T Method

method: C:\CHEM32\1\METHODS\TOGA_PARAFFINOIL.
M
Modified on: 12/10/2011 at 10:35:25 AM
Method Information
Method: C:\CHEM32\1\METHODS\TOGA_PARAFFINOIL.M
Modified: 12/10/2011 at 10:35:25 AM
Method Audit Trail

Operator
: Testing Engineer
Date
: 01\09\2011 10:53:27 AM
Change Info: This method was created at 01\09\2011 10:53:27 AM and based on
method C:\CHEM32\1\METHODS\TOGA_PARAFFINOIL.M
Operator
: Testing Engineer
Date
: 01\09\2011 10:53:27 AM
Change Info: Method saved. User comment: ""
Operator
: Testing Engineer
Date
: 05\09\2011 11:02:57 AM
Operator
: Testing Engineer
Date
: 05\09\2011 11:14:35 AM
Operator
: Testing Engineer
Date
: 06\09\2011 12:06:15 PM
Operator
: Testing Engineer
Date
: 13\09\2011 10:24:31 AM
Operator
: Testing Engineer
Date
: 14\09\2011 7:54:25 PM
Operator
: Testing Engineer
Date
: 17\09\2011 3:33:29 PM
Operator
: Testing Engineer
Date
: 12/10/2011 10:35:25 AM
Run Time Checklist
Instrument 1 13/10/2011 3:30:43 PM Testing Engineer
Page
1 of 10
method: C:\CHEM32\1\METHODS\TOGA_PARAFFINOIL.M
Modified on: 12/10/2011 at 10:35:25 AM
Pre-Run Cmd/Macro: off
Data Acquisition:
on
Standard Data Analysis:
on
Customized Data Analysis:
off
Save GLP Data:
off
Post-Run Cmd/Macro:
off
Save Method with Data:
on
Injection Source and Location

Injection Source:
Headspace Sampler
Injection Location: Front
Page
2 of 10
Modified on: 12/10/2011 at 10:35:25 AM
HEADSPACE PARAMETERS
Headspace Device:
Communications Mode:
Serial Number:
Firmware Revision:
Vial Size, mL:
Handshake Mode:
Oven Stabilization Time, min:
Pressure Units:
Carrier Connection:
Vial EPC:
Agilent G1888 Headspace Sampler

COM1
IT00943016
A.01.10
20
Headspace Proceed
1
psi
Front Inlet (EPC)
Aux1
Multi HS Extr:
Extractions Per Vial:
GC Cycle Time (Min):
Inject Time (Min):
Loop Equilibration Time (Min):
Loop Fill Time (Min):
Loop Temperature:
Oven Temperature:
Shake:
Transfer Line Temperature:
Vial Equilibration Time (Min):
Vial Pressurization Time (Min):
OFF
2
20.0
0.90
0.25
0.25
150
70
HIGH
150
1.0
0.25
=====================================================================
Agilent 7890A
=====================================================================
Oven
Equilibration Time
Oven Program
40 C for 6 min
then 24 C/min to 230 C for 0 min
Run Time
Thermal Aux 1 {Nickel Catalyst}

Heater
Temperature Program
375 C for 0 min
Run Time
0.5 min
On
13.917 min
On
On
13.917 min
Column #1
plot q + plot molesieve: Agilent toga
Page
3 of 10
Modified on: 12/10/2011 at 10:35:25 AM
plot q + plot molesieve
300 C: Packed
In: PCM C-1 ArMe
Out: Front Detector FID
Flow Program
6.8948E+05 mL/min for 0 min
Run Time
On
13.917 min
Front Detector FID

Heater
H2 Flow
Air Flow
Makeup Flow
Const Col + Makeup
Flame
Electrometer
On
On
On
On
Off
On
On
250 C
50 mL/min
400 mL/min
5 mL/min
Back Detector TCD

Heater
Reference Flow
Makeup Flow
Const Col + Makeup
Negative Polarity
Filament
On
On
On
Off
On
On
150 C
20 mL/min
5 mL/min
Valve 1
Other
Off
Aux EPC 4 ArMe

Aux EPC 5 N2
***Excluded from Affecting GC's Readiness State***
Aux EPC 6 N2
PCM C-1 ArMe: Supplies Column 1
Flow Program
15 mL/min for 0 min
Run Time
On
13.917 min
Page
4 of 10
Modified on: 12/10/2011 at 10:35:25 AM
PCM C-2 ArMe
Valve Box
Heater
On
Signals
Front Signal
Save On
20 Hz
Save On
20 Hz
Save Off
50 Hz
Save Off
50 Hz
Back Signal
Test Plot
Test Plot
Run Time Events

Time (min)
1.521
3.1
8.1
13.87
100 C
Event
Valve
Valve
Valve
Valve
Position
Valve 1
Valve 1
Valve 1
Valve 1
Setpoint
On
Off
On
Off
========================================================================
Integration Events
========================================================================
-----------------------------------------------------------------------Non signal specific Integration Events

