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\ql \li6166\sb0\sl-322\slmult0 \par\pard\ql\li6166\sb0\sl-322\slmult0 \par\pard\
ql\li6166\sb0\sl-322\slmult0 \par\pard\ql\li6166\sb0\sl-322\slmult0 \par\pard\ql
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lmult0 \par\pard\ql\li1783\ri988\sb144\sl-340\slmult0\tx4748 \up0 \expndtw-1\cha
rscalex100 PROCESOS AVANZADOS DE OXIDACIN PARA LA ELIMINACIN \line\tab \up0 \expnd
tw-1\charscalex100 DE CONTAMINANTES \par\pard\ql \li3487\sb173\sl-276\slmult0 \u
p0 \expndtw0\charscalex102 \ul0\nosupersub\cf2\f3\fs24 Xavier Domnech, Wilson F.
Jardim y Marta I. Litter \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\pard\ql\li
1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb0\sl-276\slmult0 \par\pard\ql\li17
02\sb156\sl-276\slmult0 \up0 \expndtw0\charscalex100 1. INTRODUCCIN \par\pard\qj
\li1702\sb0\sl-300\slmult0 \par\pard\qj\li1702\ri919\sb205\sl-300\slmult0\fi566
\up0 \expndtw-1\charscalex100 La creciente demanda de la sociedad para la descon
taminacin de aguas contaminadas \up0 \expndtw-2\charscalex100 de diversos orgenes,
materializada en regulaciones cada vez ms estrictas, ha impulsado, en \up0 \expn
dtw-3\charscalex100 la ltima dcada, al desarrollo de nuevas tecnologas de purificac
in. \par\pard\qj \li1702\ri914\sb187\sl-292\slmult0\fi566 \up0 \expndtw0\charscal
ex108 En la prctica, la aplicacin de los mtodos de tratamiento debe tener en cuenta
\line \up0 \expndtw0\charscalex100 fundamentalmente la naturaleza y las propied
ades fisicoqumicas de las aguas o efluentes a \line \up0 \expndtw-4\charscalex100
tratar [1]. Las aguas contaminadas por la actividad humana pueden, en general,
ser procesadas \line \up0 \expndtw0\charscalex102 eficientemente por plantas de
tratamiento biolgico, por adsorcin con carbn activado u \line \up0 \expndtw-3\chars
calex100 otros adsorbentes, o por tratamientos qumicos convencionales (oxidacin trm
ica, cloracin, \line \up0 \expndtw0\charscalex104 ozonizacin, permanganato de p
otasio, etc.). Sin embargo, en algunos casos estos \line \up0 \expndtw-3\
charscalex100 procedimientos resultan inadecuados para alcanzar el grado de pure
za requerido por ley o por \line \up0 \expndtw0\charscalex102 el uso ulterior de
l efluente tratado. En estos casos y cada vez ms crecientemente, se est \line \up0
\expndtw0\charscalex104 recurriendo en los pases industrializados al uso de las

llamadas Tecnologas o Procesos \line \up0 \expndtw-2\charscalex100 Avanzados de O
xidacin (TAOs, PAOs), muy poco aplicados y, peor an, menos difundidos \line \up0 \
expndtw-3\charscalex100 en los pases de economas emergentes como los de Amrica Lati
na. La mayora de las TAOs \line \up0 \expndtw0\charscalex103 puede aplicarse a la
remediacin y destoxificacin de aguas especiales, generalmente en \line \up0 \expn
dtw-2\charscalex100 pequea o mediana escala. Los mtodos pueden usarse solos o comb
inados entre ellos o con \line \up0 \expndtw0\charscalex100 mtodos convencionales
, pudiendo ser aplicados tambin a contaminantes de aire y suelos. \line \up0 \exp
ndtw0\charscalex100 Permiten incluso la desinfeccin por inactivacin de bacterias y
virus. \par\pard\qj \li1702\ri928\sb186\sl-295\slmult0\fi566 \up0 \expndtw0\cha
rscalex104 Las TAOs [2-6] se basan en procesos fisicoqumicos capaces de producir
cambios \line \up0 \expndtw0\charscalex106 profundos en la estructura qumica de l
os contaminantes. El concepto fue inicialmente \line \up0 \expndtw-1\charscalex1
00 establecido por Glaze y colaboradores [3, 7-8], quienes definieron los PAOs c
omo procesos \line \up0 \expndtw0\charscalex104 que involucran la generacin y uso
de especies transitorias poderosas, principalmente el \line \up0 \expndtw-3\cha
rscalex100 radical hidroxilo (HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf
2\f3\fs24 ). Este radical puede ser generado por medios fotoqumicos (incluida la
\line \up0 \expndtw-2\charscalex100 luz solar) o por otras formas de energa, y po
see alta efectividad para la oxidacin de materia \line \up0 \expndtw0\charscalex1
03 orgnica. Algunas TAOs, como la fotocatlisis heterognea, la radilisis y otras tcnic
as \line \up0 \expndtw-3\charscalex100 avanzadas, recurren adems a reductores qumi
cos que permiten realizar transformaciones en \line \up0 \expndtw-2\charscalex10
0 contaminantes txicos poco susceptibles a la oxidacin, como iones metlicos o compu
estos \line \up0 \expndtw-3\charscalex100 halogenados. \par\pard\qj \li1702\ri93
5\sb181\sl-300\slmult0\fi566 \up0 \expndtw0\charscalex103 El cuadro que sigue
da un listado de las TAOs, clasificadas en procesos no \up0 \expndtw0
\charscalex103 fotoqumicos y procesos fotoqumicos.
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}}\par\pard\sect\sectd\fs24\paperw11900\paperh16840\pard\sb0\sl-240{\bkmkstart P
g2}{\bkmkend Pg2}\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb0\sl-230\
slmult0\par\pard\li1133\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expndtw-2\charscale
x100 \ul0\nosupersub\cf4\f5\fs20 4\tab \up0 \expndtw-2\charscalex100 Domnech, Jar
dim y Litter\par\pard\li1493\sb0\sl-230\slmult0\par\pard\li1493\sb0\sl-230\slmul
t0\par\pard\li1493\sb0\sl-230\slmult0\par\pard\li1493\sb87\sl-230\slmult0\fi2035
\up0 \expndtw0\charscalex102 Cuadro I: Las Tecnologas avanzadas de oxidacin.\par\
pard\li1493\sb10\sl-230\slmult0\fi993\tx7227 \up0 \expndtw0\charscalex102 Proces
os no fotoqumicos\tab \up0 \expndtw0\charscalex102 Procesos fotoqumicos\par\pard\l
i1493\sb71\sl-230\slmult0\fi0\tx6101 \up0 \expndtw0\charscalex102 \u8226? Ozon
izacin en medio alcalino (O\ul0\sub\cf5\f6\fs19 3\ul0\nosupersub\cf4\f5\fs20 /OH\
ul0\super\cf5\f6\fs19 -\ul0\nosupersub\cf4\f5\fs20 )\tab \up0 \expndtw0\charscal
ex102 \u8226? Oxidacin en agua sub/y supercrtica\par\pard\li1493\sb72\sl-230\slm
ult0\fi0\tx6101 \up0 \expndtw0\charscalex102 \u8226? Ozonizacin con perxido de h
idrgeno\tab \up0 \expndtw0\charscalex102 \u8226? Procesos fotoqumicos\par\pard\l
i1493\sb0\sl-230\slmult0\fi360 \up0 \expndtw0\charscalex102 (O\ul0\sub\cf5\f6\fs
19 3\ul0\nosupersub\cf4\f5\fs20 /H\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\f
s20 O\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 )\par\pard\li1493\sb0\sl180\slmult0\fi4607 \up0 \expndtw0\charscalex102 \u8226? Fotlisis del agua en el
ultravioleta de vaco\par\pard\sect\sectd\sbknone\cols2\colno1\colw5941\colsr160\
colno2\colw5659\colsr160\ql \li1493\sb0\sl-180\slmult0 \up0 \expndtw0\charscalex

101 \u8226? Procesos Fenton (Fe\ul0\super\cf5\f6\fs19 2+\ul0\nosupersub\cf4\f5
\fs20 /H\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 O\ul0\sub\cf5\f6\fs19
2\ul0\nosupersub\cf4\f5\fs20 ) y relacionados\par\pard\ql \li1493\sb21\sl-230\sl
mult0 \up0 \expndtw0\charscalex103 \u8226? Oxidacin electroqumica\par\pard\qj \l
i1493\ri937\sb79\sl-228\slmult0\tx1853 \up0 \expndtw0\charscalex101 \u8226? Ra
dilisis \u947? y tratamiento con haces de \line\tab \up0 \expndtw-2\charscalex100
electrones\par\pard\ql \li1493\sb76\sl-230\slmult0 \up0 \expndtw0\charscalex105
\u8226? Plasma no trmico\par\pard\ql \li1493\sb72\sl-230\slmult0 \up0 \expndtw
0\charscalex101 \u8226? Descarga electrohidrulica - Ultrasonido\par\pard\column
\ql \li380\sb0\sl-180\slmult0 \up0 \expndtw-2\charscalex100 (UVV)\par\pard\qj \
li20\ri3085\sb0\sl-304\slmult0 \up0 \expndtw0\charscalex103 \u8226? UV/perxido
de hidrgeno \up0 \expndtw0\charscalex115 \u8226? UV/O\ul0\sub\cf5\f6\fs19 3\par
\pard\qj \li20\ri3060\sb0\sl-304\slmult0 \up0 \expndtw0\charscalex103 \ul0\nosup
ersub\cf4\f5\fs20 \u8226? Foto-Fenton y relacionadas \line \up0 \expndtw0\char
scalex103 \u8226? Fotocatlisis heterognea \par\pard\sect\sectd\sbknone \qj \li11
33\ri1500\sb256\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex107 \ul0\nosupersu
b\cf2\f3\fs24 Existen otras tecnologas que pueden incluirse tambin entre las TAOs,
como el \up0 \expndtw0\charscalex102 tratamiento con barreras permeables reacti
vas de Fe metlico (Fe cerovalente) [9-10] y la \up0 \expndtw0\charscalex100 oxida
cin con K\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 FeO\ul0\sub\cf3\f4\fs2
4 4\ul0\nosupersub\cf2\f3\fs24 (Fe(VI)) [11]. Sin embargo, en este captulo nos r
eferiremos slo a \up0 \expndtw-5\charscalex100 aquellas tecnologas que involucran
principalmente al radical HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3
\fs24 . \par\pard\qj \li1133\ri1499\sb120\sl-280\slmult0\fi566 \up0 \expndtw-1\c
harscalex100 El siguiente cuadro resume las ventajas de estas nuevas tecnologas s
obre los mtodos \up0 \expndtw-3\charscalex100 convencionales. \par\pard\ql \li302
0\sb0\sl-230\slmult0 \par\pard\ql\li3020\sb32\sl-230\slmult0 \up0 \expndtw-1\cha
rscalex100 \ul0\nosupersub\cf4\f5\fs20 Cuadro II: Ventajas de las Tecnologas avan
zadas de oxidacin. \par\pard\qj \li1491\ri1841\sb62\sl-240\slmult0\tx1846 \up0 \e
xpndtw-2\charscalex100 \u8226? No slo cambian de fase al contaminante (como ocu
rre en el arrastre con aire o en el tratamiento con \line\tab \up0 \expndtw-2\ch
arscalex100 carbn activado), sino que lo transforman qumicamente. \par\pard\ql \li
1491\ri1675\sb69\sl-230\slmult0\tx1846\tx1846 \up0 \expndtw-2\charscalex100 \u82
26? Generalmente se consigue la mineralizacin completa (destruccin) del contamin
ante. En cambio, las \line\tab \up0 \expndtw-2\charscalex100 tecnologas convencio
nales, que no emplean especies muy fuertemente oxidantes, no alcanzan a oxidar \
line \tab \up0 \expndtw-2\charscalex100 completamente la materia orgnica. \par\pa
rd\ql \li1491\sb70\sl-230\slmult0 \up0 \expndtw-2\charscalex100 \u8226? Usualm
ente no generan barros que a vez requieren de un proceso de tratamiento y/o disp
osicin. \par\pard\qj \li1491\ri2732\sb62\sl-240\slmult0\tx1846 \up0 \expndtw-2\ch
arscalex100 \u8226? Son muy tiles para contaminantes refractarios que resisten
otros mtodos de tratamiento, \line\tab \up0 \expndtw-4\charscalex100 principalmen
te el biolgico. \par\pard\ql \li1491\sb69\sl-230\slmult0 \up0 \expndtw-1\charscal
ex100 \u8226? Sirven para tratar contaminantes a muy baja concentracin (por eje
mplo, ppb). \par\pard\ql \li1491\sb70\sl-230\slmult0 \up0 \expndtw-1\charscalex1
00 \u8226? No se forman subproductos de reaccin, o se forman en baja concentrac
in. \par\pard\qj \li1491\ri1735\sb99\sl-220\slmult0\tx1846 \up0 \expndtw-2\charsc
alex100 \u8226? Son ideales para disminuir la concentracin de compuestos formad
os por pretratamientos alternativos, \line\tab \up0 \expndtw-4\charscalex100 com
o la desinfeccin. \par\pard\ql \li1491\sb72\sl-230\slmult0 \up0 \expndtw-1\charsc
alex100 \u8226? Generalmente, mejoran las propiedades organolpticas del agua tr
atada. \par\pard\ql \li1491\sb90\sl-230\slmult0 \up0 \expndtw-2\charscalex100 \u
8226? En muchos casos, consumen mucha menos energa que otros mtodos (por ejemplo
, la incineracin). \par\pard\qj \li1491\ri2330\sb79\sl-220\slmult0\tx1846 \up0 \e
xpndtw-2\charscalex100 \u8226? Permiten transformar contaminantes refractarios
en productos tratables luego por mtodos ms \line\tab \up0 \expndtw-4\charscalex10
0 econmicos como el tratamiento biolgico. \par\pard\ql \li1491\sb92\sl-230\slmult0
\up0 \expndtw-2\charscalex100 \u8226? Eliminan efectos sobre la salud de desi
nfectantes y oxidantes residuales como el cloro. \par\pard\qj \li1133\sb0\sl-273
\slmult0 \par\pard\qj\li1133\ri1501\sb22\sl-273\slmult0\fi566 \up0 \expndtw0\cha

rscalex106 \ul0\nosupersub\cf2\f3\fs24 Las TAOs son especialmente tiles como pret
ratamiento antes de un tratamiento \line \up0 \expndtw0\charscalex105 biolgico p
ara contaminantes resistentes a la biodegradacin o como proceso de \line
\up0 \expndtw0\charscalex107 postratamiento para efectuar un pulido de las agua
s antes de la descarga a los cuerpos \line \up0 \expndtw-5\charscalex100 recepto
res [12]. \par\pard\qj \li1133\ri1500\sb119\sl-283\slmult0\fi566 \up0 \expndtw0\
charscalex100 Cul es la explicacin de la eficiencia de estas tcnicas? Los procesos i
nvolucrados \line \up0 \expndtw0\charscalex105 poseen una mayor factibilidad
termodinmica y una velocidad de oxidacin muy \line \up0 \expndtw-2\charscal
ex100 incrementada por la participacin de radicales, principalmente el radical hi
droxilo, HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 . Esta \lin
e \up0 \expndtw0\charscalex106 especie posee propiedades adecuadas para atacar v
irtualmente a todos los compuestos \line \up0 \expndtw-1\charscalex100 orgnicos y
reaccionar 10\ul0\super\cf3\f4\fs24 6\ul0\nosupersub\cf2\f3\fs24 -10\ul0\super\
cf3\f4\fs24 12\ul0\nosupersub\cf2\f3\fs24 veces ms rpido que oxidantes alternativ
os como el O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 . La \line \up0 \e
xpndtw-2\charscalex100 Tabla I, que presenta potenciales de oxidacin de distintas
especies, muestra que despus del \line \up0 \expndtw-2\charscalex100 flor, el HO\
ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 es el oxidante ms enrgic
o. En la Tabla II se puede observar la gran diferencia
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g3}{\bkmkend Pg3}\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb0\sl-230\
slmult0\par\pard\li1702\sb19\sl-230\slmult0\fi0\tx10601 \up0 \expndtw-1\charscal
ex100 \ul0\nosupersub\cf4\f5\fs20 Procesos avanzados de oxidacin para la eliminac
in de contaminantes\tab \up0 \expndtw-1\charscalex100 5\par\pard\li1702\sb0\sl-27
6\slmult0\par\pard\li1702\sb0\sl-276\slmult0\par\pard\li1702\sb206\sl-276\slmult
0\fi0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf2\f3\fs24 en las constante
s de velocidad de reaccin de distintos compuestos con el radical hidroxilo y\par\
pard\li1702\sb0\sl-276\slmult0\fi0 \up0 \expndtw-1\charscalex100 con el ozono. D
e todos modos, debemos destacar que, para ser eficientes, las TAOs deben\par\par
d\li1702\sb0\sl-276\slmult0\fi0 \up0 \expndtw-1\charscalex100 generar altas conc
entraciones de radicales hidroxilo en estado estacionario.\par\pard\li1702\sb0\s
l-276\slmult0\par\pard\li1702\sb17\sl-276\slmult0\fi3064\tx7128 \up0 \expndtw-2\
charscalex100 Especie\tab \dn3 \expndtw-2\charscalex100 E\ul0\super\cf3\f4\fs24
0\ul0\nosupersub\cf2\f3\fs24 (V, 25C)\ul0\super\cf3\f4\fs24 1\par\pard\li1702\s
b41\sl-276\slmult0\fi1946\tx7596 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\c
f2\f3\fs24 Flor\tab \up0 \expndtw-2\charscalex100 3,03\par\pard\li1702\sb9\sl-276
\slmult0\fi1946\tx7596 \up0 \expndtw-2\charscalex100 Radical hidroxilo\tab \up0
\expndtw-2\charscalex100 2,80\par\pard\li1702\sb10\sl-276\slmult0\fi1946\tx7596
\up0 \expndtw-2\charscalex100 Oxgeno atmico\tab \up0 \expndtw-2\charscalex100 2,42
\par\pard\li1702\sb9\sl-276\slmult0\fi1946\tx7596 \up0 \expndtw-2\charscalex100
Ozono\tab \up0 \expndtw-2\charscalex100 2,07\par\pard\li1702\sb10\sl-276\slmult0
\fi1946\tx7596 \up0 \expndtw-2\charscalex100 Perxido de hidrgeno\tab \up0 \expndtw
-2\charscalex100 1,78\par\pard\li1702\sb12\sl-276\slmult0\fi1946\tx7596 \up0 \ex
pndtw-2\charscalex100 Radical perhidroxilo\tab \up0 \expndtw-2\charscalex100 1,7
0\par\pard\li1702\sb10\sl-276\slmult0\fi1946\tx7596 \up0 \expndtw-2\charscalex10
0 Permanganato\tab \up0 \expndtw-2\charscalex100 1,68\par\pard\li1702\sb9\sl-276
\slmult0\fi1946\tx7596 \up0 \expndtw-2\charscalex100 Dixido de cloro\tab \up0 \ex
pndtw-2\charscalex100 1,57\par\pard\li1702\sb10\sl-276\slmult0\fi1946\tx7596 \up
0 \expndtw-2\charscalex100 cido hipocloroso\tab \up0 \expndtw-2\charscalex100 1,4
9\par\pard\li1702\sb9\sl-276\slmult0\fi1946\tx7596 \up0 \expndtw-2\charscalex100
Cloro\tab \up0 \expndtw-2\charscalex100 1,36\par\pard\li1702\sb10\sl-276\slmult
0\fi1946\tx7596 \up0 \expndtw-2\charscalex100 Bromo\tab \up0 \expndtw-2\charscal
ex100 1,09\par\pard\li1702\sb10\sl-276\slmult0\fi1946\tx7596 \up0 \expndtw-2\cha
rscalex100 Yodo\tab \up0 \expndtw-2\charscalex100 0,54\par\pard\li1702\sb137\sl230\slmult0\fi0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Tabla
I. Potenciales redox de algunos agentes oxidantes [2].\par\pard\li1702\sb0\sl-27
6\slmult0\par\pard\li1702\sb12\sl-276\slmult0\fi2330\tx6334\tx8076 \up0 \expndtw
-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 Compuesto\tab \dn2 \expndtw-2\chars
calex100 HO\ul0\super\cf3\f4\fs24 \u8226?\tab \up0 \expndtw-1\charscalex100 \ul0
\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 3\par\pard\li1702\sb41\sl-276\slmu
lt0\fi1931\tx6149\tx7815 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs
24 Alquenos clorados\tab \up0 \expndtw-2\charscalex100 10\ul0\super\cf3\f4\fs24
9\ul0\nosupersub\cf2\f3\fs24 -10\ul0\super\cf3\f4\fs24 11\tab \up0 \expndtw-2\ch
arscalex100 \ul0\nosupersub\cf2\f3\fs24 10\ul0\super\cf3\f4\fs24 -1\ul0\nosupers
ub\cf2\f3\fs24 -10\ul0\super\cf3\f4\fs24 3\par\pard\li1702\sb9\sl-276\slmult0\fi
1931\tx6149\tx8043 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 Fen
oles\tab \up0 \expndtw-2\charscalex100 10\ul0\super\cf3\f4\fs24 9\ul0\nosupersub
\cf2\f3\fs24 -10\ul0\super\cf3\f4\fs24 10\tab \up0 \expndtw-2\charscalex100 \ul0
\nosupersub\cf2\f3\fs24 10\ul0\super\cf3\f4\fs24 3\par\pard\li1702\sb10\sl-276\s
lmult0\fi1931\tx6149\tx7942 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3
\fs24 Aromticos\tab \up0 \expndtw-2\charscalex100 10\ul0\super\cf3\f4\fs24 8\ul0\
nosupersub\cf2\f3\fs24 -10\ul0\super\cf3\f4\fs24 10\tab \up0 \expndtw-2\charscal

