Volumen dispensado (ml) 1 l.

micropipeta: 1ml Blanco de Dilución (ml)

Analista: Fecha: Analista:

Peso final
Peso de
(peso inicial +
Peso inicial volumen
Nº de evento volumen
(g) dispensado
dispensado)
(g)
(g)

1 5.03 5.99 0.9600

2 5.04 6.02 0.9800
3 5.19 6.12 0.9300
4 5.04 6.01 0.9700
5 5.21 6.18 0.9700
6 5.22 6.2 0.9800
7 5.1 6.04 0.9400
8 5.14 6.16 1.0200
9 5.04 6.03 0.9900
10 5.08 6.06 0.9800
11 5.17 6.02 0.8500
12 5.11 6.09 0.9800
13 5.2 6.19 0.9900
14 5.11 6.08 0.9700
15 5.11 6.11 1.0000
16 5.16 6.15 0.9900
17 5.21 6.09 0.8800
18 5.13 6.07 0.9400
19 5.15 6.14 0.9900
20 5.03 6 0.9700
Volumen
Estadísticos
dispensado

Media 0.964000

S 0.040184

S2 0.001615

RSD (w) 0.041684

RSD2 (w2) 0.001738

Incertidumbre del Volúmen dispensado del Laboratorio

Estadísticos Analista 1 a Analista 2 b Analista 3 c Analista 4

Media 0.964000 8.923000 89.611000 10.084600
 S 0.040184 0.097824 0.831092 0.020006
S2 0.001615 0.009569 0.690715 0.000400
RSD (w) 0.041684 0.010963 0.009274 0.001984
RSD2 0.001738 0.000120 0.000086 0.000004

Observaciones:

Realizado por: Revisado por:

anco de Dilución (ml) 9 Vol. Pipeta: 10 mL Blanco de Dilución (ml) 90
Fecha: Analista:

Peso final
Peso de
(peso inicial +
Peso inicial volumen Nº de evento Peso inicial
Nº de evento volumen
(g) dispensado (g)
dispensado)
(g)
(g)

1 11.61 20.5 8.8900 1 242.73

2 11.63 20.65 9.0200 2 243.74
3 11.87 20.84 8.9700 3 243.63
4 11.43 20.35 8.9200 4 243.11
5 11.52 20.33 8.8100 5 242.51
6 11.65 20.9 9.2500 6 243.45
7 11.31 20.27 8.9600 7 243.39
8 11.45 20.35 8.9000 8 242.25
9 11.55 20.38 8.8300 9 242.76
10 11.68 20.55 8.8700 10 243.54
11 11.44 20.49 9.0500 11 243.71
12 11.52 20.46 8.9400 12 243.24
13 11.41 20.27 8.8600 13 241.94
14 11.33 20.21 8.8800 14 242.98
15 11.56 20.41 8.8500 15 243.52
16 11.32 20.21 8.8900 16 243.58
17 11.53 20.38 8.8500 17 242.97
18 11.56 20.49 8.9300 18 242.12
19 11.41 20.29 8.8800 19 242.8
20 11.74 20.65 8.9100 20 242.02
Blanco de
Estadísticos
Dilución

Media 8.923000

S 0.097824

S2 0.009569

RSD (w) 0.010963

RSD2 (w2) 0.000120

laboratorio
evisado por:
Vol. Probeta: 100 mL Blanco de Dilución: 10 mL Vol. Pipeta: 10 mL
Fecha: Analista: Fecha:

Peso final Peso Final

Peso de
(peso inicial + Nº de Peso Inicial (peso inicial
volumen
volumen Analista
dispensado)
dispensado evento del frasco + volumen
(g)
(g) dispensado)