-----------------------------------------------------------------------Event
Value
|--------------------------------------------------------|-------------|
Tangent Skim Mode
Standard
Tail Peak Skim Height Ratio
0.000
Front Peak Skim Height Ratio
0.000
Skim Valley Ratio
20.000
Baseline Correction
Classical
Peak to Valley Ratio
500.000
Page
5 of 10
Modified on: 12/10/2011 at 10:35:25 AM
-----------------------------------------------------------------------Default Integration Event Table "Event"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
Initial Slope Sensitivity
1.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
Initial Height Reject
1.700
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_ADC"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
20.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_ECD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
100.000
Initial
Initial Peak Width
0.080
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_NPD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
500.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
Page
6 of 10
Modified on: 12/10/2011 at 10:35:25 AM
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_FPD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
50.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_uECD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
500.000
Initial
Initial Peak Width
0.080
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_TCD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
100.000
Initial
Initial Peak Width
0.020
Initial
Initial Area Reject
0.500
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_FID"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
50.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
10.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
Page
7 of 10
Modified on: 12/10/2011 at 10:35:25 AM
-----------------------------------------------------------------------Signal Specific Integration Event Table "Event_TCD2B"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
5.951
Initial
Initial Peak Width
0.041
Initial
Initial Area Reject
0.500
Initial
0.500
Initial
Initial Shoulders
OFF
Initial
Apply Manual Integration Events: No
=====================================================================
Calibration Table
=====================================================================
Calib. Data Modified
12/10/2011 10:33:10 AM
Rel. Reference Window :

Abs. Reference Window :
Rel. Non-ref. Window :
Abs. Non-ref. Window :
Uncalibrated Peaks
:
Partial Calibration
:
Correct All Ret. Times:
5.000 %
0.000 min
5.000 %
0.000 min
not reported
Yes, identified peaks are recalibrated
No, only for identified peaks
Curve Type
Origin
Weight
Linear
Included
Equal
:
:
:
Recalibration Settings:
Average Response
:
Average Retention Time:
Average all calibrations

Floating Average New 75%
Calibration Report Options :

Printout of recalibrations within a sequence:
Calibration Table after Recalibration
Normal Report after Recalibration
If the sequence is done with bracketing:
Results of first cycle (ending previous bracket)
Signal 1: FID1 A, Front Signal
Signal 2: TCD2 B, Back Signal
RetTime
Lvl
Amount
Area
Amt/Area Ref Grp Name
[min] Sig
[ppm]
-------|--|--|----------|----------|----------|---|--|--------------1.539 2 1
56.40000
12.61707
4.47014
Hydrogen
1.761 1 1
56.80000 415.49786 1.36703e-1
CO2
Page
8 of 10
Modified on: 12/10/2011 at 10:35:25 AM
RetTime
Lvl
Amount
Area
Amt/Area Ref Grp Name
[min] Sig
[ppm]
-------|--|--|----------|----------|----------|---|--|--------------2.327 1 1
54.20000 815.72711 6.64438e-2
Ethylene
2.563 1 1
55.80000 567.98010 9.82429e-2
Acetylene
2.817 1 1
53.10000 794.55457 6.68299e-2
Ethane
5.233 1 1
53.90000 201.16403 2.67941e-1
Methane
6.147 1 1
55.00000 391.49054 1.40489e-1
CO
8.110 2 1 108.70000
6.89525
15.76448
Nitrogen
More compound-specific settings:
Compound: Hydrogen
Compound Multiplier
: 1.097
Compound: CO2
Compound Multiplier
: 1.701
Compound: Ethylene
Compound Multiplier
: 2.331
Compound: Acetylene
Compound Multiplier
: 1.951
Compound: Ethane
Compound Multiplier
: 2.791
Compound: Methane
Compound Multiplier
: 1.431
Compound: CO
Compound Multiplier
: 1.134
Compound: Nitrogen
Compound Multiplier
: 1.181
=====================================================================
Peak Sum Table
=====================================================================
***No Entries in table***
=====================================================================
========================================================================
Sample related custom fields
========================================================================
Custom Field
Type
Mand. Default Value
-----------------------------------------------------------------------None defined
========================================================================
Compound related custom fields
========================================================================
Page
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Modified on: 12/10/2011 at 10:35:25 AM
Custom Field
Type
Mand. Default Value
-----------------------------------------------------------------------None defined
Page
10 of 10

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T Method

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method: C:\CHEM32\1\METHODS\TOGA_PARAFFINOIL.

Method Audit Trail

Run Time Checklist

Instrument 1 13/10/2011 3:30:43 PM Testing Engineer

Standard Data Analysis:

Customized Data Analysis:

Save GLP Data:

Save Method with Data:

Injection Source and Location

Injection Location: Front

Instrument 1 13/10/2011 3:30:43 PM Testing Engineer

Agilent G1888 Headspace Sampler

Thermal Aux 1 {Nickel Catalyst}

Front Detector FID

Back Detector TCD

Aux EPC 4 ArMe

Instrument 1 13/10/2011 3:30:43 PM Testing Engineer

Run Time Events

-----------------------------------------------------------------------Non signal specific Integration Events

Instrument 1 13/10/2011 3:30:43 PM Testing Engineer

Instrument 1 13/10/2011 3:30:43 PM Testing Engineer

Instrument 1 13/10/2011 3:30:43 PM Testing Engineer

Calib. Data Modified

Rel. Reference Window :

Average all calibrations

Calibration Report Options :

Instrument 1 13/10/2011 3:30:43 PM Testing Engineer

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