Calibração de Picnômetro

#5 #29 #30
621
C
T (ºC) M (g) T (ºC) M (g) T (ºC) M (g)
20.6 620.55 20.7 586.89 20.7 619.4
28.8 620.44 29.2 586.63 28.5 619.19 f(x) = - 0.021649696
620.5 R² = 0.9754884062
38.7 620.14 34.1 586.39 35.8 618.95
45.7 620.04 41.4 585.43 42.6 618.81
50.14 48.5 584.78 50.3 618.66 620

Massa do Picnômetro + água (g)

619.5
f(x) = - 0.025387128
volume do picnometro corrigido R² = 0.98907463

M2 620.55 586.89 619.4 619

M1 120.42 89.86 119.8
Vc 500.0047 500.0055 500.0055
618.5
C 1.56E-05 1.56E-05 1.56E-05
∆t 0.6 0.7 0.7
ρt (20ºC) 0.9981 0.9981 0.9981
618
ρar 0.0012 0.0012 0.0012

617.5
0.9981 20 618.9 20 588.3 20 618.3 15 20 25
0.9973 24 618.5 24 587.9 24 617.9
0.9963 28 618.0 28 587.4 28 617.4
0.9951 32 617.4 32 586.8 32 616.8
0.9944 36 617.0 36 586.5 36 616.4

630.0

620.0
f(x)
f(x) == -- 0.120001123
0.120001310
R²
R² == 0.9939603106
0.9939603106
Massa do Picnômetro + água (g)

610.0

600.0

590.0
f(x) = - 0.120001310
R² = 0.9939603106

580.0

570.0
15 20
 R² = 0.9939603106

580.0

570.0
15 20
621
Calibração experimental

f(x) = - 0.0216496967x + 621.0166823558

20.5 R² = 0.9754884062

620

19.5 620.493
f(x) = - 0.0253871282x + 619.905274022
R² = 0.98907463

619
#
5

18.5

618

17.5
15 20 25 30 35 40 45 50 55

Temperatura (ºC)

30.0
Calibração teórica

20.0
f(x)
f(x) == -- 0.1200011232x
0.1200013104x ++ 621.3046882368
620.6854696096
R²
R² == 0.9939603106
0.9939603106

10.0

00.0

90.0
f(x) = - 0.1200013104x + 590.7454696096
R² = 0.9939603106
#
80.0 5

70.0
15 20 25 30 35 40

Temperatura (ºC)
 R² = 0.9939603106
#
80.0 5

70.0
15 20 25 30 35 40

Temperatura (ºC)
 587.5
Calibração experimental
f(x) = - 0.079720637x + 588.7966837552
R² = 0.9314872979
587

586.5
Massa do Picnômetro + água (g)

586

585.5

#
585 2
9

584.5

584

583.5
15 20 25 30 35 40 45 50 55

Temperatura (ºC)

M2
618.372
617.906
#
2
9
 PROVETA (B)
18
E-556/11 E-557/11 E-558/11
h 12.8 13 12.9 16 f(x) = - 170.9090909091x + 187.054545
f(x) = - 170.9090909091x + 186.248505
C 1.2 1 1.1 14

Altura de queda (cm)

Rhmáx 9.4 9.6 9.5 12
Rh 1.05 1.05 1.05 10
Rh 0.995 0.995 0.995
8
a1 (min) 7.6 7.5 7.55
6
a2 (max) 17 17.1 17.05
V 44.78 47.3 45.28 peso do densimetro 4
A 27.78 27.78 27.78 área da seção interna da proveta 2
2A 55.56 55.56 55.56 0
a' 6.79396 6.6 6.7 0.99 1 1.01 1.02 1.03 1.04 1.05 1.06
a'' 16.2 16.2 16.2 Leitura no densimetro

18
16 f(x) = - 174.5454545455x + 190.772727
f(x) = - 174.5454545455x + 189.921327
14

Altura de queda (cm)

12
10
8
6
4
2
0
0.99 1 1.01 1.02 1.03 1.04 1.05 1.06
Leitura no densimetro

18
16 f(x) = - 172.7272727273x + 188.913636
f(x) = - 172.7272727273x + 188.098596
14
Altura de queda (cm)

12
10
8
6
4
2
0
0.99 1 1.01 1.02 1.03 1.04 1.05 1.06
Leitura no densimetro
 0
0.99 1 1.01 1.02 1.03 1.04 1.05 1.06
Leitura no densimetro

556 1.004
B A
°C dens f(x) = - 4.13231149372385E-06x^2 - 2.74376890110986E-05x + 1.0027868294
1.002
R² = 0.9850696874
41 0.995
1
37 0.996
32 0.997 32 0.997 0.998
28 0.999 27 0.999
0.996
24 1.000 23 1.000
19 1.001 21 1.000 0.994
14 1.0015 19 1.0005
0.992
10 1.0020 14 1.0015
10 1.002 0.99
0 5 10 15 20 25 30 35 40 45

557 558 1.001

°C dens °C dens
22.5 0.999 15.9 0.999 1
f(x) = - 8.07736543667935E-06x^2 + 0.0002273352x + 0.9984193557
26.5 0.999 22.5 0.998 R² = 0.9724924299
0.999
30.3 0.998 26.5 0.998
33.5 0.997 30.2 0.997 0.998
35.3 0.996 33.5 0.996
0.997
37 0.996 35.2 0.995
13.4 1.000 36.8 0.995 0.996
19.8 1.0000 14 1.000
0.995
19.8 0.999
0.994
0 5 10 15 20 25 30 35 40
70.9090909091x + 187.0545454545
70.9090909091x + 186.2485054545

556a1
Linear (556a1)
556a2
Linear (556a2)

1.02 1.03 1.04 1.05 1.06

ura no densimetro

74.5454545455x + 190.7727272727
74.5454545455x + 189.9213272727

557a1
Linear (557a1)
557a2
Linear (557a2)

1.02 1.03 1.04 1.05 1.06

ura no densimetro

72.7272727273x + 188.9136363636
72.7272727273x + 188.0985963636

558a1
Linear (558a1)
558a2
Linear (558a2)

1.02 1.03 1.04 1.05 1.06

ura no densimetro
 1.02 1.03 1.04 1.05 1.06
ura no densimetro

1.003
27868294 1.002
f(x) = - 5.95669240356642E-06x^2 + 3.22843200318723E-05x + 1.0022100157
R² = 0.9874888884
1.001
1
0.999
0.998
0.997
0.996
0.995
0.994
0 5 10 15 20 25 30 35

1.001
1
4193557 f(x) = - 4.87658956701478E-06x^2 + 4.05708414961362E-05x + 1.0000056437
0.999
R² = 0.9666428476
0.998
0.997
0.996
0.995
0.994
0.993
0.992
40 0 5 10 15 20 25 30 35 40