ex100 \ul0\nosupersub\cf2\f3\fs24 1-10\ul0\super\cf3\f4\fs24 2\par\pard\li1702\s
b9\sl-276\slmult0\fi1931\tx6149\tx8144 \up0 \expndtw-2\charscalex100 \ul0\nosupe
rsub\cf2\f3\fs24 Cetonas\tab \up0 \expndtw-2\charscalex100 10\ul0\super\cf3\f4\f
s24 9\ul0\nosupersub\cf2\f3\fs24 -10\ul0\super\cf3\f4\fs24 10\tab \up0 \expndtw2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 1\par\pard\li1702\sb10\sl-276\slmult
0\fi1931\tx6190\tx7915 \up0 \expndtw-2\charscalex100 Alcoholes\tab \up0 \expndtw
-2\charscalex100 10\ul0\super\cf3\f4\fs24 8\ul0\nosupersub\cf2\f3\fs24 -10\ul0\s
uper\cf3\f4\fs24 9\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24
10\ul0\super\cf3\f4\fs24 -2\ul0\nosupersub\cf2\f3\fs24 -1\par\pard\li1702\sb10\
sl-276\slmult0\fi1931\tx6190\tx8016 \up0 \expndtw-2\charscalex100 Alcanos\tab \u
p0 \expndtw-2\charscalex100 10\ul0\super\cf3\f4\fs24 6\ul0\nosupersub\cf2\f3\fs2
4 -10\ul0\super\cf3\f4\fs24 9\tab \up0 \expndtw-1\charscalex100 \ul0\nosupersub\
cf2\f3\fs24 10\ul0\super\cf3\f4\fs24 -2\par\pard\qj \li1702\ri966\sb138\sl-220\s
lmult0\fi0 \up0 \expndtw0\charscalex103 \ul0\nosupersub\cf4\f5\fs20 Tabla II. Co
nstantes de velocidad (k en L mol\ul0\super\cf5\f6\fs19 -1\ul0\nosupersub\cf4\f5
\fs20 s\ul0\super\cf5\f6\fs19 -1\ul0\nosupersub\cf4\f5\fs20 ) del radical hidro
xilo en comparacin con el ozono para \up0 \expndtw0\charscalex103 algunos compues
tos orgnicos [5]. \par\pard\qj \li1702\ri925\sb237\sl-273\slmult0\fi566 \up0 \exp
ndtw0\charscalex100 \ul0\nosupersub\cf2\f3\fs24 Las TAOs tienen actualmente un g
rado de desarrollo y comercializacin variado, en \up0 \expndtw0\charscalex104 con
stante cambio a medida que se avanza cientfica y tecnolgicamente en el tema. Las \
up0 \expndtw0\charscalex100 tcnicas de ozonizacin en medio alcalino, UV/H\ul0\sub\
cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\
cf2\f3\fs24 , UV/O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 , UV/H\ul0\s
ub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupers
ub\cf2\f3\fs24 /O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 , UV/Fenton y
\up0 \expndtw0\charscalex100 UV/TiO\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3
\fs24 estn total o parcialmente comercializadas. \par\pard\ql \li1702\sb0\sl-276
\slmult0 \par\pard\ql\li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb13\sl-276\
slmult0 \up0 \expndtw-1\charscalex100 2. TECNOLOGAS AVANZADAS DE OXIDACIN NO FOTOQ
UMICAS \par\pard\qj \li1702\ri924\sb261\sl-280\slmult0\fi566 \up0 \expndtw-2\char
scalex100 Estas TAOs originan especies reactivas potentes, principalmente el rad
ical hidroxilo, a \up0 \expndtw-3\charscalex100 travs de la transformacin de espec
ies qumicas o mediante la utilizacin de distintas formas \up0 \expndtw-4\charscale
x100 de energa, con excepcin de la irradiacin luminosa. \par\pard\ql \li1702\sb0\sl
-276\slmult0 \par\pard\ql\li1702\sb8\sl-276\slmult0 \up0 \expndtw-1\charscalex10
0 2.1. Ozonizacin en medio alcalino \par\pard\qj \li1702\ri919\sb261\sl-280\slmul
t0\fi566 \up0 \expndtw0\charscalex100 El ozono puede reaccionar en forma directa
con un sustrato orgnico a travs de una \up0 \expndtw0\charscalex100 reaccin lenta
y selectiva, ecuacin (1), o de una reaccin radicalaria favorecida en medio \up0 \e
xpndtw0\charscalex100 alcalino (rpida y no selectiva), ecuacin (2) [3, 8, 13-14]:
\par\pard\ql \li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \
par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb32\sl-230\slmult0 \u
p0 \expndtw-3\charscalex100 \ul0\super\cf5\f6\fs20\ul0\super\cf5\f6\fs19 1\ul0\n
osupersub\cf4\f5\fs20 Los potenciales dados en este captulo estn referidos al ele
ctrodo normal de hidrgeno.
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14500145145001451450014514500145145001451450014514500145145001451450014514500145
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304b7326a1aac2e15628e5923ed3f62cf835a97ecebfb1e7ecadf00b5b4b78f5df82ff00b3afc17f
85be20169726eed9fc43e05f875e1df0d6bf34177d6ea39f58d3af675b918f3c49e68003003e26f0
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40051451400514514005145140051451400514514005145140051451400514514005145140051451
40051451400514514005145140051451400514514005145140051451400514514005145140051451
400514514005145140051451400514514005145140051451401e21fb4afc00f017ed55fb3ffc62fd
9c3e2841793f807e35fc3df137c3bf139d36e1ad353b4d3fc49a6cf62354d2ae5788355d1ee64835
5d3249165816fecedcdc413c1e64327e7de83fb1efed55e30f8b9f03be2f7edd5fb4b7c1af13f817
f62ad17e2b6b1f09aefe04fc36f15fc1ef12f8dfc6be39f843affc16d57e3bfc71d77c51f103c61a
3785759f0c7c2df1378eeeb4cf077c33b5d33c37a678c7c5975e293af1b1f0e683a25bfeb9d3248e
39a378a544962951a39239143c7246ea55d244605591d495656055812a41071401fcd3ff00c11935
5fd8d3e2d7ed4bfb467c5bfd8b3e2cf806dfe03c9f00fc0bf04fc39f028fc703f12be3a7c789be1b
7c44f16a78cbf6ebfda43e1eeafe25d6bc51e12d63e206abad5a7c3ef02eb1f1034eb4f89be37f0d
5aea1e31f1fdbe936be2bf07e896dfd03fc30f819f05fe09b78d1be0e7c27f873f0abfe16378ae6f
1df8f93e1df833c3fe0d87c63e34b9d3ac349baf15f88e0f0f69fa7c3ab7886eb4ed2f4fb4bad5af
2396fae63b58bcf9a46058f5da1782fc1de179669fc33e13f0cf8767b88843713685a0e97a44b3c2
acaeb0cd269f6b6ef2c4acaac2372c81954819008e9a800a28a2800a28a2800a28a2800a28a2800a
28a28010107a1cf247e20e08fc0d2fafd7dffcfe5c5145002773f876faf7efd3f0e3d694e7b1c7bf
8a28a0028a28a0028a28a0028a28a0028a28a0028a28a0028a28a00fffd9}}}}}\pard\sb0\sl-24
0{\bkmkstart Pg4}{\bkmkend Pg4}\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li11
33\sb0\sl-230\slmult0\par\pard\li1133\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expnd
tw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs20 6\tab \up0 \expndtw-2\charscalex1
00 Domnech, Jardim y Litter\par\pard\li1133\sb0\sl-276\slmult0\par\pard\li1133\sb
0\sl-276\slmult0\par\pard\li1133\sb228\sl-276\slmult0\fi0\tx5093\tx5460\tx9893 \
up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 3
\ul0\nosupersub\cf2\f3\fs24 + S \u8594? S\ul0\sub\cf3\f4\fs24 ox\tab \up0 \
expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 ; k\tab \up0 \expndtw-3\char
scalex100 \u8776? 1-100 M\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\fs24 s
\ul0\super\cf3\f4\fs24 -1\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\
f3\fs24 (1)\par\pard\ql \li2393\sb125\sl-207\slmult0 \up0 \expndtw-4\charscalex1
00 \ul0\nosupersub\cf4\f5\fs20 HO\ul0\super\cf5\f6\fs19 -\par\pard\li1133\sb156\
sl-276\slmult0\fi0\tx3447\tx4256\tx9893 \dn2 \expndtw-2\charscalex100 \ul0\nosup
ersub\cf2\f3\fs24 2 O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 + H\ul0
\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O \u8594? 2 HO\ul0\super\cf3\f4\fs
24 \u8226?\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 + 2 O\u
l0\sub\cf3\f4\fs24 2\tab \dn2 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs
24 + HO\ul0\sub\cf3\f4\fs24 2\u8226? \ul0\nosupersub\cf2\f3\fs24 ; k \u8776? 1
0\ul0\super\cf3\f4\fs24 8\ul0\nosupersub\cf2\f3\fs24 -10\ul0\super\cf3\f4\fs24 1
0\ul0\nosupersub\cf2\f3\fs24 M\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\f
s24 s\ul0\super\cf3\f4\fs24 -1\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersu
b\cf2\f3\fs24 (2)\par\pard\qj \li1133\ri1498\sb164\sl-277\slmult0\fi566 \up0 \ex
pndtw-4\charscalex100 Las constantes de velocidad con compuestos orgnicos difiere
n mucho para ambos tipos \line \up0 \expndtw-3\charscalex100 de procesos, tal co
mo se ha mostrado en la Tabla II. La primera reaccin es de importancia en \line \
up0 \expndtw-1\charscalex100 medios cidos y para solutos que reaccionan muy rpido
con el ozono; ejemplos de ello son \line \up0 \expndtw0\charscalex100 los compue
stos orgnicos no saturados, con grupos cromofricos o con grupos aminos. La \line \
up0 \expndtw0\charscalex102 segunda reaccin puede iniciarse de distintos modos, c
on especies tales como HO\ul0\super\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 , H
O\ul0\sub\cf3\f4\fs24 2-\ul0\nosupersub\cf2\f3\fs24 , \line \up0 \expndtw-4\char
scalex100 HCOO\ul0\super\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 , Fe\ul0\super
\cf3\f4\fs24 2+\ul0\nosupersub\cf2\f3\fs24 o sustancias hmicas. Por lo tanto, en
principio, la ozonizacin es sensiblemente \line \up0 \expndtw-4\charscalex100 ms
eficiente en medios alcalinos. La Figura 1 muestra un esquema de las principales
especies \line \up0 \expndtw-4\charscalex100 de la descomposicin de ozono en agu
a pura iniciada por iones hidrxido [8]. \par\pard\qj \li1133\sb0\sl-240\slmult0 \
par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \pa
r\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\
pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pa
rd\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard
\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\q
j\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\
li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li
1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li11
\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\r
i1536\sb154\sl-240\slmult0 \up0 \expndtw0\charscalex100 \ul0\nosupersub\cf4\f5\f
s20 Figura 1. Esquema de las principales especies de la descomposicin de ozono en
agua pura iniciada por iones \up0 \expndtw-1\charscalex100 hidrxido [8]. \par\pa
rd\qj \li1133\ri1499\sb267\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex103 \ul
0\nosupersub\cf2\f3\fs24 Este camino indirecto es menos selectivo, ya que las es
pecies formadas tienen gran \line \up0 \expndtw-2\charscalex100 capacidad oxidan
te. Existen sin embargo compuestos refractarios, como los cidos actico y \line \up
0 \expndtw-3\charscalex100 oxlico, productos de oxidacin intermedia en ozonizacin y

otros procesos de hidroxilacin, \line \up0 \expndtw0\charscalex108 que resisten
la mineralizacin. La materia orgnica reaccionar, por lo tanto, por una \line \up0 \
expndtw-3\charscalex100 combinacin de ambas reacciones, dependiendo de la composi
cin del agua tratada, del pH y \line \up0 \expndtw0\charscalex102 de la dosis de
ozono. Debe tenerse cuidado de no elevar excesivamente el pH, debido a la \line
\up0 \expndtw-3\charscalex100 accin atrapadora de HO\ul0\super\cf3\f4\fs24 \u8226
?\ul0\nosupersub\cf2\f3\fs24 competitiva de los iones bicarbonato y carbonato (
esta competencia \line \up0 \expndtw-3\charscalex100 ocurrir en toda TOA cada vez
que se formen HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 en s
oluciones carbonatadas): \par\pard\li1133\sb211\sl-276\slmult0\fi0\tx2748\tx9895
\up0 \expndtw-4\charscalex100 HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\c
f2\f3\fs24 + HCO\ul0\sub\cf3\f4\fs24 3-\tab \up0 \expndtw-4\charscalex100 \ul
0\nosupersub\cf2\f3\fs24 \u8594?
CO\ul0\sub\cf3\f4\fs24 3\u8226?\tab \up0 \ex
pndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (3)\par\pard\li1133\sb199\sl-2
76\slmult0\fi0\tx2657\tx9895 \up0 \expndtw-4\charscalex100 HO\ul0\super\cf3\f4\f
s24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + CO\ul0\sub\cf3\f4\fs24 32-\tab \up0
\expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
CO\ul0\sub\cf3\f
4\fs24 3\u8226?-\ul0\nosupersub\cf2\f3\fs24 + HO\tab \up0 \expndtw-4\charscal
ex100 (4)\par\pard\qj \li1133\ri1502\sb159\sl-280\slmult0\fi566 \up0 \expndtw-1\
charscalex100 El ozono es un poderoso oxidante y eficiente bactericida, aplicado
exitosamente desde \line \up0 \expndtw0\charscalex100 hace mucho tiempo como de
sinfectante de aguas potables. Su uso ha permitido un notable \line \up0 \expndt
w-3\charscalex100 mejoramiento del gusto, color, caractersticas de filtracin y bio
degradabilidad de las mismas. \line \up0 \expndtw-3\charscalex100 Se ha empleado
con xito en la decoloracin de caoln y de pulpa de celulosa y, en general, \par\par
d\sect\sectd\fs24\paperw11900\paperh16840\pard\sb0\sl-240{\bkmkstart Pg5}{\bkmke
nd Pg5}\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb0\sl-230\slmult0\pa
r\pard\li1702\sb19\sl-230\slmult0\fi0\tx10601 \up0 \expndtw-1\charscalex100 \ul0
\nosupersub\cf4\f5\fs20 Procesos avanzados de oxidacin para la eliminacin de conta
minantes\tab \up0 \expndtw-1\charscalex100 7\par\pard\qj \li1702\sb0\sl-276\slmu
lt0 \par\pard\qj\li1702\sb0\sl-276\slmult0 \par\pard\qj\li1702\ri919\sb191\sl-27
6\slmult0 \up0 \expndtw0\charscalex104 \ul0\nosupersub\cf2\f3\fs24 como tratami
ento de efluentes acuosos extremadamente contaminados. El ozono se \line
\up0 \expndtw0\charscalex112 transforma slo en O\ul0\sub\cf3\f4\fs24 2\ul0\nosup
ersub\cf2\f3\fs24 y H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O, y el
mtodo no es tan txico como otros tratamientos \line \up0 \expndtw0\charscalex100 c
onvencionales que usan Cl\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 o cid
o crmico. Como los compuestos orgnicos tratados con \line \up0 \expndtw0\charscale
x103 este reactivo producen aldehdos, cetonas o cidos carboxlicos, la ozonizacin es
un buen \line \up0 \expndtw0\charscalex104 pretratamiento para procesos biolgicos
, y verstil para tcnicas combinadas. No produce \line \up0 \expndtw-2\charscalex10
0 trihalometanos (THM) u otros compuestos clorados, uno de los principales probl
emas de otros \line \up0 \expndtw0\charscalex100 tratamientos como la cloracin o
el xido de cloro. El ozono puede producirse fcilmente in \line \up0 \expndtw0\char
scalex106 situ por descarga elctrica en corriente de aire, y no deja olores ni gu
stos residuales. En \line \up0 \expndtw0\charscalex108 contraposicin con los bene
ficios anteriores y desde el punto de vista operacional y de \line \up0 \expndtw
-2\charscalex100 ingeniera, el uso de ozono no es trivial como el uso de un oxida
nte totalmente miscible con el \line \up0 \expndtw0\charscalex102 agua, como el
perxido de hidrgeno, puesto que involucra procesos de transferencia de la \line \u
p0 \expndtw0\charscalex100 molcula gaseosa a la fase acuosa, existiendo entonces
limitaciones de transferencia de masa \line \up0 \expndtw0\charscalex100 [15]. P
or ello, el proceso requiere eficiente agitacin, haciendo necesario el uso de dif
usores, \line \up0 \expndtw0\charscalex107 mezcladores en lnea, venturis y torres
de contacto. Este aspecto agrega altos costos de \line \up0 \expndtw-1\charscal
ex100 inversin a su utilizacin. Para la destruccin completa de un compuesto se nece
sita, adems, \line \up0 \expndtw0\charscalex102 una relacin molar bastante alta de
O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 a contaminante (mayor que 5
:1), con el consiguiente \line \up0 \expndtw0\charscalex103 aumento de costos.
Como hemos dicho, en algunos casos el mtodo no conduce a \line \up0 \

expndtw-2\charscalex100 mineralizacin completa. No permite trabajar a temperatura
s muy altas, ya que el burbujeo del \line \up0 \expndtw-1\charscalex100 gas pued
e volatilizar compuestos iniciales o intermedios. El tratamiento no tiene propie
dades \line \up0 \expndtw-1\charscalex100 de desinfeccin residuales. Como las agu
as tratadas no deben contener ozono residual, deben \line \up0 \expndtw-1\charsc
alex100 introducirse desgasadores finales en el circuito, aumentando ms an el cost
o del proceso. \par\pard\ql \li1702\sb0\sl-264\slmult0 \par\pard\ql\li1702\sb30\
sl-264\slmult0 \up0 \expndtw0\charscalex100 2.2. Ozono/H\ul0\sub\cf3\f4\fs24 2\u
l0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2 \par\pard\qj \li1702\ri933\sb2
63\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex103 \ul0\nosupersub\cf2\f3\fs24
La ozonizacin transforma los contaminantes en compuestos ms simples, ms \
up0 \expndtw0\charscalex100 refractarios al reactivo. Se logra una mejora agregan
do agua oxigenada [16]. El H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\
ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 es un \up0 \expndtw0\charscale
x100 cido dbil, un poderoso oxidante y un compuesto inestable, que dismuta con una
velocidad \up0 \expndtw0\charscalex100 mxima al pH de su pK\ul0\sub\cf3\f4\fs24
a\ul0\nosupersub\cf2\f3\fs24 : \par\pard\li1702\sb204\sl-276\slmult0\fi0\tx2391\
tx5662\tx10462 \up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosuper
sub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-4\charscalex100 \ul0\n
osupersub\cf2\f3\fs24 \u8594?
HO\ul0\sub\cf3\f4\fs24 2-\ul0\nosupersub\cf2\f3
\fs24 + H\ul0\super\cf3\f4\fs24 +\tab \up0 \expndtw-4\charscalex100 \ul0\nosu
persub\cf2\f3\fs24 ; pK\ul0\sub\cf3\f4\fs24 a\ul0\nosupersub\cf2\f3\fs24 =11,6\
tab \up0 \expndtw-4\charscalex100 (5)\par\pard\li1702\sb141\sl-276\slmult0\fi0\t
x5662\tx10462 \up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosupers
ub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + 2e\ul0\supe
r\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 + 2H\ul0\super\cf3\f4\fs24 +\ul0\nos
upersub\cf2\f3\fs24 \u8594? 2 H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\f
s24 O\tab \up0 \expndtw-4\charscalex100 ; E\ul0\super\cf3\f4\fs24 o\ul0\nosupers
ub\cf2\f3\fs24 = +1,78 V\tab \up0 \expndtw-4\charscalex100 (6)\par\pard\li1702\
sb197\sl-276\slmult0\fi0\tx10464 \up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\
fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\
fs24 + HO\ul0\sub\cf3\f4\fs24 2-\ul0\nosupersub\cf2\f3\fs24 \u8594? H\ul0\su
b\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O + O\ul0\sub\cf3\f4\fs24 2\ul0\nosu
persub\cf2\f3\fs24 + HO\ul0\super\cf3\f4\fs24 -\tab \up0 \expndtw-4\charscalex1
00 \ul0\nosupersub\cf2\f3\fs24 (7)\par\pard\qj \li1702\ri925\sb174\sl-276\slmult
0\fi566 \up0 \expndtw0\charscalex103 El uso de dos o ms oxidantes combinados perm
ite aprovechar los posibles efectos \line \up0 \expndtw0\charscalex103 sinrgicos
entre ellos, lo que produce una destruccin adicional de la carga orgnica. Sin \lin
e \up0 \expndtw-2\charscalex100 embargo, como existe una gran dosis de empirismo
en el uso de mezclas oxidantes, es difcil \line \up0 \expndtw0\charscalex100 pre
ver el rendimiento, que debe determinarse en ensayos de laboratorio. Entre las p
osibles \line \up0 \expndtw-1\charscalex100 mezclas de agentes oxidantes, la com
binacin perxido de hidrgeno y ozono es sin duda la \line \up0 \expndtw-1\charscalex
100 ms usada. El proceso pretende combinar la oxidacin directa (y selectiva) del o
zono con la \line \up0 \expndtw-1\charscalex100 reaccin rpida y poco selectiva de
los radicales HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 con l
os compuestos orgnicos. \par\pard\qj \li1702\ri914\sb113\sl-290\slmult0\fi566 \up
0 \expndtw-1\charscalex100 El H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 puede iniciar la descomposi
cin de O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 por transferencia de e
lectrones [3]. La \up0 \expndtw0\charscalex102 reaccin genera HO\ul0\super\cf3\f4
\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 consumiendo H\ul0\sub\cf3\f4\fs24 2\ul
0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 y O
\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 , ecuacin (8), a travs de un mec
anismo en \up0 \expndtw0\charscalex102 cadena mostrado en las Ecuaciones (5) y (
9) a (15): \par\pard\li1702\sb201\sl-276\slmult0\fi0\tx3020\tx10462 \up0 \expndt
w-3\charscalex100 O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 + H\ul0\
sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \dn2 \e
xpndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
HO\ul0\super\cf3\f
4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + O\ul0\sub\cf3\f4\fs24 2\ul0\nosup

ersub\cf2\f3\fs24 + HO\ul0\sub\cf3\f4\fs24 2\u8226?\tab \up0 \expndtw-3\chars
calex100 \ul0\nosupersub\cf2\f3\fs24 (8)\par\pard\li1702\sb137\sl-276\slmult0\fi
0\tx2391\tx5662\tx10462 \up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul
0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-3\charscalex1
00 \ul0\nosupersub\cf2\f3\fs24 = HO\ul0\sub\cf3\f4\fs24 2-\ul0\nosupersub\cf2\f
3\fs24 + H\ul0\super\cf3\f4\fs24 +\tab \up0 \expndtw-3\charscalex100 \ul0\nos
upersub\cf2\f3\fs24 ; K\ul0\sub\cf3\f4\fs24 a\ul0\nosupersub\cf2\f3\fs24 = 1,6
10\ul0\super\cf3\f4\fs24 -12\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\c
f2\f3\fs24 (5)\par\pard\li1702\sb139\sl-276\slmult0\fi0\tx2383\tx5662\tx10462 \u
p0 \expndtw-3\charscalex100 HO\ul0\sub\cf3\f4\fs24 2\u8226?\tab \up0 \expndtw-3\
charscalex100 \ul0\nosupersub\cf2\f3\fs24 =
O\ul0\sub\cf3\f4\fs24 2\u8226?-\u
l0\nosupersub\cf2\f3\fs24 + H\ul0\super\cf3\f4\fs24 +\tab \up0 \expndtw-3\cha
rscalex100 \ul0\nosupersub\cf2\f3\fs24 ; K\ul0\sub\cf3\f4\fs24 a\ul0\nosupersub\
cf2\f3\fs24 = 1,6 10\ul0\super\cf3\f4\fs24 -5\tab \up0 \expndtw-3\charscalex10
0 \ul0\nosupersub\cf2\f3\fs24 (9)\par\pard\li1702\sb139\sl-276\slmult0\fi0\tx566
2\tx10342 \up0 \expndtw-3\charscalex100 HO\ul0\sub\cf3\f4\fs24 2-\ul0\nosupersub
\cf2\f3\fs24 + O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 \u8594? O\
ul0\sub\cf3\f4\fs24 3-\ul0\nosupersub\cf2\f3\fs24 + HO\ul0\sub\cf3\f4\fs24 2\u
8226?\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 ; k = 2,8 10
\ul0\super\cf3\f4\fs24 6\ul0\nosupersub\cf2\f3\fs24 M\ul0\super\cf3\f4\fs24 -1\
ul0\nosupersub\cf2\f3\fs24 s\ul0\super\cf3\f4\fs24 -1\tab \up0 \expndtw-3\charsc
alex100 \ul0\nosupersub\cf2\f3\fs24 (10)\par\pard\sect\sectd\fs24\paperw11900\pa
perh16840\pard\sb0\sl-240{\bkmkstart Pg6}{\bkmkend Pg6}\par\pard\sect\sectd\sbkn
one\cols2\colno1\colw4933\colsr160\colno2\colw6667\colsr160\ql \li1133\sb0\sl-23
0\slmult0 \par\pard\ql \li1133\sb220\sl-230\slmult0 \up0 \expndtw-2\charscalex10
0 \ul0\nosupersub\cf4\f5\fs20 8\par\pard\ql \li1133\sb0\sl-276\slmult0 \par\pard
\ql \li1133\sb0\sl-276\slmult0 \par\pard\ql \li1133\sb228\sl-276\slmult0 \up0 \e
xpndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\u8226
?- \ul0\nosupersub\cf2\f3\fs24 + O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\f
s24 \u8594? O\ul0\sub\cf3\f4\fs24 3-\ul0\nosupersub\cf2\f3\fs24 + O\ul0\sub\
cf3\f4\fs24 2\par\pard\ql \li1133\sb135\sl-276\slmult0 \up0 \expndtw-3\charscale
x100 \ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 3-\ul0\nosupersub\cf2\f3\
fs24 + H\ul0\super\cf3\f4\fs24 + \up0 \expndtw-7\charscalex100 \ul0\nosupersub
\cf2\f3\fs24 \u8594?
HO\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 +
O\ul0\sub\cf3\f4\fs24 2\par\pard\ql \li1133\sb141\sl-276\slmult0 \up0 \expndtw2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 HO\ul0\sub\cf3\f4\fs24 3\ul0\nosuper
sub\cf2\f3\fs24 \u8594? HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\
fs24 + O\ul0\sub\cf3\f4\fs24 2\par\pard\ql \li1133\sb137\sl-276\slmult0 \up0 \
expndtw-1\charscalex100 \ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 3\ul0\
nosupersub\cf2\f3\fs24 + HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3
\fs24 \u8594? O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + HO\ul0\sub\
cf3\f4\fs24 2\u8226?\par\pard\ql \li1133\sb139\sl-276\slmult0 \up0 \expndtw-2\ch
arscalex100 \ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\c
f2\f3\fs24 + HO\ul0\sub\cf3\f4\fs24 2\u8226?\ul0\nosupersub\cf2\f3\fs24 \u8594
? 2 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + HO\ul0\super\cf3\f4\fs
24 \u8226?\par\pard\column \ql \li8050\sb0\sl-230\slmult0 \par\pard\ql \li2977\s
b221\sl-230\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Do
mnech, Jardim y Litter\par\pard\ql \li5093\sb0\sl-276\slmult0 \par\pard\ql \li509
3\sb0\sl-276\slmult0 \par\pard\ql \li20\sb227\sl-276\slmult0\tx4705 \up0 \expndt
w-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 ; k = 1,6 10\ul0\super\cf3\f4\fs24
9\ul0\nosupersub\cf2\f3\fs24 M\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\
fs24 s\ul0\super\cf3\f4\fs24 -1\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersu
b\cf2\f3\fs24 (11)\par\pard\ql \li20\sb137\sl-276\slmult0\tx4705 \up0 \expndtw-3
\charscalex100 ; k = 5,2 10\ul0\super\cf3\f4\fs24 10\ul0\nosupersub\cf2\f3\fs24
M\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\fs24 s\ul0\super\cf3\f4\fs24 1\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (12)\par\pard\ql
\li20\sb139\sl-276\slmult0\tx4705 \up0 \expndtw-3\charscalex100 ; k = 1,1 10\ul
0\super\cf3\f4\fs24 5\ul0\nosupersub\cf2\f3\fs24 s\ul0\super\cf3\f4\fs24 -1\tab
\up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (13)\par\pard\ql \li2
0\sb137\sl-276\slmult0\tx4705 \up0 \expndtw-3\charscalex100 ; k = 1,1 10\ul0\sup

er\cf3\f4\fs24 5\ul0\nosupersub\cf2\f3\fs24 s\ul0\super\cf3\f4\fs24 -1\tab \up0
\expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (14)\par\pard\ql \li4700\s
b137\sl-276\slmult0 \up0 \expndtw-3\charscalex100 (15) \par\pard\sect\sectd\sbkn
one \qj \li1133\ri1447\sb169\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex102 E
l proceso es caro pero rpido, y puede tratar contaminantes orgnicos presentes en \
up0 \expndtw-3\charscalex100 muy bajas concentraciones (ppb), a pH entre 7 y 8;
la relacin molar ptima O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 /H\ul0\s
ub\cf2\f3\fs24 es \u8773? 2:1. \up0 \expndtw-3\charscalex100 El proceso se acel
era a pH alcalino, como se deduce de los pre-equilibrios (5) y (9) [8]. \par\par
d\qj \li1133\ri1488\sb124\sl-276\slmult0\fi566 \up0 \expndtw0\charscalex103 El t
ratamiento ha resultado efectivo para descomponer compuestos organoclorados \up0
\expndtw-4\charscalex100 como tricloroetileno, tetracloroetileno, etc. Por lo t
anto, es excelente para el postratamiento de \up0 \expndtw0\charscalex103 aguas
sometidas a tratamientos de desinfeccin con cloro o dixido de cloro. Uno de los \u
p0 \expndtw0\charscalex100 principales campos de aplicacin es la degradacin de pla
guicidas presentes en aguas [17]. \up0 \expndtw0\charscalex100 Tambin se ha usado
en la decoloracin de compuestos de aguas residuales de la industria \up0 \expndt
w-3\charscalex100 papelera y otros procesos industriales. \par\pard\qj \li1133\r
i1501\sb121\sl-280\slmult0\fi566 \up0 \expndtw-4\charscalex100 Bellamy y colabor
adores [18] trataron con esta mezcla aguas subterrneas contaminadas \up0 \expndtw
-5\charscalex100 con percloroetileno \up0 \expndtw-5\charscalex100 (PCE), tric
loroetileno \up0 \expndtw-5\charscalex100 (TCE), trans-1,2-dicloroetileno \up0
\expndtw-5\charscalex100 (DCE) y \par\pard\qj \li1133\ri1483\sb0\sl-295\slmult0
\up0 \expndtw-3\charscalex100 tetracloruro de carbono (CTC). La mejor relacin mo
lar H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\u
l0\nosupersub\cf2\f3\fs24 /O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 f
ue de 0,5, y la velocidad de \up0 \expndtw0\charscalex100 remocin (que responda a
una cintica de 1er. orden) sigui el orden PCE < TCE < DCE. \up0 \expndtw-3\charsca
lex100 Karimi y otros (1997) [19] lograron reducir niveles iniciales de hasta 44
7 g/L de TCE y 163 \up0 \expndtw0\charscalex103 g/L de PCE en una planta de tratam
iento de agua en Los ngeles (EEUU), alcanzando \up0 \expndtw-2\charscalex100 nive
les inferiores al lmite impuesto por la legislacin local (5 g/L). \par\pard\qj \li1
133\ri1501\sb69\sl-276\slmult0\fi566 \up0 \expndtw0\charscalex108 Ormad y otros
[20] usaron la mezcla H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\s
ub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /O\ul0\sub\cf3\f4\fs24 3\ul0\nosuper
sub\cf2\f3\fs24 para tratar aguas residuales de la \up0 \expndtw-3\charscalex10
0 produccin de los plaguicidas dificol y tetradifon, que contenan adems clorobencen
os, DDT \up0 \expndtw-4\charscalex100 y otros compuestos organoclorados. La oxid
acin se realiz usando la relacin molar H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f
3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /O\ul0\sub\cf3\f4\fs24
3 \up0 \expndtw0\charscalex105 \ul0\nosupersub\cf2\f3\fs24 0,5, pH 9,4 y hasta
1,5 g de O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 /g TOC inicial. Con
elevadas dosis de ozono, se logr la \up0 \expndtw0\charscalex105 remocin de varios
compuestos presentes en la muestra original; sin embargo, no pudo \up0 \expndtw
0\charscalex103 eliminarse totalmente la carga orgnica original, y se detect la fo
rmacin de numerosos \up0 \expndtw-5\charscalex100 subproductos hidroxilados resid
uales. \par\pard\ql \li1133\sb0\sl-276\slmult0 \par\pard\ql\li1133\sb8\sl-276\sl
mult0 \up0 \expndtw-1\charscalex100 2.3. Reactivo de Fenton \par\pard\qj \li1133
\ri1499\sb253\sl-290\slmult0\fi566 \up0 \expndtw-4\charscalex100 Los conocidos e
nsayos de Fenton de fines del siglo XIX demostraron que las soluciones \line \up
0 \expndtw-4\charscalex100 de perxido de hidrgeno y sales ferrosas eran capaces de
oxidar los cidos tartrico y mlico, \line \up0 \expndtw-4\charscalex100 y otros com
puestos orgnicos[21]. Ms tarde, Haber y Weiss sugirieron que se formaba HO\ul0\sup
er\cf3\f4\fs24 \u8226? \par\pard\li1133\sb1\sl-276\slmult0\fi0\tx1531\tx3561 \up
0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 [3,\tab \up0 \expndtw-2\c
harscalex100 22]por la reaccin\tab \up0 \expndtw-2\charscalex100 (16). Dichos rad
icales podan reaccionar luego por dos vas, la\par\pard\li1133\sb0\sl-276\slmult0\f
i0 \up0 \expndtw-1\charscalex100 oxidacin de Fe(II) (una reaccin improductiva) y e
l ataque a la materia orgnica:\par\pard\li1133\sb199\sl-276\slmult0\fi0\tx2607\tx

