DISEO FACTORIAL PARA TRES VARIABLES (K=3)

Niveles
Inferior
Superior
70
100
24
72
500
1000

VARIABLES
Z1: Grado de Molienda (% - 200M)
Z2: Tiempo de Cianuracin (Horas)
Z3: Cianuro de Sodio (PPM)
MATRIZ DE DISEO EXPERIMENTAL (K=3)

N
1
2
3
4
5
6
7
8
9
10
11

ESCALA CODIFICADA
X1
X2
-1
1
-1
1
-1
1
-1
1
0
0
0

-1
-1
1
1
-1
-1
1
1
0
0
0

ESCALA NATURAL
Z2

X3

Z1

-1
-1
-1
-1
1
1
1
1
0
0
0

70
100
70
100
70
100
70
100
85
85
85

24
24
72
72
24
24
72
72
48
48
48

MATRIZ DE VARIABLES INDEPENDIENTES CODIFICADO

N
1
2
3
4
5
6
7
8
9
10
11

X0

X1

X2

X3

X1*X2

1
1
1
1
1
1
1
1
0
0
0

-1
1
-1
1
-1
1
-1
1
0
0
0

-1
-1
1
1
-1
-1
1
1
0
0
0

-1
-1
-1
-1
1
1
1
1
0
0
0

1
-1
-1
1
1
-1
-1
1
0
0
0

CALCULO DE EFECTOS
X0

X1

X2

X3

X1*X2

X1*X3

656.5

-0.90
-0.23
0.10

4.1
1.03
2.10

4.7
1.18
2.76

-1.7
-0.43
0.36

0.9
0.22
0.10

ALGORITMO F. YATES

METODO DE ALGORITMO DE YATES

EFECTOS

1
X1
X2

81.50
81.20
81.90

162.70
163.20
163.50

325.90
330.60
-0.90

656.50
-0.90
4.10

164.13
-0.23
1.03

X1*X2
X3

81.30

167.10

0.00

-1.70

-0.43

81.40

-0.30

0.50

4.70

1.18

X1*X3

82.10

-0.60

3.60

0.90

0.22

X2 X3

83.90

0.70

-0.30

3.10

0.78

X1*X2*X3

83.20

-0.70

-1.40

-1.10

-0.27
Efectos

ANALISIS DE LA VARIANZA (ANAVA)

El clculo de la suma de cuadrados del error (SSE) se define por:

SSE= _(i=1)^n0(Yi2
Y
0)
Y : Replicas en el punto central del diseo.
i

Y0: Promedio de todas las Replicas.

n0: Nmero de replicas en el centro del diseo.

La suma de los cuadrados para la curvatura esta dado por:

SSCurvatura = Nn0(Yi
-Y0)
N+n0 del diseo.
Y : Promedio
de los puntos exteriores
i

DETERMINACION DE SIGNIFICANCIA DE LAS VARIABLES

METODO DE W.G.COCHRAN
SSEfectos

Grados de
Libertad

Media de
Cuad.

X1
X2
X3

Fuente de
Variacion
X1
X2
X3

0.101
2.101
2.761

1
1
1

0.101
2.101
2.761

1.08
22.51
29.58

X1*X2

X1*X2

0.361

0.361

3.87

X1*X3

X1*X3

0.101

0.101

1.08

X2*X3

X2*X3

1.201

1.201

12.87

X1*X2*X3
SSCurvatura
SSE

X1*X2*X3

0.151

0.151

1.62

Curvatura
Error
Total

1.082
0.187
8.047

1
2
10

1.082
0.093

11.59

MODELO MATEMATICO A ESCALA CODIFICADO

[B] = ([X]T[X])-1 *
([X]T[Y])

[B] = ([X]T[X])-1 *
([X]T[Y])
([X]T[X])-1 = 1 /
N
Coeficiente Codificado = [DIAGONAL] *
: Numero de Pruebas = 8
([X]NT[Y])
[DIAGONAL] ([X]T[X])-1
0.125
0
0
0
0
0
0
0

0
0.125
0
0
0
0
0
0

0
0
0.125
0
0
0
0
0

0
0
0
0.125
0
0
0
0

0
0
0
0
0.125
0
0
0

0
0
0
0
0
0.125
0
0

X0

X1

X2

X3

X1*X2

X1*X3

82.06

-0.11

0.51

-0.21

0.59

0.11

Y = 82.06 -0.11X1 + 0.51X2 - 0.21X3 + 0.59 X1 X2 +0.11X1 X3 + 0.39X

Numero de Pruebas
Numero de Pruebas Centrales
Total de Pruebas
N=2k

8
3
11
8

85
48
750

ESCALA NATURAL
Z3
500
500
500
500
1000
1000
1000
1000
750
750
750

% Extrac. Au
81.5
81.2
81.9
81.3
81.4
82.1
83.9
83.2
83.1
82.5
82.7

X1*X3

X2*X3

X1*X2*X3

1
-1
1
-1
-1
1
-1
1
0
0
0

1
1
-1
-1
-1
-1
1
1
0
0
0

-1
1
1
-1
1
-1
-1
1
0
0
0

X2*X3

X1*X2*X3

3.1
0.78
1.20

-1.1
-0.27
0.15

Exi
SS Efectos

Y(Obs)
81.50
81.20
81.90
81.30
81.40
82.10
83.90
83.20
83.10
82.50
82.70
82.77

X1

82.06

-81.5
81.2
-81.9
81.3
-81.4
82.1
-83.9
83.2
-0.9

SS EFECTOS
(4TA COLUMNA)

