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Abstract—We present a viscosity sensing method based on a fiber inside the fluid. The main disadvantages of this kind of viscome-
Bragg grating (FBG), which is longitudinally excited by an acous- ter are bulky size and the time-consuming and low-precision
tic transducer. The reflection spectrum of the FBG is broadened measurements. Most commercial viscometers are based on ro-
by spatial modulation of the FBG caused by the applied acoustic
wave. The reflection bandwidth of the acoustically modulated FBG tational or vibrational techniques. The rotational viscometer is
decreases with increasing viscosity of the liquid surrounding the suitable for a wide range of applications and the measuring pro-
FBG. The sensing mechanism relies on the reduction in spatially cess is simple. However, like most viscometers, it is bulky, not
periodic strain in the FBG caused by the viscosity of the surround- portable, and not suitable in-situ measurements. The vibrational
ing fluid. Experimental results show that the bandwidth of the FBG viscometer is mostly used for low viscosity liquids. Their ad-
changes from 0.41 to 0.27 nm as the viscosity increases from 1.0 to
5.5 mPa·s. vantage lies in convenience of measurement, requiring only a
small volume of sample. Since 2011, there have been reports
Index Terms—Viscometer, acousto-optic superlattice, fiber of viscosity measurement by using optical fiber methods [5].
Bragg grating.
The application of optical fiber sensing technology to viscosity
measurement is challenging. An optical viscometer, which is
I. INTRODUCTION formed by exciting long period fiber grating (LPG) by using of
ISCOSITY is one of the main parameters used to predict acoustic flexural waves, has been described by Oliveira et al.
V the physical, chemical and biological properties of fluids.
In the manufacturing industry, viscosity sensing is necessary
[5]. They reported that the change in reflection spectrum of the
excited LPG in their viscometer is partly due to the change of
for real-time monitoring and control of the production process. the refractive index, and partly due to acoustic damping as the
At present, a variety of viscometers are in common use. These viscosity increases. Therefore, the LPG-based viscometer pos-
include the capillary viscometer (also called the Ostwald vis- sessed cross-sensitivity to refractive index and viscosity. There-
cometer) [1], the falling sphere viscometer [2] and rotational and fore, Oliviera et al. needed to add a time-varying element to the
vibrational viscometers [3], [4]. Capillary viscometer presents a LPG’s response to separate viscosity measurement from refrac-
high-precision measurement and needs small volumes of fluid, tive index.
but the measurement procedure is time-consuming and hinders In this paper, we introduce a new method for measuring the
real-time measurement. For falling sphere viscometer, the vis- liquid viscosity based on an all-fiber acousto-opitc superlattice
cosity can be obtained by measuring the velocity of a sphere modulation (AOSLM) structure, which spatially modulates a
fiber Bragg grating (FBG) inscribed in the core of a fiber by the
Manuscript received February 27, 2018; revised June 15, 2018 and July 4, applied acoustic longitudinal waves. The viscosity can be char-
2018; accepted July 20, 2018. Date of publication July 24, 2018; date of current acterized by the bandwidth of the modulated FBG in the mea-
version August 8, 2018. This work was supported in part by the National
Natural Science Foundation of China under Grants 61475128 and 61705189;
surement process. Since the light field is always guided by the
in part by the Key Project of Sichuan Provincial Science and Technology Plan fiber core, there is no evanescent field external to the cladding,
under Grant 2017GZ0091; and in part by the Fundamental Research Funds for so that there is no cross-sensitivity between the refractive index
the Central Universities under Grant 2682017CX095. (Corresponding authors:
Li-Yang Shao and Wending Zhang.)
and the viscosity. Through theoretical analysis and experimen-
H. Qian, X. Zhang, H. He, B. Luo, W. Pan, X. Zou, and L. Yan are with the tal measurement, we demonstrate the relationship between the
Center for Information Photonics and Communications, School of Information viscosity and the width of the Bragg resonant reflection peak of
Science and Technology, Southwest Jiaotong University, Chengdu 610031,
China.
the modulated FBG.
