ASAP 2020 V4.04 (V4.

04 G) Unit 1 Serial #: 428

Sample: Sonia quem

Operator:
Submitter:
File: C:\2020\DATA\000-103.SMP

Started: 25/01/2017 20:16:28 Analysis Adso

Completed: 26/01/2017 8:23:20 Analysis Bath
Report Time: 26/01/2017 13:15:21 Thermal Corr
Sample Mass: 1.0344 g Warm Free Sp
Cold Free Space: 56.8154 cm³ Equilibration
Ambient Temperature: 22.00 °C Low Pressure
Automatic Degas: Yes

Comments: SiC

Summary Report

Surface Area

Single point surface area at P/Po = 0.311045318: 0.2824 m²/g

BET Surface Area: 0.2278 m²/g

Langmuir Surface Area: 0.4246 m²/g e

t-Plot External Surface Area: 0.2813 m²/g

BJH Adsorption cumulative surface area of pores

between 17.000 Å and 3000.000 Å diameter: 0.229 m²/g

BJH Desorption cumulative surface area of pores

between 17.000 Å and 3000.000 Å diameter: 0.1824 m²/g
D-H Adsorption cumulative surface area of pores
between 17.000 Å and 3000.000 Å diameter: 0.112 m²/g

D-H Desorption cumulative surface area of pores

between 17.000 Å and 3000.000 Å diameter: 0.1737 m²/g

Pore Volume

Single point adsorption total pore volume of pores

less than 973.884 Å diameter at P/Po = 0.979879639: 0.000645 cm³/g

t-Plot micropore volume: 0.000005 cm³/g

BJH Adsorption cumulative volume of pores

between 17.000 Å and 3000.000 Å diameter: 0.000408 cm³/g

BJH Desorption cumulative volume of pores

between 17.000 Å and 3000.000 Å diameter: 0.000655 cm³/g

D-H Adsorption cumulative volume of pores

between 17.000 Å and 3000.000 Å diameter: 0.000354 cm³/g

D-H Desorption cumulative volume of pores

between 17.000 Å and 3000.000 Å diameter: 0.000644 cm³/g

Pore Size

Adsorption average pore width (4V/A by BET): 113.2464 Å

BJH Adsorption average pore diameter (4V/A): 71.261 Å

BJH Desorption average pore diameter (4V/A): 143.713 Å

D-H Adsorption average pore diameter (4V/A): 126.277 Å

D-H Desorption average pore diameter (4V/A): 148.361 Å

Nanoparticle Size

Average Particle Size 2.63E-05

 |
Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1
|
|
| Sample: Sonia quem
| Operator:
| Submitter:
| File: C:\2020\DATA\000-103.SMP
|
|
N2 | Started: 25/01/2017 2Analysis AdsoN2
-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C
No | Report Time:26/01/2017 1Thermal CorrNo
18.6504 cm³ Measured | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ Measured
60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s
1.000 cm³/g STP | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g STP
| Automatic DeYes
|
|
| Comments: SiC
|
|
|
|
| Isotherm Tabular Report
|
| Relative Pres Absolute Pre Quantity AdsElapsed TimeSaturation P
| 00:40 739.013062
| 0.01821591 13.4644899 0.05232748 01:04
| 0.04988587 36.877388 0.06094785 01:16
| 0.08824919 65.242897 0.06792775 01:27
| 0.11066301 81.8216934 0.0706619 01:39
186666.666666667 | 0.14395566 106.447289 0.07574384 01:50
| 0.17746102 131.234695 0.08063622 02:01
136661.90 | 0.21024887 155.497299 0.08432105 02:13
| 0.2437095 180.26088 0.08713565 02:24
| 0.27697735 204.888107 0.09074743 02:36
| 0.31104532 230.110275 0.09417058 02:47
| 02:49 739.80896
| 0.34467567 254.978928 0.08652768 03:01
| 0.39817174 294.537323 0.0896706 03:12
| 0.41188728 304.664856 0.08995153 03:24
| 0.46499003 343.925079 0.09269332 03:35
| 0.47861825 353.983917 0.09241838 03:47
| 0.53182909 393.316895 0.09784874 03:58
| 0.54571675 403.565491 0.09800909 04:09
| 0.59877726 442.778076 0.10542324 04:21
| 0.61261553 452.986267 0.10543348 04:32
| 0.66568635 492.201477 0.11294141 04:43
| 0.67972689 502.552887 0.11547687 04:55
| 04:57 739.337952
| 0.71317783 527.26239 0.11907922 05:08
| 0.74595232 551.473572 0.12718643 05:20
| 0.7796104 576.337952 0.13557267 05:31
| 0.81292216 600.944702 0.14914515 05:42
| 0.84658129 625.80481 0.16625566 05:54
| 0.88012396 650.578979 0.18789931 06:05
| 0.91350344 675.228943 0.22345034 06:17
| 0.94678101 699.803894 0.27982843 06:28
| 0.97987964 724.244995 0.41689481 06:39
| 0.94229703 696.442505 0.30396743 06:51
| 0.92160418 681.126587 0.26807971 07:02
| 07:04 739.061951
| 0.90137275 666.147583 0.24093848 07:15
| 0.88096927 651.044434 0.2178752 07:27
| 0.86091493 636.202393 0.2014571 07:38
| 0.84111697 621.548889 0.18746206 07:50
| 0.82095486 606.629272 0.17466105 08:01
| 0.80097995 591.848999 0.16464973 08:12
| 0.78107483 577.119507 0.15447318 08:24
| 0.78033799 576.55719 0.15218724 08:34
| 0.76045619 561.846497 0.1420413 08:46
| 0.72100128 532.677917 0.12705792 08:57
| 0.70107107 517.934143 0.11766609 09:09
| 09:11 738.770935
| 0.7004018 517.466492 0.11088343 09:21
| 0.66055427 488.060547 0.09622847 09:33
| 0.64054521 473.306732 0.08828049 09:44
| 0.6204896 458.519287 0.08147811 09:56
| 0.60054073 443.806091 0.07380834 10:07
| 0.58043447 428.974701 0.0670945 10:18
| 0.56035157 414.161072 0.06046475 10:30
| 0.54038528 399.43158 0.05459241 10:42
