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is negligible. For well-dispersed ore pulps, free (Chapter 4). Newton's law holds for particles larger
settling predominates when the percentage of solids than about 0.5cm in diameter. There is, there-
by weight is less than about 15 (Taggart, 1945). fore, an intermediate range of particle size, which
Consider a spherical particle of diameter d and corresponds to the range in which most wet clas-
density D~ falling under gravity in a viscous fluid sification is performed, in which neither law fits
of density Df under free-settling conditions, i.e. experimental data.
ideally in a fluid of infinite extent. The particle is Stokes' law (9.4) for a particular fluid can be
acted upon by three forces: a gravitational force simplified to
acting downwards, an upward buoyant force due
to the displaced fluid, and a drag force D acting 12= kld2(Ds - De) (9.7)
upwards. The equation of motion of the particle is and Newton's law (9.6) can be simplified to
m dx
mg-m'g-D= (9.1) 12 "--" k 2 [ d ( O s - Of)] 1/2 (9.8)
dt
where m is the mass of the particle, m' is the mass where k~ and k 2 are constants, and (D s - D f ) is
of the displaced fluid, x is the particle velocity, and known as the effective density of a particle of
g is the acceleration due to gravity. density D s in a fluid of density Df.
When the terminal velocity is reached, dx/dt = 0 , Both laws show that the terminal velocity of a
and hence D = (m - m')g. particle in a particular fluid is a function only of
Therefore the particle size and density. It can be seen that:
77"
D -- (-~ ) gd3 (Ds - Df ) (9.2) (1) If two particles have the same density, then
the particle with the larger diameter has the
Stokes (1891) assumed the drag force on a spherical higher terminal velocity.
particle to be entirely due to viscous resistance and (2) If two particles have the same diameter, then
deduced the expression the heavier particle has the higher terminal
D - 3'rrd'qv (9.3) velocity.
where xl is the fluid viscosity and v is the terminal Consider two mineral particles of densities D a
velocity. and D b and diameters d a and d b respectively, falling
Hence, substituting in Equation 9.2, in a fluid of density Df at exactly the same settling
71" rate. Their terminal velocities must be the same,
and hence from Stokes' law (9.7):
and da 2 ( o a - O f ) = d b 2(o b-Of)
gd2 (Ds - Df)
v- (9.4) or
18qq
This expression is known as Stokes' law.
db = D a - Df (9.9)
Newton assumed that the drag force was entirely
due to turbulent resistance, and deduced: This expression is known as the free-settling
2 2
D - 0 . 0 5 5 7 r d v Df (9.5) ratio of the two minerals, i.e. the ratio of particle
size required for the two minerals to fall at
Substituting in Equation 9.2 gives equal rates.
Similarly from Newton's law (9.8), the free
I3gd(Ds - Df) ] 1/2
v- (9.6) settling ratio of large particles is
Df
da D b -- Df
This is Newton's law for turbulent resistance. -- = (9.10)
For small particles, obeying Stokes' law, the free fall in a separation by hindered settling, the resis-
settling ratio (Equation 9.9) is tance to fall is mainly due to the turbulence created
(Swanson, 1989), and a modified form of Newton's
7 . 5 - 1 )1/2
-- 1.99
law (9.8) can be used to determine the approximate
2.65- 1 falling rate of the particles
i.e. a small particle of galena will settle at the same p- k [ d ( O s - - O p ) ] 1/2 (9.12)
rate as a small particle of quartz which has a diam-
eter 1.99 times as large. where Op is the pulp density.