6353\tx9773 \up0 \expndtw-2\charscalex100 Fe\ul0\super\cf3\f4\fs24 2+\ul0\nosupe
rsub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\s
ub\cf3\f4\fs24 2\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \
u8594?
Fe\ul0\super\cf3\f4\fs24 3+\ul0\nosupersub\cf2\f3\fs24 + HO\ul0\sup
er\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 + HO\ul0\super\cf3\f4\fs24 \u8226?
\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 ; k = 76 L mol\ul
0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\fs24 s\ul0\super\cf3\f4\fs24 -1\ta
b \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (16)\par\pard\li1133
\sb137\sl-276\slmult0\fi0\tx1798\tx2652\tx9773 \up0 \expndtw-6\charscalex100 Fe(
II)\tab \up0 \expndtw-2\charscalex100 + HO\ul0\super\cf3\f4\fs24 \u8226?\tab \u
p0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
Fe(III) + HO
\ul0\super\cf3\f4\fs24 -\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f
3\fs24 (17)\par\pard\li1133\sb141\sl-276\slmult0\fi0\tx9773 \dn2 \expndtw-2\char
scalex100 RH + HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 +
H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O
\u8594?
ROH + H\u
l0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 O\ul0\super\cf3\f4\fs24 +\ul0\no
supersub\cf2\f3\fs24
\u8594?
productos oxidados\tab \up0 \expndtw-2\chars
calex100 (18)\par\pard\li1133\sb176\sl-276\slmult0\fi540 \up0 \expndtw-1\charsca
lex100 A pH < 3, la reaccin es autocataltica, ya que el Fe(III) descompone H\ul0\s
ub\cf2\f3\fs24 en O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 y H\ul0\s
ub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\par\pard\li1133\sb0\sl-276\slmult0
\fi0 \up0 \expndtw-2\charscalex100 a travs de un mecanismo en cadena [23-26]:\par
\pard\li1133\sb199\sl-276\slmult0\fi0\tx2607\tx9773 \up0 \expndtw-2\charscalex10
0 Fe\ul0\super\cf3\f4\fs24 3+\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\f
s24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-2\cha
rscalex100 \ul0\nosupersub\cf2\f3\fs24 = Fe-OOH\ul0\super\cf3\f4\fs24 2+\ul0\no
supersub\cf2\f3\fs24 + H\ul0\super\cf3\f4\fs24 +\tab \up0 \expndtw-2\charscal
ex100 \ul0\nosupersub\cf2\f3\fs24 (19)\par\pard\sect\sectd\fs24\paperw11900\pape
rh16840\pard\sb0\sl-240{\bkmkstart Pg7}{\bkmkend Pg7}\par\pard\li1702\sb0\sl-230
\slmult0\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb19\sl-230\slmult0\
fi0\tx10601 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Procesos a
vanzados de oxidacin para la eliminacin de contaminantes\tab \up0 \expndtw-1\chars
calex100 9\par\pard\li1702\sb0\sl-276\slmult0\par\pard\li1702\sb0\sl-276\slmult0
\par\pard\li1702\sb225\sl-276\slmult0\fi0\tx2890\tx10342 \up0 \expndtw-4\charsca
lex100 \ul0\nosupersub\cf2\f3\fs24 Fe-OOH\ul0\super\cf3\f4\fs24 2+\tab \up0 \exp
ndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
HO\ul0\sub\cf3\f4\fs
24 2\u8226?\ul0\nosupersub\cf2\f3\fs24 + Fe\ul0\super\cf3\f4\fs24 2+\tab \up0
\expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (20)\par\pard\li1702\sb137
\sl-276\slmult0\fi0\tx3176\tx10342 \up0 \expndtw-4\charscalex100 Fe\ul0\super\cf
3\f4\fs24 2+\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\fs24 2\ul0\nosuper
sub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-5\charscalex100 \ul0\n
osupersub\cf2\f3\fs24 \u8594?
Fe\ul0\super\cf3\f4\fs24 3+\ul0\nosupersub\cf2\
f3\fs24 + HO\ul0\super\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 + HO\ul0\su
per\cf3\f4\fs24 \u8226?\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3
\fs24 (16)\par\pard\li1702\sb139\sl-276\slmult0\fi0\tx3168\tx10342 \up0 \expndtw
-4\charscalex100 HO\ul0\sub\cf3\f4\fs24 2\u8226?\ul0\nosupersub\cf2\f3\fs24 +
Fe\ul0\super\cf3\f4\fs24 2+\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersub\c
f2\f3\fs24 \u8594?
Fe\ul0\super\cf3\f4\fs24 3+\ul0\nosupersub\cf2\f3\fs24 +
HO\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2
\f3\fs24 (21)\par\pard\li1702\sb137\sl-276\slmult0\fi0\tx3168\tx10342 \up0 \expn
dtw-4\charscalex100 HO\ul0\sub\cf3\f4\fs24 2\u8226?\ul0\nosupersub\cf2\f3\fs24
+ Fe\ul0\super\cf3\f4\fs24 3+\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersu
b\cf2\f3\fs24 \u8594?
Fe\ul0\super\cf3\f4\fs24 2+\ul0\nosupersub\cf2\f3\fs24
+ O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + H\ul0\super\cf3\f4\
fs24 +\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (22)\par\pa
rd\li1702\sb139\sl-276\slmult0\fi0\tx3185\tx10342 \up0 \expndtw-4\charscalex100
HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f
4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-5\
charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?

H\ul0\sub\cf3\f4\fs24 2\ul0
\nosupersub\cf2\f3\fs24 O
+
HO\ul0\sub\cf3\f4\fs24 2\u8226?\tab \up0 \expn
dtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (23)\par\pard\qj \li1702\ri933\s
b171\sl-280\slmult0\fi566 \up0 \expndtw-1\charscalex100 El proceso es potencialm
ente til para destruir contaminantes, ya que es muy efectivo \up0 \expndtw-2\char
scalex100 para la generacin de HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf
2\f3\fs24 , pero un exceso de iones Fe\ul0\super\cf3\f4\fs24 2+\ul0\nosupersub\c
f2\f3\fs24 , puede atraparlos (reaccin (17)), al \up0 \expndtw-3\charscalex100 ig
ual que los halgenos, el mismo H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 o el radical perhidroxilo [
27]: \par\pard\li1702\sb214\sl-276\slmult0\fi0\tx3178\tx10342 \up0 \expndtw-4\ch
arscalex100 HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + HO\
ul0\sub\cf3\f4\fs24 2\u8226?\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\c
f2\f3\fs24 \u8594?
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + H\
ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\tab \up0 \expndtw-4\charscale
x100 (24)\par\pard\qj \li1702\ri907\sb173\sl-278\slmult0\fi566 \up0 \expndtw-3\c
harscalex100 Actualmente se cree que otras especies, de Fe(IV) o Fe(V) (como FeO
\ul0\super\cf3\f4\fs24 3+\ul0\nosupersub\cf2\f3\fs24 y complejos de \up0 \expnd
tw0\charscalex100 ferrilo), son en realidad los agentes activos del proceso [2325] y [28-29]. En presencia de \up0 \expndtw-1\charscalex100 exceso de perxido, l
a concentracin de Fe\ul0\super\cf3\f4\fs24 2+\ul0\nosupersub\cf2\f3\fs24 es pequ
ea con relacin a la de Fe\ul0\super\cf3\f4\fs24 3+\ul0\nosupersub\cf2\f3\fs24 , ya
que la \up0 \expndtw0\charscalex100 reaccin (20) es ms lenta que la (16) [23]. Am
bos radicales, el HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 y
el HO\ul0\sub\cf3\f4\fs24 2\u8226?\ul0\nosupersub\cf2\f3\fs24 reaccionan \up0
\expndtw0\charscalex108 indiscriminadamente con la materia orgnica, pero el segun
do es menos reactivo. La \up0 \expndtw-2\charscalex100 constante de velocidad pa
ra la reaccin de ion ferroso con H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs
24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 es alta, y el Fe(II) se o
xida a \up0 \expndtw0\charscalex103 Fe(III) en segundos o minutos en exceso de H
\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\no
supersub\cf2\f3\fs24 . Se cree por ello que la destruccin de \up0 \expndtw-2\char
scalex100 residuos por el reactivo de Fenton es simplemente un proceso catalizad
o por Fe(III)-H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f
4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , y \up0 \expndtw-4\charscalex100 que el rea
ctivo de Fenton con exceso de H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 . es esencialmente un proces
o de Fe\ul0\super\cf3\f4\fs24 3+\ul0\nosupersub\cf2\f3\fs24 /H\ul0\sub\cf3\f4\fs
24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs
24 . Por \up0 \expndtw-1\charscalex100 ello, estas reacciones ocurren tambin con
iones metlicos de transicin como el Fe(III) o el \up0 \expndtw-2\charscalex100 Cu(
II), y se las conoce como reacciones tipo Fenton: \par\pard\li1702\sb202\sl-276\
slmult0\fi0\tx3152\tx10342 \up0 \expndtw-3\charscalex100 M\ul0\super\cf3\f4\fs24
n+\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f
3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \dn2 \expndtw-3\charscalex100 \ul0\nosupersub
\cf2\f3\fs24 \u8594?
M\ul0\super\cf3\f4\fs24 (n+1)+\ul0\nosupersub\cf2\f3\fs2
4 + HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + HO\ul0\s
uper\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 (Fe\ul0\super\cf3\f4\fs24 3+\ul0\
nosupersub\cf2\f3\fs24 , Cu\ul0\super\cf3\f4\fs24 2+\ul0\nosupersub\cf2\f3\fs24
)\tab \up0 \expndtw-4\charscalex100 (25)\par\pard\qj \li1702\ri930\sb167\sl-275\
slmult0\fi566 \up0 \expndtw0\charscalex104 El grado y la velocidad total de mine
ralizacin son independientes, en general, del \line \up0 \expndtw0\charscalex109
estado de oxidacin inicial del Fe. En cambio, la eficiencia y la velocidad inicia
l de \line \up0 \expndtw-4\charscalex100 mineralizacin son mayores cuando se part
e de Fe(II); como contrapartida, las sales de Fe(III) \line \up0 \expndtw-1\char
scalex100 producen una concentracin estacionaria de Fe(II). Se debe usar aqu tambin
un pH menor \line \up0 \expndtw-2\charscalex100 que 2.8. \par\pard\qj \li1702\r
i928\sb125\sl-275\slmult0\fi566 \up0 \expndtw0\charscalex100 El proceso Fenton
ha resultado efectivo para degradar compuestos alifticos y \line \up0 \e
xpndtw0\charscalex102 aromticos clorados, PCBs, nitroaromticos, colorantes azo, cl
orobenceno, PCP, fenoles, \line \up0 \expndtw-3\charscalex100 fenoles clorados,

octacloro-p-dioxina y formaldehdo. Son muy pocos los compuestos que no \line \up0
\expndtw-3\charscalex100 pueden ser atacados por este reactivo, entre ellos la
acetona, el cido actico, el cido oxlico, \line \up0 \expndtw-4\charscalex100 las par
afinas y los compuestos organoclorados [30]. Es un buen oxidante de herbicidas y
otros \line \up0 \expndtw0\charscalex100 contaminantes de suelos tales como hex
adecano o Dieldrin. Puede descomponer solventes \line \up0 \expndtw0\charscalex1
02 para limpieza a seco y decolorar aguas residuales con distintos tipos de colo
rantes y otros \line \up0 \expndtw0\charscalex104 residuos industriales, reducie
ndo su DQO [31]. Tambin se ha aplicado exitosamente el \line \up0 \expndtw0\chars
calex104 reactivo de Fenton en la reduccin de DQO de aguas municipales y subterrne
as y en el \line \up0 \expndtw-2\charscalex100 tratamiento de lixiviados. Es til
como pretratamiento de compuestos no biodegradables [25]. \par\pard\qj \li1702\r
i927\sb121\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex100 Las ventajas del mto
do son varias: el Fe(II) es abundante y no txico, el perxido de \line \up0 \expndt
w-2\charscalex100 hidrgeno es fcil de manejar y ambientalmente benigno. No se form
an compuestos clorados \line \up0 \expndtw0\charscalex103 como en otras tcnicas o
xidantes, y no existen limitaciones de transferencia de masa por \line \up0 \exp
ndtw0\charscalex100 tratarse de un sistema homogneo. El diseo de reactores para la
aplicacin tecnolgica es \line \up0 \expndtw0\charscalex100 bastante sencillo [30]
. En contraposicin, requiere la adicin continua y estequiomtrica de \line \up0 \exp
ndtw-1\charscalex100 Fe(II) y H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , es decir, necesita una alt
a concentracin de Fe. Sin embargo, debe tenerse en \line \up0 \expndtw0\charscale
x100 cuenta siempre que un exceso de Fe (II) puede causar condiciones para el at
rapamiento de \line \up0 \expndtw0\charscalex100 HO\ul0\super\cf3\f4\fs24 \u8226
?\ul0\nosupersub\cf2\f3\fs24 , como se ha mencionado, de acuerdo con las ecuacio
nes (17), (23) y (24). \par\pard\sect\sectd\fs24\paperw11900\paperh16840{\shp
z-10000\shplid7
ffd8ffe000104a46494600010101006000600000ffdb004300010101010101010101010101010101
01010101010101010101010101010101010101010101010101010101010101010101010101010101
010101010101010101ffdb0043010101010101010101010101010101010101010101010101010101
0101010101010101010101010101010101010101010101010101010101010101010101010101ffc0
00110803e702c203012200021101031101ffc4001f00000105010101010101000000000000000001
02030405060708090a0bffc400b5100002010303020403050504040000017d010203000411051221
31410613516107227114328191a1082342b1c11552d1f02433627282090a161718191a2526272829
2a3435363738393a434445464748494a535455565758595a636465666768696a737475767778797a
0101010101010101010000000000000102030405060708090a0bffc400b511000201020404030407
05040400010277000102031104052131061241510761711322328108144291a1b1c109233352f015
6272d10a162434e125f11718191a262728292a35363738393a434445464748494a53545556575859
5a636465666768696a737475767778797a82838485868788898a92939495969798999aa2a3a4a5a6
0028a28a0028a2be06f891fb637c49f869fb60fc17fd9cf58fd9a6fa5f85bf1c7c6f7ff0dbc19f1c
c7c63f0041e20d5fc57a3fc14f14fc6bf116b1a07c07314be34d6fe18f83f4ff000c3784bc67e3a6
d674dbbd07c517d063c2d7da1b5b6b37801f7cd15f97ff00b60ffc149cfec95e34f8896d73fb3d78
c7e217c1ff00d9ebe1f7c1af8adfb51fc62d2fc6be12d023f85be02f8e1f10bc5bf0ff00c337de0c
f02ea5f6af107c55d67c383c0de27f1978f349827f08dae8be0fb3b59b47d5fc49e21bf87c383f4b
b54d6b47d12c1f54d6b56d3747d323f2fccd4754beb5d3ec63f39824424bbbb961b7432b32ac61a4
1bd982ae49028034a8af2c83e39fc12b9711db7c62f85970e679ed8241f107c252b9b9b63b6e6dc2
c7abb133dbb7cb3c58f3223c48aa6a4b8f8ddf062d2ccea177f177e185b582aa3b5f5c78fbc290d9
aa48e238d8dcc9ab2c2164721118be19c85524902803d3e8af261f1efe05995601f1a3e131999cc6
b08f88de0f32b48ae2268d631acef2eb21119500b072108dc40a8351fda17e0168f14f3eaff1c7e0
fe9505b471cd7336a5f133c176315bc334a208659e4b9d6e248a39662b144f232abc8446a4b90b40
1ec145791defed01f01b4c609a97c6df847a7b988ce16f7e24f836d18c2a2366982cfad467ca512c
44c98d804b19270eb9cbb9fda6ff0066db3b74bbbcfda0fe07dadac93436f1dcdcfc58f01c16f25c
5c02608126975f58de6982930c4ac5e4009456c1a00f70a2bc0a1fdabbf65bb8bd8b4db7fda4fe01
4fa8cf712d9c3610fc62f8772decd7701227b58ad53c46d3c97109044b0246658c821d5706a19ff6
b6fd952d6de0bbb9fda6bf67cb7b4b9576b6ba9fe33fc3886dee150857682793c48b14aa8cc15cc6
cc149009048a00fa0e8af9d60fdb03f64aba6d96dfb51feceb70fb917641f1b7e1a4adba4711c6bb
63f1331dd248cb1a0c659c8450588152dc7ed73fb28da4934577fb4efecf56b2dbc8f0dc4771f1a7
e1bc3241344712453249e25568a48c821e370ac8461803401f42d15f39b7ed87fb2426f2ff00b52f
ece6a113cc72df1bbe19aec8f246f7cf89c6d4c82371c2e4119c8a07ed87fb243723f6a5fd9cc8c4
6d91f1bbe199f966459216e3c4fd258dd1e33d2447565cab02403e8ca2be728ff6c4fd91a5b892d2
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7f043e1cf84fe18f846f3c5baaaeb7e26bbd03c1da3dae89a6dcebdaac76b6305eea93db5a24b793
5ad85859f9ccc965636768b0db45ed345001451595a5ebba26b6daa268bace95abbe89aadc685ad2
697a85a6a0da46b76715bcf77a36a8b6934c6c355b582eed66b8d3eec4577045736f24b0aa4d1960
0f9a2dff00654d2742f8a5fb577c6af02fc4bf1f781be26fed5be0cf84fe13d67c47a641e0bd623f
86f77f067c33e31f0cf83bc4fe02d1bc51e14d6f469b5758bc6577a86a56be32b2f14e8b7b7b6162
a74c8ed0dcdb4fe33a6ffc138fe1d68ffb48cdf1eb4af8abf16f4df0b6a1f1d4fed5daff00ecfb65
77e0c83e14f88bf6a793e109f81d75f19753bcff00843dfe2227dbbc082def6f7e1e69de35b1f87b
71e3db2b2f1d1f0f8d5a29527fd12a2800a28ac8d2fc41a0eb93eb36ba2eb7a46af73e1cd55b42f1
0dbe97a9596a13e85ada59596a4fa36b30da4d349a5eaa9a76a5a75fb69f7cb05dad95fd95d18441
7504920062fc45f0368bf13be1f78ebe1af891efa3f0efc43f07789fc0daf49a5dc25a6a71e8be2c
d12fb40d51f4ebb921b88ed6f96c7509dad2e1ede7482e04723432aa946f03b3fd97af7c2ff07fc1
ff00043e197c7cf8cdf0bfc17e00fd9867fd9a7c2373e1b7f871a8789f4992cf41f077863c1bf1a9
75ff0013fc3ed7279be2df80f43f09dcdae833b423c0f7571e28d7350d77c15aadec1a14da37d5b4
5007c81fb13feca379fb197c18d2fe05dbfc68f19fc64f06f854c56fe08bbf1df853e19f87bc45a0
e9a51e7d546b1ab7c37f07f841bc73e23f146bf71a8f8b7c5de38f1841aaf8bbc4fe29d5f56d6b59
d5af2f750b895febfa28a002bc6bc6bf033c19e3df8bdf04be35eb93eb89e2ef804bf128781edec6
f6d61d1276f8a9e1ab2f0a78924d76ce6b0b8babd78349b151a49b4bed3becb7134f25c0bb8dd625
f65a2803e2df8a7fb027ecd9fb43fc36f0dfc3cfda97c0da0fed4575e19d574ed4acbe22fc6cf06f
c3af107c4992df48f89b61f146c7413e21d2bc17a1dbe9fe1b7d4f49d2bc3dab687a1e99a4d87887
c2566da36bd0ea3f6ed46e2efec8b1b1b2d2ec6cf4cd32ced74fd374eb5b7b1d3f4fb1b78ad2cac6
cad214b7b4b3b3b5812382dad6da08e386dede1448a1891238d1514016a8a0028a28a00f9cfc23fb
34784fe1e5878f2c7e1ef8c7e23f82e4f899fb44de7ed29e35d4749d7749bcbfd5fc5bacebfe1ed6
fc51e1243e21f0f6b769a6fc3bf165b7872dbc39ade87a55a596aaba15f6a8348d7f4ad62ec6b117
89f807fe09d3f047e1e7ed2b63fb4ae97e28f8b3aa5ef8575bf8e5e2ef857f0835df15e9375f057e
0cf8eff699d5a3d7bf680f1bfc36f0dd9f866c3c4d67ad7c51d69b57d5758b2f11f8cbc4be1ad1af
fc53e2c9fc23a0f878eb97013ef8a2800a28a2803c67f68bf817e0bfda7be027c64fd9cfe235c6bd
69e01f8e3f0d7c65f0afc6575e16bfb6d2bc496fe1af1ce857be1ed666d0752bcb0d52d2c3568ac6
fe67b0bbb9d36fe082e44724b69708ad1379f7c76fd95341f8fbe03bef86de21f89bf147c31e123a
1fc3587c3b65e0fbbf04dbcfe0ef1efc21f891e1cf8a7f0f3e2e6877baff0081fc417175e37d0bc5
3e11f0e79ba7f889f5cf006afa669bf60d63c137cb777924ff0053d1401f3c7ecddfb3eafecf3e18
f19e9579f14fe237c68f15fc47f88fadfc53f1dfc46f8a09e05b5f12ebde29d6745f0e7868245a5f
c35f057c3ff06e8da3e97e1ef09787f49d334dd27c336a563b27bbbdb8bebfbbbaba97e87a28a002
bf273fe0a2ff0007b52d77e21fec8de2fd07e37fed57f0da4f1ffed53f07be0c78db46f82ffb4a7c
4df855e0cbdf005fe93f117c497e350f07786758b7d0e7d4358d5b46d2747d4f59b3b3b2d7eef4fb
88ad9f555b5b548d7f58ebc0fe3bfc0c5f8dd75f03ae1fc5d7de145f82ff001f3c13f1cfc9b2d2ed
b535f163783348f156991f846f9ae2e6d9b4db1d464f12a5f49aa5b79f736f2e99046b6d2c73cbb4
03e32f1ffc7af81ffb19f8f3f69af11788350fda83c6127ec83ff04eef047c71f1fdaeb3f15fc4df
123c2fe21f851a4f8c3f683bed24e87e1df1e78e65835bfda0efaebe19f8bad75df1febc965ac789
341baf0868babf8baeedb4d8e0d3b2aebfe0a81e26d2bc61f047c03aff00fc13eff6cbd0bc67fb50
786bc69e23fd9dbc277d2fecd2de21f18afc3dd2b42f1078bb4ef1e4107ed092693f05aef4bf0df8
934ad7cbfc45d6b4c824b55d474b6922f1459c3e1fbcf68fda7bf618b0fda5749fdb1f4abaf89daa
783d3f6bafd8e34bfd916ededbc3163ae27806d74cb9f8e372bf102c23bad56c64d72f673f1aa68e
6f0db5c68d60ebe1bb7792fe49f5032d87a078eff655b5f1c7ed1bfb207ed0b2f8eeff004db8fd92
fc2ff1dbc3567e108b42b4bad3fc787e37f837c15e109f52bed525be4bbf0fdc785e2f077daec63b
3b7d417511ac5e5a5cbc091c7330078ddcff00c14a3e19f86bf66bf8bbfb43fc4ff85bf163e165e7
c13f8e50fecdbe32f841e297f8692f8eeebe336ade2df03f837c25e1bf0debda57c44bdf85da9e8b
e32d53e24f832f348f19def8fb49f0c69fa1ea973ad78a350f0fd868fab4b67d1fec65fb7b784bf6
bdf157c6df86c7c01aa7c2ef8a9f01ae3c177be2ff00095cfc44f841f17745d47c19f12878a57c01
e34f0efc43f81be3af883e09bbb7d72efc0fe31d2f51f0cea3ab697e33f0cea5a04cbade816da7ea
3a1ea3aa637c58ff0082797837e2c7c28fda07e1aea7e38bab7bdf8c7fb50f86bf6b7f0a788f51f0
5785bc5b67f0dfe28f8225f851a9f84ad6f3c17e288f52f0bfc45f0941adfc2ab5ff00848b40f115
a5aa7887c35e22d674149f49be4b1f105b7a6fec97fb3dfc4cf815078fa6f895e30f80daf5e78baf
b423a5683fb3afeccda37ecd7e05d0ecf41b7d4a29752d474c5f1bfc4bf1678afc57e23b8d49ee75
5d435af1a3e89a55b59d869de1bf0fe9921d6f53d7802efedebf1dbc57fb317ec59fb51fed03e03b
3d0f50f1dfc24f821f10bc69e06b1f133b47e1ebbf1a695e1ebd7f09c1adb2490b1d2e4f10369cb7
b1f9f6e25b73244d736cae678fe24f8b3a2dc7fc135ff66cfd8b3c29f033c2de3ff156abaafed7df
0c747f8c9e1ff849a6e85ae7c4cfda73c79f17bc33f122efe2af88fc557fe36d674ab1d635ef88ff
0012ee60f885e35f17f8a3c5fa2dbe8763a5bea373ae69fe1cf0fc7609fa0bfb5efc056fda93f659
fda17f6728bc4b2f82eefe367c1ff1f7c35d3bc5f0da45a83f85b56f15f872ff004ad23c4274f981
8efe2d1b53b8b4d427b16d9f6c86de4b759226904a9f3efc226f14fedaff0007bf674f197c62f08f
8fbf67df8d3fb36fc79d23c45f17fe1c7883c2b3da432fc65f84fe14f14f823c5da4f85359d4a2b7
d33c61f087c5773e3393c59f0f3e2778466d4b4af13784ae3459addecb547d5f4dd240392bff00f8
29cf847e1efc2efdb13c79f1fbe067c57f843e29fd8a1bc0b7ff0013fe1559ea7f0e3e2678bbc49e
1af8b165677bf0a358f879a8782bc6573e18d7effc6f2dcdc6856fe1bbed6747d5ac7c4da65ee972
a4f6f2e97a8ea307c5ff00f828d78cbe04fc3bf875e33f8abfb1a7c5ef01eb7f193e32de7c2bf86f
e15f17fc4dfd9fb40d374bd262f006a1e3fd3bc75f1bfe28dd7c4b7f84bf046d35c8746d5fc29a3f
86f5df1a6b1e20d4bc731697e17d3edef2ff005ab3035be3affc136bc2bf1d6e3f6e69b57f8abe27
d053f6ddd0ff00662d175a8b4df0ee83747e1d8fd992f6e751d16ef447bf697fb724f15dd5c0fed6
4d4d2dd74e86245d2da3b82d755f547ed17f0c7e2f7c50f0be8da67c1cf8cfa0fc21d6b4ed6a4bad
76dbc71f073c3bf1cbe1afc44f0d5de957fa6df7837c7be06d535df056bf2e9de7dddaeb7a6ea3e0
ef887e0dd52d757d2ed23d4a7d6f409f53d06fc0347f671f8c3af7c76f84de1df895e24f851e25f8
33aaeb8d781fc17e25f16fc31f1f37d96098ad8ebba0f8dfe0f78d3c7de00f15f85b5fb368753d07
5ad1bc42ef7367305bdb1d3af229ad63f8e3c6be0e1f03ff00e0a7bf033e237c396d23c39a2fedb9
f0cbe2afc34fda4fc3d169537fc5c1f1ff00ecf1e14d37c77f007e2547716ad1d9d8f8c7c2fe0dba
f8a7e02d7f58bc492f3c51e0fbbf07e8d7af711781fc39fd99dffecebfb1978d7f666f829e0cf853
f0cfe39693e17be83f68ad63e3a7c51bbf09fc14f0ce83f0e7c57e1ff1978c356f167c42f833f0bf
e125e788f5ed2fe047813c4d26a1147a7cde18f106b9aaf86f541abf886d26bbd47c417e041aff00
853c65f1c3fe0a05f0e7c4977e07f16f84fe11fec45e06f1cea5a778e7c4ba347a7e8bf19be397ed
13e16d33c316d63f0cee2726fb54f0d7c17f85b6be2db6f1e788d238747d4bc63f14743f0ce8f35f
6a1e09f16a69e01fa054514500145145001451450014514500145145001451450014514500145145
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0014514500145145007fffd9}}}}}\pard\sb0\sl-240{\bkmkstart Pg8}{\bkmkend Pg8}\par\

pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li113
3\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\c
f4\f5\fs20 10\tab \up0 \expndtw-2\charscalex100 Domnech, Jardim y Litter\par\pard
\qj \li1133\sb0\sl-280\slmult0 \par\pard\qj\li1133\sb0\sl-280\slmult0 \par\pard\
qj\li1133\ri1489\sb181\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex100 \ul0\no
supersub\cf2\f3\fs24 A pH > 5 se genera Fe(III) particulado; si bien se generan
as barros que obligan a su \up0 \expndtw0\charscalex105 posterior gestin, es frecu
ente alcalinizar las aguas al final del proceso con el agregado \up0 \expndtw-3\
charscalex100 simultneo de un floculante para eliminar el hierro remanente. \par\
pard\qj \li1133\ri1500\sb120\sl-280\slmult0\fi566 \up0 \expndtw-1\charscalex100
Tericamente, la relacin estequiomtrica molar H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub
\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /substrato debe
oscilar entre 2 y \up0 \expndtw-1\charscalex100 10 cuando se usa el reactivo par
a la destruccin de compuestos solubles. Sin embargo, en la \up0 \expndtw0\charsca
lex102 prctica esta relacin puede ser a veces de hasta 1000, ya que en muestras am
bientales el \up0 \expndtw0\charscalex100 compuesto a destruir siempre viene aco
mpaado de otros que tambin pueden ser atacados \up0 \expndtw-3\charscalex100 por e
l HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 . La relacin perxido
/Fe/compuesto puede ser mantenida por adicin intermitente \up0 \expndtw-4\charsca
lex100 del oxidante o fijada al inicio de la reaccin. \par\pard\qj \li1133\ri1489
\sb100\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex100 En el laboratorio, el a
gregado del metal se realiza tradicionalmente en forma de sales \up0 \expndtw0\c
harscalex102 ferrosas puras, pero en escalas mayores el uso de stas se vuelve pro
hibitivamente caro, y \up0 \expndtw0\charscalex100 normalmente se usa Fe\ul0\sub
\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 (NH\ul0\sub\cf3\f4\fs24 4\ul0\nosupers
ub\cf2\f3\fs24 )\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 SO\ul0\sub\cf3
\f4\fs24 4\ul0\nosupersub\cf2\f3\fs24 , que contiene 20% de hierro activo. Se ha
n usado otros \up0 \expndtw-1\charscalex100 compuestos de hierro, incluyendo slid
os como la goetita, por ejemplo, en la destruccin de \up0 \expndtw-3\charscalex10
0 tricloroetileno [32]. No se logra en estos casos, por lo general, la mineraliz
acin completa; se \up0 \expndtw0\charscalex100 forman intermediarios resistentes
al tratamiento, (cidos carboxlicos) que reaccionan muy \up0 \expndtw-3\charscalex1
00 lentamente con el HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24
, y predomina la reaccin improductiva (17). A veces, como muestra la \up0 \expnd
tw0\charscalex103 Figura 2, pueden formarse productos ms txicos que los iniciales,
como quinonas, cuya \up0 \expndtw-3\charscalex100 presencia debe controlarse cu
idadosamente. \par\pard\ql \li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl
-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-2
30\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230
\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\s
lmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slm
ult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmul
t0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0
\par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \
par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \pa
r\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\
pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pa
rd\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb52\sl-230\slmult0 \up0 \ex
pndtw0\charscalex102 \ul0\nosupersub\cf4\f5\fs20 Figura 2. Oxidacin de clorobence
no con el reactivo de Fenton. Condiciones iniciales: [Fe\ul0\super\cf5\f6\fs19 2
+\ul0\nosupersub\cf4\f5\fs20 ] = 5.0 mM; pH \par\pard\ql \li1133\sb10\sl-230\slm
ult0 \up0 \expndtw0\charscalex101 3.0 [33]. \par\pard\qj \li1133\ri1500\sb269\sl
-280\slmult0\fi566 \up0 \expndtw0\charscalex100 \ul0\nosupersub\cf2\f3\fs24 Reci
entemente, Rivas y colaboradores [34] estudiaron la oxidacin con el reactivo de \
line \up0 \expndtw-1\charscalex100 Fenton de cido p-hidroxibenzoico \up0 \expndtw
-1\charscalex100 (pHB), un contaminante comn en efluentes de la \par\pard\qj \li1
133\ri1493\sb0\sl-280\slmult0 \up0 \expndtw-3\charscalex100 industria de aliment
os. Se estableci una relacin molar ptima Fe/H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\
cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /pHB de alrededor
de \up0 \expndtw-1\charscalex100 5 10\ul0\super\cf3\f4\fs24 -3\ul0\nosupersub\c

f2\f3\fs24 /2.65/1 10\ul0\super\cf3\f4\fs24 -2\ul0\nosupersub\cf2\f3\fs24 . El a
gregado de alcohol terbutlico, un atrapador de HO\ul0\super\cf3\f4\fs24 \u8226?\u
l0\nosupersub\cf2\f3\fs24 , influye poco \up0 \expndtw-4\charscalex100 en el pro
ceso, lo que sugiere la participacin de otros radicales, como se seal ms arriba. La
\up0 \expndtw0\charscalex102 formacin de fenol, catecol, hidroquinona y trihidrox
ibenceno sugieren un mecanismo de \up0 \expndtw-3\charscalex100 degradacin va desc
arboxilacin. \par\pard\li1133\sb118\sl-276\slmult0\fi566\tx9829 \up0 \expndtw0\ch
arscalex107 Tambin pueden destruirse con el reactivo de Fenton cido frmico, fenol,\
tab \up0 \expndtw0\charscalex106 2,4-\par\pard\li1133\sb0\sl-276\slmult0\fi0\tx2
507\tx5476 \up0 \expndtw-3\charscalex100 diclorofenol,\tab \up0 \expndtw0\charsc
alex103 4-clorofenol y nitrobenceno\tab \up0 \expndtw0\charscalex106 [35]. El tr
atamiento oxidativo hace disminuir\par\pard\sect\sectd\fs24\paperw11900\paperh16
840\pard\sb0\sl-240{\bkmkstart Pg9}{\bkmkend Pg9}\par\pard\li1702\sb0\sl-230\slm
ult0\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb19\sl-230\slmult0\fi0\
tx10500 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Procesos avanz
ados de oxidacin para la eliminacin de contaminantes\tab \up0 \expndtw-1\charscale
x100 11\par\pard\qj \li1702\sb0\sl-280\slmult0 \par\pard\qj\li1702\sb0\sl-280\sl
mult0 \par\pard\qj\li1702\ri927\sb180\sl-280\slmult0 \up0 \expndtw0\charscalex10
2 \ul0\nosupersub\cf2\f3\fs24 apreciablemente la carga orgnica original, aum
entando la biodegradabilidad. Usando \up0 \expndtw-1\charscalex100 diferentes
relaciones molares H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub
\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /4-clorofenol y H\ul0\sub\cf3\f4\fs24
2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
/Fe\ul0\super\cf3\f4\fs24 2+\ul0\nosupersub\cf2\f3\fs24 , se pudo concluir que l
a primera \up0 \expndtw0\charscalex105 regula la extensin de la destruccin del com
puesto, mientras que la segunda controla la \up0 \expndtw-3\charscalex100 cintica
de destruccin. \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb128
\sl-276\slmult0 \up0 \expndtw0\charscalex102 2.4. Oxidacin electroqumica \par\pard
\qj \li1702\ri927\sb261\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex100 La apl
icacin de corriente elctrica (2-20 A) entre dos electrodos adecuados [36]. en \up0
\expndtw0\charscalex100 agua produce reacciones qumicas primarias, con la genera
cin de HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 , que oxida lu
ego la \up0 \expndtw-1\charscalex100 materia orgnica: \par\pard\li1702\sb215\sl-2
76\slmult0\fi0\tx2309\tx5662\tx10342 \up0 \expndtw-4\charscalex100 H\ul0\sub\cf3
\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\tab \up0 \expndtw-4\charscalex100 \u8594
?
HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + H\ul0\supe
r\cf3\f4\fs24 +\ul0\nosupersub\cf2\f3\fs24 + e\ul0\super\cf3\f4\fs24 -\tab \u
p0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 ; oxidacin andica\tab \up0
\expndtw-4\charscalex100 (26)\par\pard\li1702\sb139\sl-276\slmult0\fi0\tx3667\t
x5662\tx10343 \up0 \expndtw-4\charscalex100 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupers
ub\cf2\f3\fs24 + 2 H\ul0\super\cf3\f4\fs24 +\ul0\nosupersub\cf2\f3\fs24 +
2 e\ul0\super\cf3\f4\fs24 -\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf
2\f3\fs24 \u8594?
H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\su
b\cf3\f4\fs24 2\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 ;
reduccin catdica\tab \up0 \expndtw-4\charscalex100 (27)\par\pard\qj \li1702\ri922\
sb180\sl-274\slmult0\fi566 \up0 \expndtw0\charscalex105 La eficiencia del sistem
a puede mejorarse por agregado de Fe(II), y el proceso se \line \up0 \expndtw0\c
harscalex100 conoce como electro-Fenton. Si se usa un nodo de sacrificio de Fe, q
ue provee cantidades \line \up0 \expndtw0\charscalex107 estequiomtricas de Fe
para la reaccin de Fenton, el proceso se conoce como \line \up0 \expndtw
0\charscalex100 peroxicoagulacin. Por ejemplo, la degradacin por oxidacin andica de
una solucin de \line \up0 \expndtw0\charscalex106 anilina mediante una corriente
de 20 A conduce a un 18 % de eliminacin del carbono \line \up0 \expndtw-1\charsca
lex100 orgnico total (COT) al cabo de 6 horas. Si el proceso se lleva a cabo empl
eando el mtodo \line \up0 \expndtw-3\charscalex100 electro-Fenton, se consigue un
61% de disminucin del COT al cabo de 2 horas, mientras que \line \up0 \expndtw-3
\charscalex100 por peroxicoagulacin se elimina un 91 % en slo 1 hora en iguales co
ndiciones. \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb29\sl-2
76\slmult0 \up0 \expndtw-1\charscalex100 2.5. Radilisis \u947? y procesos con hac
es de electrones \par\pard\qj \li1702\ri922\sb221\sl-280\slmult0\fi566 \up0 \exp

ndtw0\charscalex105 Estos procesos se basan en la generacin de electrones altamen
te reactivos, iones \line \up0 \expndtw-3\charscalex100 radicales y radicales ne
utros por exposicin de las aguas a tratar a haces de partculas msicas \line \up0 \e
xpndtw-4\charscalex100 u ondas electromagnticas de alta energa [37]. Se puede usar
rayos \u947? (Gammacell, \ul0\super\cf3\f4\fs24 60\ul0\nosupersub\cf2\f3\fs24 C
o) [38], \line \up0 \expndtw0\charscalex102 rayos X o aceleradores de haz de ele
ctrones como los de tipo Van-de-Graaf o los lineales \line \up0 \expndtw0\charsc
alex102 (LINAC) [39]. \par\pard\qj \li1702\ri911\sb120\sl-280\slmult0\fi566 \up0
\expndtw0\charscalex104 Cuando el haz de electrones penetra en el agua, los ele
ctrones pierden energa por \up0 \expndtw-2\charscalex100 colisiones no elsticas co
n las molculas de H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O, y se gene
ran especies reactivas: \par\pard\li1702\sb201\sl-276\slmult0\fi0\tx2309\tx10342
\up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs2
4 O\tab \dn2 \expndtw-3\charscalex100 \u8594?
e\ul0\super\cf3\f4\fs24 -aq\ul0
\nosupersub\cf2\f3\fs24 + H\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\
f3\fs24 + HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + H\
ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\fs24 2\ul
0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 +
H\ul0\super\cf3\f4\fs24 +\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2
\f3\fs24 (28)\par\pard\qj \li1702\ri932\sb156\sl-290\slmult0\fi566 \up0 \expndtw
-3\charscalex100 Las tres primeras especies son los productos primarios de la ra
dilisis del agua. Los e\ul0\super\cf3\f4\fs24 -aq \line \up0 \expndtw-1\charscale
x100 \ul0\nosupersub\cf2\f3\fs24 y los H\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosup
ersub\cf2\f3\fs24 son reductores fuertes, que atacan a la materia orgnica por me
canismos diferentes: \line \up0 \expndtw0\charscalex104 mientras que e\ul0\super
\cf3\f4\fs24 -aq\ul0\nosupersub\cf2\f3\fs24 produce abstraccin de tomos de halgeno
(E\ul0\super\cf3\f4\fs24 o\ul0\nosupersub\cf2\f3\fs24 = 2,77 V), H\ul0\super\c
f3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 produce \line \up0 \expndtw-2\cha
rscalex100 adicin o abstraccin de hidrgeno. Por su parte, el HO\ul0\super\cf3\f4\fs
24 \u8226?\ul0\nosupersub\cf2\f3\fs24 acta como oxidante, como en otras \line \u
p0 \expndtw-3\charscalex100 TAOs. \par\pard\qj \li1702\ri931\sb119\sl-280\slmult
0\fi566 \up0 \expndtw0\charscalex102 El mtodo es ideal para el tratamiento de com
puestos orgnicos voltiles (en ingls, \line \up0 \expndtw0\charscalex102 VOCs) y sem
ivoltiles (SVOCs) en aguas subterrneas, residuales, potables y lixiviados. \line \
up0 \expndtw-1\charscalex100 Ataca principalmente a compuestos halogenados como
los bifenilos policlorados (en ingls, \line \up0 \expndtw-2\charscalex100 PCBs),
difcilmente oxidables y atacables por HO\ul0\super\cf3\f4\fs24 \u8226? \up0 \expn
dtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 [38]. Los compuestos pueden ser
\par\pard\qj \li1702\ri930\sb5\sl-275\slmult0 \up0 \expndtw-2\charscalex100 mine
ralizados o bien degradados a productos de menor peso molecular. El mtodo no gene
ra \line \up0 \expndtw-1\charscalex100 residuos, barros u otros desechos que nec
esiten tratamiento posterior, ni compuestos txicos \line \up0 \expndtw-2\charscal
ex100 como las dioxinas. Como contrapartida, si las dosis de radiacin son bajas,
se pueden formar \line \up0 \expndtw-3\charscalex100 aldehdos, cidos orgnicos y SVO
Cs resistentes. El proceso requiere alto consumo elctrico, \line \up0 \expndtw-3\
charscalex100 no es efectivo econmicamente para concentraciones altas de contamin
antes y, por lo tanto, es \par\pard\sect\sectd\fs24\paperw11900\paperh16840\pard
\sb0\sl-240{\bkmkstart Pg10}{\bkmkend Pg10}\par\pard\li1133\sb0\sl-230\slmult0\p
ar\pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb18\sl-230\slmult0\fi0\tx8050
\up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs20 12\tab \up0 \expndtw2\charscalex100 Domnech, Jardim y Litter\par\pard\qj \li1133\sb0\sl-280\slmult0 \
par\pard\qj\li1133\sb0\sl-280\slmult0 \par\pard\qj\li1133\ri1489\sb181\sl-280\sl
mult0 \up0 \expndtw0\charscalex104 \ul0\nosupersub\cf2\f3\fs24 un mtodo relativam
ente caro. Se encuentra en etapa de planta piloto pero se prev una \up0 \expndtw3\charscalex100 implementacin comercial cercana. La combinacin con ozono aumenta s
u eficiencia, debido \up0 \expndtw-1\charscalex100 a la rpida formacin de especies
reactivas adicionales. En un contexto relacionado, existen \up0 \expndtw0\chars
calex104 algunas plantas de irradiacin de barros cloacales con radiacin \u947? (\u
l0\super\cf3\f4\fs24 60\ul0\nosupersub\cf2\f3\fs24 Co), cuyo objetivo \up0 \expn
dtw-2\charscalex100 esencial es la desinfeccin de los mismos para permitir su uso

agrcola. \par\pard\ql \li1133\sb0\sl-276\slmult0 \par\pard\ql\li1133\sb8\sl-276\
slmult0 \up0 \expndtw0\charscalex100 2.6. Plasma no trmico \par\pard\qj \li1133\s
b0\sl-276\slmult0 \par\pard\qj\li1133\ri1485\sb8\sl-276\slmult0\fi566 \up0 \expn
dtw-2\charscalex100 El plasma es considerado el cuarto estado de la materia que
contiene iones y electrones \line \up0 \expndtw0\charscalex103 libres (gas elctri
co). El plasma puede generarse, en forma no trmica, por una descarga \line \up0 \
expndtw0\charscalex100 elctrica o bombardeo de un gas con un haz de electrones de
alta energa; la energa de los \line \up0 \expndtw0\charscalex103 electrones en el
plasma es de unos 10 eV, lo que equivale a temperaturas elevadas. Estos \line \
up0 \expndtw0\charscalex102 plasmas son buenas fuentes de especies reactivas alt
amente reductoras y oxidantes, como \line \up0 \expndtw-3\charscalex100 O(\ul0\s
uper\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 P), HO\ul0\super\cf3\f4\fs24 \u822
6?\ul0\nosupersub\cf2\f3\fs24 , N, H, NH, CH, O\ul0\sub\cf3\f4\fs24 3\ul0\nosupe
rsub\cf2\f3\fs24 , O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 (\ul0\supe
r\cf3\f4\fs24 1\ul0\nosupersub\cf2\f3\fs24 \u8710?), los propios electrones de p
lasma, etc. La presencia de \line \up0 \expndtw-3\charscalex100 estas especies p
ermite la utilizacin del mtodo en mltiples aplicaciones: remocin de SO\ul0\sub\cf3\f
4\fs24 x\ul0\nosupersub\cf2\f3\fs24 y \line \up0 \expndtw-3\charscalex100 NO\ul
0\sub\cf3\f4\fs24 x\ul0\nosupersub\cf2\f3\fs24 de gases de escape, descomposicin
de hidrocarburos alifticos y alifticos halogenados, \line \up0 \expndtw-3\charsca
lex100 tratamiento de gases de salida industriales y de incineradores, tratamien
to de VOCs en suelos \line \up0 \expndtw-3\charscalex100 y aguas subterrneas (pre
via transferencia a la fase vapor por bombeo), tratamiento de slidos \line \up0 \
expndtw-3\charscalex100 contaminados con VOCs (previa aplicacin de calor y fluidi
zacin en un gas inerte), etc. [40]. \par\pard\qj \li1133\ri1502\sb1\sl-280\slmult
0\fi566 \up0 \expndtw-2\charscalex100 La tcnica no genera subproductos txicos, com
o dioxinas o furanos, opera a presiones \line \up0 \expndtw-3\charscalex100 y t
emperaturas cercanas a la ambiente, no requiere combustible \up0 \expndtw
-3\charscalex100 (minimiza residuos \par\pard\qj \li1133\ri1488\sb6\sl-273\slmu
lt0 \up0 \expndtw0\charscalex100 secundarios), y puede eliminar simultneamente or
gnicos peligrosos y emisiones del tipo \up0 \expndtw0\charscalex100 SO\ul0\sub\cf
3\f4\fs24 x\ul0\nosupersub\cf2\f3\fs24 /NO\ul0\sub\cf3\f4\fs24 x\ul0\nosupersub\
cf2\f3\fs24 , No requiere catalizadores. Existen facilidades a gran escala en Eu
ropa que usan \up0 \expndtw0\charscalex102 generadores de plasma de distintos ti
pos: de barrera dielctrica, corona pulsado, de lecho \up0 \expndtw-3\charscalex10
0 electrificado empaquetado, de haces de electrones, etc. [40]. \par\pard\ql \li
1133\sb0\sl-276\slmult0 \par\pard\ql\li1133\sb9\sl-276\slmult0 \up0 \expndtw0\ch
arscalex101 2.7. Descarga electrohidrulica - Ultrasonido \par\pard\ql \li1700\sb2
64\sl-276\slmult0\tx6796\tx7231 \up0 \expndtw0\charscalex104 Esta tecnologa usa u
ltrasonido de alta potencia \tab \up0 \expndtw-3\charscalex100 (de \tab \up0 \ex
pndtw0\charscalex111 15 kHz hasta 1 MHz), y se \par\pard\qj \li1133\ri1499\sb4\s
l-276\slmult0 \up0 \expndtw0\charscalex103 aprovecha la cavitacin electrohidrulica
, es decir, el crecimiento y colapsado cclico de \line \up0 \expndtw0\charscalex1
03 burbujas de gas. El gas implota y se alcanzan temperaturas y presiones locale
s muy altas \line \up0 \expndtw0\charscalex105 (4.000-10.000 K y 1.000-10.000 ba
rios en el centro de las burbujas colapsadas) [3]. La \line \up0 \expndtw-2\char
scalex100 degradacin de materia orgnica por sonlisis ocurre a travs de tres procesos
: reacciones de \line \up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\
nosupersub\cf2\f3\fs24 O supercrtica (vase 2.8), pirlisis directa, y reacciones con
los radicales generados por la \line \up0 \expndtw-3\charscalex100 reaccin trmica
(29), o por las reacciones (31)-(33) en presencia de oxgeno. La reaccin \par\pard
\qj \li1133\ri1503\sb21\sl-280\slmult0 \up0 \expndtw0\charscalex100 (30) muestra
la formacin de perxido de hidrgeno que, junto con el HO\ul0\super\cf3\f4\fs24 \u82
26?\ul0\nosupersub\cf2\f3\fs24 , es un oxidante \line \up0 \expndtw-5\charscalex
100 til. \par\pard\li1133\sb203\sl-276\slmult0\fi0\tx1740\tx9773 \up0 \expndtw-4\
charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\tab \dn2 \exp
ndtw-4\charscalex100 \u8594?
H\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\c
f2\f3\fs24 + HO\ul0\super\cf3\f4\fs24 \u8226?\tab \up0 \expndtw-5\charscalex1
00 \ul0\nosupersub\cf2\f3\fs24 (29)\par\pard\li1133\sb137\sl-276\slmult0\fi0\tx1
853\tx9773 \up0 \expndtw-4\charscalex100 2HO\ul0\super\cf3\f4\fs24 \u8226?\tab \

up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
H\ul0\sub\cf
3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw
-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (30)\par\pard\li1133\sb139\sl-276\s
lmult0\fi0\tx1568\tx9773 \up0 \expndtw-4\charscalex100 O\ul0\sub\cf3\f4\fs24 2\t
ab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
2 O\ul0\
super\cf3\f4\fs24 \u8226?\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\
f3\fs24 (31)\par\pard\li1133\sb137\sl-276\slmult0\fi0\tx2189\tx9773 \up0 \expndt
w-4\charscalex100 H\ul0\nosupersub\cf3\f4\fs16 \u8226?\ul0\nosupersub\cf2\f3\fs2
4 + O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub
\cf2\f3\fs24 \u8594?
HO\ul0\sub\cf3\f4\fs24 2\u8226?\tab \up0 \expndtw-5\char
scalex100 \ul0\nosupersub\cf2\f3\fs24 (32)\par\pard\li1133\sb199\sl-276\slmult0\
fi0\tx2189\tx9773 \up0 \expndtw-4\charscalex100 H\ul0\nosupersub\cf3\f4\fs16 \u8
226?\ul0\nosupersub\cf2\f3\fs24 + O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-4
\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
HO\ul0\super\cf3\f4\fs24 \
u8226?\ul0\nosupersub\cf2\f3\fs24 + O\ul0\super\cf3\f4\fs24 \u8226?\tab \up0
\expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (33)\par\pard\qj \li1133\ri
1501\sb110\sl-275\slmult0\fi566 \up0 \expndtw0\charscalex100 La tcnica es econmica
mente competitiva y simple, y la degradacin se completa en \line \up0 \expndtw-3\
charscalex100 tiempos breves (minutos a horas) [41]. El mtodo es muy bueno para t
ratar sustratos voltiles, \line \up0 \expndtw-2\charscalex100 ya que la combustin
se realiza directamente dentro de las burbujas calientes colapsantes. Se \line \
up0 \expndtw0\charscalex106 aplic para abstraer el cloro de clorobenceno y m-dic
lorobenceno, para descomponer \line \up0 \expndtw-3\charscalex100 hidrocarburos
alifticos y alifticos clorados (CCl\ul0\sub\cf3\f4\fs24 4\ul0\nosupersub\cf2\f3\fs
24 , CHCl\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 ), para degradar p-ni
trofenol, TNT, \par\pard\sect\sectd\fs24\paperw11900\paperh16840\pard\sb0\sl-240
{\bkmkstart Pg11}{\bkmkend Pg11}\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1
702\sb0\sl-230\slmult0\par\pard\li1702\sb19\sl-230\slmult0\fi0\tx10500 \up0 \exp
ndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Procesos avanzados de oxidacin p
ara la eliminacin de contaminantes\tab \up0 \expndtw-1\charscalex100 13\par\pard\
qj \li1702\sb0\sl-280\slmult0 \par\pard\qj\li1702\sb0\sl-280\slmult0 \par\pard\q
j\li1702\ri923\sb180\sl-280\slmult0 \up0 \expndtw0\charscalex105 \ul0\nosupersub
\cf2\f3\fs24 para descomponer y decolorar colorantes azo, para degradar Tritn X-1
00 y surfactantes \up0 \expndtw0\charscalex100 relacionados, para descomponer to
talmente H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 S, paratin, para degr
adar ter metilterbutilco \up0 \expndtw0\charscalex100 (MTBE), etc. Puede mejorarse
por agregado de H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf
3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\
cf2\f3\fs24 Fe(II), y por eliminacin de O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\c
f2\f3\fs24 y \up0 \expndtw-1\charscalex100 operacin en atmsfera inerte (Ar). \par
\pard\qj \li1702\ri933\sb0\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex106 Se
ha descrito recientemente la degradacin de surfactantes [42], de azobenceno y \li
ne \up0 \expndtw0\charscalex100 colorantes relacionados \up0 \expndtw0\charscale
x106 (incluyendo el aumento de eficiencia a travs de reacciones de \par\pard\qj \
li1702\ri933\sb0\sl-280\slmult0 \up0 \expndtw0\charscalex104 Fenton) [41] y los
efectos sinrgicos de la sonlisis combinada con la ozonlisis para la \up0 \expndtw0\
charscalex105 oxidacin de azobenceno y naranja de metilo [43]. Este ltimo procedim
iento (proceso \up0 \expndtw0\charscalex102 \u8220?sonozono\u8221?) aumenta no
tablemente la velocidad de transformacin. El aumento del \up0 \expndtw0\ch
arscalex100 coeficiente de transferencia de masa del O\ul0\sub\cf3\f4\fs24 3\ul0
\nosupersub\cf2\f3\fs24 debido a efectos mecnicos (mayor mezclado y \up0 \expndt
w0\charscalex100 ruptura de las burbujas de gas), favorece la disolucin del O\ul0
\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 en agua, y la descomposicin \up0 \
expndtw0\charscalex109 trmica de ozono en burbujas colapsantes parece ser el prin
cipal mecanismo para la \up0 \expndtw-5\charscalex100 destruccin de contaminantes
, a travs de la generacin de HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f
3\fs24 [44]. \par\pard\li1702\sb183\sl-276\slmult0\fi0\tx2136\tx10341 \up0 \exp
ndtw-4\charscalex100 O\ul0\sub\cf3\f4\fs24 3\tab \dn2 \expndtw-5\charscalex100 \
ul0\nosupersub\cf2\f3\fs24 \u8594?
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2
\f3\fs24 + O(\ul0\super\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 P)\tab \up0

