Conc NO2 (ug/mL)

No, Sampel Ulangan Rata-Rata Selisih %RPD

1 2
1 0.0494 0.0498 0.0496 0.0004 0.81
2 0.0514 0.0500 0.0507 0.0014 2.76
3 0.0486 0.0489 0.0488 0.0003 0.62
4 0.0470 0.0475 0.0473 0.0005 1.06
5 0.0500 0.0508 0.0504 0.0008 1.59
6 0.0490 0.0499 0.0495 0.0009 1.82
7 0.0481 0.0485 0.0483 0.0004 0.83
8 0.0506 0.0506 0.0506 0.0000 0.00
9 0.0488 0.0483 0.0486 0.0005 1.03
10 0.0520 0.0517 0.0519 0.0003 0.58
11 0.0513 0.0512 0.0513 0.0001 0.20
12 0.0489 0.05 0.0495 0.0011 2.22
13 0.0479 0.048 0.0480 0.0001 0.21
14 0.0482 0.0485 0.0484 0.0003 0.62
15 0.049 0.0493 0.0492 0.0003 0.61
16 0.0521 0.0518 0.0520 0.0003 0.58
17 0.0478 0.0482 0.0480 0.0004 0.83
18 0.0499 0.0503 0.0501 0.0004 0.80
19 0.0502 0.0489 0.0496 0.0013 2.62
20 0.0515 0.0509 0.0512 0.0006 1.17
Rata-rata 1.05
Standar Deviasi 0.78
 Batas Peringatan Atas ( UWL) 2.60
Batas Peringatan Bawah ( LWL -0.51
Batas Tindakan Atas ( UAL) 3.38
Batas Tindakan Bawah ( LAL) -1.28
Rata-rata 1.05

No Sampel Rata-rata UWL LWL UAL LAL

1 1.05 2.60 -0.51 3.38 -1.28
2 1.05 2.60 -0.51 3.38 -1.28
3 1.05 2.60 -0.51 3.38 -1.28
4 1.05 2.60 -0.51 3.38 -1.28
5 1.05 2.60 -0.51 3.38 -1.28
6 1.05 2.60 -0.51 3.38 -1.28
7 1.05 2.60 -0.51 3.38 -1.28
8 1.05 2.60 -0.51 3.38 -1.28
9 1.05 2.60 -0.51 3.38 -1.28
10 1.05 2.60 -0.51 3.38 -1.28
11 1.05 2.60 -0.51 3.38 -1.28
12 1.05 2.60 -0.51 3.38 -1.28
13 1.05 2.60 -0.51 3.38 -1.28
14 1.05 2.60 -0.51 3.38 -1.28
15 1.05 2.60 -0.51 3.38 -1.28
16 1.05 2.60 -0.51 3.38 -1.28
17 1.05 2.60 -0.51 3.38 -1.28
18 1.05 2.60 -0.51 3.38 -1.28
19 1.05 2.60 -0.51 3.38 -1.28
20 1.05 2.60 -0.51 3.38 -1.28
 waktu Ulangan Reta-
Selisih %RPD
Pengukuran rata
1 2
2-Jan-18 0.0502 0.0505 0.05035 0.0003 0.595829
3-Jan-18 0.048 0.0482 0.0481 0.0002 0.4158
4-Jan-18 0.045 0.0453 0.04515 0.0003 0.664452
5-Jan-18 0.0477 0.048 0.04785 0.0003 0.626959
6-Jan-18 0.056 0.05 0.053 0.006 11.32075
 CONTROL CHART PRESISI ANALISIS KADAR NO2 DALAM
SAMPEL AIR SUMUR

12.00
11.32075472

10.00

8.00
Rata-rata
UWL
6.00 LWL
%RPD

UAL
LAL
4.00
%RPD

2.00

0.595829196 0.664451827 0.626959248

0.415800416
0.00
2-Jan-18 3-Jan-18 4-Jan-18 5-Jan-18 6-Jan-18

-2.00
No, Sampel Conc COD ( mg O2/L ) Nilai Sertifikat %Recorvery

1 198.5 99.25
2 189.5 94.75
3 195.0 97.50
4 198.6 99.30
5 202.4 101.20
200
6 197.6 98.80
7 204.5 102.25
8 190.4 95.20
9 188.8 94.40
10 194.3 97.15
Rerata 97.98
Standar Deviasi 2.68

