 2.11
1 3 2.37 2.85 2.17 < 10 1.89 1.92
1 4 2.30 2.71 2.24 < 10 2.04 2.05
1 5 2.36 2.75 2.30 < 10 1.88 2.15
1 6 2.40 2.47 2.22 < 10 2.04 2.11
Mean 2.36 2.66 2.22 1.94 2.02
Median 2.37 2.68 2.21 1.90 2.08
Std Dev. 0.034 0.136 0.049 0.077 0.135
Rel.Std.Dev. 1.43% 5.12% 2.22% 3.94% 6.68%
PDM3 2.37% 15.45% -3.91% -15.83% -12.32%
Analytical results for Tm in OREAS 700 (Indicative Value 0.15 ppm)

Tm Round Replicate Lab Lab Lab Lab
No No 1.03 1.04 1.09 1.10
1 1 0.18 0.14 <5 0.14

1 2 0.18 0.14 <5 0.15
1 3 0.17 0.14 <5 0.14
1 4 0.18 0.14 <5 0.13
1 5 0.17 0.14 <5 0.15
1 6 0.17 0.14 <5 0.15
Mean 0.18 0.14 0.14
Median 0.18 0.14 0.14
Std Dev. 0.005 0.003 0.006
Rel.Std.Dev. 3.13% 1.89% 4.32%
PDM3 15.68% -9.66% -6.01%
Analytical results for U in OREAS 700 (Indicative Value 4.46 ppm)

U Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.09 1.10
1 1 4.71 5.13 4.08 3.49 3.52 4.45

1 2 4.71 5.02 3.70 3.48 4.29 4.67
1 3 4.75 4.92 3.96 3.45 3.79 4.55
1 4 5.03 4.99 4.16 3.67 4.16 4.46
1 5 4.79 5.07 4.32 3.49 4.35 4.55
1 6 4.73 4.99 4.14 3.76 4.15 4.50
Mean 4.79 5.02 4.06 3.56 4.04 4.53
Median 4.74 5.01 4.11 3.49 4.15 4.52
Std Dev. 0.126 0.073 0.212 0.127 0.323 0.082
Rel.Std.Dev. 2.62% 1.45% 5.21% 3.56% 8.00% 1.81%
PDM3 7.24% 12.50% -9.01% -20.29% -9.39% 1.49%
Z-Score (Absolute) 0.29 0.68 0.65 1.41 0.67 0.00
Analytical results for V in OREAS 700 (Certified Value 56 ppm)

V Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.06 1.08 1.09 1.10
AR*OES/MS AR*OES AR*OES AR*OES/MS AR*MS AR*OES
1 1 64 60 98 52 55 54
1 2 64 60 97 54 60 53
1 3 64 59 99 54 55 53
1 4 62 63 99 53 56 53
1 5 70 59 99 52 58 54
1 6 66 59 98 53 57 53
Mean 65 60 98 53 57 53
Median 64 60 99 53 57 53
Std Dev. 2.6 1.5 0.8 0.9 2.0 0.3
Rel.Std.Dev. 3.99% 2.58% 0.83% 1.69% 3.51% 0.49%
PDM3 15.60% 6.77% 74.98% -5.69% 1.24% -5.15%
Z-Score (Absolute) 2.92 1.04 16.79 1.55 0.02 1.43
Analytical results for W in OREAS 700 (Indicative Value 0.44 wt.%)

No No 1.01 1.03 1.04 1.06 1.08 1.11
1 1 0.366 > 200 0.387 0.355 0.763 0.485

1 2 0.351 > 200 0.423 0.357 0.777 0.486
1 3 0.352 > 200 0.436 0.355 0.823 0.502
1 4 0.405 > 200 0.445 0.355 0.793 0.488
1 5 0.359 > 200 0.515 0.347 0.792 0.507
1 6 0.348 > 200 0.480 0.367 0.776 0.494
Mean 0.364 0.448 0.356 0.787 0.494
Median 0.355 0.441 0.355 0.784 0.491
Std Dev. 0.021 0.045 0.006 0.021 0.009
Rel.Std.Dev. 5.84% 10.00% 1.75% 2.65% 1.84%
PDM3 -17.37% 1.74% -19.12% 78.92% 12.20%
Z-Score (Absolute) 1.38 NA 0.01 1.37 5.03 0.67
Analytical results for Y in OREAS 700 (Certified Value 11.5 ppm)

Y Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 12.9 13.1 10.9 10.0 10.4 10.0

1 2 12.9 12.4 11.8 10.0 10.6 11.7
1 3 12.7 13.0 10.9 10.0 10.6 10.4
1 4 11.8 12.9 10.7 10.0 11.3 11.3
1 5 12.9 12.6 10.9 10.0 10.1 12.0
1 6 13.1 12.3 11.3 10.0 11.1 11.7
Mean 12.7 12.7 11.1 10.0 10.7 11.2
Median 12.9 12.7 10.9 10.0 10.6 11.5
Std Dev. 0.5 0.3 0.4 0.0 0.4 0.8
Rel.Std.Dev. 3.67% 2.68% 3.63% 0.00% 4.11% 7.07%
PDM3 10.18% 9.88% -3.94% -13.33% -7.28% -3.01%
Z-Score (Absolute) 0.97 0.84 0.14 0.67 0.28 0.00
Analytical results for Yb in OREAS 700 (Indicative Value 0.95 ppm)

Yb Round Replicate Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.08 1.10
AR*OES/MS AR*MS AR*MS AR*OES/MS AR*MS
1 1 0.94 1.13 0.77 1.00 0.95

1 2 0.92 1.07 0.78 1.00 0.94
1 3 0.94 1.05 0.76 1.00 0.92
1 4 0.85 1.05 0.77 1.00 0.92
1 5 0.95 1.07 0.78 1.00 0.95
1 6 0.94 1.11 0.77 1.00 0.94
Mean 0.92 1.08 0.77 1.00 0.94
Median 0.94 1.07 0.77 1.00 0.94
Std Dev. 0.036 0.033 0.008 0.000 0.016
Rel.Std.Dev. 3.94% 3.04% 0.98% 0.00% 1.75%
PDM3 -2.29% 14.28% -18.34% 5.82% -0.96%
Z-Score (Absolute) 0.00 1.54 1.79 0.67 0.02
No No 1.01 1.03 1.04 1.06 1.08 1.09
1 1 210 199 198 220 182 200