For particles obeying Newton's law, the free The lower the density of the particle, the more
settling ratio (Equation 9.10) is marked is the effect of reduction of the effective
density, D s - Dp, and the greater is the reduction in
7.5- 1
= 3.94 falling velocity. Similarly, the larger the particle,
2.65- 1 the greater is the reduction in falling rate as the
The free-settling ratio is therefore larger for pulp density increases.
coarse particles obeying Newton's law than for fine This is important in classifier design; in effect,
particles obeying Stokes' law. This means that the hindered-settling reduces the effect of size, while
density difference between the particles has a more increasing the effect of density on classification.
pronounced effect on classification at coarser size This is illustrated by considering a mixture of
ranges. This is important where gravity concen- quartz and galena particles settling in a pulp of
tration is being utilised. Over-grinding of the ore density 1.5. The hindered-settling ratio can be
must be avoided, such that particles are fed to derived from Equation 9.12 as
the separator in as coarse a state as possible, so
that a rapid separation can be made, exploiting the d___~= D b - Dp (9.13)
db D a - Dp
enhanced effect of specific gravity difference. The
enhanced gravity effect does, however, mean that Therefore, in this system,
fine heavy minerals are more likely to be over-
da 7 . 5 - 1.5
ground in conventional ball mill-classifier circuits, =5.22
so it is preferable where possible to use rod mills db 2 . 6 5 - 1.5
for the primary coarse grind. A particle of galena will thus fall in the pulp at
The general expression for free-settling ratio can the same rate as a particle of quartz which has a
be deduced from Equations 9.9 and 9.10 as diameter 5.22 times as large. This compares with
the free-settling ratio, calculated as 3.94 for turbu-
bd--2a--(Db-Df
d nD ) a -- Df (9.11) lent resistance.
The hindered-settling ratio is always greater
where n = 0.5 for small particles obeying Stokes' than the free-settling ratio, and the denser the pulp,
law and n = 1 for large particles obeying the greater is the ratio of the diameter of equal
Newton' s law. settling particles. For quartz and galena, the greatest
The value of n lies in the range 0 . 5 - 1 for particles hindered-settling ratio that we can attain practically
in the intermediate size range of 50 p~m-0.5 cm. is about 7.5. Hindered-settling classifiers are used
to increase the effect of density on the separation,
whereas free-settling classifiers use relatively dilute
Hindered settling
suspensions to increase the effect of size on the
As the proportion of solids in the pulp increases, the separation (Figure 9.2). Relatively dense slurries
effect of particle crowding becomes more apparent are fed to certain gravity concentrators, particularly
and the falling rate of the particles begins to those treating heavy alluvial sands. This allows
decrease. The system begins to behave as a heavy high tonnages to be treated, and enhances the effect
liquid whose density is that of the pulp rather than of specific gravity difference on the separation.
that of the carrier liquid; hindered-settling condi- The efficiency of separation, however, may be
tions now prevail. Because of the high density and reduced since the viscosity of a slurry increases
viscosity of the slurry through which a particle must with density. For separations involving feeds with
206 Wills' Mineral Processing Technology
0
0 9 greatest at the bottom of the column. A particle falls
9 9 until it reaches a point where its falling velocity
9 9 9 equals that of the rising current. The particle can
now fall no further. Many particles reach this condi-
e9 0
0
9 tion, and as a result, a mass of particles becomes
trapped above the constriction and pressure builds
Hydraulic classifiers
These are characterised by the use of water addi-
tional to that of the feed pulp, introduced so that its
direction of flow opposes that of the settling parti-
T
Water Water
cles. They normally consist of a series of sorting
columns through each of which a vertical current
of water is rising and particles are settling out
Figure 9.3 Teeter chambers (Figure 9.4).
The rising currents are graded from a relatively
Such hindered-settling sorting columns are high velocity in the first sorting column, to a rela-
known as teeter chambers. Due to the constric- tively low velocity in the last, so that a series of
tion, the velocity of the introduced water current is spigot products can be obtained, with the coarser,
Classification 207
Feed~
Slimes
Sorting
column
--~F .i--Water 7 r-l- Water
denser particles in the first spigot and the fines in 4th Spigot 9
the latter spigots. Very fine slimes overflow the
final sorting column of the classifier. The size of
each successive vessel is increased, partly because
the amount of liquid to be handled includes all the
water used for classifying in the previous vessels
9 O
and partly because it is desired to reduce, in stages, 3rd Spigot
the surface velocity of the fluid flowing from one
vessel to the next.