| 0.51960368 384.095123 0.04835971 10:53
| 0.48046473 355.185944 0.02597122 11:04
| 0.46036301 340.349304 -0.0003573 11:16
 | 11:18 739.314941
| 0.44034568 325.554138 -0.0162706 11:30
| 0.41982419 310.382294 -0.0225202 11:41
| 0.37988697 280.85611 -0.0331939 11:53
|
|
1.62E+05 |
| |
| ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1
| |
| |
| Sample: Sonia quem | Sample: Sonia quem
| Operator: | Operator:
| Submitter: | Submitter:
| File: C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
| |
| |
| Started: 25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2
| Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8
| Report Time:26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1
| Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g
| Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³
| Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C
| Automatic DeYes | Automatic DeYes
| |
| |
| Comments: SiC | Comments: SiC
| |
| |
| |
| |
| Isotherm Linear Plot | Isotherm Log Plot
| |
| |
| Sonia quem - Adsorption Sonia quem - Desorption | Sonia quem - Adsorption
| Relative Pres Quantity AdsRelative Pres Quantity Ads | Relative Pres Quantity Ads
| 0.01821591 0.05232748 0.97987964 0.41689481 | 0.01821591 0.05232748
| 0.04988587 0.06094785 0.94229703 0.30396743 | 0.04988587 0.06094785
| 0.08824919 0.06792775 0.92160418 0.26807971 | 0.08824919 0.06792775
| 0.11066301 0.0706619 0.90137275 0.24093848 | 0.11066301 0.0706619
| 0.14395566 0.07574384 0.88096927 0.2178752 | 0.14395566 0.07574384
| 0.17746102 0.08063622 0.86091493 0.2014571 | 0.17746102 0.08063622
| 0.21024887 0.08432105 0.84111697 0.18746206 | 0.21024887 0.08432105
| 0.2437095 0.08713565 0.82095486 0.17466105 | 0.2437095 0.08713565
| 0.27697735 0.09074743 0.80097995 0.16464973 | 0.27697735 0.09074743
| 0.31104532 0.09417058 0.78107483 0.15447318 | 0.31104532 0.09417058
| 0.34467567 0.08652768 0.78033799 0.15218724 | 0.34467567 0.08652768
| 0.39817174 0.0896706 0.76045619 0.1420413 | 0.39817174 0.0896706
| 0.41188728 0.08995153 0.72100128 0.12705792 | 0.41188728 0.08995153
| 0.46499003 0.09269332 0.70107107 0.11766609 | 0.46499003 0.09269332
| 0.47861825 0.09241838 0.7004018 0.11088343 | 0.47861825 0.09241838
| 0.53182909 0.09784874 0.66055427 0.09622847 | 0.53182909 0.09784874
| 0.54571675 0.09800909 0.64054521 0.08828049 | 0.54571675 0.09800909
| 0.59877726 0.10542324 0.6204896 0.08147811 | 0.59877726 0.10542324
| 0.61261553 0.10543348 0.60054073 0.07380834 | 0.61261553 0.10543348
| 0.66568635 0.11294141 0.58043447 0.0670945 | 0.66568635 0.11294141
| 0.67972689 0.11547687 0.56035157 0.06046475 | 0.67972689 0.11547687
| 0.71317783 0.11907922 0.54038528 0.05459241 | 0.71317783 0.11907922
| 0.74595232 0.12718643 0.51960368 0.04835971 | 0.74595232 0.12718643
| 0.7796104 0.13557267 0.48046473 0.02597122 | 0.7796104 0.13557267
| 0.81292216 0.14914515 0.46036301 -0.0003573 | 0.81292216 0.14914515
| 0.84658129 0.16625566 0.44034568 -0.0162706 | 0.84658129 0.16625566
| 0.88012396 0.18789931 0.41982419 -0.0225202 | 0.88012396 0.18789931
| 0.91350344 0.22345034 0.37988697 -0.0331939 | 0.91350344 0.22345034
| 0.94678101 0.27982843 | 0.94678101 0.27982843
| 0.97987964 0.41689481 | 0.97987964 0.41689481
| |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
 | |
Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1 |
| |
| |
| Sample: Sonia quem |
| Operator: |
| Submitter: |
C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP |
| |
| |
Analysis AdsoN2 | Started: 25/01/2017 2Analysis AdsoN2 |
Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C |
Thermal CorrNo | Report Time:26/01/2017 1Thermal CorrNo |
Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ |
Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s |
Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g |
| Automatic DeYes |
| |
| |
| Comments: SiC |
| |
| |
| |
| |
| Isotherm Linear Absolute Plot |
| |
| |
Sonia quem - Desorption | Sonia quem - Adsorption Sonia quem - Desorption |
Relative Pres Quantity Ads | Absolute Pre Quantity AdsAbsolute Pre Quantity Ads |
0.97987964 0.41689481 | 13.4644899 0.05232748 724.244995 0.41689481 |
0.94229703 0.30396743 | 36.877388 0.06094785 696.442505 0.30396743 |
0.92160418 0.26807971 | 65.242897 0.06792775 681.126587 0.26807971 |
0.90137275 0.24093848 | 81.8216934 0.0706619 666.147583 0.24093848 |
0.88096927 0.2178752 | 106.447289 0.07574384 651.044434 0.2178752 |
0.86091493 0.2014571 | 131.234695 0.08063622 636.202393 0.2014571 |
0.84111697 0.18746206 | 155.497299 0.08432105 621.548889 0.18746206 |
0.82095486 0.17466105 | 180.26088 0.08713565 606.629272 0.17466105 |
0.80097995 0.16464973 | 204.888107 0.09074743 591.848999 0.16464973 |
0.78107483 0.15447318 | 230.110275 0.09417058 577.119507 0.15447318 |