1 2 214 199 200 220 187 217
1 3 212 190 202 220 187 198
1 4 194 199 195 220 187 206
1 5 218 198 201 220 180 212
1 6 223 191 195 220 186 207
Mean 212 196 199 220 185 207
Median 213 199 199 220 187 206
Std Dev. 10 4 3 0 3 7
Rel.Std.Dev. 4.60% 2.19% 1.52% 0.00% 1.66% 3.43%
PDM3 2.45% -5.18% -3.97% 6.43% -10.58% -0.01%
Z-Score (Absolute) 0.28 1.00 0.80 0.94 1.90 0.13
Analytical results for Zr in OREAS 700 (Certified Value 24.9 ppm)

Zr Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.03 1.04 1.06 1.08 1.10
1 1 23.7 32.4 22.0 23.0 26.6 26.9

1 2 23.9 30.6 23.0 23.0 27.2 26.4
1 3 24.0 31.7 23.0 23.0 27.2 26.9
1 4 21.8 32.0 22.0 24.0 26.7 26.3
1 5 24.5 30.7 23.0 23.0 26.3 26.4
1 6 22.7 30.6 23.0 24.0 27.0 26.1
Mean 23.4 31.3 22.7 23.3 26.8 26.5
Median 23.8 31.2 23.0 23.0 26.9 26.4
Std Dev. 0.984 0.799 0.516 0.516 0.361 0.346
Rel.Std.Dev. 4.20% 2.55% 2.28% 2.21% 1.35% 1.31%
PDM3 -6.06% 25.61% -9.14% -6.46% 7.57% 6.17%
Z-Score (Absolute) 0.77 2.06 1.04 0.80 0.45 0.33
1.10 1.11 1.12 1.13 1.14 1.15
AR*MS AR*OES AR*OES AR*MS AR*OES AR*OES
0.440 0.400 0.500 0.590 0.500 0.700

0.423 0.200 0.400 0.510 0.600 0.600
0.438 0.200 0.400 0.520 0.500 0.600
0.429 0.200 0.400 0.570 0.500 0.500
0.435 0.200 0.300 0.510 0.500 0.500
0.408 0.300 0.400 0.520 0.500 0.600
0.429 0.250 0.400 0.537 0.517 0.583
0.432 0.200 0.400 0.520 0.500 0.600
0.012 0.084 0.063 0.034 0.041 0.075
2.78% 33.47% 15.81% 6.42% 7.90% 12.90%
-14.10% -49.94% -19.91% 7.46% 3.45% 16.80%
0.64 2.47 0.72 0.30 0.12 0.70

1.10 1.11 1.12 1.13 1.14 1.15
AR*OES AR*OES AR*OES AR*MS AR*OES AR*OES
3.24 3.17 3.42 3.19 3.05 3.00

3.24 2.99 3.48 3.40 3.05 2.96
3.21 2.97 3.19 3.35 3.06 3.03
3.35 3.07 3.39 3.25 3.05 3.09
3.32 3.09 3.12 3.38 3.07 3.06
3.28 3.08 3.22 3.46 2.99 3.09
3.28 3.06 3.30 3.34 3.05 3.04
3.26 3.08 3.31 3.37 3.05 3.05
0.054 0.073 0.145 0.100 0.028 0.052
1.64% 2.38% 4.40% 3.00% 0.92% 1.71%
4.52% -2.32% 5.39% 6.51% -2.85% -3.06%
1.29 0.05 1.44 1.65 0.05 0.09

1.10 1.11 1.12 1.13 1.14 1.15
4.18 4.00 4.00 4.10 5.00 8.00

4.29 4.00 7.00 3.70 5.00 7.00
4.16 2.00 4.00 3.80 <2 4.00
4.10 2.00 5.00 4.00 5.00 5.00
4.25 3.00 4.00 3.60 4.00 9.00
4.25 5.00 5.00 3.80 3.00 7.00
4.21 3.33 4.83 3.83 4.40 6.67
4.22 3.50 4.50 3.80 5.00 7.00
0.070 1.211 1.169 0.186 0.894 1.862
1.68% 36.33% 24.19% 4.86% 20.33% 27.93%
8.33% -14.15% 24.48% -1.28% 13.32% 71.69%
0.26 0.67 0.46 0.14 0.83 2.87
Lab Lab Lab Lab

1.11 1.12 1.13 1.14
0.510 0.467 0.600 NSS

0.495 0.461 0.500 NSS
0.495 0.502 0.500 0.486
0.483 0.426 0.600 0.499
0.506 0.459 0.500 0.502
0.556 0.454 0.500 0.507
0.508 0.462 0.533 0.499
0.501 0.460 0.500 0.501
0.026 0.024 0.052 0.009
5.04% 5.30% 9.68% 1.80%
0.58% -8.54% 5.70% -1.21%
0.27 2.04 1.46 0.24
Lab Lab
1.14 1.15
AR*OES AR*OES
10.0 < 10
10.0 < 10
10.0 < 10
10.0 < 10
10.0 < 10
10.0 < 10
10.0
10.0
0.0
0.00%
NA NA
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
AR*OES AR*OES AR*MS AR*OES AR*OES
80 90 80 80 70
80 90 90 80 70
80 90 90 80 70
80 90 80 80 70
80 80 90 80 70
80 80 90 80 70
80 87 87 80 70
80 90 90 80 70
0.0 5.2 5.2 0.0 0.0
0.00% 5.96% 5.96% 0.00% 0.00%
-1.35% 6.87% 6.87% -1.35% -13.68%
0.00 0.67 0.67 0.00 1.01
Lab Lab Lab Lab

1.12 1.13 1.14 1.15
AR*OES AR*MS AR*OES AR*OES
0.80 0.69 0.70 0.70

0.80 0.71 0.70 0.70
0.70 0.75 0.80 0.70
0.80 0.74 0.70 0.70
0.70 0.73 0.80 0.70
0.80 0.74 0.70 0.70
0.77 0.73 0.73 0.70
0.80 0.74 0.70 0.70
0.052 0.023 0.052 0.000
6.74% 3.10% 7.04% 0.00%
4.86% -0.61% 0.30% -4.26%
0.07 0.37 0.30 0.67

