1-28-208 3:@5PM FROM METSS 6147972201 P.2 SMI, Inc. 12219 SW 131 Avenue Phone: (305) 971-7047 Miami, Florida 33186-6491 USA Fax: (305) 971-7048 eer Attn: Bill Ricks Date: 14-Jan-2003 Metss Corgioration 300 Westdale Avenue SMUREF: 02DEC514 Westerville. OH 43082 Product; METSS ATO Aircraft Toilet Deodorant; 12/06/02 (rec'd 09-Dec-2002) Dilution: Ready to Use Page 1 of 6 Partial Testing in Accordance with AMS 1476B DEODORANT, AIRCRAFT TOILET. 3.2.2, Deodorant in Diliited Form 3.2.2.1. Viscosity Conforms 3.222 Foam Volune Conforms 3.22.3 . Surface Tension Conforms 3.2.24 Waste Matirial Reactivity Conforms 3.2.3, Deodorant Tested both as Concentrate and Diluted Form Concentrate Dilute pH 7.0 86 Effect on Unpainted Surfaces Con Conforms Effect on Painted Surfaces Conforms : form: Effect on Metallic Surfaces Sandwich Corrosion Conforms Conforms Total Immersion Corrosion e ms Temperature Stability Co Conforms Fabric Stain Test Conforms Conforms. Solubility Not applicable Conforms Effect on Rubber and Plastic Matarials Conforms Conforms Effect on Polycarbonate Plastic Conforms Conforms Miscit Conforms. ectfull STi Patricia D- Vieni, Mino ine. SCIENTIFIC MATERIAL INTERNATIONAL www.smiine.com1-20-203 3:07PM Client: Product: Dilutior FROM METSS 6147972201 Metss Corsoration Date: 14-Jan-2003 METSS ATD Aircraft Toilet Deodorant; 12/06/02 Ready to Use SMUREF: 02DEC514 Page 2 of 8 3.2.2 Deodorant in Dilu ed Form: Shall be as foltows, determined on deodorant diluted to the prime charge {See 8.2) with ASTM D1193, Type IV, water. 3.2.24 3.2.2.2 3.2.2.2.1 3.2.23 3.2.24 3.2.244 Viscosity: Shall not exceed by more than 10% the viscosity of ASTM 01193, Type IV, water at 10°C (50°F) and 30°C (80°F), determined in accordance with ASTM D445. Result, Conforms Foam Volime: Shall not exceed 5 mL after testing in accordance with 3.2.2.2.1. 100mL of the deodorant shall be put into @ stoppered 250 mL graduated cylinder and inverted.10 times in 16 seconds and the initial foam volume. recorded; after standing undisturbed for 150 seconds +1, the foam value shall again be measured and recorded. The second reading shall not exceed bmL. "Foam volume: less than 5 ml Result Conforms ‘Surface Tension: The deodorant shall have weiting characteristics such that it reduces tne surface tension of water to 10% below that of ASTM D1193, Type IV, dilutent water, determined in accordance with ASTM 01331 at 25°C43 (77°F 45). Result, Conforms Waste Material Reactivity: The deodorant shall mask the color and odor of human waste materials. A green-blue color and odor, which remains slightly perfumed, riever offensive or overpowering, shall be retained after testing as specified in paragraph 3.2.2.4.1.1. To1 pint (47’5mL) of deodorant shall be added 4 pint (600mL) of raw sewage (the raw sewage shall be made up of 120 g of fresh feces and 825ml fresh urine thoroughly mixed in Waring blender, or similar high speed mixing device). A 1-gallon container or SL. beaker is suitable for this purpose. The resultant mxture shall be agitated for 5 minutes using a 1 inch (25mm) diameter 3 bladed propeller type stirrer running at 1000 rpm + 100. The remaining urine/feces mixture shall be diluted with an equal volume of water ang retained for use as the control sample when evaluating the odor of the deodorantivaste mixture as in paragraph 3.2.2.4.1.1.1-20-283 3:27PM FROM METSS 6147972201 Pla Metss Corsoration Date: 14-Jan-2003 METSS AD Aircraft Toilet Deodorant; 12/06/02 Dilution: Ready to Use SMUREF: 02DEC514 AMS 14768 _Page 3 of 6 3.2.2.4 Waste Material Reactivity: (continued): 3.22.4.1.1. After a lapse of 8 hours the odor control sample shall be rated as 4+, the deodorantiwaste shall be rated as follows: 4+ = Very strong odor Strong odor Moderate odor (reodorant detectable) Slight odor (reodorant noticeable) No presence of odor (reodorant predominant) Rating after 8 hours: 1 + Result, Conforms 3.2.3 Deodorant Tested Both as Concentrate as defined in 3.2.1 and in Diluted Form as defined in 8.2. 3.2.3.1 BH: Shall be determined in accordance with ASTM E70 and reported. Realy tose: 7.8 Result____Informational__ 3.2.3.2 Effect on U»painted Surfaces: There shall be no visible stains or residue on test panels: tested in accordance with ASTM F485. Result____Conforms 3.2.3.3 Effect on Painted Surfaces: The product shall neither decrease the hardness of the paint film by more than 2 pencil hardness levels nor shall it produce any streaki7g, discoloration, or blistering of the paint film, determined in accordance with ASTM F502. Ready to Use: PASS Result, Conforms 32.3.4 . Effect on Matallic Surfaces: $.2.3.4.1 Sandwich Corrosion: Specimens of AMS 4049 aluminum alloy, after testing in accordance with ASTM F 1110, shall show no evidence of corrosion worse els tested in ASTM D 1193, Type IV, water. than specimen AMS 4049 Alclad Ready to Use i Control (Water)1-20-283 3:@8PM Client: Product: Dilution: AMS 14763 3.2.3.4.2 3.23.5 3.2.3.6 3.2.3.7 3.2.3.7.1 FROM METSS 6147972201 Metss Corporation Date: 14-Jan-2003 METSS