L.-Y. Shao is with the Center for Information Photonics and Communications,
School of Information Science and Technology, Southwest Jiaotong University, II. PRINCIPLE
Chengdu 610031, China, and also with the Department of Electrical and Elec-
tronic Engineering, Southern University of Science and Technology, Shenzhen In 1986, Russell showed that planes of a FBG can be modu-
518055, China (e-mail:,shaoly@sustc.edu.cn). lated with the use of acoustic waves. This effect was also called
W. Zhang is with the MOE Key Laboratory of Material Physics and Chemistry
Under Extraordinary Conditions and Shaanxi Key Laboratory of Optical Infor- acousto-optic superlattice modulation (AOSLM) [6]. Since then
mation Technology, School of Science, Northwestern Polytechnical University, AOSLM has attracted much attention. We know that the sen-
Xi’an 710072, China (e-mail:,zhangwd@nwpu.edu.cn). sitivity of FBGs to temperature and strain allows FBGs to be
Color versions of one or more of the figures in this paper are available online
at http://ieeexplore.ieee.org. modulated by temperature and strain gradients [7], [8]. Both
Digital Object Identifier 10.1109/JLT.2018.2859239 methods will change the shape of the reflection spectrum by
0733-8724 © 2018 IEEE. Personal use is permitted, but republication/redistribution requires IEEE permission.
See http://www.ieee.org/publications standards/publications/rights/index.html for more information.
4124 JOURNAL OF LIGHTWAVE TECHNOLOGY, VOL. 36, NO. 18, SEPTEMBER 15, 2018
Fig. 4. (a) PZT vibration modes and qualitative displacement behavior in (d) of Fig. 5 were 26 με, 90 με, 130 με and 180 με, respectively.
resonances; (b) Modulator frequency response in terms of the fiber transversal
and axial displacements. As the driving voltage of the PZT increases, the axial strain of
the FBG becomes larger and the spectrum becomes wider ac-
cordingly. The change of the simulated spectrum is in qualita-
deformations that excite acoustic flexural waves in the fiber. In tive agreement with the change of the experimentally measured
the higher frequency range, the main deformation of PZT is lon- spectrum. These results confirm that in the low-frequency do-
gitudinal deformation and the acoustic longitudinal waves are main, although the acoustic longitudinal wave does not occupy
excited. This is consistent with previous research conclusions a dominant position, it plays a major role in broadening the
[13], [14]. In addition to the analysis of the type of the acoustic spectrum.
wave excited by PZT, we can also calculate the strain distri-
bution in the fiber through FEM. The coupled mode equations D. Viscosity Measurement and Results
are used to analyze the spectral properties of the FBG subjected
In the experiments, we immersed the grating in the liquid to
to acoustic waves. We used the transfer-matrix method (TMM)
be measured and investigated how the spectrum of the modu-
solve the coupled mode equations.
lated grating changed with the viscosity of immersion liquid.
First, we established a model incorporating the dimensions of
Anhydrous glucose (C6 H12 O6 ) dissolved in distilled water was
the FBG and the characteristics of the acousto-optic modulator.
used as a calibration solution whose refractive index and vis-
Then we employed the finite element method (FEM) to analyze
cosity as a function of concentration are well known [17]. We
the mechanical properties of the model. We calculated the axial
prepared seven different glucose solution samples, which con-
strain s(z) along the axis of the fiber. The wavelength of FBG
centrations range from 0% to 40%, and the viscosities range
subjected to the strain was used as the input to the transfer matrix
from 1.01 mPa·s to 5.5 mPa·s. In the whole experiment, the
calculations. The combination of the FEM and TMM was made
temperature was set at 20 °C, the driving voltage and frequency
through the wavelength shift in every single segment of fiber
were set at 140 V and 201.6 kHz respectively.
submitted to the strain field s(z). The relations was given as [16]
Fig. 6 shows that the reflection spectra of the modulated FBG
λB (z) = λB 0 (1 + (1 − χ) s (z)) , (4) vary with viscosity of the glucose solution. Fig. 6(b) shows how
the 3 dB bandwidth depends on the viscosity, for an optical
where λB 0 is the Bragg wavelength in the FBG without strain. fiber with a diameter of 125 μm. A quadratic fit to the data in
This equation establishes a bridge connecting FEM and TMM. 6(b) yields the relationship between measured spectral width
Finally, λB is applied to the TMM method, and the spectrum of and viscosity as:
FBG can be calculated. The numerical approach was employed
Δλ = 0.0018η 2 − 0.0258η + 0.5040 (5)
to qualitatively investigate the effect of the strain S on the modu-
lated FBG spectrum. At the same frequency (f = 271 kHz) and It can be seen that the sensitivity decreases as the viscosity
different voltages, the experimentally measured and simulated increases. When the diameter of the grating is etched down to
spectra are shown in Fig. 5. In the simulation, we only consider 68 μm by hydrofluoric acid, the spectrum can be satisfacto-
the longitudinal strain. The axial strains used in (a), (b), (c) and rily broadened at a smaller drive voltage compared to unetched
QIAN et al.: FIBER-OPTIC VISCOMETER WITH ALL-FIBER ACOUSTO-OPTIC SUPERLATTICE MODULATED STRUCTURE 4127
Wending Zhang received the B.S. degree from Northwestern Polytechnical Wei Pan is a currently a Full Professor and the Dean of the School of Informa-
University, Xi’an, China, in 2007, and the Master’s degree in 2010 in optics tion Science and Technology, Southwest Jiaotong University, Chengdu, China.