1.10 1.11 1.12 1.13 1.14 1.15
6.60 4.00 7.00 7.03 5.00 9.00

6.67 8.00 8.00 7.10 <2 5.00
6.78 9.00 6.00 7.27 5.00 6.00
6.80 7.00 8.00 7.25 <2 6.00
6.59 5.00 6.00 7.21 2.00 7.00
6.69 7.00 6.00 7.32 6.00 9.00
6.69 6.67 6.83 7.20 4.50 7.00
6.68 7.00 6.50 7.23 5.00 6.50
0.087 1.862 0.983 0.110 1.732 1.673
1.30% 27.93% 14.39% 1.53% 38.49% 23.90%
-2.88% -3.20% -0.78% 4.50% -34.66% 1.64%
0.12 0.72 0.12 0.72 3.72 0.39
1.10 1.11 1.12 1.13 1.14 1.15
4.57 4.12 5.03 4.04 4.22 4.29

4.56 4.03 5.08 4.09 4.24 4.27
4.46 3.96 4.75 3.94 4.28 4.29
4.55 4.10 4.96 4.01 4.19 4.40
4.46 4.09 4.64 3.97 4.27 4.33
4.59 4.16 4.81 4.03 4.22 4.34
4.53 4.08 4.88 4.01 4.24 4.32
4.55 4.10 4.89 4.02 4.23 4.31
0.058 0.071 0.172 0.053 0.034 0.047
1.28% 1.75% 3.53% 1.32% 0.80% 1.10%
1.94% -8.32% 9.71% -9.74% -4.72% -2.84%
0.21 0.71 0.91 0.83 0.38 0.21

1.10 1.11 1.12 1.13 1.14 1.15
0.14 < 0.5 < 0.5 < 0.01 < 0.5 0.70
0.15 < 0.5 < 0.5 < 0.01 < 0.5 0.70
0.13 < 0.5 < 0.5 < 0.01 < 0.5 0.70
0.15 < 0.5 < 0.5 < 0.01 < 0.5 0.70
0.15 < 0.5 < 0.5 < 0.01 < 0.5 < 0.5
0.14 < 0.5 < 0.5 < 0.01 < 0.5 < 0.5
0.14 0.70
0.14 0.70
0.008 0.000
5.79% 0.00%
0.10 NA NA NA NA 3.21
Lab Lab
1.12 1.13
AR*OES AR*MS
70.0 40.7
70.0 42.1
70.0 42.2
70.0 42.2
70.0 42.8
70.0 42.4
70.0 42.1
70.0 42.2
0.0 0.7
0.00% 1.70%
59.36% -4.23%
3.02 0.16

1.10 1.11 1.12 1.13 1.14 1.15
16.2 20.0 22.0 14.9 15.0 22.0

16.3 21.0 23.0 15.0 16.0 22.0
16.2 22.0 21.0 15.1 16.0 23.0
16.6 20.0 22.0 15.4 16.0 23.0
16.4 21.0 21.0 14.9 16.0 23.0
16.3 17.0 21.0 15.3 16.0 22.0
16.3 20.2 21.7 15.1 15.8 22.5
16.3 20.5 21.5 15.1 16.0 22.5
0.148 1.722 0.816 0.210 0.408 0.548
0.91% 8.54% 3.77% 1.39% 2.58% 2.43%
7.44% 32.56% 42.42% -0.74% 4.08% 47.90%
0.19 2.32 3.16 0.51 0.00 3.63

1.10 1.11 1.12 1.13 1.14 1.15
51 48 53 49 50 48
51 47 53 49 50 48
52 47 50 48 50 49
52 49 52 49 49 50
51 48 49 48 50 49
51 48 51 49 49 49
51 48 51 49 50 49
51 48 52 49 50 49
0.3 0.8 1.6 0.5 0.5 0.8
0.67% 1.57% 3.18% 1.06% 1.04% 1.54%
1.48% -5.47% 1.45% -3.82% -1.85% -3.49%
0.31 0.97 0.30 0.66 0.30 0.60
Lab
1.13
AR*MS
7.4
8.2
4.6
10.4
9.6
4.4
7.4
7.8
2.5
33.62%
-83.50%
0.52

1.10 1.11 1.12 1.13 1.14 1.15
AR*OES AR*OES AR*OES AR*MS AR*OES AR*OES/AAS
0.187 0.215 0.266 0.255 0.203 0.201

0.191 0.190 0.240 0.214 0.208 0.222
0.186 0.199 0.219 0.212 0.204 0.209
0.186 0.196 0.231 0.244 0.194 0.207
0.191 0.196 0.205 0.213 0.202 0.211
0.190 0.198 0.222 0.222 0.197 0.197
0.189 0.199 0.231 0.227 0.201 0.208
0.189 0.197 0.227 0.218 0.203 0.208
0.003 0.008 0.021 0.018 0.005 0.009
1.34% 4.26% 9.11% 8.10% 2.51% 4.18%
-6.93% -1.81% 13.78% 11.89% -0.62% 2.59%
1.65 0.73 3.73 3.24 0.01 0.82
1.10 1.11 1.12 1.13 1.14 1.15
14.62 14.80 16.90 13.45 14.00 14.70

14.55 13.80 17.20 14.40 14.05 14.50
14.67 14.10 15.90 14.80 14.00 14.60
14.70 14.15 17.00 13.75 13.90 14.90
14.57 14.60 15.60 14.15 14.00 14.80
14.51 13.65 16.20 15.30 13.50 14.25
14.60 14.18 16.47 14.31 13.91 14.63
14.60 14.13 16.55 14.28 14.00 14.65
0.074 0.446 0.656 0.679 0.206 0.232
0.51% 3.14% 3.99% 4.75% 1.48% 1.59%
-0.38% -3.25% 12.33% -2.39% -5.12% -0.23%
0.01 0.55 2.37 0.39 0.80 0.01