\expndtw-5\charscalex100 (34)\par\pard\li1702\sb139\sl-276\slmult0\fi0\tx3231\tx
10342 \up0 \expndtw-5\charscalex100 O(\ul0\super\cf3\f4\fs24 3\ul0\nosupersub\cf
2\f3\fs24 P) + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\tab \up0 \
expndtw-5\charscalex100 \u8594?
2 HO\ul0\super\cf3\f4\fs24 \u8226?\tab \up0 \
expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (35)\par\pard\ql \li1702\sb1
70\sl-276\slmult0 \up0 \expndtw0\charscalex101 2.8. Oxidacin en agua sub/y superc
rtica \par\pard\qj \li1702\sb0\sl-273\slmult0 \par\pard\qj\li1702\ri930\sb14\sl-2
73\slmult0\fi566 \up0 \expndtw0\charscalex100 Estas tcnicas permiten la oxidacin d
e los contaminantes en una mezcla en agua con \line \up0 \expndtw-3\charscalex10
0 oxgeno o aire, a altas presiones y temperaturas [45-47]. El proceso que opera e
n condiciones \line \up0 \expndtw0\charscalex100 subcrticas es llamado tambin oxid
acin en aire hmedo (Wet Air Oxidation o WAO); se \line \up0 \expndtw0\charscalex10
0 trabaja a presiones entre \up0 \expndtw0\charscalex100 10-220 barios y tempera
turas entre 150-370 \ul0\super\cf3\f4\fs24 \ul0\nosupersub\cf2\f3\fs24 C. El meca
nismo \par\pard\qj \li1702\ri932\sb30\sl-270\slmult0 \up0 \expndtw-4\charscalex1
00 involucra la carbonizacin primaria de los sustratos orgnicos y su posterior rea
ccin con HO\ul0\super\cf3\f4\fs24 \u8226? \line \up0 \expndtw0\charscalex109 \ul0
\nosupersub\cf2\f3\fs24 producidos en la transformacin cataltica del O\ul0\sub\cf3
\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 disuelto en la superficie del centro \lin
e \up0 \expndtw-1\charscalex100 carbonoso, ecuaciones \up0 \expndtw0\charscalex1
09 (36)-(37). El nitrgeno, los halgenos y el azufre son tambin \par\pard\qj \li1702
\ri929\sb2\sl-280\slmult0 \up0 \expndtw0\charscalex100 mineralizados, ecuaciones
(38)-(40). La ecuacin (41) muestra el origen de los principales \up0 \expndtw0\c
harscalex100 subproductos. \par\pard\li1702\sb206\sl-276\slmult0\fi0\tx2136\tx10
342 \up0 \expndtw-5\charscalex100 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-6\ch
arscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
H\ul0\sub\cf3\f4\fs24 2\ul0\n
osupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
\u8
594?
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 y HO\ul0\super\cf3\f
4\fs24 \u8226?\tab \up0 \expndtw-6\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (36
)\par\pard\li1702\sb137\sl-276\slmult0\fi0\tx2837\tx10342 \up0 \expndtw-6\charsc
alex100 HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + C\tab \
up0 \expndtw-6\charscalex100 \u8594?
CO\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\
cf2\f3\fs24 + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\tab \up0 \
expndtw-6\charscalex100 (37)\par\pard\li1702\sb141\sl-276\slmult0\fi0\tx10342 \u
p0 \expndtw-6\charscalex100 N
\u8594? NH\ul0\sub\cf3\f4\fs24 3\ul0\nosupersu
b\cf2\f3\fs24 , NO\ul0\sub\cf3\f4\fs24 3-\ul0\nosupersub\cf2\f3\fs24 N elementa
l\tab \up0 \expndtw-6\charscalex100 (38)\par\pard\li1702\sb137\sl-276\slmult0\fi
0\tx10342 \up0 \expndtw-6\charscalex100 X
\u8594?
X\tab \up0 \expndtw-6\ch
arscalex100 (39)\par\pard\li1702\sb137\sl-276\slmult0\fi0\tx2016\tx10342 \up0 \e
xpndtw-6\charscalex100 S\tab \dn2 \expndtw-6\charscalex100 \u8594?
SO\ul0\sub
\cf3\f4\fs24 42-\tab \up0 \expndtw-6\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (
40)\par\pard\li1702\sb139\sl-276\slmult0\fi0\tx10343 \up0 \expndtw-6\charscalex1
00 C + HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24
\u8594?
cidos orgnicos de bajo peso molecular\tab \up0 \expndtw-6\charscalex100 (41)\p
ar\pard\qj \li1702\ri932\sb171\sl-276\slmult0\fi566 \up0 \expndtw-4\charscalex10
0 El proceso puede autosoportarse si se oxidan residuos de 20.000 mg/L; en compa
racin, \line \up0 \expndtw-2\charscalex100 la incineracin requiere para ello resid
uos de entre 300.000 y 400.000 mg/L [48]. El proceso \line \up0 \expndtw-2\chars
calex100 ya ha sido comercializado, y en 1995 existan unos 200 procesos WAO opera
tivos en todo el \line \up0 \expndtw0\charscalex100 mundo. El agregado de un oxi
dante como O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , H\ul0\sub\cf3\f4
\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3
\fs24 o persulfato de potasio [45] mejora la \line \up0 \expndtw-1\charscalex10
0 eficiencia. Se puede tratar cualquier tipo de residuo, incluyendo barros, resi
duos acuosos de \line \up0 \expndtw0\charscalex100 alto DQO, residuos no biotrat
ables, barros cloacales municipales, residuos de destilera, de \line \up0 \expndt
w-3\charscalex100 pulpa de papel, \u8220?black liquor\u8221? de aguas textiles,
residuos acuosos con CN\ul0\super\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 y ni
trilos, residuos \line \up0 \expndtw-2\charscalex100 adsorbidos sobre el carbn us
ado en tratamientos de efluentes (para su regeneracin), etc. Se \line \up0 \expnd

tw0\charscalex103 pueden destruir polifenoles, perclorofenoles, compuestos alifti
cos y policloroalifticos, \line \up0 \expndtw0\charscalex102 hidrocarburos aromtic
os (tolueno, pireno y sustituidos con grupos no halogenados), y el \line \up0 \e
xpndtw0\charscalex102 mtodo es excelente para la destruccin de hidratos de carbono
. En contraste con la \par\pard\sect\sectd\fs24\paperw11900\paperh16840{\shp
z-10000\shplid11
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5001451450014514500145145001451450014514500145145001451450014573daef8bbc29e1736c
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0b2f0e7ff2ca803d028af3ff00f85b3f0aff00e8a5fc3fff00c2cbc39ffcb2a3fe16cfc2bffa297f
0fff00f0b2f0e7ff002ca803d028af3fff0085b3f0affe8a5fc3ff00fc2cbc39ff00cb2a3fe16cfc
2bff00a297f0ff00ff000b2f0e7ff2ca803d028af3ff00f85b3f0aff00e8a5fc3fff00c2cbc39ffc
b2a3fe16cfc2bffa297f0fff00f0b2f0e7ff002ca803d028af3fff0085b3f0affe8a5fc3ff00fc2c
bc39ff00cb2a3fe16cfc2bff00a297f0ff00ff000b2f0e7ff2ca803d028af3ff00f85b3f0aff00e8
a5fc3fff00c2cbc39ffcb2ab169f13be1b5fdddb58587c42f03dedf5edc4369676769e2cd06e6eee
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07e407fc381ffe08dbff0048f6f801ff00828d77ff0097d47fc381ff00e08dbff48f6f801ff828d7
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8ef01f8afc31e38f087ec19f02741f167833c43a2f8afc2fae59e91acfdb346f11787752b6d5f44d
56d7ced6e587ed3a76a5676d79079b1491f9b0af991bae54feaf5140051451400514514005145140
05145140051451400514514005145140051451400514514005145140051451400514514005145140
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05145140051451400514514005145140051451400514514005145140051451400514514005145140
05145140051451401fffd9}}}}}\pard\sb0\sl-240{\bkmkstart Pg12}{\bkmkend Pg12}\par\
pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li113
3\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\c
f4\f5\fs20 14\tab \up0 \expndtw-2\charscalex100 Domnech, Jardim y Litter\par\pard
\qj \li1133\sb0\sl-280\slmult0 \par\pard\qj\li1133\sb0\sl-280\slmult0 \par\pard\
qj\li1133\ri1499\sb181\sl-280\slmult0 \up0 \expndtw0\charscalex106 \ul0\nosupers
ub\cf2\f3\fs24 incineracin, hay poca interaccin con el ambiente y puede acoplarse
fcilmente con un \up0 \expndtw-3\charscalex100 tratamiento biolgico. \par\pard\qj
\li1133\ri1500\sb6\sl-273\slmult0\fi566 \up0 \expndtw0\charscalex102 Entre los i
nconvenientes, se debe mencionar que la mineralizacin es incompleta por \line \up
0 \expndtw0\charscalex104 formacin de cidos carboxlicos de bajo PM, alcoholes, alde
hdos o cetonas. Los cidos \line \up0 \expndtw0\charscalex102 actico y propinico son
muy resistentes y requieren catalizadores para su destruccin, y lo \line \up0 \ex
pndtw0\charscalex102 mismo ocurre con los compuestos aromticos halogenados \up0 \
expndtw0\charscalex102 (1,2-dihalobencenos, PCBs, \par\pard\qj \li1133\ri1491\sb
2\sl-280\slmult0 \up0 \expndtw0\charscalex100 perclorofenoles). La solubilidad d
el O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 en agua genera problemas
de transferencia de masa, \up0 \expndtw0\charscalex102 que pueden limitar su efi
ciencia. Su mayor desventaja es el requerimiento de materiales de \up0 \expndtw3\charscalex100 construccin muy caros. \par\pard\qj \li1133\ri1484\sb0\sl-280\slm
ult0\fi566 \up0 \expndtw0\charscalex106 El proceso conocido como Oxidacin en Aire
Hmedo Catalizada (CWAO) [46] \up0 \expndtw-1\charscalex100 (Figura 3) usa catali
zadores homogneos y heterogneos, para mejorar la eficiencia. Se han \up0 \expndtw3\charscalex100 usado como catalizadores sales de Cu(II) disueltas homogneamente,
Cu/carbn activado, Cu \up0 \expndtw-3\charscalex100 soportado en \u947? almina, c
ompuestos de Mn(V) y de Cr activado, Co/Bi, Mn/Cu, MnO\ul0\sub\cf3\f4\fs24 2\ul0
\nosupersub\cf2\f3\fs24 , CuO, \up0 \expndtw0\charscalex105 Fe\ul0\sub\cf3\f4\fs
24 , xidos de Zn. Los mejores resultados se obtuvieron con catalizadores de Pd-Pt
-\line \up0 \expndtw0\charscalex102 Ce/almina. El principal problema de esta tcnic
a es precisamente la separacin final del \up0 \expndtw-3\charscalex100 catalizado
r. El mtodo puede mejorarse con inyeccin de Fe\ul0\super\cf3\f4\fs24 2+\ul0\nosupe
rsub\cf2\f3\fs24 /H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\c
f3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 . \par\pard\qj \li1133\sb0\sl-240\slmult
0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0
\par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \p
ar\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par
\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\p
ard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\par
d\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\
qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj
\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\l
i1133\ri1534\sb74\sl-240\slmult0 \up0 \expndtw0\charscalex108 \ul0\nosupersub\cf
4\f5\fs20 Figura 3. Mejoramiento de tratamientos WAO para la oxidacin de cido p-cu
mrico por agregado de \up0 \expndtw0\charscalex100 catalizadores [49]. \par\pard\
qj \li1133\ri1501\sb212\sl-275\slmult0\fi566 \up0 \expndtw0\charscalex100 \ul0\n

osupersub\cf2\f3\fs24 La oxidacin con agua supercrtica o mtodo OXAS [47] usa agua e
n condiciones de \line \up0 \expndtw0\charscalex100 presin y temperatura superior
es que las del punto crtico\ul0\super\cf3\f4\fs24 1\ul0\nosupersub\cf2\f3\fs24 ,
entre 450 y 700 C y presiones \line \up0 \expndtw0\charscalex103 cercanas a los 2
5 MPa. En estado supercrtico, el agua se comporta como un fluido cuya \line \up0
\expndtw0\charscalex100 viscosidad, densidad y constante dielctrica son rel
ativamente bajas. En condiciones \line \up0 \expndtw-1\charscalex100 supercrti
cas, disminuye el nmero de uniones puente hidrgeno, aumenta la solubilidad de \lin
e \up0 \expndtw0\charscalex100 los compuestos orgnicos y gases y disminuye la sol
ubilidad de los electrolitos. Por ello, el \line \up0 \expndtw0\charscalex100 OX
AS posee caractersticas que lo llevan a ser un excepcional sistema de tratamiento
, con \line \up0 \expndtw0\charscalex102 una eficiencia de oxidacin mayor que 99,
99% en tiempos de contacto muy breves (5-60 \line \up0 \expndtw-3\charscalex100
segundos), que no requiere ningn tratamiento adicional de los productos gaseosos.
Debido a \line \up0 \expndtw0\charscalex100 la alta solubilidad del O\ul0\sub\c
f3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 en el agua supercrtica, no existen probl
emas de transferencia de \line \up0 \expndtw-3\charscalex100 masa. Como adems la
tensin superficial es nula, el O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
penetra en los poros ms pequeos y \line \up0 \expndtw-2\charscalex100 puede oxid
ar cualquier sustancia orgnica. Por otra parte, es posible remover los compuestos
\line \up0 \expndtw0\charscalex103 inorgnicos por precipitacin. El proceso puede
autoabastecerse en energa si se queman \line \up0 \expndtw-1\charscalex100 compue
stos orgnicos de concentraciones superiores al 5%, y se puede recuperar el calor
de \line \up0 \expndtw-1\charscalex100 combustin como calor de proceso a alta tem
peratura o potencia. No hay formacin \par\pard\ql \li1133\sb0\sl-230\slmult0 \par
\pard\ql\li1133\sb113\sl-230\slmult0 \up0 \expndtw-3\charscalex100 \ul0\super\cf
5\f6\fs20\ul0\super\cf5\f6\fs19 1\ul0\nosupersub\cf4\f5\fs20 Puntos crticos del
agua: T\ul0\sub\cf5\f6\fs19 c\ul0\nosupersub\cf4\f5\fs20 = 374 C y P\ul0\sub\cf5
\f6\fs19 c\ul0\nosupersub\cf4\f5\fs20 = 22.1 Mpa. \par\pard\sect\sectd\fs24\pap
erw11900\paperh16840\pard\sb0\sl-240{\bkmkstart Pg13}{\bkmkend Pg13}\par\pard\li
1702\sb0\sl-230\slmult0\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb19\
sl-230\slmult0\fi0\tx10500 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\
fs20 Procesos avanzados de oxidacin para la eliminacin de contaminantes\tab \up0 \
expndtw-1\charscalex100 15\par\pard\qj \li1702\sb0\sl-280\slmult0 \par\pard\qj\l
i1702\sb0\sl-280\slmult0 \par\pard\qj\li1702\ri919\sb180\sl-280\slmult0 \up0 \ex
pndtw0\charscalex100 \ul0\nosupersub\cf2\f3\fs24 apreciable de NO\ul0\sub\cf3\f4
\fs24 x\ul0\nosupersub\cf2\f3\fs24 , SO\ul0\sub\cf3\f4\fs24 x\ul0\nosupersub\cf2
\f3\fs24 u O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 . En contraposicin
, el proceso requiere condiciones severas de \up0 \expndtw-2\charscalex100 opera
cin; es adems poco atractivo para aguas diluidas, y se pueden producir dibenzofura
nos \up0 \expndtw0\charscalex104 y dioxinas. Al igual que el WAO, necesita mater
iales de construccin especiales para alta \up0 \expndtw-3\charscalex100 temperatu
ra y presiones, de alto coste. \par\pard\qj \li1702\ri923\sb104\sl-276\slmult0\f
i566 \up0 \expndtw0\charscalex100 Se puede aplicar OXAS al tratamiento de residu
os orgnicos convencionales acuosos, \up0 \expndtw0\charscalex104 barros, solvente
s clorados y nitrogenados, plaguicidas y herbicidas clorados, fosforados y \up0
\expndtw0\charscalex104 nitrogenados, PCBs, colorantes, plastificantes, mate
riales plsticos, subproductos de la \up0 \expndtw-2\charscalex100 industria qumica
y farmacutica, productos militares como explosivos, propelentes o gases de \up0
\expndtw0\charscalex100 guerra, etc. Es altamente promisorio para residuos pelig
rosos. En la Argentina, el proceso se \up0 \expndtw-1\charscalex100 encuentra de
sarrollado a nivel de laboratorio. \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\
pard\ql\li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb12\sl-276\slmult0 \up0 \
expndtw0\charscalex103 3. TECNOLOGAS FOTOQUMICAS \par\pard\qj \li1702\ri931\sb261\
sl-280\slmult0\fi566 \up0 \expndtw0\charscalex103 La discusin de las tecnologas no
fotoqumicas debe haber dejado en claro que las \up0 \expndtw0\charscalex102 mism
as proveen una amplia batera de mtodos, cada uno de los cuales tiene una serie de
\up0 \expndtw0\charscalex100 capacidades y de limitaciones. La excelente capacid
ad de los radicales hidroxilo de oxidar \up0 \expndtw-1\charscalex100 compuestos
orgnicos sugiere tambin la utilidad de explorar su generacin fotoqumica. El \up0 \e

xpndtw-3\charscalex100 Cuadro III muestra que el uso de luz proporciona ciertas
ventajas en el tratamiento de aguas y \up0 \expndtw-4\charscalex100 efluentes, q
ue no se limitan al aprovechamiento del HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nos
upersub\cf2\f3\fs24 como oxidante. \par\pard\ql \li4119\sb0\sl-230\slmult0 \par
\pard\ql\li4119\sb92\sl-230\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersu
b\cf4\f5\fs20 Cuadro III: Ventajas de las tecnologas fotoqumicas. \par\pard\ql \li
1882\ri1103\sb14\sl-250\slmult0\tx2240\tx2240\tx2240\tx2240 \up0 \expndtw-2\char
scalex100 \u8226? En algunos casos, es posible utilizar los procesos fotolticos
directos, sin el agregado de reactivo qumico \line\tab \up0 \expndtw-3\charscale
x100 alguno. Este proceso es importante para compuestos que reaccionan lentament
e con HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf4\f5\fs20 . La destruccin
\line \tab \up0 \expndtw-3\charscalex100 de compuestos orgnicos clorados tales c
omo trihalometanos (THM), clorometanos, cloroetanos, \line \tab \up0 \expndtw-3\
charscalex100 aromticos y fenoles mediante el uso de irradiacin de 254 nm se halla
bien documentada en la literatura \line \tab \up0 \expndtw-4\charscalex100 [2,
5]. \par\pard\qj \li1882\ri1034\sb75\sl-220\slmult0\tx2240 \up0 \expndtw-2\chars
calex100 \u8226? Evita el uso de O\ul0\sub\cf5\f6\fs19 3\ul0\nosupersub\cf4\f5
\fs20 o reduce su proporcin, con la consiguiente reduccin de costos, riesgos para
la salud y \line\tab \up0 \expndtw-4\charscalex100 preocupaciones ambientales.
\par\pard\qj \li1882\ri1150\sb100\sl-220\slmult0\tx2240 \up0 \expndtw-2\charscal
ex100 \u8226? Aumenta la velocidad de reaccin en comparacin con la misma tcnica e
n ausencia de luz. Esto evita el \line\tab \up0 \expndtw-2\charscalex100 uso de
tanques grandes y hace ms compactos a los sistemas de tratamiento. \par\pard\ql \
li1882\sb72\sl-230\slmult0 \up0 \expndtw-2\charscalex100 \u8226? Evita cambios
de pH drsticos (por ejemplo, el O\ul0\sub\cf5\f6\fs19 3\ul0\nosupersub\cf4\f5\fs
20 necesita pH altos, como ya se ha visto). \par\pard\qj \li1882\ri1161\sb99\sl
-220\slmult0\tx2240 \up0 \expndtw-2\charscalex100 \u8226? Aumenta la flexibili
dad del sistema ya que permite el uso de una variedad de oxidantes y condiciones
de \line\tab \up0 \expndtw-3\charscalex100 operabilidad. \par\pard\ql \li1882\s
b72\sl-230\slmult0 \up0 \expndtw-1\charscalex100 \u8226? Reduce costos operati
vos debido a un menor consumo de potencia para generar HO\ul0\super\cf5\f6\fs19
\u8226?\ul0\nosupersub\cf4\f5\fs20 . \par\pard\qj \li1702\sb0\sl-280\slmult0 \pa
r\pard\qj\li1702\ri931\sb29\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex106 \u
l0\nosupersub\cf2\f3\fs24 La eficiencia de la destruccin fotoqumica de un determin
ado compuesto puede \line \up0 \expndtw0\charscalex106 alterarse drsticamente en
funcin del diseo del reactor \up0 \expndtw0\charscalex106 (tipo de lmpara, geometra,
\par\pard\qj \li1702\ri913\sb0\sl-280\slmult0 \up0 \expndtw0\charscalex102 hidr
odinmica, etc.), lo que incide sobre el consumo de energa elctrica y los costos. La
s \up0 \expndtw0\charscalex100 TAOs mediadas por luz no son adecuadas para proce
sar mezclas de sustancias de elevada \up0 \expndtw0\charscalex107 absortividad,
o con altos tenores de slidos en suspensin, pues la eficiencia cuntica \up0 \expndt
w-2\charscalex100 disminuye por prdida de luz, por dispersin y/o absorcin competiti
va. \par\pard\ql \li1702\sb264\sl-276\slmult0 \up0 \expndtw-1\charscalex100 3.1.
Fotlisis del agua en el ultravioleta de vaco (UVV) \par\pard\qj \li1702\ri933\sb2
61\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex100 Este proceso aprovecha la i
rradiacin a longitudes de onda menores que la UV-C, es \line \up0 \expndtw-3\char
scalex100 decir, ms bajas que 190 nm, y usa generalmente lmparas de excmeros de Xe
(\u955? = 172 nm). \line \up0 \expndtw-2\charscalex100 La excitacin bajo estas lo
ngitudes de onda conduce, en la mayora de los casos, a la ruptura \line \up0 \exp
ndtw-4\charscalex100 homoltica de uniones qumicas, y puede producir la degradacin d
e materia orgnica en fases \line \up0 \expndtw-4\charscalex100 condensadas y gase
osas (por ejemplo, hidrocarburos fluorados y clorados) [2,4]. Sin embargo,
}
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d9}}}}}\pard\sb0\sl-240{\bkmkstart Pg14}{\bkmkend Pg14}\par\pard\li1133\sb0\sl-2
0\fi0\tx8050 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs20 16\tab \u
p0 \expndtw-2\charscalex100 Domnech, Jardim y Litter\par\pard\qj \li1133\sb0\sl-2
80\slmult0 \par\pard\qj\li1133\sb0\sl-280\slmult0 \par\pard\qj\li1133\ri1501\sb1
81\sl-280\slmult0 \up0 \expndtw0\charscalex109 \ul0\nosupersub\cf2\f3\fs24 el us
o ms importante de la radiacin VUV es la fotlisis del agua (ecuacin (29)) en \up0 \e
xpndtw0\charscalex102 presencia de luz), que produce radicales hidroxilo y tomos
de hidrgeno con rendimientos \up0 \expndtw-1\charscalex100 cunticos dependientes d
e la longitud de onda de irradiacin (por ejemplo 0,30 y 0,70 a 185 y \up0 \expndt
w-2\charscalex100 147 nm respectivamente) [50]: \par\pard\li1133\sb204\sl-276\sl
mult0\fi0\tx9773 \dn2 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosup
ersub\cf2\f3\fs24 O + h\u957? \u8594? HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nos
upersub\cf2\f3\fs24 + H\ul0\super\cf3\f4\fs24 \u8226?\tab \up0 \expndtw-3\chars
calex100 \ul0\nosupersub\cf2\f3\fs24 (29)\par\pard\li1133\sb176\sl-276\slmult0\f
i708 \up0 \expndtw-2\charscalex100 Tambin se producen electrones acuosos, pero co
n bajos rendimientos cunticos:\par\pard\li1133\sb201\sl-276\slmult0\fi0\tx2362\tx
5093\tx9773 \up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub
\cf2\f3\fs24 O + h\u957?\tab \up0 \expndtw-3\charscalex100 \u8594?
HO\ul0\s
uper\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + H\ul0\super\cf3\f4\fs24
+\ul0\nosupersub\cf2\f3\fs24 + e\ul0\super\cf3\f4\fs24 -aq\tab \up0 \expndtw
-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 ; \u966?\ul0\sub\cf3\f4\fs24 185 nm
\ul0\nosupersub\cf2\f3\fs24 = 0.04\tab \up0 \expndtw-3\charscalex100 (42)\par\p
ard\li1133\sb197\sl-276\slmult0\fi708 \up0 \expndtw-2\charscalex100 A partir de
los radicales primarios se generan rpidamente HO\ul0\sub\cf3\f4\fs24 2\u8226?\ul0
\nosupersub\cf2\f3\fs24 y O\ul0\sub\cf3\f4\fs24 2\u8226?-\ul0\nosupersub\cf2\f3
\fs24 :\par\pard\li1133\sb197\sl-276\slmult0\fi0\tx2249\tx5093\tx9773 \up0 \expn
dtw-3\charscalex100 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + H\ul
0\super\cf3\f4\fs24 \u8226?\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf
2\f3\fs24 \u8594?
HO\ul0\sub\cf3\f4\fs24 2\u8226?\tab \up0 \expndtw-3\charsc
alex100 \ul0\nosupersub\cf2\f3\fs24 ; k\ul0\sub\cf3\f4\fs24 HO2\u8226?\ul0\nosup
ersub\cf2\f3\fs24 = 1 10\ul0\super\cf3\f4\fs24 10\ul0\nosupersub\cf2\f3\fs24 M
\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\fs24 s\ul0\super\cf3\f4\fs24 -1