331.53 88.8 1 CS 24.219 34.279

333.77 90.03 2 CS 18.299 28.395
332.09 88.46 3 CS 21.856 31.901
334.07 90.96 4 CS 16.438 26.52
331.01 88.5 5 CS 18.003 28.106
331.99 88.54 6 CS 15.171 25.235
332.98 89.59 7 CS 15.617 25.696
331.81 89.56 8 CS 17.074 27.163
332.7 89.94 9 CS 16.518 26.609
333.25 89.71 10 CS 18.137 28.226
333.95 90.24 11 CS 22.461 32.564
332.9 89.66 12 CS 24.263 34.331
331.65 89.71 13 CS 24.014 34.072
333.21 90.23 14 CS 20.113 30.215
334.15 90.63 15 CS 23.705 33.83
334.27 90.69 16 CS 19.737 29.824
331.65 88.68 17 CS 17.296 27.374
330.24 88.12 18 CS 19.962 30.077
333.12 90.32 19 CS 20.923 31.01
331.87 89.85 20 CS 18.846 28.917
Estadísticos Blanco de Estadísticos
Dilución

Media 89.611000 Media

S 0.831092 S

S2 0.690715 S2

RSD (w) 0.009274 RSD (w)

RSD2 0.000086 RSD2

 Peso de
Volumen
Dispensado
(g)

10.060
10.096
10.045
10.082
10.103
10.064
10.079
10.089
10.091
10.089
10.103
10.068
10.058
10.102
10.125
10.087
10.078
10.115
10.087
10.071
Blanco de
Dilución

10.084600

0.020006

0.000400

0.001984

0.000004
 6.4.3. Incertidumbre Relativa del Volumen dispensado

Analista: 1. Rosa Romo

2. Giannina Aguilar

Volumen dispensado (99 mL) Volumen dispensado (1 mL) Volumen dispensado (0.1 mL)

Peso Final (g) Peso Peso Final (g) Peso Peso Final (g) Peso
Peso Inicial (g) Peso de Volumen Peso Inicial (g) Peso de Volumen Peso Inicial (g) Peso de Volumen
inicial + volumen inicial + volumen inicial + volumen
Frasco vacio Dispensado (g) Frasco vacio Dispensado (g) Frasco vacio Dispensado (g)
dispensado dispensado dispensado