0.78033799 0.15218724 | 254.978928 0.08652768 576.55719 0.15218724 |
0.76045619 0.1420413 | 294.537323 0.0896706 561.846497 0.1420413 |
0.72100128 0.12705792 | 304.664856 0.08995153 532.677917 0.12705792 |
0.70107107 0.11766609 | 343.925079 0.09269332 517.934143 0.11766609 |
 0.7004018 0.11088343 | 353.983917 0.09241838 517.466492 0.11088343 |
0.66055427 0.09622847 | 393.316895 0.09784874 488.060547 0.09622847 |
0.64054521 0.08828049 | 403.565491 0.09800909 473.306732 0.08828049 |
0.6204896 0.08147811 | 442.778076 0.10542324 458.519287 0.08147811 |
0.60054073 0.07380834 | 452.986267 0.10543348 443.806091 0.07380834 |
0.58043447 0.0670945 | 492.201477 0.11294141 428.974701 0.0670945 |
0.56035157 0.06046475 | 502.552887 0.11547687 414.161072 0.06046475 |
0.54038528 0.05459241 | 527.26239 0.11907922 399.43158 0.05459241 |
0.51960368 0.04835971 | 551.473572 0.12718643 384.095123 0.04835971 |
0.48046473 0.02597122 | 576.337952 0.13557267 355.185944 0.02597122 |
0.46036301 -0.0003573 | 600.944702 0.14914515 340.349304 -0.0003573 |
0.44034568 -0.0162706 | 625.80481 0.16625566 325.554138 -0.0162706 |
0.41982419 -0.0225202 | 650.578979 0.18789931 310.382294 -0.0225202 |
0.37988697 -0.0331939 | 675.228943 0.22345034 280.85611 -0.0331939 |
| 699.803894 0.27982843 |
| 724.244995 0.41689481 |
| |
 |
ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428
|
|
Sample: Sonia quem | Sample: Sonia quem
Operator: | Operator:
Submitter: | Submitter:
File: C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
Started: 25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis Adso
Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath
Report Time:26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal Corr
Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp
Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration
Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure
Automatic DeYes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
Isotherm Log Absolute Plot | Isotherm Pressure Composition
|
|
Sonia quem - Adsorption Sonia quem - Desorption | Sonia quem - Adsorption Sonia quem - Desorption
Absolute Pre Quantity AdsAbsolute Pre Quantity Ads | Weight % N2 Absolute Pre Weight % N2
13.4644899 0.05232748 724.244995 0.41689481 | 0.00046692 13.4644899 0.00371993
36.877388 0.06094785 696.442505 0.30396743 | 0.00054383 36.877388 0.00271229
65.242897 0.06792775 681.126587 0.26807971 | 0.00060612 65.242897 0.00239206
81.8216934 0.0706619 666.147583 0.24093848 | 0.00063051 81.8216934 0.00214988
106.447289 0.07574384 651.044434 0.2178752 | 0.00067586 106.447289 0.00194409
131.234695 0.08063622 636.202393 0.2014571 | 0.00071951 131.234695 0.00179759
155.497299 0.08432105 621.548889 0.18746206 | 0.00075239 155.497299 0.00167272
180.26088 0.08713565 606.629272 0.17466105 | 0.00077751 180.26088 0.00155849
204.888107 0.09074743 591.848999 0.16464973 | 0.00080974 204.888107 0.00146916
230.110275 0.09417058 577.119507 0.15447318 | 0.00084028 230.110275 0.00137836
254.978928 0.08652768 576.55719 0.15218724 | 0.00077208 254.978928 0.00135796
294.537323 0.0896706 561.846497 0.1420413 | 0.00080013 294.537323 0.00126743
304.664856 0.08995153 532.677917 0.12705792 | 0.00080263 304.664856 0.00113373
343.925079 0.09269332 517.934143 0.11766609 | 0.0008271 343.925079 0.00104993
353.983917 0.09241838 517.466492 0.11088343 | 0.00082465 353.983917 0.00098941
393.316895 0.09784874 488.060547 0.09622847 | 0.0008731 393.316895 0.00085864
403.565491 0.09800909 473.306732 0.08828049 | 0.00087453 403.565491 0.00078772
442.778076 0.10542324 458.519287 0.08147811 | 0.00094069 442.778076 0.00072703
452.986267 0.10543348 443.806091 0.07380834 | 0.00094078 452.986267 0.00065859
492.201477 0.11294141 428.974701 0.0670945 | 0.00100777 492.201477 0.00059868
502.552887 0.11547687 414.161072 0.06046475 | 0.00103039 502.552887 0.00053952
527.26239 0.11907922 399.43158 0.05459241 | 0.00106254 527.26239 0.00048713
551.473572 0.12718643 384.095123 0.04835971 | 0.00113488 551.473572 0.00043151
576.337952 0.13557267 355.185944 0.02597122 | 0.00120971 576.337952 0.00023174
600.944702 0.14914515 340.349304 -0.0003573 | 0.00133082 600.944702 -3.1884E-06
625.80481 0.16625566 325.554138 -0.0162706 | 0.00148349 625.80481 -0.0001452
650.578979 0.18789931 310.382294 -0.0225202 | 0.00167662 650.578979 -0.0002009
675.228943 0.22345034 280.85611 -0.0331939 | 0.00199384 675.228943 -0.0002962
699.803894 0.27982843 | 0.0024969 699.803894
724.244995 0.41689481 | 0.00371993 724.244995
|
 | |
Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4
| |
| |
| Sample: Sonia quem | Sample:
| Operator: | Operator:
| Submitter: | Submitter:
A\000-103.SMP | File: C:\2020\DATA\000-103.SMP | File:
| |
| |
N2 | Started: 25/01/2017 2Analysis AdsoN2 | Started:
-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed:
No | Report Time:26/01/2017 1Thermal CorrNo | Report Time:
18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass
60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa
1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp
| Automatic DeYes | Automatic De
| |
| |
| Comments: SiC | Comments: SiC
| |
| |
| |
| |
| BET Surface Area Report | BET Surface Area Plot
| |
| BET Surface A0.2278 ± 0.0148 m²/g |
Sonia quem - Desorption | Slope: 19.990270 ± 1.194669 g/cm³ STP | Sonia quem
Absolute Pre | Y-Intercept: -0.877998 ± 0.335470 g/cm³ STP | Relative Pres
724.244995 | C: -21.768022 | 0.11066301
696.442505 | Qm: 0.0523 cm³/g STP | 0.14395566
681.126587 | Correlation Co
0.9860128 | 0.17746102
666.147583 | Molecular Cro0.1620 nm² | 0.21024887
651.044434 | | 0.2437095
636.202393 | | 0.27697735
621.548889 | Relative Pres Quantity Ads1/[Q(Po/P - 1)] | 0.31104532
606.629272 | 0.11066301 0.0706619 1.76096539 | 0.34467567
591.848999 | 0.14395566 0.07574384 2.22016457 | 0.39817174
577.119507 | 0.17746102 0.08063622 2.67557007 | 0.41188728
576.55719 | 0.21024887 0.08432105 3.15723878 |
561.846497 | 0.2437095 0.08713565 3.69817901 |
532.677917 | 0.27697735 0.09074743 4.22141454 |
517.934143 | 0.31104532 0.09417058 4.79421784 |
517.466492 | 0.34467567 0.08652768 6.07854023 |
488.060547 | 0.39817174 0.0896706 7.37815507 |
473.306732 | 0.41188728 0.08995153 7.7859078 |
458.519287 | |
443.806091 | |
428.974701 |
414.161072 |
399.43158 |
384.095123 |
355.185944 |
340.349304 |
325.554138 |
310.382294 |
280.85611 |
|
|
|
 |
Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1
|
|
Sonia quem | Sample: Sonia quem
| Operator:
| Submitter:
C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis AdsoN2
26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C
26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal CorrNo
1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³
56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s
22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g
Yes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
BET Surface Area Plot | Langmuir Surface Area Report
|
| Langmuir Sur0.4246 ± 0.0118 m²/g
| Slope: 10.251301 ± 0.285894 g/cm³ STP
1/[Q(Po/P - 1)] | Y-Intercept: 238.710538 ± 48.434624 mmHg·g/cm³
1.76096539 | b: 0.042944 1/mmHg
2.22016457 | Qm: 0.0975 cm³/g STP
2.67557007 | Correlation Co
0.996134
3.15723878 | Molecular Cro0.1620 nm²
3.69817901 |
4.22141454 |
4.79421784 | Pressure (m Quantity AdsP/Q (mmHg·g/cm³ STP)
6.07854023 | 13.4644899 0.05232748 257.312005
7.37815507 | 36.877388 0.06094785 605.064584
7.7859078 | 65.242897 0.06792775 960.474881
| 81.8216934 0.0706619 1157.93227
| 106.447289 0.07574384 1405.35897
| 131.234695 0.08063622 1627.49072
| 155.497299 0.08432105 1844.11017
| 180.26088 0.08713565 2068.73854
| 204.888107 0.09074743 2257.78408
| 230.110275 0.09417058 2443.54737
| 254.978928 0.08652768 2946.79045
| 294.537323 0.0896706 3284.65874
|
|
| |
| ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1
| |
| |
| Sample: Sonia quem | Sample: Sonia quem
| Operator: | Operator:
| Submitter: | Submitter:
| File: C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
| |
| |
| Started: 25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2
| Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8
| Report Time:26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1
| Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g
| Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³
| Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C
| Automatic DeYes | Automatic DeYes
| |
| |
| Comments: SiC | Comments: SiC
| |
| |
| |
| |
| Langmuir Surface Area Plot | Freundlich Reports
| |
| | Primary Data
| Sonia quem | 4057- At least two data points are needed for
| Pressure (m P/Q (mmHg·g/cm³ STP) | Primary Data
| 13.4644899 257.312005 | 4057- At least two data points are needed for
| 36.877388 605.064584 |
| 65.242897 960.474881 |
| 81.8216934 1157.93227 |
| 106.447289 1405.35897 |
| 131.234695 1627.49072 |
| 155.497299 1844.11017 |
| 180.26088 2068.73854 |
| 204.888107 2257.78408 |
| 230.110275 2443.54737 |
| 254.978928 2946.79045 |
| 294.537323 3284.65874 |
| |
|
|
|
|
|
|
|
|
 | |
Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1 |
| |
| |
| Sample: Sonia quem |
| Operator: |
| Submitter: |
C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP |
| |
| |
Analysis AdsoN2 | Started: 25/01/2017 2Analysis AdsoN2 |
Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C |
Thermal CorrNo | Report Time:26/01/2017 1Thermal CorrNo |
Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ |
Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s |
Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g |
| Automatic DeYes |
| |
| |
| Comments: SiC |
