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FACULTAD DE QUIMICA
LABORATORIO DE INGENIERA QUMICA II
EXPERIMENTO 1.
Descarga de Tanques
MXICO
UNAM
2015
I.
PROBLEMA
DIAGRAMA DE FLUJO
III.
h (cm)
122
112
102
92
82
72
62
52
42
32
22
12
2
DATOS EXPERIMENTALES
t1 (s)
0
9.42
19.83
30.61
42.26
54.58
68.30
82.17
97.89
115.48
136.14
161.42
201.26
t2 (s)
0
9.86
19.82
31.00
42.70
55.02
68.70
82.80
98.64
116.16
136.67
163.16
202.07
t3 (s)
0
9.93
20.12
30.93
42.71
55.10
68.56
82.72
98.37
116.40
136.40
162.10
202.42
t4 (s)
0
10.10
20.52
31.09
42.56
54.64
67.77
81.91
96.92
115.10
135.22
160.80
201.95
t5 (s)
0
10.11
20.55
31.51
42.69
55.25
68.11
82.47
97.63
115.77
135.59
161.55
203.03
T6 (s)
0
9.95
20.26
31.16
42.42
54.73
67.70
81.76
97.54
114.73
135.20
160.67
202.60
t7 (s)
0
10.23
20.39
31.02
42.60
55.00
68.07
82.20
97.80
115.10
135.45
161.42
202.13
t8 (s)
0
10.09
20.69
31.39
42.63
59.99
68.33
82.29
97.55
115.35
136.02
161.29
201.29
10.14
10.00
9.88
9.95
20.42
20.36
20.77
20.45
31.39
31.10
31.59
31.30
42.80
42.76
42.85
42.86
54.86
55.20
55.30
55.02
68.04
68.39
68.36
68.11
t
promedio
(s)
0
9.971666
67
20.34833
33
31.17416
67
42.65333
33
55.39083
33
68.20333
33
82.23
82.36
82.45
82.45
82.3175
10
97.83
97.26
97.49
98.08
10
115.08
115.45
115.88
115.51
135.14
135.32
136.05
135.39
161.04
160.51
161.73
161.30
202.02
202.67
203.41
202.50
97.75
115.5008
33
135.7158
33
161.4158
33
202.2791
67
t9 (s)
t10 (s)
t11 (s)
t12 (s)
0
h (cm)
t
promedio
(s)
h/t
(cm/s)
EXP
0
9.971666
67
10.37666
10
67
10.82583
10
33
11.47916
10
67
10
10
10
10
10
10
10
1.002841
38
0.963700
61
0.923716
42
0.871143
38
0.785083
12.7375
42
0.780487
12.8125
8
14.11416
67 0.708508
0.647983
15.4325
15
17.75083 0.563353
33
83
0.494682
20.215
17
0.389105
25.7
06
40.86333 0.244718
33
17
Balance de Energa
P1
g
v1
P2
g
v2
+Z 1 +
+Wf =
+Z 2 +
+ HF
1
gc 2 gc
gc 2 gc
Wf =
( Z 2Z 1 ) g
gc
](
+
)(
P2P1
V V 1
+ 2
+ HF
2 gc
Z2=0
Zi= h(z,h,t)
P=atm 2
P2= atm
Z g V V 1
0= 1 + 2
gc
2 gc
Z 1 g V 2V 1
=
gc
2 gc
Z 1 g V 2V 1
=
gc
2 gc
Z 1 g 2 gc
=V 22V 21
gc
2hg +V 1=V 2
Z 1 g 2=V 2V 1
Como Z1=h
Si Vi es despreciable
2hg=V 2
dh
A =V 2 A2
dt 1
dh
A = 2 hg A2
dt 1
despejando.
h2
A2 t
dh
h = 2 g A dt
h1
1 0
t=
Integrando y
A 1 2 ( h1 h 2)
A2 2 g
IV.
CUESTIONARIO
1. Hacer la grfica: pendiente versus la variable que causa su cambio.
f(x) = NaN x^NaN
R = NaN
Se ocup como mejor opcin una funcin del tipo exponencial. Y se encontr la
siguiente relacin:
y = 0.0612x0.5887
R = 0.9921
3. Recuerde grafico valores discretos. Escriba la ecuacin en la taba 2.
Ecuacin identificada:
n
y=k h
0.5887
y=0.0612 h
Dnde:
y = h/t
h = altura
Ecuacin modificada:
dh
=k hn
dt
h1
=k dt
dh
n
h2 h
0
t=
+1
+1
hn
( hn
)
1
2
k (n+1 )
h
0.5887
=0.0612 h
t
h
=0.0612 h0.5887
t
De donde, se obtiene.
h
= t
0.5887
(0.0612 h
)
62
t
promedio
(s)
0
9.971666
67
20.34833
33
31.17416
67
42.65333
33
55.39083
33
68.20333
33
52
82.3175
42
97.75
115.5008
33
135.7158
33
161.4158
33
202.2791
67
h (cm)
122
112
102
92
82
72
32
22
12
2
h (cm)
t desc
(seg) EXP
% Error
t
ecuacion
ident.
% Error
20.39236
52
20.00090
46
19.45967
55
19.79051
38
23.15494
95
18.08793
41
19.36149
76
18.74539
48
20.31165
59
17.91823
98
18.07531
07
13.87236
09
10.15953
73
10.73459
48
11.40687
5
12.20636
53
13.17761
87
14.39022
52
15.96016
62
18.09846
41
21.24060
03
26.48282
71
37.83855
81
108.6506
23
1.849204
34
3.334342
51
5.093785
13
5.957536
22
3.339895
61
10.96386
73
11.56629
27
14.73033
34
16.42970
01
23.66751
52
32.07986
43
62.39015
26
0
9.971666
67
10.37666
10
67
10.82583
10
33
11.47916
10
67
10
10
12.7375
10
12.8125
14.11416
10
67
10
15.4325
17.75083
10
33
10
10
20.215
25.7
40.86333
10
33
h (cm)
h (cm)
122
112
10
102
10
92
10
82
10
72
10
62
10
52
10
42
10
32
10
22
10
12
10
10
t desc
t desc
(seg) TEO (seg) EXP
7.938207
98
8.301239
46
8.719161
29
9.207380
6
9.788138
3
10.49498
34
11.38145
26
12.53961
7
14.14534
51
16.59282
78
21.05464
52
35.19462
43
9.971666
67
10.37666
67
10.82583
33
11.47916
67
12.7375
12.8125
14.11416
67
15.4325
17.75083
33
20.215
25.7
40.86333
33
% Error
20.39236
52
20.00090
46
19.45967
55
19.79051
38
23.15494
95
18.08793
41
19.36149
76
18.74539
48
20.31165
59
17.91823
98
18.07531
07
13.87236
09