ATD Aircraft Toilet Deodorant; 12/06/02 Ready to Use ‘SMUREF: Page 4 of 6 ‘Total immersion Corrosion: The deodorant shall neither show evidence of corrosion cf the panels nor cause a weight change greater than 0.3 mg/cm? per 24hrs for any panel of AMS 4049 aluminum alloy, determined in accordance with ASTM F483. Ready toUse: — <0.01 mg/em* Result____Conforms ‘Temperature Stability: The deodorant shall show no chemical or physical deterioraticn, including evidence of discoloration, layering or other change denoting Icss of stability after being exposed for 120 hours +1 to 2°C#2 (85°F #5) and to 50°C-+5 (120°F +10). Result, Conforms. O2DEC514 Fabric Stain Test: ‘The deodorant shall not stain 2X2 inch (50X60mm) samples of white 100% cotton, light colored nylon, and light colored wool when spotied with the deodorant. The spotted fabric samples shall be allowed to viry at 60°C+3 (140°F+5), washed with a commercial detergent, rinsed and dried. The presence of any stain remaining on any of the three types of fatiic shall be reported. no stain Result, Conforms ‘Solubility: ‘The detergent shall be fully soluble in both hard and soft water and shall produce no detectable precipitate, determined in accordance with 3.2.3.7.4. One set of two samples of the deodorant shall be diluted in accordance with Paragraph ‘i.2.2; the other sample shall be diluted using 20 grain hard water solution made up by dissolving 0.40 g + 0.005 of analytical reagent calcium acetate (Cz(C,H,0,), and 0.28 g+0.006 of analytical reagent magnesium sulfate (Mg$O,7H,0) in 4 L of boiling ASTM D1193 Type IV water. After stirring vigorously for not less than 1 minute, both samples shall be allowed to stand uridisturbed for 15 minutes #1, and examined for evidence of precipitation. hard water: no precipitate present. soft water: no precipitate present. Result Conforms.120-203 3:08PM FROM METSS 6147972201 Client: Metss Corporation Date: 14-Jan-2003 Product: METSS ATD Aircraft Toilet Deodorant; 12/06/02 Dilution: Ready to Use SMUREF:. O2DEC514 AMS 14768 3.23.8 n Rubber and Plastic Materials: The deodorant shall neither cause swelling gnaater than 10%, determined in accordance with ASTM D471, nor cause stairing, discoloration, or evidence of degradation of rubber or plastic materials normally incorporated in aircraft lavatory systems. Materials listed in 3.2.3,8.1 shall be tested in accordance with 3.2.3.8.2. When specified by purchaser, tests to determine changes in tensile strength and elongation shall be performed in accordance with ASTM D471 and the results obtained ‘on exposed specimens shall not be lower than 75% of the tensile strength and elongation values. determined on unexposed specimens. 3.2.3.8.1 Test specimens shall be composed of: Observed Effect after immersion ethylene propylens (EPM) no effect no effect fivorositicone (FVIAQ) no effect no effect methy!-phenyl-silicone (PMQ) no effect no effect chloroprene (CR) no effect no effect acrylonitrile butadiene (NBR) no effect no effect fluorocarbons (FKM) no effect no effect rubbers no effect no effect acetal no affect no effect polysulfone no effect no effect nylon no effect no effect polycarbonate plastics no effect no effect epoxy-glass laminates no effect no effect glass fabric no effect no effect 3.2.3.8.2 Duplicate s:rips of material listed in 3.2.3.8.1 shall be placed in test tubes containing ihe deodorant. Strips for determining volume change shail be totally immorsed. Strips for determination of staining, discoloration, and evidence of degradation shall be partially immersed so that the bottom halfis in the deodorant and the top haif is in the air. The test tubes shall be capped and stored at ambient temperature for 30 days. After this exposure the immersed and non-immersed area of each of the partially immersed ‘specimens shall be compared visually for evidence of staining, discoloration, ‘or degradat on and the results noted, Volume change shall be determined on the totally immersed specimens and the values compared with those of untreated samples from the same source. Any change in volume shall be reported. Result Conforms1-28-2083 3:Q9PM Client: Product: Dilution: 4761 3.2.3.8.3 3.2.3.9 FROM METSS 6147972201 Metss Corporation Date: 14-Jan-2003, METSS ATD Aircraft Toilet Deodorant; 12/06/02 Ready to Use SMIREF: 02DEC514 Pa Effect on Polycarbonate Plastics: Deodorant shall not craze, stain or discolor Mil-P-83310 polycarbonate plastic, determined in accordance with test procedures specified in ASTM F484 on specimens stressed for 30 minutes +2 to an outer fiber stress of 2000 psi(13.8MPa). Reaiy to Use: No crazing, staining, or discoloration. Result. Conforms Misoibility: The deodorant shall be miscible in mixtures of water and either ethylene glycol or propylene glycol. A solution made up in accordance with 3.2.2, except that 50% of the dilutent water shall be replaced with elther ‘ethylene glycol or propylene glycol, shall show complete stability after storage for 7 days at 24°C +3(75°F +5). Result_____Conforms ___