\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (43)\par\pard\li1
133\sb139\sl-276\slmult0\fi0\tx2295\tx5093\tx9773 \up0 \expndtw-3\charscalex100
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + e\ul0\super\cf3\f4\fs24
-aq\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594? O\ul0
\sub\cf3\f4\fs24 2\u8226?\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\
f3\fs24 ; k\ul0\sub\cf3\f4\fs24 O2\u8226?-\ul0\nosupersub\cf2\f3\fs24 = 2 10\ul
0\super\cf3\f4\fs24 10\ul0\nosupersub\cf2\f3\fs24 M\ul0\super\cf3\f4\fs24 -1\ul
0\nosupersub\cf2\f3\fs24 s\ul0\super\cf3\f4\fs24 -1\tab \up0 \expndtw-3\charsca
lex100 \ul0\nosupersub\cf2\f3\fs24 (44)\par\pard\qj \li1133\ri1478\sb196\sl-274\
slmult0\fi566 \up0 \expndtw0\charscalex102 Los oxidantes (HO\ul0\super\cf3\f4\fs
24 \u8226?\ul0\nosupersub\cf2\f3\fs24 , HO\ul0\sub\cf3\f4\fs24 2\u8226?\ul0\nosu
persub\cf2\f3\fs24 , O\ul0\sub\cf3\f4\fs24 2\u8226?-\ul0\nosupersub\cf2\f3\fs24
) y reductores (H\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 , e\u
l0\super\cf3\f4\fs24 -aq\ul0\nosupersub\cf2\f3\fs24 , HO\ul0\sub\cf3\f4\fs24 2\u
8226?\ul0\nosupersub\cf2\f3\fs24 , O\ul0\sub\cf3\f4\fs24 2\u8226?-\ul0\nosupersu
b\cf2\f3\fs24 ) generados pueden \line \up0 \expndtw0\charscalex106 llevar a cab
o simultneamente reducciones y oxidaciones. La tcnica se utiliza para la \line \up
0 \expndtw-3\charscalex100 degradacin de contaminantes en aguas y en corriente de
aire con alto contenido de humedad, \line \up0 \expndtw0\charscalex100 para la
obtencin de agua ultrapura y para el tratamiento de compuestos difciles de oxidar
\line \up0 \expndtw0\charscalex100 (clorados y fluorados como ClCH\ul0\sub\cf3\f
4\fs24 3\ul0\nosupersub\cf2\f3\fs24 ). El proceso posee alta eficiencia por la i
ntensidad de la \line \up0 \expndtw-3\charscalex100 iluminacin y la alta seccin ef
icaz de absorcin del H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O a las l
ongitudes de onda usadas. Por \line \up0 \expndtw0\charscalex104 otra parte, no
es necesario agregar agentes qumicos, y resulta un mtodo competitivo y \line \up0
\expndtw0\charscalex103 simple. Sin embargo requiere el suministro de oxgeno, el
uso de material de cuarzo y la \line \up0 \expndtw-1\charscalex100 provisin de al
ta potencia. La tcnica no est an comercializada, y se encuentra en la etapa \line \
up0 \expndtw0\charscalex102 de desarrollo. Gonzlez y Braun han estudiado diversas
reacciones con esta tcnica, tales \line \up0 \expndtw0\charscalex100 como la fotl
isis de nitrato y nitrito [50-51] y la mineralizacin de la atrazina, un pesticida
\line \up0 \expndtw-2\charscalex100 muy resistente [52]. Los resultados de este
ltimo trabajo se muestran en la Figura 4. \par\pard\ql \li1133\sb0\sl-230\slmult
0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0
\par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \p
ar\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par
\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\p
ard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\par
d\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\
\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\l
i1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1
3\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\
sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb
193\sl-230\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Fig
ura 4. Degradacin de atrazina por fotlisis del agua bajo irradiacin UVV en argn (\u9
675?), aire (\u9679?) y oxgeno \par\pard\ql \li1133\sb30\sl-230\slmult0 \up0 \exp
ndtw-1\charscalex100 (\u9632?); [atrazina]\ul0\sub\cf5\f6\fs19 o\ul0\nosupersub\
cf4\f5\fs20 = 1 10\ul0\super\cf5\f6\fs19 -4\ul0\nosupersub\cf4\f5\fs20 mol L\ul
0\super\cf5\f6\fs19 -1\ul0\nosupersub\cf4\f5\fs20 . \par\pard\sect\sectd\fs24\pa
perw11900\paperh16840\pard\sb0\sl-240{\bkmkstart Pg15}{\bkmkend Pg15}\par\pard\l
i1702\sb0\sl-230\slmult0\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb19
\sl-230\slmult0\fi0\tx10500 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5
\fs20 Procesos avanzados de oxidacin para la eliminacin de contaminantes\tab \up0
\expndtw-1\charscalex100 17\par\pard\ql \li1702\sb0\sl-264\slmult0 \par\pard\ql\
li1702\sb0\sl-264\slmult0 \par\pard\ql\li1702\sb245\sl-264\slmult0 \up0 \expndtw
-1\charscalex100 \ul0\nosupersub\cf2\f3\fs24 3.2. UV/H\ul0\sub\cf3\f4\fs24 2\ul0
\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2 \par\pard\qj \li1702\ri933\sb255

\sl-290\slmult0\fi566 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf2\f3\fs24
El clivaje de la molcula de H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\
ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 por fotones con energa superior
a la de la unin O-\line \up0 \expndtw0\charscalex106 O\ul0\super\cf3\f4\fs24 1\u
l0\nosupersub\cf2\f3\fs24 : tiene un rendimiento cuntico casi unitario (\u966?\ul
0\sub\cf3\f4\fs24 HO\u8226?\ul0\nosupersub\cf2\f3\fs24 = 0,98 a 254 nm), y prod
uce casi \up0 \expndtw-5\charscalex100 cuantitativamente dos HO\ul0\super\cf3\f4
\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 por cada molcula de H\ul0\sub\cf3\f4\fs
24 : \par\pard\li1702\sb214\sl-276\slmult0\fi0\tx10342 \up0 \expndtw-2\charscale
x100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\
ul0\nosupersub\cf2\f3\fs24 + h\u957? \u8594? 2 HO\ul0\super\cf3\f4\fs24 \u822
6?\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (45)\par\pard\q
j \li1702\ri932\sb177\sl-270\slmult0\fi566 \up0 \expndtw-1\charscalex100 La fotli
sis del H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24
2\ul0\nosupersub\cf2\f3\fs24 se realiza casi siempre utilizando lmparas de vapo
r de mercurio \line \up0 \expndtw-3\charscalex100 de baja o media presin. Cerca d
el 50% del consumo energtico se pierde en forma de calor o \line \up0 \expndtw-4\
charscalex100 de emisiones por debajo de \up0 \expndtw-4\charscalex100 185
nm, que son absorbidas por la camisa de cuarzo. \par\pard\qj \li1702\ri9
29\sb2\sl-280\slmult0 \up0 \expndtw-4\charscalex100 Generalmente se usan lmparas
de 254 nm, pero como la absorcin del H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f
3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 es mxima a 220 \up0 \e
xpndtw0\charscalex100 nm, sera ms conveniente el uso de lmparas de Xe/Hg, ms caras,
pero que emiten en el \up0 \expndtw0\charscalex100 rango 210-240 nm. \par\pard\q
j \li1702\ri925\sb144\sl-276\slmult0\fi566 \up0 \expndtw0\charscalex103 Adems del
H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\
nosupersub\cf2\f3\fs24 (\u949? = 18,6 M\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub
\cf2\f3\fs24 cm\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\fs24 a 254 nm),
otras especies pueden absorber los \up0 \expndtw0\charscalex100 fotones. Si los
contaminantes se fotolizan directamente, mejora la eficiencia del proceso de \u
p0 \expndtw-2\charscalex100 destruccin oxidativa. Como la intensidad de la radiac
in UV decae exponencialmente hacia \up0 \expndtw0\charscalex100 el seno de la sol
ucin, es necesario establecer condiciones de flujo turbulento para renovar \up0 \
expndtw-1\charscalex100 continuamente la solucin en las cercanas de la fuente lumi
nosa. El proceso fotoqumico es \up0 \expndtw-1\charscalex100 ms eficiente en medio
alcalino, ya que la base conjugada del perxido de hidrgeno (HO\ul0\sub\cf3\f4\fs2
4 2-\ul0\nosupersub\cf2\f3\fs24 ) \up0 \expndtw-2\charscalex100 tiene una absort
ividad mayor (\u949?\ul0\sub\cf3\f4\fs24 254\ul0\nosupersub\cf2\f3\fs24 = 240 M
\ul0\super\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\fs24 cm\ul0\super\cf3\f4\fs24 1\ul0\nosupersub\cf2\f3\fs24 ). \par\pard\qj \li1702\ri932\sb121\sl-280\slmult0\
fi566 \up0 \expndtw0\charscalex102 El uso de UV/perxido ofrece grandes ventajas:
el oxidante es comercialmente muy \line \up0 \expndtw0\charscalex102 accesible,
es trmicamente estable y puede almacenarse en el lugar \up0 \expndtw0\charscalex1
02 (con los recaudos \par\pard\qj \li1702\ri931\sb0\sl-283\slmult0 \up0 \expndtw
-1\charscalex100 necesarios). Como posee solubilidad infinita en agua, no existe
n problemas de transferencia \up0 \expndtw0\charscalex102 de masa asociados a ga
ses, como en el caso del ozono. Ya hemos mencionado que es una \up0 \expndtw-3\c
harscalex100 fuente efectiva de HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\
cf2\f3\fs24 , produciendo 2 HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\
f3\fs24 por cada H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\c
f3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 . La inversin de capital es mnima \up0 \ex
pndtw-3\charscalex100 y la operacin es simple. En contraposicin, dada la baja secc
in eficaz de absorcin de H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\
sub\cf3\f4\fs24 2 \up0 \expndtw0\charscalex103 \ul0\nosupersub\cf2\f3\fs24 a 254
nm, se necesitan altas concentraciones del oxidante. El mtodo no es efectivo par
a \up0 \expndtw0\charscalex100 degradar alcanos fluorados o clorados, que no son
atacados por HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 , y ti
ene baja eficiencia \up0 \expndtw-1\charscalex100 para tratar aguas de alta abso
rbancia a \u955? < 300 nm. \par\pard\qj \li1702\ri920\sb138\sl-280\slmult0\fi566

\up0 \expndtw0\charscalex103 En exceso de perxido y con altas concentraciones de
HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 , tienen lugar reac
ciones \line \up0 \expndtw0\charscalex102 competitivas que producen un efect
o inhibitorio para la degradacin. Los HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\
nosupersub\cf2\f3\fs24 son \line \up0 \expndtw0\charscalex102 susceptibles de
recombinarse o de reaccionar de acuerdo con el siguiente esquema [53]: \par\pard
\li1702\sb214\sl-276\slmult0\fi0\tx3185\tx10342 \up0 \expndtw-3\charscalex100 HO
\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\
fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-3\ch
arscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
HO\ul0\sub\cf3\f4\fs24 2\u822
6?\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3
\fs24 O\tab \up0 \expndtw-3\charscalex100 (23)\par\pard\li1702\sb137\sl-276\slmu
lt0\fi0\tx3267\tx10342 \up0 \expndtw-3\charscalex100 HO\ul0\sub\cf3\f4\fs24 2\u8
226?\ul0\nosupersub\cf2\f3\fs24 + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\
f3\fs24 O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersu
b\cf2\f3\fs24 \u8594?
HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\
fs24 + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O + O\ul0\sub\cf3
\f4\fs24 2\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (46)\pa
r\pard\li1702\sb139\sl-276\slmult0\fi0\tx2563\tx10342 \up0 \expndtw-3\charscalex
100 2 HO\ul0\sub\cf3\f4\fs24 2\u8226?\tab \dn2 \expndtw-3\charscalex100 \ul0\nos
upersub\cf2\f3\fs24 \u8594?
H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs2
4 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 \ul0\sub\cf3\f4\fs24 \ul
0\nosupersub\cf2\f3\fs24 + O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-3\charsca
lex100 \ul0\nosupersub\cf2\f3\fs24 (47)\par\pard\li1702\sb137\sl-276\slmult0\fi0
\tx3178\tx10342 \up0 \expndtw-3\charscalex100 HO\ul0\sub\cf3\f4\fs24 2\u8226?\ul
0\nosupersub\cf2\f3\fs24 + HO\ul0\super\cf3\f4\fs24 \u8226?\tab \up0 \expndtw
-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
H\ul0\sub\cf3\f4\fs24 2\
ul0\nosupersub\cf2\f3\fs24 O + O\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-3\cha
rscalex100 \ul0\nosupersub\cf2\f3\fs24 (24)\par\pard\li1702\sb199\sl-276\slmult0
\fi566\tx3830\tx4541 \up0 \expndtw-3\charscalex100 Las reacciones\tab \up0 \expn
dtw-3\charscalex100 (23) y\tab \up0 \expndtw-3\charscalex100 (24) consumen HO\ul
0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 y disminuyen la probabil
idad de oxidacin.\par\pard\qj \li1702\ri925\sb12\sl-260\slmult0 \up0 \expndtw-4\c
harscalex100 Se debe determinar en cada caso la cantidad ptima de H\ul0\sub\cf3\f
4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f
3\fs24 , para evitar un exceso que podra \up0 \expndtw-5\charscalex100 retardar l
a degradacin. \par\pard\qj \li1702\ri931\sb124\sl-280\slmult0\fi566 \up0 \expndtw
-2\charscalex100 El mtodo UV/H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O
\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 es uno de los PAOs ms antiguos
, y ha sido usado con xito en la \line \up0 \expndtw0\charscalex103 remocin de c
ontaminantes presentes en aguas y efluentes industriales, incluyendo \lin
e \up0 \expndtw0\charscalex103 organoclorados alifticos, aromticos, fenoles (clora
dos y sustituidos) y plaguicidas [2]. La \par\pard\ql \li1702\sb0\sl-230\slmult0
\par\pard\ql\li1702\sb172\sl-230\slmult0 \up0 \expndtw-3\charscalex100 \ul0\sup
er\cf5\f6\fs20\ul0\super\cf5\f6\fs19 1 \ul0\nosupersub\cf4\f5\fs20 213 kJ/mol, c
orrespondiente a luz de longitud de onda menor\ul0\super\cf5\f6\fs19 \ul0\nosup
ersub\cf4\f5\fs20 que 280 nm.
}
g16}{\bkmkend Pg16}\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb0\sl-23
0\slmult0\par\pard\li1133\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expndtw-2\charsca
lex100 \ul0\nosupersub\cf4\f5\fs20 18\tab \up0 \expndtw-2\charscalex100 Domnech,
Jardim y Litter\par\pard\li1133\sb0\sl-276\slmult0\par\pard\li1133\sb0\sl-276\sl
mult0\par\pard\li1133\sb207\sl-276\slmult0\fi0\tx1912\tx7685 \up0 \expndtw0\char
scalex104 \ul0\nosupersub\cf2\f3\fs24 Figura\tab \up0 \expndtw0\charscalex104 5
muestra un ejemplo de la industria textil peruana\tab \up0 \expndtw0\charscal
ex104 [54]. El mtodo mejora\par\pard\li1133\sb0\sl-276\slmult0\fi0 \up0 \expndtw0
\charscalex104 sensiblemente combinndolo con ultrasonido [55].\par\pard\sect\sect
d\sbknone\cols3\colno1\colw2191\colsr20\colno2\colw3683\colsr160\colno3\colw5716
\colsr160\ql \li1812\sb0\sl-161\slmult0 \par\pard\ql \li1812\sb0\sl-161\slmult0
\par\pard\ql \li1812\sb49\sl-161\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosu
persub\cf8\f9\fs14 1.2\par\pard\ql \li1812\sb151\sl-161\slmult0 \up0 \expndtw-2\
charscalex100 1.0\par\pard\ql \li1812\sb156\sl-161\slmult0 \up0 \expndtw-2\chars
calex100 0.8\par\pard\ql \li1812\sb151\sl-161\slmult0 \up0 \expndtw-2\charscalex
100 0.6\par\pard\ql \li1812\sb153\sl-161\slmult0 \up0 \expndtw-2\charscalex100 0
.4\par\pard\ql \li1812\sb151\sl-161\slmult0 \up0 \expndtw-2\charscalex100 0.2\pa
r\pard\ql \li1812\sb151\sl-161\slmult0 \up0 \expndtw-2\charscalex100 0.0\par\par
d\ql \li2096\sb53\sl-161\slmult0 \up0 \expndtw-3\charscalex100 0\par\pard\column
\ql \li2211\sb0\sl-161\slmult0 \par\pard\ql \li20\sb87\sl-161\slmult0 \up0 \exp
ndtw-1\charscalex100 C/C\ul0\nosupersub\cf9\f10\fs9 0\ul0\nosupersub\cf8\f9\fs14
9\par\pard\ql \li4800\sb0\sl-92\slmult0 \par\pard\ql \li4800\sb0\sl-92\slmult0
\par\pard\ql \li4800\sb0\sl-92\slmult0 \par\pard\ql \li4800\sb0\sl-92\slmult0 \p
ar\pard\ql \li4800\sb0\sl-92\slmult0 \par\pard\ql \li4800\sb0\sl-92\slmult0 \par
\pard\ql \li4800\sb0\sl-92\slmult0 \par\pard\ql \li4800\sb0\sl-92\slmult0 \par\p
ard\ql \li4800\sb0\sl-92\slmult0 \par\pard\ql \li4800\sb0\sl-92\slmult0 \par\par
d\ql \li4800\sb0\sl-92\slmult0 \par\pard\ql \li2609\sb56\sl-92\slmult0 \up0 \exp
ndtw-1\charscalex100 \ul0\nosupersub\cf10\f11\fs8 UV/H2O2\par\pard\ql \li2609\sb
90\sl-92\slmult0 \up0 \expndtw-1\charscalex100 UV/sin H2O2\par\pard\ql \li2619\s
b0\sl-161\slmult0 \par\pard\ql \li2619\sb0\sl-161\slmult0 \par\pard\ql \li2619\s
b0\sl-161\slmult0 \par\pard\ql \li2619\sb0\sl-161\slmult0 \par\pard\ql \li428\sb
69\sl-161\slmult0\tx997\tx1570\tx2141\tx2706\tx3277 \up0 \expndtw-2\charscalex10
0 \ul0\nosupersub\cf8\f9\fs14 10\tab \up0 \expndtw-2\charscalex100 20\tab \up0 \
expndtw-3\charscalex100 30\tab \up0 \expndtw-3\charscalex100 40\tab \up0 \expndt
w-3\charscalex100 50\tab \up0 \expndtw-2\charscalex100 60\par\pard\ql \li1141\sb
79\sl-161\slmult0 \up0 \expndtw0\charscalex102 Tiempo (min)\par\pard\column \ql
\li507\sb71\sl-184\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf7\f8\
fs16 Disminucin de COT ( mg/L)\par\pard\ql \li6044\sb0\sl-161\slmult0 \par\pard\q
l \li20\sb10\sl-161\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf8\f9
\fs14 15\par\pard\ql \li6044\sb0\sl-161\slmult0 \par\pard\ql \li6044\sb0\sl-161\
slmult0 \par\pard\ql \li6044\sb0\sl-161\slmult0 \par\pard\ql \li20\sb21\sl-161\s
lmult0 \up0 \expndtw-3\charscalex100 10\par\pard\ql \li6127\sb0\sl-161\slmult0 \
par\pard\ql \li6127\sb0\sl-161\slmult0 \par\pard\ql \li6127\sb0\sl-161\slmult0 \
par\pard\ql \li103\sb28\sl-161\slmult0 \up0 \expndtw-2\charscalex100 5\par\pard\
ql \li6127\sb0\sl-161\slmult0 \par\pard\ql \li6127\sb0\sl-161\slmult0 \par\pard\
ql \li6127\sb0\sl-161\slmult0 \par\pard\ql \li103\sb21\sl-161\slmult0 \up0 \expn
dtw-2\charscalex100 0\par\pard\ql \li271\sb50\sl-161\slmult0\tx553\tx783\tx1059\
tx1335\tx1611\tx1892\tx2168\tx2444\tx2720\tx2996\tx3276\tx3553 \up0 \expndtw-2\c
harscalex100 0\tab \up0 \expndtw-2\charscalex100 5\tab \up0 \expndtw-2\charscale
x100 10\tab \up0 \expndtw-2\charscalex100 15\tab \up0 \expndtw-2\charscalex100 2
0\tab \up0 \expndtw-2\charscalex100 25\tab \up0 \expndtw-3\charscalex100 30\tab
\up0 \expndtw-3\charscalex100 35\tab \up0 \expndtw-3\charscalex100 40\tab \up0 \
expndtw-3\charscalex100 45\tab \up0 \expndtw-3\charscalex100 50\tab \up0 \expndt
w-3\charscalex100 55\tab \up0 \expndtw-3\charscalex100 60\par\pard\ql \li1580\sb
136\sl-161\slmult0 \up0 \expndtw0\charscalex102 Tiempo (min) \par\pard\sect\sect
d\sbknone \qj \li1133\ri1503\sb186\sl-240\slmult0 \up0 \expndtw0\charscalex100 \
ul0\nosupersub\cf4\f5\fs20 Figura 5. Tratamiento de un colorante azo por UV/perxi
do [54]: (a), degradacin del colorante con UV y con \up0 \expndtw-3\charscalex100
UV7perxido; (b) disminucin del COT con UV/perxido. \par\pard\ql \li1133\sb241\sl-2
64\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 3.3. UV/O\u
l0\sub\cf3\f4\fs24 3 \par\pard\qj \li1133\ri1487\sb263\sl-280\slmult0\fi566 \up0