SS EFECTOS
(5TA COLUMNA)

53874.03
0.10
2.10

3367.13
0.01
0.13

0.36

0.02

2.76

0.17

0.10

0.01

1.20

0.08

0.15

0.01
SS Efectos

Yi
Y0
SSE

82.06

SSCurvatura

1.082

RIABLES
Significancia

]T[X])-1 *

No
Si
Si
No
No
No
No
No

F al 95%

LEER NOTA

18.51

82.77
0.187

]T[X])-1 *
T
[X])-1 = 1 /

GONAL] *

)-1

[X]T[Y]
0
0
0
0
0
0
0.125
0

0
0
0
0
0
0
0
0.125

X2*X3

X1*X2*X3

0.39

-0.14

.11X1 X3 + 0.39X2 X3 - 0.14X1 X2 X13

656.50
-0.90
4.10
-1.70
4.70
0.90
3.10
-1.10

X2

X3

X1*X2

X1*X3

X2*X3

X1*X2*X3

-81.5
-81.2
81.9
81.3
-81.4
-82.1
83.9
83.2

-81.5
-81.2
-81.9
-81.3
81.4
82.1
83.9
83.2

81.5
-81.2
-81.9
81.3
81.4
-82.1
-83.9
83.2

81.5
-81.2
81.9
-81.3
-81.4
82.1
-83.9
83.2

81.5
81.2
-81.9
-81.3
-81.4
-82.1
83.9
83.2

-81.5
81.2
81.9
-81.3
81.4
-82.1
-83.9
83.2

4.1

4.7

-1.7

0.9

3.1

-1.1

VARIABLES
Z1: Xantato z-11 (g/TM)
Z2: pH de la Pulpa

N
1
2
3
4
5
6
7
8
1

NIVEL
inferior
superior
50
100
7
10

Centro de diseo
Z
75
8.5

DISEO HEXAGONAL
CODIFICADO
X1
X2
Z1
1
0
100.0
0.5
0.866
87.5
-0.5
0.866
62.5
-1
0
50.0
-0.5
-0.866
62.5
0.5
-0.866
87.5
0
0
75.0
0
0
75.0
0
0
75.0

NATURAL

CODIFICADO
N
1
2
3
4
5
6
7
8
9

MATRIZ [X]
Xo
1
1
1
1
1
1
1
1
1

X1
1.000
0.500
-0.500
-1.000
-0.500
0.500
0.000
0.000
0.000

X2
0.000
0.866
0.866
0.000
-0.866
-0.866
0.000
0.000
0.000

1
1
0
1
0
0

1
0.5
0.866
0.250
0.750
0.433

1
-0.5
0.866
0.250
0.750
-0.433

9
0
0

0
3
0

TRANSPUESTA [X

PRODUCTO DE LAS MATRICES ([X]^T)*[X]

0
0
2.999824

3
2.999824
0

0
0
0

0
0
0

INVERSA DE LA MATRIZ (([X]^T)*[X])^-1 MATRIZ DE CORRE

0.333333
0.0
0.0
0.0
0.333333
0.0
0.0
0.0
0.333353
-0.333333
0.0
0.0
-0.333353
0.0
0.0
0.0
0.0
0.0

PRODUCTO ([X]^T)*[Y]
781.90
4.15
1.30
260.83
262.26
0.22

( ([X]^T) * [X] )^-1 * ([X]^T) * [Y]

86.27
1.38
0.43
0.43
1.40
0.29

MODELO MATEMATICO CO
Y

86.27

1.38

X1

DISEO HEXAGONAL

Radio de diseo
Z
25
1.5

AL
NATURAL

Z2
8.50
9.80
9.80
8.50
7.20
7.20
8.50
8.50
8.50

87.7
89
86.6
85.7
86.1
88
86.6
86
86.2

X1^2
1.00
0.25
0.25
1.00
0.25
0.25
0.00
0.00
0.00

X2^2
0.00
0.75
0.75
0.00
0.75
0.75
0.00
0.00
0.00

DIFICADO
MATRIZ [X]

TRANSPUESTA [X]^T
1
1
-1
-0.5
0
-0.866
1
0.250
0
0.750
0
0.433

TO DE LAS MATRICES ([X]^T)*[X]

3
2.999824
0
0
0
0

X1X2
0.00
0.43
-0.43
0.00
0.43
-0.43
0.00
0.00
0.00

VECTOR [Y]
Y
87.7
89
86.6
85.7
86.1
88
86.6
86
86.2

1
0.5
-0.866
0.250
0.750
-0.433

1
0
0
0
0
0

0
0
0

1
0
0
0
0
0

1
0
0
0
0
0

2.25
0.749956
0

0.749956
2.249736008
0

0
0
0.749956

IZ (([X]^T)*[X])^-1 MATRIZ DE CORRELACION

-0.333333
-0.333353
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.833333
0.166676
0.0
0.166676
0.833431
0.0
0.0
0.0
1.333412

MODELO MATEMATICO CODIFICADO

0.43
X2
0.43

X1^2

1.40

X2^2

0.29

X1*X2