1 158.96 258.64 99.68 1 1 30.6238 31.6114 0.9876 1 31.6114 31.7095 0.0981

1 159.15 258.84 99.69 2 1 30.1551 31.1744 1.0193 1 31.1744 31.2803 0.1059
1 159.04 258.54 99.50 3 1 30.4486 31.4450 0.9964 1 31.445 31.5411 0.0961
1 158.88 258.42 99.54 4 1 30.6054 31.6054 1.0000 1 31.6054 31.7069 0.1015
1 159.19 258.83 99.64 5 1 29.0200 30.0245 1.0045 1 30.0245 30.1245 0.1000
1 161.18 260.68 99.50 6 1 30.4419 31.4410 0.9991 1 31.441 31.5373 0.0963
1 159.54 259.1 99.56 7 1 29.1982 30.1927 0.9945 1 30.1927 30.2916 0.0989
1 161.05 260.44 99.39 8 1 30.5361 31.5340 0.9979 1 31.534 31.6352 0.1012
1 159.63 259.36 99.73 9 1 35.6761 36.6716 0.9955 1 36.6716 36.7668 0.0952
1 158.32 257.84 99.52 10 1 35.9400 36.9372 0.9972 1 36.9372 37.0378 0.1006
1 159.78 259.39 99.61 11 1 35.6596 36.6614 1.0018 1 36.6614 36.7550 0.0936
1 158.95 258.36 99.41 12 1 35.5128 36.5143 1.0015 1 36.5143 36.6392 0.1249
1 158.64 258.32 99.68 13 1 35.8655 36.8598 0.9943 1 36.8598 36.9614 0.1016
1 158.9 258.43 99.53 14 1 35.5743 36.5616 0.9873 1 36.5616 36.6610 0.0994
1 162.15 261.67 99.52 15 1 35.6022 36.6008 0.9986 1 36.6008 36.6975 0.0967
1 158.98 258.6 99.62 16 1 35.6022 36.6581 1.0559 1 36.6881 36.7849 0.0968
1 159.73 259.3 99.57 17 1 35.6978 36.6987 1.0009 1 36.6987 36.7989 0.1002
1 160.00 259.56 99.56 18 1 35.2647 36.2659 1.0012 1 36.2659 36.3708 0.1049
1 160.97 260.69 99.72 19 1 35.2169 36.2209 1.0040 1 36.2209 36.3348 0.1139
1 159.33 258.87 99.54 20 1 31.3640 32.3698 1.0058 1 32.3698 32.4689 0.0991
1 161.45 261.44 99.99 21 1 30.5470 31.5636 1.0166 1 21.6744 21.7741 0.0997
1 159.72 259.13 99.41 22 1 30.8086 31.8269 1.0183 1 21.6744 21.7741 0.0997
1 161.24 260.87 99.63 23 1 30.5168 31.5536 1.0368 1 20.6868 20.7906 0.1038
1 161.62 261.21 99.59 24 1 30.3762 31.4026 1.0264 1 21.2753 21.3775 0.1022
1 158.85 258.53 99.68 25 1 30.7104 31.7357 1.0253 1 21.6408 21.7056 0.0648
1 161.84 261.34 99.50 26 1 31.0960 32.1154 1.0194 1 21.6744 21.7741 0.0997
1 159.10 258.59 99.49 27 1 30.5247 31.5495 1.0248 1 21.6744 21.7741 0.0997
1 161.47 261.19 99.72 28 1 30.1613 31.1849 1.0236 1 21.4466 21.5494 0.1028
1 161.00 260.52 99.52 29 1 35.6274 36.6465 1.0191 1 21.6744 21.7741 0.0997
1 160.10 259.29 99.19 30 1 35.7772 36.8031 1.0259 1 21.9644 22.0651 0.1007
1 159.50 259.28 99.78 31 1 35.3679 36.3850 1.0171 1 22.0092 22.1152 0.1060
1 162.04 261.29 99.25 32 1 35.2694 36.2885 1.0191 1 21.5431 21.6412 0.0981
1 158.45 257.89 99.44 33 1 35.3322 36.3477 1.0155 1 21.6744 21.7741 0.0997
1 159.85 259.62 99.77 34 1 36.0415 37.0623 1.0208 1 21.6744 21.7741 0.0997
1 158.98 258.37 99.39 35 1 35.4696 36.4968 1.0272 1 20.9384 21.0381 0.0997
1 161.96 261.77 99.81 36 1 35.9254 36.9481 1.0227 1 22.3201 22.4276 0.1075
1 160.34 260.01 99.67 37 1 35.9423 36.9609 1.0186 1 21.5366 21.6394 0.1028
1 159.7 259.31 99.61 38 1 35.6498 36.6598 1.0100 1 21.8608 21.9656 0.1048
1 161.52 260.59 99.07 39 1 35.2169 36.2397 1.0228 1 22.5431 22.6422 0.0991
1 161.73 261.19 99.46 40 1 35.6482 36.6690 1.0208 1 21.7744 21.8741 0.0997
2 159.86 259.78 99.92 41 2 23.2543 24.2420 0.9877 2 24.2420 24.3457 0.1037
2 159.22 258.9 99.68 42 2 23.0156 24.0041 0.9885 2 24.0041 24.1033 0.0992
2 160.47 259.88 99.41 43 2 23.2259 24.2193 0.9934 2 24.2193 24.3179 0.0986