and the Ph.D. degree in photonics and photon technical from Nankai University, He has authored/coauthored more than 200 papers in high-impact refereed jour-
Tianijn China, in 2013. He is currently an Associate Professor with Northwestern nals. His research interests include semiconductor lasers, nonlinear dynamic
Polytechnical University. His research interest focuses on the acousto-optic systems, and optical communications. Prof. Pan was appointed as the steer-
interaction in optical fiber. ing and consultancy expert of the highest level national project (973 Project)
of China. He was also awarded as the Academic and Technology Leader of
Sichuan province, China.
Xihua Zou is currently a Full Professor with the Center for Information Pho-
Xinpu Zhang received the Ph.D. degree in optical engineering from the Depart- tonics and Communications, Southwest Jiaotong University, Chengdu, China.
ment of Physics, Dalian University of Technology, Dalian, China, in 2016, and He has authored or coauthored more than 80 academic papers in high-impact
then joined the faculty of the School of Information Science and Technology, refereed journals. His current interests include microwave photonics, radio over
Southwest Jiaotong University, Chengdu, China. fiber, and optical communications. Dr. Zou was the recipient of the Alexander
He is currently a Lecturer of the School of Information Science and Technol- von Humboldt Research Fellowship, National Outstanding Expert in Science
ogy, Southwest Jiaotong University. His research interests include optical fiber and Technology of China, the Nomination Award for the National Excellent
sensors, fiber laser, fiber grating, and micro/nano optoelectronic devices. Doctoral Dissertation of China, the Science and Technology Award for Young
Scientist of Sichuan Province, China, and the Outstanding Reviewer of Op-
tics Communications. He currently serves as an Associate Editor of the IEEE
JOURNAL OF QUANTUM ELECTRONICS, the Guest Editor for a Special Section
on Microwave Photonics in IEEE/OSA JOURNAL OF LIGHTWAVE TECHNOLOGY,
and once as the Editor and the Coordinator for a Focus Issue on Microwave Pho-
Haijun He received the B.S. degree from the Southwest Jiaotong University, tonics in the IEEE JOURNAL OF QUANTUM ELECTRONICS, and the leading Guest
Chengdu, China, in 2014. He is currently working toward the Ph.D. degree Editor for a Special Section on Microwave Photonics in Optical Engineering.
with the School of Information Science and Technology, Southwest Jiaotong
University. His research interests include optical fiber sensors (especially for
the distributed optical fiber sensors) and nonlinear fiber optics.
Lianshan Yan is currently a Full Professor and the Director of Center for
Information Photonics and Communications, Southwest Jiaotong University,
Chengdu, China.
Dr. Yan is a Fellow of the Optical Society of America (OSA). He was the
recipient of the IEEE Photonics Society Distinguished Lecturer Award for 2011–
2013 and the IEEE LEOS Graduate Fellowship in 2002. He currently serves as
Bin Luo received the Ph.D. degree from Southwest Jiaotong University, the Chair of the Fiber Optics Technology Technical Group, OSA. He served as
Chengdu, China, in 1995. the Co-Chair or the TPC member of more than 20 international conferences,
He is currently a Professor with the School of Information Science and Tech- including the Optical Fiber Communication Conference and Exposition (OFC,
nology, Southwest Jiaotong University. He is the author or coauthor of more since 2013), the European Conference on Optical Communication (ECOC, since
than 80 research papers. His current research interests include semiconductor 2013), the Asia Communications and Photonics Conference (ACP, 2010–2012),
optical amplifiers and optical communication. etc. He was an Associate Editor of the IEEE PHOTONICS JOURNAL.