1.10 1.11 1.12 1.13 1.14 1.15
73 110 130 118 110 110

74 100 130 120 110 110
75 110 120 122 110 110
73 110 130 121 110 110
74 110 120 121 110 110
73 110 120 125 110 110
74 108 125 121 110 110
74 110 125 121 110 110
1 4 5 2 0 0
0.97% 3.77% 4.38% 1.83% 0.00% 0.00%
-34.37% -3.54% 11.30% 7.74% -2.06% -2.06%
2.37 0.00 0.98 0.72 0.00 0.00
Lab
1.13
AR*MS
0.77
0.79
0.79
0.78
0.78
0.78
0.78
0.78
0.008
0.96%
-3.78%
0.22
Lab Lab Lab Lab

1.12 1.13 1.14 1.15
<1 5.60 1.00 <1

<1 5.82 1.00 <1
<1 5.59 1.00 <1
<1 5.08 1.00 <1
<1 5.04 1.00 <1
<1 4.79 1.00 <1
5.32 1.00
5.34 1.00
0.405 0.000
7.60% 0.00%
498.87% 12.57%
NA 4.19 0.17 NA
Lab Lab
1.10 1.13
AR*MS AR*MS
2.28 1.47
2.20 1.51
2.23 1.54
2.29 1.52
2.25 1.51
2.23 1.56
2.25 1.52
2.24 1.52
0.031 0.030
1.39% 2.00%
34.90% -8.94%
6.50 1.70

1.10 1.11 1.12 1.13 1.14 1.15
1.21 1.25 1.42 1.29 1.21 1.22

1.20 1.18 1.45 1.27 1.22 1.21
1.19 1.16 1.36 1.27 1.22 1.22
1.21 1.19 1.42 1.26 1.21 1.24
1.19 1.21 1.33 1.26 1.22 1.23
1.18 1.23 1.37 1.30 1.21 1.24
1.20 1.20 1.39 1.28 1.22 1.23
1.19 1.20 1.40 1.27 1.22 1.23
0.012 0.033 0.045 0.016 0.005 0.012
0.99% 2.76% 3.26% 1.29% 0.45% 0.99%
-3.23% -2.62% 12.62% 3.18% -1.68% -0.74%
0.77 0.65 2.46 0.53 0.46 0.27

1.10 1.11 1.12 1.13 1.14 1.15
19.5 20.0 20.0 21.5 20.0 20.0

19.3 20.0 20.0 22.3 20.0 20.0
19.4 20.0 20.0 22.4 20.0 20.0
19.3 20.0 20.0 22.6 20.0 20.0
19.5 20.0 20.0 22.8 20.0 20.0
19.6 20.0 20.0 22.6 20.0 20.0
19.4 20.0 20.0 22.4 20.0 20.0
19.4 20.0 20.0 22.5 20.0 20.0
0.116 0.000 0.000 0.459 0.000 0.000
0.60% 0.00% 0.00% 2.05% 0.00% 0.00%
-5.63% -2.93% -2.93% 8.56% -2.93% -2.93%
0.24 0.00 0.00 1.04 0.00 0.00
Lab Lab
1.12 1.13
AR*OES AR*MS
90 82
90 80
80 86
90 87
80 85
80 90
85 85
85 86
5.5 3.4
6.44% 4.05%
1.65% 1.79%
0.20 0.21
Lab Lab Lab Lab Lab
1.11 1.12 1.13 1.14 1.15
0.910 1.040 0.860 0.880 0.930

0.880 1.050 0.910 0.880 0.920
0.870 0.980 0.890 0.880 0.930
0.910 1.030 0.870 0.870 0.950
0.900 0.960 0.900 0.880 0.940
0.900 0.990 0.910 0.850 0.950
0.895 1.008 0.890 0.873 0.937
0.900 1.010 0.895 0.880 0.935
0.016 0.037 0.021 0.012 0.012
1.84% 3.63% 2.36% 1.39% 1.29%
-5.62% 6.33% -6.15% -7.91% -1.23%
0.60 1.04 0.67 0.85 0.00

1.10 1.11 1.12 1.13 1.14 1.15
0.297 0.230 0.268 0.247 0.229 0.230

0.297 0.217 0.271 0.247 0.231 0.228
0.292 0.214 0.252 0.240 0.233 0.231
0.296 0.224 0.262 0.244 0.230 0.237
0.292 0.222 0.246 0.241 0.232 0.234
0.297 0.228 0.253 0.247 0.231 0.233
0.295 0.223 0.259 0.244 0.231 0.232
0.297 0.223 0.258 0.246 0.231 0.232
0.003 0.006 0.010 0.003 0.001 0.003
0.87% 2.78% 3.82% 1.31% 0.61% 1.37%
24.80% -5.98% 9.30% 3.24% -2.39% -1.90%
2.47 1.08 0.68 0.02 0.67 0.61
1.10 1.11 1.12 1.13 1.14 1.15
73 74 87 85 74 73
72 71 87 86 76 74
74 70 81 88 74 73
74 73 86 87 74 76
73 73 80 86 75 74
74 73 83 89 72 77
73 72 84 87 74 75
73 73 85 86 74 74
1 2 3 1 1 2
0.80% 2.08% 3.69% 1.63% 1.79% 2.21%
-12.26% -13.29% 0.70% 4.17% -11.09% -10.69%
0.76 0.82 0.05 0.27 0.69 0.66

1.10 1.11 1.12 1.13 1.14 1.15
0.432 0.170 0.210 0.150 0.150 0.160

0.434 0.150 0.210 0.160 0.150 0.150
0.440 0.150 0.200 0.150 0.140 0.150
0.436 0.150 0.200 0.150 0.150 0.150
0.433 0.160 0.190 0.160 0.150 0.140
0.433 0.170 0.190 0.160 0.140 0.150
0.435 0.158 0.200 0.155 0.147 0.150
0.434 0.155 0.200 0.155 0.150 0.150
0.003 0.010 0.009 0.005 0.005 0.006
0.65% 6.21% 4.47% 3.53% 3.52% 4.22%
164.69% -3.63% 21.73% -5.66% -10.73% -8.70%
8.04 0.05 1.25 0.05 0.29 0.19
Lab Lab
1.12 1.13
AR*OES AR*MS
10.0 11.5
10.0 11.9
10.0 12.4
10.0 11.5
10.0 11.4
10.0 12.1
10.0 11.8
10.0 11.7
0.0 0.4
0.00% 3.47%
-3.87% 13.11%
0.27 0.27