| |
| |
| |
| |
| Temkin Reports |
| |
| Primary Data |
t two data points are needed for Freund | 4058- At least two data points are needed for Temkin |
| Primary Data |
t two data points are needed for Freund | 4058- At least two data points are needed for Temkin |
| |
| |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
 |
ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428
|
|
Sample: Sonia quem | Sample: Sonia quem
Operator: | Operator:
Submitter: | Submitter:
File: C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
Started: 25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis Adso
Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath
Report Time:26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal Corr
Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp
Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration
Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure
Automatic DeYes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
t-Plot Report | t-Plot
| Harkins and Jura
Micropore Vo0.000005 cm³/g |
Micropore Ar* | Sonia quem
External Surf 0.2813 m²/g | Thickness (Å)Quantity Adsorbed (cm³/g STP)
Slope: 0.018188 ± 0.000602 cm³/g·Å STP | 3.58539234 0.06792775
Y-Intercept: 0.002920 ± 0.002551 cm³/g STP | 3.7591686 0.0706619
Correlation Co0.997272 | 3.99681013 0.07574384
Surface Area 1.000 | 4.22184722 0.08063622
Density Conve0.0015468 | 4.43499089 0.08432105
Total Surface 0.2278 m²/g | 4.64958203 0.08713565
Thickness Ra 3.5000 Å to 5.0000 Å | 4.86307556 0.09074743
Thickness EquHarkins and Jura |
|
|
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
|
Relative Pres Statistical Th Quantity AdsFitted |
0.01821591 2.80858282 0.05232748 |
0.04988587 3.23595129 0.06094785 |
0.08824919 3.58539234 0.06792775 * |
0.11066301 3.7591686 0.0706619 * |
0.14395566 3.99681013 0.07574384 * |
0.17746102 4.22184722 0.08063622 * |
0.21024887 4.43499089 0.08432105 * |
0.2437095 4.64958203 0.08713565 * |
0.27697735 4.86307556 0.09074743 * |
0.31104532 5.08439708 0.09417058 |
0.34467567 5.30774618 0.08652768 |
0.39817174 5.67805031 0.0896706 |
0.41188728 5.7767959 0.08995153 |
0.46499003 6.17786589 0.09269332 |
0.47861825 6.28638004 0.09241838 |
0.53182909 6.73709819 0.09784874 |
0.54571675 6.86288485 0.09800909 |
0.59877726 7.38187306 0.10542324 |
0.61261553 7.52879935 0.10543348 |
0.66568635 8.14789297 0.11294141 |
0.67972689 8.32900262 0.11547687 |
0.71317783 8.79644205 0.11907922 |
0.74595232 9.31336391 0.12718643 |
0.7796104 9.92150667 0.13557267 |
0.81292216 10.623895 0.14914515 |
0.84658129 11.4703912 0.16625566 |
0.88012396 12.5055771 0.18789931 |
0.91350344 13.8161504 0.22345034 |
0.94678101 15.5643551 0.27982843 |
0.97987964 18.073767 0.41689481 |
|
|
* The micropore area is not reported because either t |
|
 | |
Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4
| |
| |
| Sample: Sonia quem | Sample:
| Operator: | Operator:
| Submitter: | Submitter:
A\000-103.SMP | File: C:\2020\DATA\000-103.SMP | File:
| |
| |
N2 | Started: 25/01/2017 2Analysis AdsoN2 | Started:
-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed:
No | Report Time:26/01/2017 1Thermal CorrNo | Report Time:
18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass
60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa
1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp
| Automatic DeYes | Automatic De
| |
| |
| Comments: SiC | Comments: SiC
| |
| |
| |
| |
| Alpha-S Method | f-Ratio Method
| |
| Primary Data | Primary Data
| 4029- At least two fitted data points are needed for | A reference file has not been chos
orbed (cm³/g STP) | 4029- At least two fitted data points are needed for |
| |
| |
|
|
|
|
|
|
 |
Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1
|
|
Sonia quem | Sample: Sonia quem
| Operator:
| Submitter:
C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis AdsoN2
26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C
26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal CorrNo
1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ Measured
56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s
22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g STP
Yes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
-Ratio Method | BJH Adsorption Pore Distribution Report
|
Primary Data | Faas Correction
A reference file has not been chosen. | Harkins and Jura
| t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5
|
|
| Diameter Ran17.000 Å to 3000.000 Å
| Adsorbate Pro9.53000 Å
| Density Conve0.0015468
| Fraction of P 0.00
|
|
| Pore DiameteAverage DiamIncremental Cumulative P
| 377.6 - 236.2 274.302879 0.00010605 0.00010605
| 236.2 - 172.2 193.719071 6.8375E-05 0.00017442
| 172.2 - 135.3 149.031149 4.1522E-05 0.00021594
| 135.3 - 111.2 120.70572 3.3021E-05 0.00024896