Hydraulic classifiers may be free- or hindered-
settling types. The former are rarely used; they are
2nd Spigot
O
simple and have high capacities, but are inefficient
in sizing and sorting. They are characterised by
the fact that each sorting column is of the same
cross-sectional area throughout its length.
The greatest use for hydraulic classifiers in the
mineral industry is for sorting the feed to certain Ist Spigot contains high
gravity concentration processes so that the size proportion of heavy mineral
effect can be suppressed and the density effect
enhanced (Chapter 10). Such classifiers are of the
hindered-settling type. These differ from the free-
settling classifiers in that the sorting column is Figure 9.5 Added increment of hindered-settling
constricted at the bottom in order to produce a teeter classifier
chamber (Figure 9.3). The hindered-settling clas-
sifier uses much less water than the free-settling During classification the teeter bed tends to
type, and is more selective in its action, due to grow, as it is easier for particles to become entan-
the scouring action in the teeter chamber, and the gled in the bed rather than leave it. This tends to
buoyancy effect of the pulp, as a whole, on those alter the character of the spigot discharge, as the
particles which are to be rejected. Since the ratio of density builds up. In modern multi-spigot hydro-
sizes of equally falling particles is high, the classi- sizers the teeter bed composition is automatically
fier is capable of performing a concentrating effect, controlled. The Stokes hydrosizer (Figure 9.6) is
and the first spigot product is normally of higher commonly used to sort the feed to gravity concen-
grade than the other products (Figure 9.5). trators (Mackie et al., 1987).
This is known as the added increment of the Each teeter chamber is provided at its bottom
classifier and the first spigot product may in some with a supply of water under constant head which
cases be rich enough to be classed as a concentrate. is used for maintaining a teetering condition in the
208 Wills' Mineral Processing Technology
efficiency of the separation. Washing sprays are Spiral classifiers (Figure 9.11) use a continuously
often directed on the emergent sands to wash the revolving spiral to move the sands up the slope.
released slimes back into the pool. They can be operated at steeper slopes than the
rake classifier, in which the sands tend to slip back
The rake classifier (Figure 9.10) utilises rakes when the rakes are removed. Steeper slopes aid the
actuated by an eccentric motion, which causes them drainage of sands, giving a cleaner, drier product.
to dip into the settled material and to move it up Agitation in the pool is less than in the rake classi-
the incline for a short distance. The rakes are then fier which is important in separations of very fine
withdrawn, and return to the starting-point, where material.
the cycle is repeated; the settled material is thus The size at which the separation is made and the
slowly moved up the incline to the discharge. quality of the separation depend on a number of
In the duplex type shown, one set of rakes is factors.
moving up, while the other set returns; Simplex and Increasing the feed rate increases the horizontal
quadruplex machines are also made in which there carrying velocity and thus increases the size of
are one or four raking assemblies. particle leaving in the overflow. The feed should
space of the thickener, oxidation of liberated parti- which prevents short-circuiting of feed directly into
cles may occur in the thickener, which may affect the overflow.
subsequent processes, especially froth flotation. The feed is introduced under pressure through the
tangential entry which imparts a swirling motion
to the pulp. This generates a vortex in the cyclone,
The hydrocyclone
with a low-pressure zone along the vertical axis.