1.10 1.11 1.12 1.13 1.14 1.15
24.7 28.0 26.0 24.3 24.0 29.0

25.4 28.0 27.0 24.7 25.0 27.0
25.7 27.0 24.0 25.0 24.0 26.0
25.7 28.0 24.0 25.1 23.0 28.0
25.3 27.0 27.0 24.5 24.0 25.0
25.1 28.0 25.0 25.1 23.0 25.0
25.3 27.7 25.5 24.8 23.8 26.7
25.4 28.0 25.5 24.9 24.0 26.5
0.4 0.5 1.4 0.3 0.8 1.6
1.55% 1.87% 5.41% 1.36% 3.16% 6.12%
3.34% 12.96% 4.12% 1.19% -2.69% 8.88%
0.26 0.94 0.31 0.11 0.17 0.65
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
0.348 0.400 0.349 0.340 0.339

0.334 0.406 0.368 0.342 0.339
0.329 0.375 0.361 0.341 0.340
0.344 0.400 0.353 0.337 0.348
0.342 0.370 0.366 0.339 0.346
0.345 0.386 0.367 0.331 0.350
0.340 0.390 0.361 0.338 0.344
0.343 0.393 0.364 0.340 0.343
0.007 0.015 0.008 0.004 0.005
2.14% 3.80% 2.21% 1.18% 1.43%
0.17% 14.64% 6.15% -0.42% 1.15%
0.00 5.45 2.25 0.22 0.37
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
6.00 7.00 5.10 10.00 7.00

6.00 8.00 4.60 9.00 8.00
5.00 8.00 4.60 8.00 8.00
5.00 6.00 4.70 10.00 8.00
5.00 10.00 4.40 9.00 5.00
6.00 7.00 4.50 9.00 6.00
5.50 7.67 4.65 9.17 7.00
5.50 7.50 4.60 9.00 7.50
0.548 1.366 0.243 0.753 1.265
9.96% 17.82% 5.22% 8.21% 18.07%
7.84% 50.33% -8.82% 79.74% 37.26%
0.06 1.62 0.62 2.70 1.14
Lab
1.13
AR*MS
308
327
296
325
330
296
314
317
16
5.00%
-13.21%
0.68

1.10 1.11 1.12 1.13 1.14 1.15
0.271 0.300 0.350 0.330 0.300 0.300

0.272 0.280 0.310 0.300 0.390 0.310
0.271 0.290 0.290 0.290 0.300 0.290
0.272 0.290 0.300 0.330 0.290 0.320
0.279 0.280 0.280 0.300 0.300 0.290
0.279 0.280 0.300 0.310 0.280 0.320
0.274 0.287 0.305 0.310 0.310 0.305
0.272 0.285 0.300 0.305 0.300 0.305
0.004 0.008 0.024 0.017 0.040 0.014
1.34% 2.85% 7.96% 5.40% 12.90% 4.52%
-7.80% -3.52% 2.65% 4.33% 4.33% 2.65%
1.42 0.56 0.07 1.01 0.07 0.67
Lab Lab
1.13 1.15
AR*MS AR*OES
0.32 <2
0.37 <2
0.32 <2
0.27 <2
0.31 <2
0.28 <2
0.31
0.32
0.035
11.37%
-9.82%
1.23 NA

1.10 1.11 1.12 1.13 1.14 1.15
9.03 7.00 9.00 7.20 8.00 7.00

9.01 7.00 9.00 7.20 8.00 7.00
8.70 7.00 8.00 7.30 8.00 7.00
8.37 8.00 9.00 7.40 8.00 7.00
8.78 8.00 8.00 7.20 8.00 7.00
8.79 7.00 8.00 7.40 8.00 7.00
8.78 7.33 8.50 7.28 8.00 7.00
8.79 7.00 8.50 7.25 8.00 7.00
0.239 0.516 0.548 0.098 0.000 0.000
2.73% 7.04% 6.44% 1.35% 0.00% 0.00%
0.11% -16.39% -3.09% -16.96% -8.79% -20.19%
0.24 0.64 0.07 0.67 0.23 0.85
Lab
1.13
AR*MS
2.40
2.10
2.10
2.40
2.20
2.10
2.22
2.15
0.147
6.64%
10.41%
1.64
Lab Lab Lab
1.10 1.12 1.13
AR*MS AR*OES AR*MS
104 110 107

104 110 109
105 100 111
104 100 111
105 100 110
105 100 112
104 103 110
104 100 110
1 5 2
0.59% 5.00% 1.79%
-4.96% -6.00% -0.16%
0.67 0.82 0.00

1.10 1.11 1.12 1.13 1.14 1.15
66.4 50.0 52.0 46.3 44.0 45.0

66.8 43.0 55.0 46.3 45.0 44.0
68.1 44.0 49.0 48.5 43.0 44.0
67.3 45.0 52.0 47.3 43.0 45.0
66.1 45.0 47.0 47.2 44.0 44.0
68.8 48.0 47.0 49.3 44.0 45.0
67.2 45.8 50.3 47.5 43.8 44.5
67.0 45.0 50.5 47.3 44.0 44.5
1.047 2.639 3.204 1.204 0.753 0.548
1.56% 5.76% 6.37% 2.54% 1.72% 1.23%
45.72% -0.66% 9.09% 2.92% -5.00% -3.55%
3.58 0.14 0.64 0.14 0.49 0.38
Lab
1.13
AR*MS
< 0.01
< 0.01
< 0.01
< 0.01
< 0.01
< 0.01
NA
Lab Lab Lab
1.10 1.12 1.13
AR*MS AR*OES AR*MS
0.22 < 10 0.18