| 111.2 - 94.3 101.253747 2.6104E-05 0.00027507
| 94.3 - 81.6 86.9429718 1.467E-05 0.00028974
| 81.6 - 71.9 76.0714242 1.4804E-05 0.00030454
| 71.9 - 64.0 67.4144195 3.9094E-06 0.00030845
| 64.0 - 61.1 62.4306344 4.4495E-06 0.0003129
| 61.1 - 51.9 55.6452951 1.2094E-05 0.00032499
| 51.9 - 43.4 46.2355705 1.3273E-05 0.00033827
| 43.4 - 36.8 39.0709502 8.4273E-06 0.00034669
| 36.8 - 27.3 28.7796645 2.7061E-06 0.0003494
| 27.3 - 23.7 24.5325836 1.0182E-05 0.00035958
| 23.7 - 22.0 22.7918099 6.1361E-06 0.00036572
| 22.0 - 20.4 21.1267483 1.035E-05 0.00037607
| 20.4 - 18.8 19.4850353 1.5846E-05 0.00039191
| 18.8 - 17.1 17.8292588 1.56E-05 0.00040751
|
|
 | |
| ASAP 2020 V4Unit 1 Serial #: 428 Page 1 |
| |
| |
| Sample: Sonia quem |
| Operator: |
| Submitter: |
| File: C:\2020\DATA\000-103.SMP |
| |
| |
| Started: 25/01/2017 2Analysis AdsoN2 |
| Completed: 26/01/2017 8Analysis Bath-196.033 °C |
| Report Time:26/01/2017 1Thermal CorrNo |
18.6504 cm³ Measured | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ |
| Cold Free Spa56.8154 cm³ Equilibration 60 s |
1.000 cm³/g STP | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g |
| Automatic DeYes |
| |
| |
| Comments: SiC |
| |
| |
| |
| |
| BJH Adsorption Cumulative Pore Volume (Larger) |
| Harkins and Jura : Faas Correction |
| |
| Sonia quem |
| Pore Diameter
Pore Volume (cm³/g) |
| 236.238418 0.00010605 |
| 172.200168 0.00017442 |
| 135.305747 0.00021594 |
| 111.195974 0.00024896 |
| 94.3254005 0.00027507 |
| 81.5813503 0.00028974 |
| 71.9035361 0.00030454 |
| 63.9522347 0.00030845 |
Incremental PCumulative Po | 61.0577436 0.0003129 |
0.01546398 0.01546398 | 51.8783521 0.00032499 |
0.01411835 0.02958233 | 43.4099049 0.00033827 |
0.01114442 0.04072675 | 36.8495976 0.00034669 |
0.01094281 0.05166956 | 27.2556006 0.0003494 |
0.01031248 0.06198205 | 23.7273029 0.00035958 |
 0.0067492 0.06873125 | 22.0195709 0.00036572 |
0.00778415 0.0765154 | 20.394816 0.00037607 |
0.00231961 0.07883501 | 18.7546695 0.00039191 |
0.00285085 0.08168586 | 17.1044283 0.00040751 |
0.00869328 0.09037914 | |
0.01148334 0.10186248 |
0.00862773 0.11049021 |
0.00376119 0.1142514 |
0.01660131 0.13085271 |
0.0107689 0.14162161 |
0.01959553 0.16121714 |
0.03252973 0.19374688 |
0.03499905 0.22874593 |
|
|
 |
ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428
|
|
Sample: Sonia quem | Sample: Sonia quem
Operator: | Operator:
Submitter: | Submitter:
File: C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
Started: 25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis Adso
Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath
Report Time:26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal Corr
Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp
Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration
Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure
Automatic DeYes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
BJH Adsorption dV/dD Pore Volume | BJH Adsorption dV/dlog(D) Pore Volume
Harkins and Jura : Faas Correction | Harkins and Jura : Faas Correction
|
Sonia quem | Sonia quem
Pore Diameter
Pore Volume (cm³/g·Å) | Pore Diameter
dV/dlog(D) Pore Volume (cm³/g)
274.302879 7.5028E-07 | 274.302879 0.00052071
193.719071 1.0677E-06 | 193.719071 0.00049793
149.031149 1.1254E-06 | 149.031149 0.00039651
120.70572 1.3696E-06 | 120.70572 0.00038745
101.253747 1.5473E-06 | 101.253747 0.0003653
86.9429718 1.1511E-06 | 86.9429718 0.00023272
76.0714242 1.5297E-06 | 76.0714242 0.00026994
67.4144195 4.9166E-07 | 67.4144195 7.6813E-05
62.4306344 1.5372E-06 | 62.4306344 0.0002212
55.6452951 1.3175E-06 | 55.6452951 0.00017092
46.2355705 1.5674E-06 | 46.2355705 0.0001715
39.0709502 1.2846E-06 | 39.0709502 0.00011843
28.7796645 2.8207E-07 | 28.7796645 2.0661E-05
24.5325836 2.8858E-06 | 24.5325836 0.00016911
22.7918099 3.5931E-06 | 22.7918099 0.00018915
21.1267483 0.00000637 | 21.1267483 0.00031091
19.4850353 9.6614E-06 | 19.4850353 0.00043521
17.8292588 9.4533E-06 | 17.8292588 0.00039
|
 | |
Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4
| |
| |
| Sample: Sonia quem | Sample:
| Operator: | Operator:
| Submitter: | Submitter:
A\000-103.SMP | File: C:\2020\DATA\000-103.SMP | File:
| |
| |
N2 | Started: 25/01/2017 2Analysis AdsoN2 | Started:
-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed:
No | Report Time:26/01/2017 1Thermal CorrNo | Report Time:
18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass
60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa
1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp
| Automatic DeYes | Automatic De
| |
| |
| Comments: SiC | Comments: SiC
| |
| |
| |
| |
Pore Volume | BJH Adsorption Cumulative Pore Area (Larger) | BJH Adsorption dA/dD Pore Area