\expndtw0\charscalex100 \ul0\nosupersub\cf2\f3\fs24 La irradiacin del ozono en a
gua produce H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\
fs24 2\ul0\nosupersub\cf2\f3\fs24 en forma cuantitativa. El perxido de \up0 \exp
ndtw0\charscalex100 hidrgeno as generado se fotoliza a su vez (ver ecuacin (45)) ge
nerando radicales HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 ,
y \up0 \expndtw-2\charscalex100 reacciona con el exceso de ozono, generando tamb
in radicales (ecuacin (8)): \par\pard\li1133\sb220\sl-276\slmult0\fi0\tx2991\tx977
3 \up0 \expndtw-4\charscalex100 O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs
24 + h\u957? + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\tab \up
0 \expndtw-4\charscalex100 \u8594?
H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2
\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 + O\ul0\sub\cf3\f
4\fs24 2\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (48)\par\
pard\qj \li1133\ri1508\sb160\sl-286\slmult0\fi566 \up0 \expndtw0\charscalex105 P
or lo tanto, este mtodo podra considerarse en principio slo una forma cara de \line
\up0 \expndtw-2\charscalex100 generar H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf
2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 y luego HO\ul0\sup
er\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 . En realidad, se trata de una
combinacin de UV/H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf
3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 y O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub
\cf2\f3\fs24 /H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f
4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , \line \up0 \expndtw-4\charscalex100 de acu
erdo al mecanismo visto en secciones previas, pero la ventaja es que el ozono po
see una \line \up0 \expndtw-5\charscalex100 absorptividad molar mayor que el
H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2 \up
0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (\u949?\ul0\sub\cf3\f4\fs
24 254 \up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 3300 M\ul0\sup
er\cf3\f4\fs24 -1\ul0\nosupersub\cf2\f3\fs24 cm\ul0\super\cf3\f4\fs24 -1\ul0\n
osupersub\cf2\f3\fs24 ), y puede usarse, por \par\pard\qj \li1133\ri1501\sb4\
sl-275\slmult0 \up0 \expndtw-3\charscalex100 consiguiente, para tratar aguas con
alto fondo de absorcin de UV. La eficiencia es superior a \line \up0 \expndtw0\c
harscalex100 la de O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 o UV dire
cta, y el reactor no necesita ser de cuarzo pues se puede irradiar con luz \line
\up0 \expndtw-3\charscalex100 UV-B (280-330 nm). El mtodo se ha aplicado a la po
tabilizacin de aguas, en el tratamiento \line \up0 \expndtw-2\charscalex100 de ag
uas residuales altamente contaminadas, en desinfeccin, en decoloracin de aguas de
la \line \up0 \expndtw-2\charscalex100 industria del papel, en la degradacin de h
idrocarburos alifticos clorados \up0 \expndtw-3\charscalex100 (saturados e \par\p
ard\qj \li1133\ri1498\sb1\sl-280\slmult0 \up0 \expndtw-1\charscalex100 insaturad
os). Es el mejor mtodo para el tratamiento de PCBs. Si la irradiacin se produce a
\line \up0 \expndtw-1\charscalex100 longitudes de onda menores que 310 nm, el mto
do puede aprovechar la fotlisis de O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\
fs24 , que \line \up0 \expndtw-1\charscalex100 produce una cantidad adicional de
HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 y otros oxidantes,
con el consiguiente aumento de la \line \up0 \expndtw-3\charscalex100 eficienci
a \par\pard\li1133\sb216\sl-276\slmult0\fi0\tx2189\tx9773 \up0 \expndtw-3\charsc
alex100 O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 + h\u957?\tab \up0
\expndtw-3\charscalex100 \u8594? O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3
\fs24 (\ul0\super\cf3\f4\fs24 1\ul0\nosupersub\cf2\f3\fs24 \u8710?\ul0\sub\cf3\
f4\fs24 g\ul0\nosupersub\cf2\f3\fs24 ) + O(\ul0\super\cf3\f4\fs24 1\ul0\nosuper
sub\cf2\f3\fs24 D)\tab \up0 \expndtw-4\charscalex100 (49)\par\pard\li1133\sb137\
sl-276\slmult0\fi0\tx2700\tx9773 \up0 \expndtw-3\charscalex100 O(\ul0\super\cf3\
f4\fs24 1\ul0\nosupersub\cf2\f3\fs24 D) + H\ul0\sub\cf3\f4\fs24 2\ul0\nosupers
ub\cf2\f3\fs24 O\tab \up0 \expndtw-3\charscalex100 \u8594?
2 HO\ul0\super\cf3
\f4\fs24 \u8226?\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (
50)\par\pard\qj \li1133\ri1472\sb156\sl-280\slmult0\fi566 \up0 \expndtw0\charsca
lex100 El uso de ozono, como ya se ha comentado, implica siempre altos costos de
capital y \up0 \expndtw0\charscalex100 equipamiento adicional para la destruccin
del ozono remanente, problemas de seguridad y \up0 \expndtw-4\charscalex100 sal
ud, y limitaciones de transferencia de masa por la baja solubilidad del O\ul0\su
b\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 en agua, as como \up0 \expndtw-4\char

scalex100 el peligro del escape a la atmsfera de VOCs causado por el burbujeo del
reactivo\ul0\sub\cf3\f4\fs24 . \par\pard\qj \li1133\ri1462\sb126\sl-273\slmult0
\fi566 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf2\f3\fs24 Tambin puede uti
lizarse la combinacin UV/H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0
\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /O\ul0\sub\cf3\f4\fs24 3\ul0\nosup
ersub\cf2\f3\fs24 , que acelera el proceso trmico, \line \up0 \expndtw-3\charscal
ex100 especialmente la ecuacin (8) que es muy lenta (ver \ul0\nosupersub\cf11\f12
\fs24 Seccin 2.2\ul0\nosupersub\cf2\f3\fs24 ). La adicin de luz al proceso \line \
up0 \expndtw-3\charscalex100 H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24
O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /O\ul0\sub\cf3\f4\fs24 3\ul0\
nosupersub\cf2\f3\fs24 produce un aumento neto de la eficiencia, y los estudios
de aplicacin se encuentran \line \up0 \expndtw-3\charscalex100 ya a escala de
planta piloto. Las tcnicas UV/O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3
\fs24 y UV/H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4
\fs24 2\ul0\nosupersub\cf2\f3\fs24 estn comercialmente
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g17}{\bkmkend Pg17}\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb0\sl-23
0\slmult0\par\pard\li1702\sb19\sl-230\slmult0\fi0\tx10500 \up0 \expndtw-1\charsc
alex100 \ul0\nosupersub\cf4\f5\fs20 Procesos avanzados de oxidacin para la elimin
acin de contaminantes\tab \up0 \expndtw-1\charscalex100 19\par\pard\qj \li1702\sb
0\sl-280\slmult0 \par\pard\qj\li1702\sb0\sl-280\slmult0 \par\pard\qj\li1702\ri91
2\sb180\sl-280\slmult0 \up0 \expndtw0\charscalex107 \ul0\nosupersub\cf2\f3\fs24
disponibles. Los tres procesos UV/H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\
fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , UV/O\ul0\sub\cf3\f4\fs
24 3\ul0\nosupersub\cf2\f3\fs24 y UV/H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2
\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 /O\ul0\sub\cf3\f4\fs
24 3\ul0\nosupersub\cf2\f3\fs24 han mostrado ser muy \up0 \expndtw-2\charscalex
100 efectivos para la descontaminacin de aguas subterrneas y remediacin de suelos [
3-4]. \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb8\sl-276\slm
ult0 \up0 \expndtw0\charscalex102 3.4. Foto-Fenton \par\pard\qj \li1702\ri931\sb
221\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex112 Ya se ha mencionado que lo
s procesos Fenton no conducen generalmente a la \up0 \expndtw0\charscalex100 min
eralizacin y que debe utilizarse la irradiacin luminosa para promover una degradac
in \up0 \expndtw0\charscalex100 ms importante del contaminante (ver \ul0\nosupersu
b\cf11\f12\fs24 seccin 2.3\ul0\nosupersub\cf2\f3\fs24 ) [23-26, 56]. \par\pard\ql
\li4680\sb0\sl-230\slmult0 \par\pard\ql\li4680\sb72\sl-230\slmult0 \up0 \expndt
w0\charscalex102 \ul0\nosupersub\cf4\f5\fs20 Cuadro IV: Ventajas de Foto-Fenton.
\par\pard\ql \li2645\sb30\sl-230\slmult0 \up0 \expndtw0\charscalex100 La reaccin
de Fenton aumenta su eficiencia por iluminacin debido a varios factores: \par\pa
rd\ql \li1702\ri965\sb62\sl-240\slmult0\tx2062\tx2062 \up0 \expndtw-2\charscalex
100 \ul0\nosupersub\cf12\f13\fs20 \ ul0\nosupersub\cf4\f5\fs20 La fotlisis de hidro
xocomplejos de Fe\ul0\super\cf5\f6\fs19 3+\ul0\nosupersub\cf4\f5\fs20 es una fu
ente adicional de HO\ul0\super\cf5\f6\fs19 \u8226?\ul0\nosupersub\cf4\f5\fs20 (
ver ecuacin (51)), a continuacin \line\tab \up0 \expndtw0\charscalex100 del cuadro
).El rendimiento cuntico de esta reaccin es bajo pero aumenta a longitudes de onda
menores \line \tab \up0 \expndtw0\charscalex100 (\u966?\ul0\sub\cf5\f6\fs19 HO\
ul0\nosupersub\cf4\f5\fs20 \u8226? = 0.017 a 360 nm y 0.14 a 313 nm). \par\pard\
li1702\sb144\sl-230\slmult0\fi0\tx3826\tx10438 \up0 \expndtw-2\charscalex100 \ul
0\nosupersub\cf12\f13\fs20 \ul0\nosupersub\cf4\f5\fs20 Fe(III)(OH)\ul0\super\cf5\
f6\fs19 2+\ul0\nosupersub\cf4\f5\fs20 + h\u957?\tab \up0 \expndtw-2\charscale
x100 \u8594?
Fe(II) + HO\ul0\super\cf5\f6\fs19 \u8226?\tab \up0 \expndtw-2\
charscalex100 \ul0\nosupersub\cf4\f5\fs20 (51)\par\pard\qj \li1702\ri966\sb84\sl
-220\slmult0\tx2062 \up0 \expndtw0\charscalex102 \ul0\nosupersub\cf12\f13\fs20 \ul
0\nosupersub\cf4\f5\fs20 El Fe(II) fotogenerado de esta manera genera HO\ul0\su
per\cf5\f6\fs19 \u8226?\ul0\nosupersub\cf4\f5\fs20 adicionales a travs de la ecu
acin (16) y contina el \line\tab \up0 \expndtw-4\charscalex100 ciclo. \par\pard\ql
\li1702\sb52\sl-230\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf12\
f13\fs20 \ ul0\nosupersub\cf4\f5\fs20 Permite el uso de longitudes de onda desde 3
00 nm hasta el visible. \par\pard\qj \li1702\ri963\sb79\sl-220\slmult0\tx2062 \u
p0 \expndtw0\charscalex100 \ul0\nosupersub\cf12\f13\fs20 \ ul0\nosupersub\cf4\f5\fs
20 Las concentraciones de Fe(II) a emplearse pueden ser rdenes de magnitud menor
es que en la reaccin de \line\tab \up0 \expndtw-1\charscalex100 Fenton convencion
al. \par\pard\qj \li1702\ri966\sb100\sl-220\slmult0\tx2062 \up0 \expndtw0\charsc
alex102 \ul0\nosupersub\cf12\f13\fs20 \ ul0\nosupersub\cf4\f5\fs20 Si se usan radi
aciones menores que 360 nm, se puede aprovechar la produccin de HO\ul0\super\cf5\

f6\fs19 \u8226?\ul0\nosupersub\cf4\f5\fs20 por fotlisis del \line\tab \up0 \expn
dtw-4\charscalex100 H\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 O\ul0\sub
\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 (ecuacin (45)). \par\pard\qj \li1702\s
b0\sl-273\slmult0 \par\pard\qj\li1702\ri904\sb44\sl-273\slmult0\fi566 \up0 \expn
dtw0\charscalex103 \ul0\nosupersub\cf2\f3\fs24 El mtodo es eficiente pero ti
ene la desventaja de que debe agregarse H\ul0\sub\cf3\f4\fs24 2\ul0\nosup
ersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2 \up0 \expndtw-4\charscalex100 \ul0\nos
upersub\cf2\f3\fs24 continuamente y mantener condiciones cidas. Los usos ms frecue
ntes de esta tecnologa han \up0 \expndtw-1\charscalex100 sido en el tratamiento d
e aguas industriales, suelos y lixiviados. Trata con xito compuestos \up0 \expndt
w-1\charscalex100 nitroaromticos, fenoles policlorados, herbicidas (2,4-D y 2,4,5
-T) y plaguicidas. \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\s
b9\sl-276\slmult0 \up0 \expndtw0\charscalex101 3.5. Ferrioxalato y otros complej
os de Fe(III) \par\pard\qj \li1702\ri930\sb261\sl-280\slmult0\fi566 \up0 \expndt
w0\charscalex100 En presencia de ciertos ligandos orgnicos tales como cidos carboxl
icos, el Fe(III) \line \up0 \expndtw0\charscalex102 puede formar complejos es
tables o pares inicos asociados que exhiben bandas de \line \up0 \expndtw
0\charscalex102 transferencia de carga del ligando al metal \up0 \expndtw0
\charscalex102 (TCLM) en el espectro UV-visible, son \par\pard\ql \li1702\s
b4\sl-276\slmult0 \up0 \expndtw-4\charscalex100 fotoqumicamente activos y generan
Fe(II) por irradiacin: \par\pard\li1702\sb204\sl-276\slmult0\fi0\tx4030\tx10342
\dn2 \expndtw-4\charscalex100 Fe(III)(O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2
\f3\fs24 CR)\ul0\super\cf3\f4\fs24 2+\ul0\nosupersub\cf2\f3\fs24 + h\u957?\ta
b \dn2 \expndtw-4\charscalex100 \u8594?
Fe(II) + CO\ul0\sub\cf3\f4\fs24 2\u
l0\nosupersub\cf2\f3\fs24 + R\ul0\super\cf3\f4\fs24 \u8226?\tab \up0 \expndtw
-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (52)\par\pard\qj \li1702\ri933\sb15
3\sl-290\slmult0\fi566 \up0 \expndtw0\charscalex102 Por ejemplo, el cido oxlico fo
rma complejos que absorben fuertemente desde 250 \line \up0 \expndtw0\charscalex
104 hasta 580 nm, con valores de \u949?\ul0\sub\cf3\f4\fs24 max\ul0\nosupersub\c
f2\f3\fs24 del orden de 10\ul0\super\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 10\ul0\super\cf3\f4\fs24 4\ul0\nosupersub\cf2\f3\fs24 , correspondiente a una ba
nda de \line \up0 \expndtw0\charscalex101 TCLM. La fotlisis del trisoxalatoferrat
o(III) \up0 \expndtw0\charscalex104 (ferrioxalato, FeOx) se aprovecha para la \p
ar\pard\qj \li1702\ri933\sb0\sl-290\slmult0 \up0 \expndtw-1\charscalex100 medicin
de intensidades de luz, y constituye el actinmetro qumico ms utilizado [57]. La \l
ine \up0 \expndtw-1\charscalex100 reaccin tiene un alto rendimiento cuntico (\u966
? = 1-1,2), casi independiente de la longitud de \line \up0 \expndtw-2\charscale
x100 onda: \par\pard\li1702\sb177\sl-276\slmult0\fi0\tx3776\tx10342 \up0 \expndt
w-3\charscalex100 [Fe(C\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\s
ub\cf3\f4\fs24 4\ul0\nosupersub\cf2\f3\fs24 )\ul0\sub\cf3\f4\fs24 3\ul0\nosupers
ub\cf2\f3\fs24 ]\ul0\super\cf3\f4\fs24 3-\ul0\nosupersub\cf2\f3\fs24 + h\u957
?\tab \up0 \expndtw-3\charscalex100 \u8594?
[Fe(C\ul0\sub\cf3\f4\fs24 2\ul0\n
osupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 4\ul0\nosupersub\cf2\f3\fs24 )\ul0\s
ub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 ]\ul0\super\cf3\f4\fs24 2-\ul0\nosup
ersub\cf2\f3\fs24 + C\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\
sub\cf3\f4\fs24 4\u8226?-\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\
f3\fs24 (53)\par\pard\li1702\sb139\sl-276\slmult0\fi0\tx4152\tx10342 \dn2 \expnd
tw-3\charscalex100 C\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\
cf3\f4\fs24 4\u8226?-\ul0\nosupersub\cf2\f3\fs24 + [Fe(C\ul0\sub\cf3\f4\fs24
2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 4\ul0\nosupersub\cf2\f3\fs24
)\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 ]\ul0\super\cf3\f4\fs24 3-\ta
b \dn2 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
[Fe(C\ul0
\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 4\ul0\nosupe
rsub\cf2\f3\fs24 )\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 ]\ul0\super\
cf3\f4\fs24 2-\ul0\nosupersub\cf2\f3\fs24 + C\ul0\sub\cf3\f4\fs24 2\ul0\nosup
ersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 42-\ul0\nosupersub\cf2\f3\fs24 + 2 CO
\ul0\sub\cf3\f4\fs24 2\tab \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\
fs24 (54)\par\pard\li1702\sb135\sl-276\slmult0\fi0\tx3075\tx10342 \up0 \expndtw3\charscalex100 C\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3
\f4\fs24 4\u8226?-\ul0\nosupersub\cf2\f3\fs24 + O\ul0\sub\cf3\f4\fs24 2\tab \u

p0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
O\ul0\sub\cf3
\f4\fs24 2\u8226?-\ul0\nosupersub\cf2\f3\fs24 + 2 CO\ul0\sub\cf3\f4\fs24 2\ta
b \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (55)\par\pard\qj \li
1702\ri931\sb178\sl-270\slmult0\fi566 \up0 \expndtw0\charscalex104 Si se agrega
H\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\n
osupersub\cf2\f3\fs24 , la reduccin fotoqumica del complejo de Fe(III) se acopla a
la \line \up0 \expndtw-2\charscalex100 reaccin de Fenton (ecuacin (16)) [26, 58].
Recientemente, Nogueira y Jardim demostraron \line \up0 \expndtw-2\charscalex10
0 la alta eficiencia del uso de mezclas iluminadas de H\ul0\sub\cf3\f4\fs24 2\ul
0\nosupersub\cf2\f3\fs24 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 y F
eOx para la fotodegradacin de
}
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}}
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}}
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d9}}}}}\pard\sb0\sl-240{\bkmkstart Pg18}{\bkmkend Pg18}\par\pard\li1133\sb0\sl-2
0\fi0\tx8050 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs20 20\tab \u
p0 \expndtw-2\charscalex100 Domnech, Jardim y Litter\par\pard\qj \li1133\sb0\sl-2
75\slmult0 \par\pard\qj\li1133\sb0\sl-275\slmult0 \par\pard\qj\li1133\ri1486\sb2
15\sl-275\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf2\f3\fs24 cont
aminantes orgnicos [59]. El mtodo es til para tratar aguas con alta absorbancia a \
u955? < \up0 \expndtw0\charscalex100 300 nm (debido a la elevada absorbancia del
ferrioxalato), y permite usar luz solar, lo cual \up0 \expndtw0\charscalex102 h
ace a la tcnica muy atractiva desde el punto de vista econmico. Los reactivos son
muy \up0 \expndtw-4\charscalex100 solubles en agua, no existen limitaciones de t
ransferencia de masa, el proceso es de bajo costo \up0 \expndtw0\charscalex105 y
el oxidante es accesible. Se utiliza para el tratamiento de hidrocarburos aromti
cos y \up0 \expndtw0\charscalex100 cloroaromticos, etilenos clorados, teres, alcoh
oles, cetonas y otros compuestos. De todos \up0 \expndtw-1\charscalex100 modos,
la mineralizacin total no es fcil de alcanzar y los contaminantes se transforman e
n \up0 \expndtw-4\charscalex100 otros compuestos orgnicos. La Figura 6 compara la
destruccin de 2-butanona por tres TAOs \up0 \expndtw0\charscalex100 diferentes,
y muestra la alta eficiencia del ferrioxalato. La Figura 7 compara la foto-Fento
n \up0 \expndtw-3\charscalex100 solar y el ferrioxalato para el tratamiento de t
olueno. \par\pard\ql \li1700\sb125\sl-276\slmult0\tx8095 \up0 \expndtw0\charscal
ex105 Potencialmente, se pueden usar otros carboxilatos de hierro \tab \up0 \exp
ndtw0\charscalex103 [59-60]. Cuando ese \par\pard\qj \li1133\ri1499\sb1\sl-280\s
lmult0 \up0 \expndtw0\charscalex103 carboxilato es el contaminante que se desea
destruir, por ejemplo EDTA, el agregado de \up0 \expndtw0\charscalex100 oxalato
slo compite por el Fe(III), y puede ocasionar una disminucin de la eficiencia. En
\up0 \expndtw-3\charscalex100 estos casos no es necesaria ni conveniente la adic
in de oxalato [61]. \par\pard\qj \li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\s
b0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0
\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\s
l-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-24
0\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\
slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\sl
mult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmu
lt0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\ri1535\sb234\sl-2
40\slmult0 \up0 \expndtw0\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Figura 6. Co
mparacin de la destruccin de tolueno en un agua subterrnea contaminada por irradiac
in solar \up0 \expndtw-2\charscalex100 en presencia de ferrioxalato/H\ul0\sub\cf5
\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 O\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4
\f5\fs20 y Fe(III)/H\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 O\ul0\sub
\cf5\f6\fs19 2 \ul0\nosupersub\cf4\f5\fs20 [25]. \par\pard\qj \li1133\sb0\sl-24
lt0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult
\pard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\p
ard\qj\li1133\sb0\sl-240\slmult0 \par\pard\qj\li1133\sb0\sl-240\slmult0 \par\par
d\qj\li1133\ri1535\sb160\sl-240\slmult0 \up0 \expndtw0\charscalex100 Figura 7. C
omparacin de la destruccin de tolueno en un agua subterrnea contaminada por irradia
cin solar \up0 \expndtw-2\charscalex100 en presencia de ferrioxalato/H\ul0\sub\cf
5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 O\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf
4\f5\fs20 y Fe(III)/H\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 O\ul0\su
b\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 [25]. \par\pard\sect\sectd\fs24\pape
rw11900\paperh16840{\shp
z-10000\shplid18
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aa08c28c2e76263915d6c1f04fe0d5ac1f65b5f849f0c6dadbcd137d9e0f017856183ce023026f26
3d2963f3408a2024dbbf11c633f22e3d3a8a00e4adfc03e04b4fb4fd97c15e12b6fb6645e7d9fc39
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28f250470e2486047fdd46ab1c5f37eed142a614015b145001451450021cf18c75e73e9edef4b451
4005145140051451400514514005145140051451400514514005145140051451400514018e9ea4fa
f5393d7dcfe1d071450014514500145155365ffda23637369f650f706587ec530b874658c5aac773
fda06389e1712b5c3b5a4a2e55e358e3b43133cc016e8a28a0028a28a0028a28a0028a28a0028a28
a0028a28a0028a28a0028a28a00fffd9}}}}}\pard\sb0\sl-240{\bkmkstart Pg19}{\bkmkend
Pg19}\par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb0\sl-230\slmult0\par\
pard\li1702\sb19\sl-230\slmult0\fi0\tx10500 \up0 \expndtw-1\charscalex100 \ul0\n
osupersub\cf4\f5\fs20 Procesos avanzados de oxidacin para la eliminacin de contami
nantes\tab \up0 \expndtw-1\charscalex100 21\par\pard\ql \li1702\sb0\sl-276\slmul
t0 \par\pard\ql\li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb0\sl-276\slmult0
\par\pard\ql\li1702\sb195\sl-276\slmult0 \up0 \expndtw0\charscalex101 \ul0\nosu
persub\cf2\f3\fs24 3.6. UV/Peryodato \par\pard\ql \li2268\sb0\sl-276\slmult0 \pa
r\pard\ql\li2268\sb128\sl-276\slmult0 \up0 \expndtw-2\charscalex100 El cido perydi
co, H\ul0\sub\cf3\f4\fs24 5\ul0\nosupersub\cf2\f3\fs24 IO\ul0\sub\cf3\f4\fs24 6\

ul0\nosupersub\cf2\f3\fs24 , y el peryodato, IO\ul0\sub\cf3\f4\fs24 4-\ul0\nosup
ersub\cf2\f3\fs24 , son oxidantes fuertes: \par\pard\li1702\sb262\sl-276\slmult0
\fi0\tx3816\tx5958\tx10341 \up0 \expndtw-4\charscalex100 H\ul0\sub\cf3\f4\fs24 5
\ul0\nosupersub\cf2\f3\fs24 IO\ul0\sub\cf3\f4\fs24 6\ul0\nosupersub\cf2\f3\fs24
+ H\ul0\super\cf3\f4\fs24 +\ul0\nosupersub\cf2\f3\fs24 + 2 e\ul0\super\cf3
\f4\fs24 -\tab \dn2 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
IO\ul0\sub\cf3\f4\fs24 3-\ul0\nosupersub\cf2\f3\fs24 + 3 H\ul0\sub\cf3\f4
\fs24 2\ul0\nosupersub\cf2\f3\fs24 O\tab \up0 \expndtw-4\charscalex100 ; E\ul0\s
uper\cf3\f4\fs24 o\ul0\nosupersub\cf2\f3\fs24 = + 1.60 V\tab \up0 \expndtw-4\ch
arscalex100 (56)\par\pard\qj \li1702\ri927\sb216\sl-313\slmult0\fi566 \up0 \expn
dtw-3\charscalex100 La irradiacin de soluciones de peryodato con luz UV corta gen
era radicales (IO\ul0\super\cf3\f4\fs24 3\u8226?\ul0\nosupersub\cf2\f3\fs24 , HO
\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 , \line \up0 \expndtw2\charscalex100 IO\ul0\sub\cf3\f4\fs24 4\u8226?\ul0\nosupersub\cf2\f3\fs24 ) y o
tras especies oxidantes (IO\ul0\sub\cf3\f4\fs24 3-\ul0\nosupersub\cf2\f3\fs24 ,
O\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 ). El ataque a contaminantes
orgnicos se vuelve as \line \up0 \expndtw0\charscalex102 menos selectivo pero ms ef
iciente [62]. El mecanismo es complejo y est ilustrado en la \line \up0 \expndtw0
\charscalex102 Figura 8. \par\pard\qj \li1702\sb0\sl-240\slmult0 \par\pard\qj\li
\sb0\sl-240\slmult0 \par\pard\qj\li1702\sb0\sl-240\slmult0 \par\pard\qj\li1702\s
b0\sl-240\slmult0 \par\pard\qj\li1702\sb0\sl-240\slmult0 \par\pard\qj\li1702\sb0
\sl-240\slmult0 \par\pard\qj\li1702\sb0\sl-240\slmult0 \par\pard\qj\li1702\sb0\s
l-240\slmult0 \par\pard\qj\li1702\sb0\sl-240\slmult0 \par\pard\qj\li1702\sb0\sl240\slmult0 \par\pard\qj\li1702\sb0\sl-240\slmult0 \par\pard\qj\li1702\sb0\sl-24
lt0 \par\pard\qj\li1702\sb0\sl-240\slmult0 \par\pard\qj\li1702\sb0\sl-240\slmult
\pard\qj\li1702\ri967\sb28\sl-240\slmult0 \up0 \expndtw0\charscalex100 \ul0\nosu
persub\cf4\f5\fs20 Figura 8. Posibles caminos de reduccin de peryodato a yoduro b
asados en estudios de radilisis e irradiacin \up0 \expndtw-1\charscalex100 UV de e
species de yodo [62]. \par\pard\qj \li1702\sb0\sl-303\slmult0 \par\pard\qj\li170
2\ri929\sb65\sl-303\slmult0\fi566 \up0 \expndtw0\charscalex108 \ul0\nosupersub\c
f2\f3\fs24 Con esta tcnica se puede destruir una amplia variedad de compuestos en
bajas \line \up0 \expndtw-3\charscalex100 concentraciones. Se utiliza para la d
ecoloracin de aguas con colorantes y para el tratamiento \line \up0 \expndtw-2\ch
arscalex100 de otras aguas residuales. Para una mejor efectividad del reactivo,
las aguas deben tener baja \line \up0 \expndtw0\charscalex106 absorbancia. Por o
tra parte, no existen en la legislacin requerimientos de descarga de \line \up0 \
expndtw-1\charscalex100 compuestos de yodo, de las cuales I\ul0\sub\cf3\f4\fs24
2\ul0\nosupersub\cf2\f3\fs24 y I\ul0\super\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\
fs24 son las ms txicas, pero aun as de baja toxicidad. \line \up0 \expndtw-3\chars
calex100 Por otra parte, el yodo se puede recuperar por intercambio inico, para r
egenerar el peryodato \line \up0 \expndtw-4\charscalex100 electroqumicamente. \pa
r\pard\sect\sectd\fs24\paperw11900\paperh16840\pard\sb0\sl-240{\bkmkstart Pg20}{
\bkmkend Pg20}\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb0\sl-230\slm
ult0\par\pard\li1133\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expndtw-2\charscalex10
0 \ul0\nosupersub\cf4\f5\fs20 22\tab \up0 \expndtw-2\charscalex100 Domnech, Jardi
m y Litter\par\pard\ql \li3322\sb0\sl-230\slmult0 \par\pard\ql\li3322\sb0\sl-230
\slmult0 \par\pard\ql\li3322\sb0\sl-230\slmult0 \par\pard\ql\li3322\sb92\sl-230\
slmult0 \up0 \expndtw0\charscalex101 Cuadro V: Resumen de las TAOs discutidas ha
sta ahora. \par\pard\qj \li1133\ri1533\sb30\sl-230\slmult0\fi566 \up0 \expndtw0\
charscalex110 Como se ver en el \ul0\nosupersub\cf13\f14\fs20 Captulo 3\ul0\nosupe
rsub\cf4\f5\fs20 , los caudales a tratar y las concentraciones de los contaminan
tes \line \up0 \expndtw0\charscalex107 determinan a grandes rasgos condiciones e