0.23 < 10 0.15
0.21 < 10 0.17
0.21 < 10 0.19
0.21 < 10 0.16
0.22 < 10 0.16
0.22 0.17
0.21 0.17
0.008 0.015
3.87% 8.74%
15.88% -9.45%
0.79 NA 0.67
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
< 20 < 20 8.20 < 20 < 20

< 20 < 20 8.20 < 20 < 20
< 20 < 20 8.50 < 20 < 20
< 20 < 20 8.40 < 20 < 20
< 20 < 20 8.30 < 20 < 20
< 20 < 20 8.70 < 20 < 20
8.38
8.35
0.194
2.32%
16.60%
NA NA 1.46 NA NA
Lab Lab Lab Lab Lab
1.11 1.12 1.13 1.14 1.15
0.090 0.100 0.098 0.100 0.100

0.100 0.100 0.099 0.100 0.100
0.090 0.100 0.096 0.100 0.100
0.100 0.100 0.096 0.100 0.100
0.100 0.100 0.096 0.100 0.100
0.090 0.100 0.098 0.090 0.100
0.095 0.100 0.097 0.098 0.100
0.095 0.100 0.097 0.100 0.100
0.005 0.000 0.001 0.004 0.000
5.77% 0.00% 1.37% 4.15% 0.00%
-1.65% 3.53% 0.59% 1.80% 3.53%
0.52 0.67 0.00 0.67 0.67

1.10 1.11 1.12 1.13 1.14 1.15
2.29 < 10 < 10 2.65 < 10 < 10

2.25 10.00 < 10 2.69 < 10 < 10
2.26 10.00 < 10 2.72 < 10 < 10
2.29 10.00 < 10 2.66 < 10 < 10
2.26 10.00 < 10 2.66 < 10 < 10
2.28 < 10 < 10 2.66 < 10 < 10
2.27 10.00 2.67
2.27 10.00 2.66
0.017 0.000 0.027
0.74% 0.00% 0.99%
-1.64% 333.48% 15.88%
0.10 16.18 NA 0.75 NA NA
Lab Lab Lab Lab Lab
1.11 1.12 1.13 1.14 1.15
< 10 < 10 5.22 < 10 < 10

< 10 < 10 5.24 < 10 < 10
< 10 < 10 5.40 < 10 < 10
< 10 < 10 5.34 < 10 < 10
< 10 < 10 5.31 < 10 < 10
< 10 < 10 5.48 < 10 < 10
5.33
5.33
0.098
1.84%
19.48%
NA NA 1.12 NA NA
Lab Lab Lab Lab Lab

1.11 1.12 1.13 1.14 1.15
56 59 57 56 54
55 62 58 58 54
55 57 56 57 55
57 60 57 56 56
56 56 56 57 56
56 57 57 57 56
56 59 57 57 55
56 58 57 57 56
0.8 2.3 0.8 0.8 1.0
1.35% 3.86% 1.32% 1.32% 1.78%
-0.65% 4.10% 1.13% 1.13% -1.83%
0.40 0.67 0.00 0.00 0.67
Lab Lab Lab Lab

1.12 1.13 1.14 1.15
0.374 0.469 0.445 0.479

0.434 0.487 0.471 0.528
0.428 0.450 0.474 0.512
0.487 0.437 0.458 0.529
0.394 0.433 0.460 0.552
0.480 0.413 0.428 0.531
0.433 0.448 0.456 0.522
0.431 0.444 0.459 0.529
0.045 0.027 0.017 0.025
10.41% 5.93% 3.77% 4.71%
-1.63% 1.86% 3.64% 18.60%
0.23 0.00 0.12 1.22
Lab Lab Lab

1.10 1.12 1.13
AR*MS AR*OES AR*MS
13.0 10.0 12.1

13.0 10.0 12.0
13.3 10.0 12.5
13.4 10.0 12.4
13.0 10.0 12.2
13.1 10.0 12.7
13.1 10.0 12.3
13.1 10.0 12.3
0.2 0.0 0.3
1.30% 0.00% 2.20%
13.91% -13.33% 6.53%
1.10 0.67 0.62
Lab Lab Lab Lab Lab
1.11 1.12 1.13 1.14 1.15
212 225 219 209 207