2 159.84 258.91 99.07 44 2 23.0888 24.0797 0.9909 2 24.0797 24.1787 0.0990
2 161.54 260.59 99.05 45 2 23.5754 24.5685 0.9931 2 24.5685 24.6689 0.1004
2 161.32 260.72 99.40 46 2 23.3401 24.3372 0.9971 2 24.3372 24.4400 0.1028
2 159.22 258.63 99.41 47 2 23.3404 24.3253 0.9849 2 24.3553 24.4274 0.0721
2 161.58 261.19 99.61 48 2 22.9752 23.9669 0.9917 2 23.9669 24.0628 0.0959
2 159.14 258.71 99.57 49 2 23.7646 24.7539 0.9893 2 24.7539 24.8539 0.1000
2 159.18 258.86 99.68 50 2 23.1388 24.1378 0.9990 2 24.1378 24.2385 0.1007
2 159.81 259.43 99.62 51 2 23.3709 24.3586 0.9877 2 24.3586 24.4596 0.1010
2 158.97 258.51 99.54 52 2 23.0225 24.0202 0.9977 2 24.0202 24.1171 0.0969
2 159.37 258.84 99.47 53 2 23.5325 24.5237 0.9912 2 24.5237 24.6177 0.0940
2 159.97 259.46 99.49 54 2 23.3389 24.3259 0.9870 2 24.3259 24.4268 0.1009
2 159.12 258.74 99.62 55 2 22.9353 23.9244 0.9891 2 23.9244 24.0226 0.0982
2 162.14 261.79 99.65 56 2 22.9824 23.9781 0.9957 2 23.0797 23.1787 0.0990
2 161.58 261.16 99.58 57 2 23.0054 24.0010 0.9956 2 21.9669 22.0628 0.0959
2 161.86 261.48 99.62 58 2 22.6598 23.6600 1.0002 2 24.8372 24.9400 0.1028
2 158.69 258.42 99.73 59 2 23.0040 24.0006 0.9966 2 24.5539 24.6639 0.1100
2 161.32 261.01 99.69 60 2 23.0546 24.0409 0.9863 2 23.0202 23.1171 0.0969
2 160.94 260.60 99.66 61 2 26.4602 27.4709 1.0107 2 27.4709 27.5809 0.1100
2 158.49 258.01 99.52 62 2 26.0909 27.1099 1.0190 2 27.1099 27.2259 0.1160
2 161.64 261.27 99.63 63 2 26.5910 27.6109 1.0199 2 27.6109 27.7199 0.1090
2 160.32 259.97 99.65 64 2 26.2668 27.2589 0.9921 2 27.2589 27.3599 0.1010
2 158.97 258.94 99.97 65 2 26.1332 27.1259 0.9927 2 27.1259 27.2289 0.1030
2 159.45 259.10 99.65 66 2 26.5324 27.5408 1.0084 2 27.5408 27.6388 0.0980
2 159.27 258.85 99.58 67 2 26.5674 27.5698 1.0024 2 27.5698 27.6809 0.1111
2 159.25 258.78 99.53 68 2 26.2123 27.2291 1.0168 2 27.2291 27.3304 0.1013
2 161.38 260.87 99.49 69 2 26.3077 27.3209 1.0132 2 27.3209 27.4319 0.1110
2 161.69 261.32 99.63 70 2 26.9054 27.9185 1.0131 2 27.9185 28.0429 0.1244
2 161.92 261.58 99.66 71 2 26.8264 27.8481 1.0217 2 27.8481 27.9644 0.1163
2 159.91 259.53 99.62 72 2 26.7406 27.7350 0.9944 2 27.7350 27.8461 0.1111
2 159.05 258.73 99.68 73 2 26.4607 27.4499 0.9892 2 27.4499 27.5488 0.0989
2 161.26 260.00 98.74 74 2 26.5952 27.6191 1.0239 2 27.6191 27.7199 0.1008
2 161.71 260.81 99.10 75 2 26.5200 27.5399 1.0199 2 27.5399 27.6500 0.1101
2 159.44 259.03 99.59 76 2 26.9430 27.9666 1.0236 2 27.9666 28.0814 0.1148
2 159.05 258.60 99.55 77 2 26.6132 27.5999 0.9867 2 27.5999 27.6990 0.0991
2 159.86 259.78 99.92 78 2 27.3266 28.3210 0.9944 2 28.3210 28.4301 0.1091
2 161.12 259.78 98.66 79 2 26.1610 27.1629 1.0019 2 27.1629 27.2779 0.1150
2 159.32 259.08 99.76 80 2 26.3249 27.3333 1.0084 2 27.3333 27.4465 0.1132
Valor Mínimo 98.66 Valor Mínimo 0.9849 Valor Mínimo 0.0648
Valor Máximo 99.99 Valor Máximo 1.0559 Valor Máximo 0.1249
PROMEDIO 99.55 PROMEDIO 1.01 PROMEDIO 0.10
Limite Inferior (99 + 2mL) 97 mL
Limite Superior (99 + 2mL) 101 mL

MEDIA 99.55 MEDIA 1.0059 MEDIA 0.1020

S 0.2261 S 0.0146 S 0.0084
S² 0.0511 S² 0.0002 S² 0.0001
RSD (W) 0.0023 RSD (W) 0.0145 RSD (W) 0.0825
RSD² (W2) 0.000005160 RSD² (W2) 0.0002 RSD² (W2) 0.0068