Batas Peringatan Atas ( UWL)

103.34
Batas Peringatan Bawah ( LWL
92.62
Batas Tindakan Atas ( UAL)
106.01
Batas Tindakan Bawah ( LAL)
89.95
Rata-rata
97.98
 No, Waktu Conc COD
Rata-rata UWL LWL UAL LAL %Recorvery
Sampel Pengukuran (mg O2/L)

1 97.98 103.34 92.62 106.01 89.95 2-Jan-18 197.5 98.75

2 97.98 103.34 92.62 106.01 89.95 3-Jan-18 211.3 105.65
3 97.98 103.34 92.62 106.01 89.95 4-Jan-18 203.7 101.85
4 97.98 103.34 92.62 106.01 89.95 5-Jan-18 199.8 99.9
5 97.98 103.34 92.62 106.01 89.95 6-Jan-18 222.8 111.4
6 97.98 103.34 92.62 106.01 89.95 11-Jun-18 187 93.5
7 97.98 103.34 92.62 106.01 89.95
8 97.98 103.34 92.62 106.01 89.95
9 97.98 103.34 92.62 106.01 89.95
10 97.98 103.34 92.62 106.01 89.95
 CONTROL CHART AKURASI (HASIL PENGUKURAN SAMPEL CRM COD)

114.00 110.00

112.00

110.00 105.00
108.00

106.00
100.00
104.00 %Recorvery
%Recorvery

Rata-rata
102.00
95.00 UWL
100.00
LWL
98.00 UAL
90.00
96.00 LAL

94.00

92.00 85.00

90.00

88.00 80.00
1-Jan-00 2-Jan-00 3-Jan-00 4-Jan-00 5-Jan-00 6-Jan-00
 Conc NH3 ( mg /L )

No, Sampel

Sampel Sampel + Spike %Recorvery

Spike
1 0.2882 0.3892 0.1 101.00
2 0.2765 0.3750 0.1 98.50
3 0.2213 0.3156 0.1 94.30
4 0.2487 0.3475 0.1 98.80
5 0.1876 0.2882 0.1 100.60
6 0.3065 0.4053 0.1 98.80
7 0.3522 0.4525 0.1 100.30
8 0.2876 0.3863 0.1 98.70
9 0.2390 0.3380 0.1 99.00
10 0.2400 0.3358 0.1 95.80
Rata-rata 98.58
Standar Deviasi 2.1
Batas Peringatan Atas ( UWL)
102.76
Batas Peringatan Bawah ( LWL
94.40
Batas Tindakan Atas ( UAL)
104.84
Batas Tindakan Bawah ( LAL)
92.32
Rata-rata
98.58
 Conc NH3 ( mg /L )

No, Rata- Waktu

UWL LWL UAL LAL
Sampel rata Pengukuran
Sampel +
Sampel %Recorvery
Spike
Spike

1 98.58 102.76 94.40 104.84 92.32 2-Jan-18 0.2171 0.3192 0.1 102.10

2 98.58 102.76 94.40 104.84 92.32 3-Feb-18 0.1988 0.3050 0.1 106.20

3 98.58 102.76 94.40 104.84 92.32 7-Mar-18 0.2290 0.3156 0.1 86.60

4 98.58 102.76 94.40 104.84 92.32 8-Apr-18 0.1879 0.3075 0.1 119.60

5 98.58 102.76 94.40 104.84 92.32 10-May-18 0.2236 0.3187 0.1 95.10

6 98.58 102.76 94.40 104.84 92.32 11-Jun-18 0.3766 0.4853 0.1 108.70

7 98.58 102.76 94.40 104.84 92.32 13-Jul-18 0.4216 0.5523 0.1 130.70

8 98.58 102.76 94.40 104.84 92.32 14-Aug-18 0.2008 0.3063 0.1 105.50

9 98.58 102.76 94.40 104.84 92.32

10 98.58 102.76 94.40 104.84 92.32
 CONTROL CHART AKURASI (METODE SPIKING ANALISA KAAR NH3)

110 140.00

120.00

105
%Recorvery, 105.50
100.00

100
80.00
%Recorvery

Rata-rata

60.00
95 UWL

LWL
40.00
UAL

90 LAL
20.00
%Recorvery

85 0.00
1-Jan-18 1-Feb-18 1-Mar-18 1-Apr-18 1-May-18 1-Jun-18 1-Jul-18 1-Aug-18