198 227 219 210 206
192 215 213 211 206
201 223 216 207 212
199 211 214 210 209
209 218 219 209 210
202 220 217 209 208
200 221 218 210 208
7 6 3 1 2
3.67% 2.82% 1.26% 0.65% 1.16%
-2.36% 6.35% 4.82% 1.27% 0.79%
0.53 0.93 0.67 0.08 0.00
Lab Lab
1.12 1.13
AR*OES AR*MS
25.0 26.8
26.0 26.7
24.0 27.4
25.0 27.4
23.0 27.1
25.0 27.8
24.7 27.2
25.0 27.3
1.033 0.415
4.19% 1.52%
-1.12% 9.04%
0.33 0.58
Certified
1.00
ppm
3.00
3.00
1.000
7.000
16.000
0.499
72.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
3.13
73.00
Certified
1.00
ppm
2.00
2.00
1.00
3.00
16.00
3.88
74.00
Certified
1.00
ppm
3.00
3.00
1.000
#N/A
16.000
0.505
75.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
< 30
76.0
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
81
77
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.73
78.00
Certified
1.00
ppm
2.00
2.00
1.00
8.00
16.00
6.89
79.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
4.45
80.00
Certified
1.00
ppm
2.00
2.00
1.00
9.00
16.00
< 0.5
81.00
Certified
1.00
ppm
1.00
1.00
1.0
10.0
16.0
43.9
82.0
Certified
1.00
ppm
1.00
2.00
1.0
5.0
16.0
15.2
83.0
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
51
84
Indicative
1.00
ppm
1.00
1.00
1.0
15.0
16.0
45.0
21.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.203
85.000
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
2.27
22.00
Indicative
1.00
ppm
2.00
2.00
1.00
12.00
16.00
1.07
23.00
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
0.63
24.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
14.66
86.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
112
87
Indicative
1.00
ppm
2.00
2.00
1.00
19.00
16.00
3.18
25.00
Indicative
1.00
ppm
2.00
2.00
1.00
20.00
16.00
2.82
26.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.81
88.00
Indicative
1.00
ppm
2.00
2.00
1.00
21.00
16.00
0.89
27.00
Indicative
1.00
ppm
2.00
2.00
1.00
22.00
16.00
0.41
28.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.67
89.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.24
90.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
20.6
91.0
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
84
92
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.13
93.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.948
94.000
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.237
95.000
Certified
1.00
ppm
0.00
0.00
1
4
16
83
96
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.164
97.000
Certified
1.00
ppm
1.00
1.00
1.0
11.0
16.0
10.4
98.0
Indicative
1.00
ppm
1.00
1.00
1.0
23.0
16.0
19.9
29.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
24.5
99.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.340
100.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.10
101.00
Indicative
1.00
ppb
0.00
0.00
1
1
16
< 10
21
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
4.69
22.00
Indicative
1.00
ppb
0.00
0.00
1
1
16
<1
23
Indicative
1.00
ppm
0.00
0.00
1
18
16
361
24
Indicative
1.00
ppm
3.00
3.00
1.000
19.000
16.000
0.045
25.000
Certified
1.00
wt.%
3.00
3.00
1.000
25.000
16.000
0.297
102.000
Indicative
1.00
ppm
2.00
2.00
1.00
20.00
16.00
0.35
26.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
8.77
103.00
Certified
1.00
ppm
2.00
3.00
1.00
8.00
16.00
2.01
104.00
Indicative
1.00
wt.%
3.00
3.00
1.000
21.000
16.000
0.139
27.000
Indicative
1.00
ppm
2.00
2.00
1.00
22.00
16.00
3.86
28.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
110
105
Certified
1.00
ppm
1.00
2.00
1.0
5.0
16.0
46.1
106.0
Indicative
1.00
ppm
2.00
2.00
1.00
23.00
16.00
0.21
29.00
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
0.45
21.00
Certified
1.00
ppm
2.00
2.00
1.00
12.00
16.00
0.19
107.00
Indicative
1.00
ppm
2.00
2.00
1.00
16.00
16.00
7.19
22.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.097
108.000
Indicative
1.00
ppm
2.00
2.00
1.00
17.00
16.00
2.31
23.00
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
0.15
24.00
Indicative
1.00
ppm
2.00
2.00
1.00
19.00
16.00
4.46
25.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
56
109
Indicative
1.00
wt.%
3.00
3.00
1.000
20.000
16.000
0.440
26.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
11.5
110.0
Indicative
1.00
ppm
2.00
2.00
1.00
21.00
16.00
0.95
27.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
207
111
Certified
1.00
ppm
1.00
2.00
1.0
3.0
16.0
24.9
112.0
Analytical results for S in OREAS 700 (Indicative Value 0.325 wt.%)
S Round Replicate Lab
No No 1.07
IRC
1 1 0.320
1 2 0.330
1 3 0.320
1 4 0.330
1 5 0.320
1 6 0.330
Mean 0.325
Median 0.325
Std Dev. 0.005
Rel.Std.Dev. 1.69%
PDM3 0.00%
Indicative
1.00
wt.%
3.00
3.00
1.000
25.000
16.000
0.325
31.000
Analytical results for FeO in OREAS 700 (Certified Value 12.07 wt.%)
FeO Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.02 1.03 1.04 1.06 1.07
AD*TITR AD*TITR AD*TITR AD*TITR AD*TITR AD*TITR
1 1 12.53 12.51 11.85 12.50 11.75 11.50

1 2 12.92 11.95 11.85 12.30 11.82 11.80
1 3 12.85 11.92 11.82 12.10 11.94 11.80
1 4 12.83 11.61 11.90 12.20 10.16 11.70
1 5 12.85 11.90 11.95 12.10 11.75 11.80
1 6 12.55 12.10 11.81 12.30 12.07 11.60
Mean 12.76 12.00 11.86 12.25 11.58 11.70
Median 12.84 11.94 11.85 12.25 11.79 11.75
Std Dev. 0.169 0.297 0.053 0.152 0.707 0.126
Rel.Std.Dev. 1.33% 2.48% 0.44% 1.24% 6.11% 1.08%
PDM3 5.69% -0.58% -1.70% 1.50% -4.04% -3.06%
Z-Score (Absolute) 1.96 0.07 0.27 0.70 0.26 0.67
1.08 1.09 1.10 1.11 1.16 1.17
AD*TITR AD*TITR AD*TITR AD*TITR AD*TITR AD*TITR
11.52 12.60 10.95 11.80 12.10 12.08

11.59 12.90 11.51 11.80 11.90 12.17
11.59 12.60 10.88 11.95 12.20 12.18
11.40 12.50 10.55 12.15 12.00 12.24
11.23 12.60 10.98 11.85 12.20 12.20
11.43 12.60 10.55 12.10 11.90 12.57
11.46 12.63 10.90 11.94 12.05 12.24
11.48 12.60 10.92 11.90 12.05 12.19
0.138 0.137 0.354 0.153 0.138 0.170
1.20% 1.08% 3.24% 1.28% 1.14% 1.39%
-5.05% 4.68% -9.67% -1.05% -0.16% 1.42%
1.27 1.66 2.67 0.07 0.20 0.67
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
12.07
114.00
Analytical results for MassRec in OREAS 700 (Certified Value 11.28 wt.%)
MassRec Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.02 1.06 1.08 1.14 1.20
DTR-REC DTR-REC DTR-REC DTR-REC DTR-REC DTR-REC
1 1 10.59 11.90 11.26 10.50 11.30 10.90

1 2 10.40 11.64 11.49 10.70 10.75 11.00
1 3 10.04 11.44 11.39 6.60 11.35 11.00
1 4 NA
1 5 NA
1 6 10.15 NA
Mean 10.30 11.66 11.38 9.27 11.13 10.97
Median 10.28 11.64 11.39 10.50 11.30 11.00
Std Dev. 0.249 0.231 0.115 2.312 0.333 0.058
Rel.Std.Dev. 2.42% 1.98% 1.01% 24.94% 2.99% 0.53%
PDM3 -8.73% 3.34% 0.86% -17.87% -1.32% -2.80%
Z-Score (Absolute) 5.17 2.28 0.74 10.81 0.60 1.52
Lab Lab Lab Lab
3.01 3.02 3.04 3.05
DTR-REC DTR-REC DTR-REC DTR-REC
11.10 11.43 11.26 11.35