This is a continuously operating classifying device An air core develops along the axis, normally
that utilises centrifugal force to accelerate the connected to the atmosphere through the apex
settling rate of particles. It is one of the most impor- opening, but in part created by dissolved air coming
tant devices in the minerals industry, its main use in out of solution in the zone of low pressure.
mineral processing being as a classifier, which has The classical theory of hydrocyclone action is that
proved extremely efficient at fine separation sizes. particles within the flow pattern are subjected to two
It is widely used in closed-circuit grinding oper- opposing forces- an outward centrifugal force and an
ations (Napier-Munn et al., 1996) but has found inwardly acting drag (Figure 9.14). The centrifugal
many other uses, such as de-sliming, de-gritting, force developed accelerates the settling rate of the
and thickening. particles thereby separating particles according to
It has replaced mechanical classifiers in many size, shape, and specific gravity. Faster settling
applications, its advantages being simplicity and particles move to the wall of the cyclone, where
high capacity relative to its size. A variant, the the velocity is lowest, and migrate to the apex
"water-only-cyclone", has been used for the cleaning opening. Due to the action of the drag force, the
of fine coal (Osborne, 1985) and other minerals. slower-settling particles move towards the zone of
A typical hydrocyclone (Figure 9.13) consists low pressure along the axis and are carried upward
of a conically shaped vessel, open at its apex, or through the vortex-finder to the overflow.
underflow, joined to a cylindrical section, which
has a tangential feed inlet. The top of the cylin-
drical section is closed with a plate through which ~~~Radius of orbiting particle
passes an axially mounted overflow pipe. The pipe
is extended into the body of the cyclone by a short, Centrifugal _
force - rce
removable section known as the vortex finder,
Motion of particle
Overflow
i
Inlet -- i
I
i
i
i
i
~
Envelop i
vertical, i
i
Underflow
Figure 9.16 Regions of similar size distribution
Figure 9.15 Distribution of the vertical and radial within cyclone
components of velocity in a hydrocyclone
Table 9.1
(9.17)
tions for the cut-size, and these have increased
significantly since then. Bradley's own equa- where D c, Di, D o, and D u are the inside diame-
tion based on the equilibrium orbit hypothesis ters of the cyclone, inlet, vortex finder, and apex
(Figures 9.14 and 9.15) was: respectively (cm), B is the liquid viscosity (cP), Cv
is the feed solids volume concentration (%), h is
[ Dc3r/ ] n (9.16) the distance between apex and end of vortex finder
ds0 - k Qf(ps - pl)
(cm), k is a hydrodynamic exponent to be estimated
where D c = cyclone diameter, p = fluid viscosity, from data (default value for laminar flow 0.5), Qf
Q f - - feed flow rate, Ps = solids density, Pl = is the feed flow rate (1/min), and p~ is the solids
fluid density, n = hydrodynamic constant (0.5 for density (g/cm3). Note that for non-circular inlets,
particle laminar flow), k = constant incorporating D i - - ~ / 4 A / ~ where A (cm 2) is the cross-sectional
other factors, particularly cyclone geometry. This area of the inlet.
Classification 217
The equation for the volumetric flow rate of 1999), inferring cyclone product size from geom-
slurry to the cyclone, Qf, is: etry and operating variables as an alternative to
F2 p .0 56D 0e921DiO.53hO.16(D2u+Do2)0.49 using an on-line sizer (Chapter 4).
Qf = (9.18)
exp(0.0031Cv)
where P is the pressure drop across the cyclone in Scale-up and design of
kPa (1 psi = 6.896 kPa). F 1 and F 2 in Equations 9.17 hydrocyclones
and 9.18 are material-specific constants that must A preliminary scale-up from a known situation (e.g.
be determined from tests with the feed material a laboratory or pilot plant test) to the unknown
concerned. (e.g. a full production installation) can be done via
Plitt also reports equations for the flow split the basic relationships between cut-size, cyclone
between underflow and overflow, and for the effi- diameter, flow rate, and pressure drop. These are:
ciency parameter in the reduced efficiency curve.