n las cuales las TAOs (fotoqumicas o no) pueden resultar una \line \up0 \expndtw0
\charscalex100 variante interesante a los procesos de cloracin tradicional o de t
ratamiento biolgico. En general, las TAOs son \line \up0 \expndtw0\charscalex106
ms adecuadas para tratar caudales (o volmenes) pequeos, y concentraciones no muy el
evadas. Su gran \line \up0 \expndtw0\charscalex100 utilidad est centrada en el pr
ocesamiento de aguas residuales resistentes a los tratamientos convencionales. E
n \line \up0 \expndtw0\charscalex107 ese sentido, las TAOs son tcnicas complement
arias con las tradicionales (en especial con el tratamiento \line \up0 \expndtw2\charscalex100 biolgico). \par\pard\qj \li1133\ri1533\sb71\sl-229\slmult0\fi566
\up0 \expndtw-1\charscalex100 Este Captulo ha ilustrado la gran cantidad de varia
bles y combinaciones exploradas en busca de procesos \line \up0 \expndtw-1\chars
calex100 del tipo TAO. Esa variedad puede generar confusin respecto de cules son l
as potencialidades de uso prctico, y \line \up0 \expndtw-1\charscalex100 respecto
de cmo escoger la tcnica ms adecuada para una aplicacin especfica. Bsicamente, la ele
ccin de la \line \up0 \expndtw0\charscalex103 tcnica debe hacerse sobre la base de
su efectividad y de su costo. La efectividad de cada una de las tcnicas \line \u
p0 \expndtw0\charscalex100 discutidas depende de la naturaleza de los contaminan
tes a destruir, y el costo est fuertemente determinado por \line \up0 \expndtw0\c
harscalex100 el equipamiento necesario, la energa requerida, y la posible necesid
ad de tratamientos posteriores para eliminar \line \up0 \expndtw0\charscalex100
las sustancias empleadas en el proceso. De all el inters de minimizar el agregado
de reactivos qumicos (para \line \up0 \expndtw0\charscalex104 simplificar el post
-tratamiento), y de recurrir a la energa solar en los procesos fotoqumicos (para b
ajar los \line \up0 \expndtw-1\charscalex100 costos energticos). Dentro de los re
activos qumicos, las ventajas de usar O\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\
f5\fs20 o H\ul0\sub\cf5\f6\fs19 2\ul0\nosupersub\cf4\f5\fs20 O\ul0\sub\cf5\f6\f
s19 2\ul0\nosupersub\cf4\f5\fs20 como oxidantes son claras, \line \up0 \expndtw
0\charscalex102 ya que son baratos, fciles de manejar y no generan sustancias que
deban removerse posteriormente. El ozono \line \up0 \expndtw0\charscalex107 com
parte la ltima ventaja, pero su manipulacin no es sencilla. Las tcnicas que operan
en condiciones \line \up0 \expndtw-2\charscalex100 drsticas \up0 \expndtw0\charsc
alex107 (WAO, OXAS) estn fuertemente penalizadas por los costos de insta
lacin \up0 \expndtw-3\charscalex100 (incluyendo \par\pard\ql \li1133\sb11\sl-230\
slmult0 \up0 \expndtw-3\charscalex100 mantenimiento), por lo que su uso apunta a
residuos muy especiales. \par\pard\qj \li1133\ri1534\sb50\sl-230\slmult0\fi566
\up0 \expndtw0\charscalex100 Este libro se centra en la fotocatlisis heterognea, tc
nica que se introduce a continuacin. Sin embargo, \up0 \expndtw0\charscalex100 qu
eda claro que la disponibilidad de una tcnica no es motivo suficiente para postul
ar su uso indiscriminado. Es \up0 \expndtw-1\charscalex100 importante en todo mo
mento conocer las opciones para elegir la ms adecuada. \par\pard\ql \li1133\sb0\s
l-276\slmult0 \par\pard\ql\li1133\sb0\sl-276\slmult0 \par\pard\ql\li1133\sb40\sl
-276\slmult0 \up0 \expndtw0\charscalex102 \ul0\nosupersub\cf2\f3\fs24 3.7. Fotoc
atlisis heterognea \par\pard\qj \li1133\ri1491\sb264\sl-276\slmult0\fi566 \up0 \ex
pndtw0\charscalex110 La fotocatlisis heterognea es un proceso que se basa en la ab
sorcin directa o \up0 \expndtw-1\charscalex100 indirecta de energa radiante (visib
le o UV) por un slido (el fotocatalizador heterogneo, que \up0 \expndtw0\charscale
x106 normalmente es un semiconductor de banda ancha). En la regin interfacial ent
re slido \up0 \expndtw0\charscalex109 excitado y la solucin tienen lugar las reacc
iones de destruccin o de remocin de los \up0 \expndtw0\charscalex108 contaminantes
, sin que el catalizador sufra cambios qumicos. La excitacin del \up0 \e
xpndtw-3\charscalex100 semiconductor puede tener lugar de dos formas: \par\pard\
qj \li1133\sb0\sl-260\slmult0 \par\pard\qj\li1133\ri1782\sb58\sl-260\slmult0\tx1
416 \up0 \expndtw0\charscalex104 \u8226? Por excitacin directa del semiconductor
, de manera que ste es el que absorbe los \line\tab \up0 \expndtw-3\charscalex100
fotones usados en el proceso. \par\pard\qj \li1133\ri1762\sb24\sl-280\slmult0\t
x1416 \up0 \expndtw-2\charscalex100 \u8226? Por excitacin inicial de molculas ads
orbidas en la superficie del catalizador, las que a \line\tab \up0 \expndtw-2\ch
arscalex100 su vez son capaces de inyectar cargas (electrones) en el semiconduct
or. \par\pard\qj \li1133\ri1496\sb260\sl-280\slmult0\fi566 \up0 \expndtw-3\chars
calex100 En esta seccin se discute slo el primer caso, que corresponde al caso ms g
eneral y de \up0 \expndtw0\charscalex105 mayor aplicabilidad en fotocatlisis hete
rognea. En el \ul0\nosupersub\cf11\f12\fs24 Captulo 6\ul0\nosupersub\cf2\f3\fs24
se hablar de las del \up0 \expndtw-3\charscalex100 segundo tipo (TiO\ul0\sub\cf3\
f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 +colorantes). \par\pard\qj \li1133\ri1488\s
b125\sl-275\slmult0\fi566 \up0 \expndtw0\charscalex108 La Figura 9 esquematiza l
os procesos qumicos que ocurren en una partcula de \line \up0 \expndtw0\charscalex
100 semiconductor cuando sta es excitada con luz suficientemente energtica
. En estas \line \up0 \expndtw0\charscalex111 condiciones, se crean pares elec
trn-hueco cuya vida media est en el rango de los \line \up0 \expndtw-3\charscalex1
00 nanosegundos; en ese lapso deben migrar a la superficie y reaccionar con espe
cies adsorbidas \line \up0 \expndtw-3\charscalex100 (procesos c y d) [63].Los pa
res electrn-hueco que no alcanzan a separarse y a reaccionar con \line \up0 \expn
dtw-4\charscalex100 especies en la superficie se recombinan y la energa se disipa
. Esta recombinacin puede tener \line \up0 \expndtw-2\charscalex100 lugar tanto e
n la superficie como en el seno de la partcula (procesos a y b, respectivamente).
\line \up0 \expndtw-3\charscalex100 El proceso neto es la catlisis de la reaccin
entre el oxidante B y el reductor A (por ejemplo, \line \up0 \expndtw-4\charscal
ex100 O\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 y materia orgnica).
}
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0028a28a0028a28a0028a28a0028a28a0028a28a0028a28a0028a28a00ffd9}}}}}\pard\sb0\sl240{\bkmkstart Pg21}{\bkmkend Pg21}\par\pard\li1702\sb0\sl-230\slmult0\par\pard\
li1702\sb0\sl-230\slmult0\par\pard\li1702\sb19\sl-230\slmult0\fi0\tx10500 \up0 \
expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Procesos avanzados de oxidac
in para la eliminacin de contaminantes\tab \up0 \expndtw-1\charscalex100 23\par\pa
rd\ql \li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\par
\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\l
i1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1
sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb
0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\
sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl
-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-2
30\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230
\slmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb0\sl-230\s
lmult0 \par\pard\ql\li1702\sb0\sl-230\slmult0 \par\pard\ql\li1702\sb141\sl-230\s
lmult0 \up0 \expndtw0\charscalex100 Figura 9. Procesos que ocurren en la interfa

z semiconductor-electrolito bajo iluminacin. \par\pard\qj \li1702\sb0\sl-305\slmu
lt0 \par\pard\qj\li1702\ri929\sb64\sl-305\slmult0\fi566 \up0 \expndtw-1\charscal
ex100 \ul0\nosupersub\cf2\f3\fs24 Existen diversos materiales con propiedades idn
eas para actuar como catalizadores y \line \up0 \expndtw0\charscalex100 llevar a
cabo reacciones fotosensibilizadas como, por ejemplo, TiO\ul0\sub\cf3\f4\fs24 2
\ul0\nosupersub\cf2\f3\fs24 , ZnO, CdS, xidos de \line \up0 \expndtw-3\charscalex
100 hierro, WO\ul0\sub\cf3\f4\fs24 3\ul0\nosupersub\cf2\f3\fs24 , ZnS, etc. Esto
s materiales son econmicamente asequibles, e incluso muchos de \line \up0 \expndt
w0\charscalex109 ellos participan en procesos qumicos en la naturaleza. Adems, la
mayora de estos \line \up0 \expndtw-1\charscalex100 materiales puede excitarse co
n luz de no muy alta energa, absorbiendo parte de la radiacin \line \up0 \expndtw1\charscalex100 del espectro solar que incide sobre la superficie terrestre (\u9
55? > 310 nm), lo cual incrementa el \line \up0 \expndtw0\charscalex102 inters p
ara un posible aprovechamiento de la luz solar. Los fotocatalizadores
ms \line \up0 \expndtw-1\charscalex100 investigados hasta el momento son los xidos
metlicos semiconductores de banda ancha y, \line \up0 \expndtw0\charscalex100 pa
rticularmente, el TiO\ul0\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , el cual
presenta una elevada estabilidad qumica que lo hace apto \line \up0 \expndtw0\ch
arscalex110 para trabajar en un amplio rango de pH, al mismo tiempo que es capaz
de producir \line \up0 \expndtw-3\charscalex100 transiciones electrnicas por abs
orcin de luz en el ultravioleta cercano (UV-A). Este tema se \line \up0 \expndtw4\charscalex100 discute en detalle en el \ul0\nosupersub\cf11\f12\fs24 Captulo 3\
ul0\nosupersub\cf2\f3\fs24 . \par\pard\qj \li1702\ri926\sb113\sl-308\slmult0\fi5
66 \up0 \expndtw0\charscalex108 La fuerza impulsora del proceso de transferencia
electrnica en la interfaz es la \up0 \expndtw-2\charscalex100 diferencia de ener
ga entre los niveles del semiconductor y el potencial redox de las especies \up0
\expndtw0\charscalex100 adsorbidas. En la Figura 10 se representan los procesos
termodinmicamente posibles que \up0 \expndtw-3\charscalex100 ocurren en la interf
az: los huecos fotogenerados dan lugar a la reaccin de oxidacin Red\ul0\sub\cf3\f4
\fs24 2\ul0\nosupersub\cf2\f3\fs24 \u8594? \up0 \expndtw-3\charscalex100 Ox\ul0
\sub\cf3\f4\fs24 2\ul0\nosupersub\cf2\f3\fs24 , mientras que los electrones de l
a banda de conduccin dan lugar al proceso Ox\ul0\sub\cf3\f4\fs24 1\ul0\nosupersub
\cf2\f3\fs24 \u8594? Red\ul0\sub\cf3\f4\fs24 1\ul0\nosupersub\cf2\f3\fs24 . \up
0 \expndtw-2\charscalex100 Los semiconductores ms usuales presentan bandas de val
encia con potencial oxidante (+1 a \up0 \expndtw-3\charscalex100 +3,5 V) y banda
s de conduccin moderadamente reductoras (+0,5 a -1,5 V) [64]. As pues, en \up0 \ex
pndtw-1\charscalex100 presencia de especies redox adsorbidas en la partcula de se
miconductor y bajo iluminacin, \up0 \expndtw0\charscalex108 ocurren simultneamente
reacciones de oxidacin y de reduccin en la superficie del \up0 \expndtw-3\charsca
lex100 semiconductor. Este tema se discute en detalle en los \ul0\nosupersub\cf1
1\f12\fs24 Captulos 3\ul0\nosupersub\cf2\f3\fs24 -\ul0\nosupersub\cf11\f12\fs24 5
\ul0\nosupersub\cf2\f3\fs24 . \par\pard\sect\sectd\fs24\paperw11900\paperh16840{
\shp
z-10000\shplid21
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00514514005145140051451400514514005145140051451400514514005145140051451400514514
00514514005145140051451400514514005145140051451400514514005145140051451400514514
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ff00675ffe77347fc3a77fe0965ff48d3fd803ff0010dff675ff00e7735f7fd1401f007fc3a77fe0
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f7fd1401f007fc3a77fe0965ff0048d3fd803ff10dff00675ffe77347fc3a77fe0965ff48d3fd803
ff0010dff675ff00e7735f7fd1401f007fc3a77fe0965ff48d3fd803ff0010dff675ff00e77347fc
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f10dff00675ffe77347fc3a77fe0965ff48d3fd803ff0010dff675ff00e7735f7fd1401f007fc3a7
7fe0965ff48d3fd803ff0010dff675ff00e77347fc3a77fe0965ff0048d3fd803ff10dff00675ffe
7735f7fd1401f007fc3a77fe0965ff0048d3fd803ff10dff00675ffe77347fc3a77fe0965ff48d3f
d803ff0010dff675ff00e7735f7fd1401f007fc3a77fe0965ff48d3fd803ff0010dff675ff00e773
47fc3a77fe0965ff0048d3fd803ff10dff00675ffe7735f7fd1401f1efc30ff82797ec05f04bc73a
17c4ff00831fb0dfec7bf08fe25f85defe4f0cfc43f861fb33fc16f00f8e7c3afaae977da1ea8fa1
78b7c29e09d275fd21f52d1753d4b47bf6d3f50b7379a5ea17da7dc192d2ee7864fb0a8a2800a28a
2800a28a2800a28a2800a28a2800a28a2800a28a2803ffd9}}}}}\pard\sb0\sl-240{\bkmkstart
Pg22}{\bkmkend Pg22}\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb0\sl230\slmult0\par\pard\li1133\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expndtw-2\chars
calex100 \ul0\nosupersub\cf4\f5\fs20 24\tab \up0 \expndtw-2\charscalex100 Domnech
, Jardim y Litter\par\pard\ql \li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0
\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\s
l-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-23
0\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\
slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\sl
mult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmu
lt0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult
0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0
\par\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \p
ar\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par
\pard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\p
ard\ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb0\sl-230\slmult0 \par\par
ql\li1133\sb0\sl-230\slmult0 \par\pard\ql\li1133\sb192\sl-230\slmult0 \up0 \expn
dtw0\charscalex100 Figura 10. Procesos redox en la interfaz semiconductor-electr
olito bajo iluminacin. \par\pard\qj \li1133\ri1490\sb273\sl-275\slmult0\fi566 \up
0 \expndtw0\charscalex105 \ul0\nosupersub\cf2\f3\fs24 La eficiencia de la reaccin

fotocataltica depende de diversos factores. Uno de los \up0 \expndtw0\charscalex
102 aspectos ms crticos es la alta probabilidad de recombinacin electrn-hueco, que c
ompite \up0 \expndtw0\charscalex100 con la separacin entre las cargas fotogenerad
as. Por otra parte, como no hay una separacin \up0 \expndtw-2\charscalex100 fsica
entre los sitios de las reacciones andicas (oxidacin por huecos) y catdicas (reducc
in \up0 \expndtw0\charscalex103 por electrones), pueden tener importancia la
s reacciones inversas. La baja eficiencia, \up0 \expndtw0\charscalex107 espec
ialmente con luz visible, es una de las limitaciones ms severas de la fotocatlisis
\up0 \expndtw0\charscalex105 heterognea. Para aumentar la eficiencia del proceso
fotocataltico, se intentado diversas \up0 \expndtw0\charscalex104 estrategias, q
ue se resumen en el cuadro siguiente. Todos estos conceptos sern vistos en \up0 \
expndtw-3\charscalex100 mayor profundidad en los \ul0\nosupersub\cf11\f12\fs24 C
aptulos 3\ul0\nosupersub\cf2\f3\fs24 -\ul0\nosupersub\cf11\f12\fs24 6\ul0\nosuper
sub\cf2\f3\fs24 . \par\pard\ql \li2494\sb0\sl-230\slmult0 \par\pard\ql\li2494\sb
93\sl-230\slmult0 \up0 \expndtw0\charscalex102 \ul0\nosupersub\cf4\f5\fs20 Cuadr
o VII: Estrategias para mejorar la eficiencia del proceso fotocataltico. \par\par
d\ql \li1133\ri1533\sb54\sl-226\slmult0\tx1493\tx1493\tx1493\tx1493\tx1493\tx149
3 \up0 \expndtw-1\charscalex100 \u8226? Modificacin del semiconductor: ya sea p
ara extender su respuesta a radiaciones de mayor longitud de onda \line\tab \up0
\expndtw0\charscalex102 o bien para incrementar la eficiencia en la separacin el
ectrn-hueco y minimizar su recombinacin. La \line \tab \up0 \expndtw-2\charscalex1
00 separacin efectiva de las cargas fotogeneradas puede conseguirse, por ejemplo,
por medio de la deposicin \line \tab \up0 \expndtw0\charscalex106 de metales en
la superficie del semiconductor [65-66]. La presencia de depsitos metlicos sobre l
a \line \tab \up0 \expndtw-2\charscalex100 superficie del semiconductor altera l
as propiedades elctricas de ste, puesto que se crean nuevas interfaces \line \tab
\up0 \expndtw0\charscalex106 de tipo metal-semiconductor. Otro aspecto muy estud
iado ha sido el dopado del semiconductor con \line \tab \up0 \expndtw-3\charscal
ex100 impurezas de metales de transicin. Este tema se discute en detalle en los \
ul0\nosupersub\cf13\f14\fs20 Captulos 3\ul0\nosupersub\cf4\f5\fs20 y \ul0\nosupe
rsub\cf13\f14\fs20 7\ul0\nosupersub\cf4\f5\fs20 . \par\pard\ql \li1133\ri1534\sb
91\sl-230\slmult0\tx1491\tx1491 \up0 \expndtw0\charscalex100 \u8226? Uso de un
sistema de semiconductores acoplados: la iluminacin de uno de los dos produce un
a respuesta \line\tab \up0 \expndtw0\charscalex100 en el otro semiconductor o en
la interfaz entre los dos [67]. Con ello se logra aumentar la eficiencia de la
\line \tab \up0 \expndtw-3\charscalex100 separacin de cargas fotogeneradas y exte
nder la respuesta a irradiaciones menos energticas. \par\pard\ql \li1133\ri1532\s
b70\sl-230\slmult0\tx1491\tx1491 \up0 \expndtw0\charscalex100 \u8226? Uso de f
otocatalizadores soportados, con aplicacin de potenciales elctricos: de esta forma
, se separan las \line\tab \up0 \expndtw-1\charscalex100 reacciones andicas y catd
icas, y se reduce drsticamente la recombinacin electrn - hueco. Este tema se \line
\tab \up0 \expndtw-4\charscalex100 discute en el \ul0\nosupersub\cf13\f14\fs20 C
aptulo 7\ul0\nosupersub\cf4\f5\fs20 . \par\pard\qj \li1133\sb0\sl-280\slmult0 \pa
r\pard\qj\li1133\ri1500\sb9\sl-280\slmult0\fi566 \up0 \expndtw0\charscalex100 \u
l0\nosupersub\cf2\f3\fs24 A pesar de estas limitaciones, los procesos fotocatalti
cos basados en el material ms \line \up0 \expndtw0\charscalex100 comn, el dixido de
titanio, han alcanzado un elevado grado de madurez tecnolgica, y el \line \up0 \
expndtw0\charscalex100 objeto de este libro es precisamente ilustrar el grado de
desarrollo de estas aplicaciones. Si \par\pard\sect\sectd\fs24\paperw11900\pape
rh16840\pard\sb0\sl-240{\bkmkstart Pg23}{\bkmkend Pg23}\par\pard\li1702\sb0\sl-2
0\fi0\tx10500 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Procesos
avanzados de oxidacin para la eliminacin de contaminantes\tab \up0 \expndtw-1\cha
rscalex100 25\par\pard\qj \li1702\sb0\sl-280\slmult0 \par\pard\qj\li1702\sb0\sl280\slmult0 \par\pard\qj\li1702\ri927\sb180\sl-280\slmult0 \up0 \expndtw0\charsc
alex102 \ul0\nosupersub\cf2\f3\fs24 bien el rendimiento cuntico (nmero de eventos
producidos por fotn absorbido) suele ser \up0 \expndtw0\charscalex110 bajo en trmi
nos de conversin qumica, los rendimientos obtenidos, en trminos de \up0 \expndtw0\c
harscalex103 conversin en funcin del tiempo, aprovechando luz solar o iluminacin co
n lmparas son \up0 \expndtw0\charscalex103 adecuadamente elevados en muchos casos

[68]. \par\pard\qj \li1702\ri919\sb100\sl-280\slmult0\fi566 \up0 \expndtw-3\cha
rscalex100 Los huecos, despus de migrar a la superficie, reaccionan con sustancia
s adsorbidas, en \up0 \expndtw0\charscalex108 particular con el agua o los ione
s OH\ul0\super\cf3\f4\fs24 -\ul0\nosupersub\cf2\f3\fs24 adsorbidos, generando r
adicales HO\ul0\super\cf3\f4\fs24 \u8226?\ul0\nosupersub\cf2\f3\fs24 y/o otros
\up0 \expndtw0\charscalex100 radicales. La fotocatlisis comparte pues con las otr
as TAOs la caracterstica de involucrar \up0 \expndtw-2\charscalex100 radicales hi
droxilo en el mecanismo de reaccin. Normalmente, en aplicaciones ambientales, \up
0 \expndtw0\charscalex100 los procesos fotocatalticos se llevan a cabo en ambient
es aerbicos, con lo cual el oxgeno \up0 \expndtw-1\charscalex100 adsorbido es la p
rincipal especie aceptora de electrones: \par\pard\li1702\sb215\sl-276\slmult0\f
i0\tx2669\tx10342 \up0 \expndtw-5\charscalex100 O\ul0\sub\cf3\f4\fs24 2\ul0\nosu
persub\cf2\f3\fs24 + e\ul0\super\cf3\f4\fs24 -\tab \up0 \expndtw-5\charscalex
100 \ul0\nosupersub\cf2\f3\fs24 \u8594?
O\ul0\sub\cf3\f4\fs24 2\u8226?-\tab \
up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs24 (57)\par\pard\qj \li170
2\ri927\sb178\sl-270\slmult0\fi566 \up0 \expndtw-1\charscalex100 Si las aguas co
ntienen iones metlicos nobles o pesados, los electrones de la banda de \up0 \expn
dtw-4\charscalex100 conduccin pueden reducirlos a un estado de oxidacin ms bajo, e
incluso precipitarlos como \up0 \expndtw-5\charscalex100 metales sobre el semico
nductor: \par\pard\li1728\sb220\sl-276\slmult0\fi0\tx3149\tx10375 \up0 \expndtw5\charscalex100 M\ul0\super\cf3\f4\fs24 z+\ul0\nosupersub\cf2\f3\fs24 + n e\u
l0\super\cf3\f4\fs24 -bc\tab \up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\f
3\fs24 \u8594?
M\ul0\super\cf3\f4\fs24 (z-n)+\tab \up0 \expndtw-6\charscalex1
00 \ul0\nosupersub\cf2\f3\fs24 (58)\par\pard\qj \li1702\ri930\sb167\sl-280\slmul
t0\fi566 \up0 \expndtw-2\charscalex100 La factibilidad del proceso depende crtica
mente de la estabilidad del semiconductor, y \line \up0 \expndtw0\charscalex103
ello limita severamente las opciones de eleccin de los materiales, como se discut
e en el \line \up0 \expndtw-5\charscalex100 \ul0\nosupersub\cf11\f12\fs24 Captulo
3\ul0\nosupersub\cf2\f3\fs24 . \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\par
d\ql\li1702\sb268\sl-276\slmult0 \up0 \expndtw0\charscalex101 AGRADECIMIENTOS \p
ar\pard\qj \li1702\sb0\sl-230\slmult0 \par\pard\qj\li1702\ri966\sb52\sl-230\slmu
lt0\fi566 \up0 \expndtw0\charscalex100 \ul0\nosupersub\cf4\f5\fs20 Este trabajo
es parte del proyecto CNEA-CAC-UAQ #95-Q-03-05. M.I.L. agradece a la Red CYTED \
line \up0 \expndtw0\charscalex100 VIII-G, al CONICET y a la ANPCYT (Argentina) p
or fondos para esta investigacin. M.I.L. es miembro de \line \up0 \expndtw0\chars
calex100 CONICET. \par\pard\ql \li1702\sb0\sl-276\slmult0 \par\pard\ql\li1702\sb
276\sl-276\slmult0 \up0 \expndtw0\charscalex101 \ul0\nosupersub\cf2\f3\fs24 BIBL
IOGRAFA \par\pard\li1702\sb0\sl-230\slmult0\par\pard\li1702\sb5\sl-230\slmult0\fi
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start Pg24}{\bkmkend Pg24}\par\pard\li1133\sb0\sl-230\slmult0\par\pard\li1133\sb
0\sl-230\slmult0\par\pard\li1133\sb18\sl-230\slmult0\fi0\tx8050 \up0 \expndtw-2\
charscalex100 \ul0\nosupersub\cf4\f5\fs20 26\tab \up0 \expndtw-2\charscalex100 D
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