11.30 11.31 11.38 11.40
11.20 11.12 11.36 11.15
11.20 11.29 11.33 11.30

11.20 11.31 11.36 11.35
0.100 0.158 0.064 0.132
0.89% 1.40% 0.57% 1.17%
-0.73% 0.04% 0.45% 0.15%
0.24 0.24 0.49 0.31
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
11.28
116.00
Analytical results for Fe3O4 in OREAS 700 (Certified Value 10.91 wt.%)
Fe3O4 Round Replicate Lab Lab Lab Lab Lab Lab
No No 1.01 1.06 1.08 1.14 1.16 3.01
MAG-SUS MAG-SUS MAG-SUS MAG-SUS MAG-SUS MAG-SUS
1 1 10.70 11.02 10.07 10.92 11.10

1 2 10.60 11.07 10.28 10.83 11.40
1 3 10.80 11.02 10.31 10.83 10.83 11.30
1 4 --- NA --
1 5 --- NA --
1 6 10.90 NA --
Mean 10.75 11.04 10.22 10.83 10.86 11.27
Median 10.75 11.02 10.28 10.83 10.83 11.30
Std Dev. 0.129 0.029 0.131 0.052 0.153
Rel.Std.Dev. 1.20% 0.26% 1.28% 0.48% 1.36%
PDM3 -1.50% 1.13% -6.35% -0.72% -0.49% 3.24%
Z-Score (Absolute) 0.61 0.74 3.10 0.21 0.09 1.82
Lab Lab Lab Lab
3.02 3.03 3.04 3.05
MAG-SUS MAG-SUS MAG-SUS MAG-SUS
11.04 10.98 10.65 12.30

10.95 10.86 10.74 12.45
10.95 10.86 10.65 12.40
10.98 10.90 10.68 12.38

10.95 10.86 10.65 12.40
0.052 0.069 0.052 0.076
0.47% 0.64% 0.49% 0.62%
0.61% -0.12% -2.14% 13.47%
0.47 0.09 0.94 7.07
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
10.91
118.00

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STD - Ore - Sevenhundred Paquete Datos

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Table 1.

Abbreviations used for OREAS 700

Batch & Limits

one sigma standard deviation

- Outlying individual values

- Outlying laboratory batch data sets and superfluous limit values

Constituent Unit Value Constituent Unit Value Constituent Unit Value

Certified Absolute Standard Deviations Relative Standard Deviations 5% window

Analytical results for Pd in OREAS 700 (Indicative Value 5 ppb)

Analytical results for Pt in OREAS 700 (Indicative Value < 5 ppb)

0.530 0.523 0.499 0.502 0.500 0.469 0.500

1 1 10.60 10.63 10.70 10.48 10.80 10.82

Analytical results for As in OREAS 700 (Indicative Value 33.3 ppm)

1 1 < 100 30.0 30.0 50.0 30.0 < 10

1 1 113 150 130 130 170 150

1 1 8.00 7.96 8.13 7.82 7.74 8.02

Analytical results for Cl in OREAS 700 (Certified Value 158 ppm)

1 1 220 180 120 160 140

Analytical results for Co in OREAS 700 (Indicative Value 17.2 ppm)

1 1 < 100 20.0 20.0 < 10 10.0 < 10

Analytical results for Cr2O3 in OREAS 700 (Indicative Value 79 ppm)

1 1 < 100 < 100 85 60 51 70

Analytical results for Cu in OREAS 700 (Certified Value 0.204 wt.%)

1 1 0.212 0.200 0.204 0.192 0.192 0.224

1 1 16.40 16.20 17.00 16.76 16.18 16.00

1 1 1.95 1.92 1.91 1.87 1.89 1.77

1 1 1.72 1.75 1.65 1.68 1.70 1.78

1 1 0.410 0.430 0.370 0.400 0.381 0.412

Analytical results for Mo in OREAS 700 (Indicative Value 118 ppm)

1 1 1.66 1.73 1.49 1.57 1.60 1.66

Analytical results for Ni in OREAS 700 (Certified Value < 50 ppm)

Analytical results for P in OREAS 700 (Certified Value 0.353 wt.%)

1 1 0.360 0.356 0.353 0.340 0.359 0.348

1 1 < 100 < 10 < 10 < 10 < 10 20.0

Analytical results for S in OREAS 700 (Certified Value 0.304 wt.%)

1 1 0.320 0.320 0.200 0.301 0.300 0.304

1 1 47.30 47.50 47.30 47.36 47.88 47.10

Analytical results for Sn in OREAS 700 (Certified Value 182 ppm)

1 1 150 230 58 200 170 150

Analytical results for Sr in OREAS 700 (Indicative Value 47.5 ppm)

1 1 100.0 60.0 < 10 30.0 50.0

1 1 0.330 0.330 0.290 0.430 0.340 0.317

1 1 < 100 120 110 70 110 110

Analytical results for W in OREAS 700 (Certified Value 1.13 wt.%)

1 1 1.14 1.25 1.14 1.15 1.14 0.96

1 1 200 240 220 210 220 240

Analytical results for Zr in OREAS 700 (Indicative Value 53 ppm)

10.65 10.55 10.70 10.50 10.64 10.75

7.86 7.70 7.85 7.72 7.91 7.77

16.15 15.94 15.91 15.84 15.78 16.19 16.00 16.02

Lab Lab Lab Lab Lab Lab

1.87 1.90 1.92 1.87 1.94 1.88

Lab Lab Lab Lab Lab Lab

1.76 1.72 1.78 1.70 1.75 1.78

Lab Lab Lab Lab Lab

0.416 0.424 0.412 0.427 0.411

Lab Lab Lab Lab

1.71 1.62 1.65 1.64

Lab Lab Lab Lab Lab Lab

0.350 0.352 0.364 0.355 0.351 0.354

0.275 0.311 0.301 0.350 0.317

Lab Lab Lab Lab Lab Lab Lab Lab Lab

47.56 49.21 47.30 46.30 47.00 46.60 47.40 48.00 47.60