Nageswararao's model includes correlations for D2 nl n2 n3 n4
and optimisation using dedicated computer simula- Classification efficiency can sometimes be
tors such as JKSimMet (Napier-Munn et al., 1996) improved by arranging several cyclones in series
and MODSIM (King, 2001), or the flowsheet simu- to re-treat overflow, underflow or both. Svarovsky
lator Limn (Hand and Wiseman, 2002). They can (1984) has pointed out that if N cyclones with iden-
also be used as a virtual instrument or "soft sensor" tical classification curves are arranged in series,
(Morrison and Freeman, 1990; Smith and Swartz, each treating the overflow of the previous one, then
218 Wills' Mineral Processing Technology
the overall recovery of size d to the combined to the more common single stage, would allow a 6%
coarse product, Rd(T), is given by increase in grinding circuit throughput. Without the
aid of cyclone modelling, such work would be costly
Rdo3 = 1 -- (1 - Rd) N (9.23) and time-consuming.
The equations can also be very valuable in the
where R a = recovery of size d in one cyclone.
selection of cyclones for a particular duty, the final
The appropriate way of specifying a cyclone
control of cut-point and capacity made by adjusting
installation is by process simulation using a simula-
the size of inlet, vortex-finder, and apex.
tion package such as those mentioned above. These
For example, consider a primary grinding mill,
packages incorporate empirical cyclone models such
fed with ore (sp. gr. 3.7 g cm -3) at the rate of
as those by Plitt and Nageswararao, and can be
201.5 t h -~. The mill is to be in closed circuit with
used for optimising processing circuits incorporating
cyclones, to produce a circulating load of 300%
hydrocyclones (e.g. Morrison and Morrell, 1998).
and a cut-point of 74 txm.
An alternative is to use the simple empirical
The total cyclone feed is therefore 806th -~.
methods of sizing cyclones for a particular duty
Assuming 50% solids in the cyclone feed, then the
developed by the manufacturers. Arterburn (1982)
slurry density (Equation 3.6) is 1.574kg 1-I, and
published a method based on the performance of
the volumetric flow rate to the cyclones (Equa-
a "typical" Krebs cyclone with graphical correc- tion 3.7) is 1024m 3 h -1.
tions for other conditions; from this the required The volumetric % solids in the feed is 1.574 •
cut-point can be calculated, and thus the cyclone 50/3.7 = 21.3%. Combining Equations 9.19 and
size, capacity, and number of units determined. A 9.24:
version of this paper is available on the Krebs Engi- 12.67Dc~
neers website, and a more recent approach was ds~ = P~ 1)~
given by Olson and Turner (2002).
e x p ( - 0 . 3 0 1 + 0.0945V - 0.00356V 2 + 0.0000684V 3)
Mular and Jull (1978) developed empirical • /'~ (S - 1)~
formulae from the graphical information for
"typical" cyclones, relating ds0 to the operating (9.25)
variables for cyclones of varying diameter. For a cyclone cutting at 74 ixm (ds0(c)) operating
A "typical" cyclone has an inlet area of about at a pressure of, say, 12 psi (82.74 kPa), D c = 66cm.
7% of the cross-sectional area of the feed chamber, Therefore, 660 mm cyclones, or their nearest manu-
a vortex finder of diameter 35-40% of the cyclone factured equivalent, would probably be chosen; final
diameter, and an apex diameter normally not less adjustments to the cut-size being made by changing
than 25% of the vortex-finder diameter. the vortex-finder, spigot openings, pressure, etc.
The equation for the cyclone cut-point is:
The maximum volume handled by 660mm
0.77D~ .875 cyclones at 12 psi is 372.5 m 3 (Equation 9.20), so
d50(c) -- Q0.6 (S - 1 )0.5 three cyclones would be required to handle the total
e x p ( - 0 . 3 0 1 + 0.0945V - 0.00356V 2 + 0.0000684V 3) flow rate.
Q0.6(S - 1) 0.5
Decreases with flow rate effect, finer particles are carried to the underflow,
Increases with small apex or large vortex finder and ds0 is decreased, but the change has to be large
Increases with cyclone inclination to vertical to have a significant effect. Figure 9.21 shows the
effect of pressure on the capacity and cut-point of
Classification efficiency cyclones.
Increases with correct cyclone size selection
Decreases with feed solids concentration and/or
viscosity 2,4"
finder 1.8-
o
ut3
Decreases with flow-rate
Decreases with inclined cyclones (especially low .~_ 1 . 6 -
,4...,
pressure)
Increases with feed solids concentration and/or t- 1.4-
O
viscosity
Flow rate
Increases with pressure
==
I1)
UJ
1.2-
1.0
/ 1~3~0
Pressure drop (Ib/in2)
Increases with cyclone diameter
Decreases (at a given pressure) with feed solids Figure 9.21 Effect of pressure on capacity and
concentration and/or viscosity cut-point of hydrocyclones
Figure 9.25 Hydrocyclone performance chart (Krebs) (from Napier-Munn et al., 1996; Courtesy JKMRC, The
University of Queensland)
222 Wills' Mineral Processing Technology
to be connected in parallel if high capacity is use of Mozley cyclone assemblies (Anon., 1983).
required (Figure 9.26). Cyclones used for desliming A 16 x 44 mm assembly is shown in Figure 9.27.
duties are usually of very small diameter, and a The feed is introduced into a housing via a central
large number may be required if substantial flow inlet at pressures of up to 50psi (344.8kPa).
rates must be handled. The desliming plant at the The housing contains an assembly of 16 x 44 mm
Mr. Keith Nickel concentrator in Western Australia cyclones, the feed being forced through a trash
has 4000 such cyclones. The practical problems screen and into each cyclone without the need
of distributing the feed evenly and minimising for separate distributing ports (Figure 9.28). The
blockages have been largely overcome by the overflow from each cyclone leaves via the inner
Figure 9.26 A nest of 150 mm cyclones at the Century Zinc mine, Australia (Courtesy JKMRC and JKTech
Pry Ltd)
whole assembl
cSlarnh;g~176 !it,rS/ : i " iiiliiiii~ii!ii'iii~ feBase
edmOunting.inlefor
t.driled
pressure plate, and leaves the housing through the Asomah, I.K. and Napier-Munn, T.J. (1997). An empir-
single overflow pipe on the side. The assembly ical model of hydrocyclones, incorporating angle of
design reduces maintenance to a minimum, the cyclone inclination, Minerals Eng., 10(3), 339-347.
Austin, L.G. and Klimpel, R.R. (1981). An improved
removal of the top cover allowing easy access so
method for analysing classifier data, Powder Tech.,
that individual cyclones can be removed without 29(Jul./Aug.), 227.
disconnecting feed or overflow pipework. Bradley, D. (1965). The Hydrocyclone, Pergamon Press,
Since separation at large particle size requires Oxford.
large diameter cyclones with consequent high Brennan, M., Subramanian, V., Rong, R.X., Lyman,
capacities, in many cases, where coarse separations G.J., Holtham, P.N., and Napier-Munn, T.J. (2003).
are required, cyclones cannot be utilised, as the Towards a new understanding of the cyclone sepa-
rator, XXII Int. Min. Proc. Cong., Cape Town, Oct.
plant throughput is not high enough. This is often
Flintoff, B.C., Plitt, L.R., and Turak, A.A. (1987).
a problem in pilot plants where simulation of the Cyclone modelling: A review of present technology,
full-size plant cannot be achieved, as scaling down CIM Bull., 80(905), Sept. 39-50.
the size of cyclones to allow for smaller capacity Hand, P. and Wiseman, D. (2002). Optimisation of mois-
also reduces the cut-point produced. ture adjusted products using spreadsheets, XIV Inter-
national Coal Preparation Congress and Exhibition
(XIV ICPC), SAIMM, Johannesburg, Mar.
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224 Wills' Mineral Processing Technology
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