| Harkins and Jura : Faas Correction | Harkins and Jura : Faas Correction
| |
| Sonia quem | Sonia quem
re Volume (cm³/g) | Pore Diameter
Pore Area (m²/g) | Pore Diameter
| 236.238418 0.01546398 | 274.302879
| 172.200168 0.02958233 | 193.719071
| 135.305747 0.04072675 | 149.031149
| 111.195974 0.05166956 | 120.70572
| 94.3254005 0.06198205 | 101.253747
| 81.5813503 0.06873125 | 86.9429718
| 71.9035361 0.0765154 | 76.0714242
| 63.9522347 0.07883501 | 67.4144195
| 61.0577436 0.08168586 | 62.4306344
| 51.8783521 0.09037914 | 55.6452951
| 43.4099049 0.10186248 | 46.2355705
| 36.8495976 0.11049021 | 39.0709502
| 27.2556006 0.1142514 | 28.7796645
| 23.7273029 0.13085271 | 24.5325836
| 22.0195709 0.14162161 | 22.7918099
| 20.394816 0.16121714 | 21.1267483
| 18.7546695 0.19374688 | 19.4850353
| 17.1044283 0.22874593 | 17.8292588
| |
 |
Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1
|
|
Sonia quem | Sample: Sonia quem
| Operator:
| Submitter:
C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis AdsoN2
26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C
26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal CorrNo
1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³
56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s
22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g
Yes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
BJH Adsorption dA/dD Pore Area | BJH Adsorption dA/dlog(D) Pore Area
Harkins and Jura : Faas Correction | Harkins and Jura : Faas Correction
|
| Sonia quem
Pore Area (m²/g·Å) | Pore Diameter
dA/dlog(D) Pore Area (m²/g)
0.00010941 | 274.302879 0.07593143
0.00022047 | 193.719071 0.1028158
0.00030206 | 149.031149 0.10642382
0.00045387 | 120.70572 0.12839578
0.00061127 | 101.253747 0.14431047
0.0005296 | 86.9429718 0.10706605
0.00080433 | 76.0714242 0.14194127
0.00029173 | 67.4144195 0.04557673
0.00098492 | 62.4306344 0.14172787
0.00094704 | 55.6452951 0.12286524
0.00135602 | 46.2355705 0.14836871
0.00131514 | 39.0709502 0.12125076
0.00039204 | 28.7796645 0.02871642
0.00470519 | 24.5325836 0.27573549
0.00630596 | 22.7918099 0.3319684
0.01206061 | 21.1267483 0.58864777
0.01983343 | 19.4850353 0.89341932
0.02120845 | 17.8292588 0.87495773
|
| |
| ASAP 2020 V4Unit 1 Serial #: 428 Page 1 |
| |
| |
| Sample: Sonia quem |
| Operator: |
| Submitter: |
| File: C:\2020\DATA\000-103.SMP |
| |
| |
| Started: 25/01/2017 2Analysis AdsoN2 |
| Completed: 26/01/2017 8Analysis Bath-196.033 °C |
| Report Time:26/01/2017 1Thermal CorrNo |
| Sample Mass1.0344 g Warm Free Sp18.6504 cm³ Measured |
| Cold Free Spa56.8154 cm³ Equilibration 60 s |
| Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g STP |
| Automatic DeYes |
| |
| |
| Comments: SiC |
| |
| |
| |
| |
| BJH Desorption Pore Distribution Report |
| |
| Faas Correction |
| Harkins and Jura |
| t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
| |
| |
| Diameter Ran17.000 Å to 3000.000 Å |
| Adsorbate Pro9.53000 Å |
| Density Conve0.0015468 |
| Fraction of P 0.00 |
| |
| |
| Pore DiameteAverage DiamIncremental Cumulative PIncremental PCumulative Po |
| 973.9 - 351.3 417.085537 0.00020345 0.00020345 0.01951164 0.01951164 |
| 351.3 - 261.9 292.96436 6.5628E-05 0.00026908 0.00896053 0.02847217 |
| 261.9 - 210.2 229.996827 5.0688E-05 0.00031977 0.00881541 0.03728759 |
| 210.2 - 175.5 189.471732 4.3917E-05 0.00036368 0.00927156 0.04655914 |
| 175.5 - 151.1 161.291723 3.1146E-05 0.00039483 0.0077242 0.05428334 |
| 151.1 - 132.8 140.664077 2.6815E-05 0.00042165 0.00762533 0.06190867 |
| 132.8 - 118.3 124.613904 2.4823E-05 0.00044647 0.00796799 0.06987665 |
| 118.3 - 106.6 111.781323 1.9055E-05 0.00046552 0.00681852 0.07669518 |
| 106.6 - 97.1 101.351043 2.0039E-05 0.00048556 0.00790882 0.084604 |
| 97.1 - 96.7 96.909136 5.4282E-06 0.00049099 0.00224052 0.08684452 |
| 96.7 - 88.8 92.3700196 2.0422E-05 0.00051141 0.00884369 0.09568821 |
| 88.8 - 76.1 81.3562742 2.899E-05 0.0005404 0.01425345 0.10994166 |
| 76.1 - 70.9 73.3256341 2.0019E-05 0.00056042 0.01092074 0.1208624 |
| 70.9 - 70.8 70.8593954 1.8158E-05 0.00057858 0.01025013 0.13111252 |
| 70.8 - 62.2 65.8339637 2.9347E-05 0.00060793 0.01783062 0.14894314 |
| 62.2 - 58.5 60.2066213 1.6876E-05 0.0006248 0.01121229 0.16015543 |
| 58.5 - 55.2 56.7410516 1.386E-05 0.00063866 0.00977075 0.16992617 |
| 55.2 - 52.2 53.6076697 1.6747E-05 0.00065541 0.01249634 0.18242251 |
| |
| |
 |
ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428
|
|
Sample: Sonia quem | Sample: Sonia quem
Operator: | Operator:
Submitter: | Submitter:
File: C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
Started: 25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis Adso
Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath
Report Time:26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal Corr
Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp
Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration
Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure
Automatic DeYes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
BJH Desorption dV/dD Pore Volume | Dollimore-Heal Adsorption Pore Distribution Report
Harkins and Jura : Faas Correction |
| Harkins and Jura
Sonia quem | t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5
Pore Diameter
Pore Volume (cm³/g·Å) |
417.085537 3.2677E-07 |
292.96436 7.3389E-07 | Diameter Ran17.000 Å to 3000.000 Å
229.996827 9.8055E-07 | Adsorbate Pro9.53000 Å
189.471732 1.2659E-06 | Density Conve0.0015468
161.291723 1.2752E-06 |
140.664077 1.4701E-06 |
124.613904 1.704E-06 | Pore DiameteAverage DiamIncremental
111.781323 1.6385E-06 | 379.7 - 238.3 308.984457 0.00010388
101.351043 2.0951E-06 | 238.3 - 174.3 206.295091 6.8134E-05
96.909136 1.684E-05 | 174.3 - 137.4 155.828756 4.1951E-05
92.3700196 2.5577E-06 | 137.4 - 113.3 125.326659 3.3711E-05
81.3562742 2.294E-06 | 113.3 - 96.4 104.836485 2.6921E-05
73.3256341 3.8609E-06 | 96.4 - 83.7 90.0291733 1.5378E-05
70.8593954 0.00011146 | 83.7 - 74.0 78.8182411 1.5602E-05
65.8339637 3.406E-06 | 74.0 - 66.0 70.0036833 4.3657E-06
60.2066213 4.6161E-06 | 66.0 - 63.1 64.5807871 4.8323E-06
56.7410516 4.1901E-06 | 63.1 - 54.0 58.5438458 1.2936E-05
53.6076697 5.604E-06 | 54.0 - 51.9 52.9408144 0
| 51.9 - 45.2 48.5616493 1.4139E-05
| 45.2 - 43.7 44.4276601 0
| 43.7 - 38.4 41.0495283 9.1061E-06
| 38.4 - 33.0 35.740588 0
| 33.0 - 32.1 32.5477485 0
| 32.1 - 28.5 30.2817697 3.1037E-06
|
|
 |
Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1
|
|
| Sample: Sonia quem
| Operator:
| Submitter:
A\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
N2 | Started: 25/01/2017 2Analysis AdsoN2
-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C
No | Report Time:26/01/2017 1Thermal CorrNo
18.6504 cm³ Measured | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ Measured
60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s
1.000 cm³/g STP | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g STP
| Automatic DeYes
|
|
| Comments: SiC
|
|
|
|
Pore Distribution Report | Dollimore-Heal Desorption Pore Distribution Report
|
| Harkins and Jura
| t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5
|
|
| Diameter Ran17.000 Å to 3000.000 Å
| Adsorbate Pro9.53000 Å
| Density Conve0.0015468
|
|
Cumulative PIncremental PCumulative Po | Pore DiameteAverage DiamIncremental Cumulative P
0.00010388 0.01344808 0.01344808 | 973.9 - 351.3 662.579882 0.00019032 0.00019032
0.00017202 0.01321101 0.02665908 | 351.3 - 261.9 306.56286 0.00006543 0.00025575
0.00021397 0.01076854 0.03742762 | 261.9 - 210.2 236.003568 5.076E-05 0.00030651
0.00024768 0.01075927 0.04818689 | 210.2 - 175.5 192.810969 4.4053E-05 0.00035056
0.0002746 0.01027163 0.05845852 | 175.5 - 151.0 163.253016 3.1414E-05 0.00038197
0.00028998 0.00683244 0.06529096 | 151.0 - 132.8 141.921 2.7089E-05 0.00040906
0.00030558 0.00791776 0.07320872 | 132.8 - 118.2 125.517533 2.5081E-05 0.00043414
0.00030994 0.00249454 0.07570326 | 118.2 - 106.6 112.41924 1.9345E-05 0.00045349
0.00031478 0.00299305 0.07869631 | 106.6 - 97.0 101.822155 2.0278E-05 0.00047377
0.00032771 0.00883817 0.08753448 | 97.0 - 96.7 96.8786472 5.4407E-06 0.00047921
0.00032771 0 0.08753448 | 96.7 - 88.7 92.7251302 2.0623E-05 0.00049983
0.00034185 0.01164633 0.09918082 | 88.7 - 76.1 82.4139522 2.9005E-05 0.00052883
0.00034185 0 0.09918082 | 76.1 - 70.9 73.5025476 2.0159E-05 0.00054899
0.00035096 0.00887327 0.10805408 | 70.9 - 70.7 70.8285178 1.8149E-05 0.00056714
0.00035096 0 0.10805408 | 70.7 - 62.1 66.4390108 2.9259E-05 0.0005964
0.00035096 0 0.10805408 | 62.1 - 58.5 60.3029698 1.7009E-05 0.00061341
0.00035406 0.00409981 0.1121539 | 58.5 - 55.2 56.821058 1.4017E-05 0.00062743
| 55.2 - 52.2 53.6729 1.6849E-05 0.00064428
|
|
 | |
| ASAP 2020 V4Unit 1 Serial #: 428 Page 1 |
| |
| |
| Sample: Sonia quem |
| Operator: |
| Submitter: |
| File: C:\2020\DATA\000-103.SMP |
| |
| |
| Started: 25/01/2017 2Analysis AdsoN2 |
| Completed: 26/01/2017 8Analysis Bath-196.033 °C |
| Report Time:26/01/2017 1Thermal CorrNo |
18.6504 cm³ Measured | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ |
| Cold Free Spa56.8154 cm³ Equilibration 60 s |
1.000 cm³/g STP | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g |
| Automatic DeYes |
| |
| |
| Comments: SiC |
| |
| |
| |
| |
| Horvath-Kawazoe Reports |
| |
| Primary Data |
| 4036- Fewer than 2 points available for Horvath-Kaw |
| 4037- Computations failed while processing the prim |
| 4036- Fewer than 2 points available for Horvath-Kaw |
| 4037- Computations failed while processing the prim |
| |
| |
|
|
Incremental PCumulative Po |
0.01148935 0.01148935 |
0.00853724 0.0200266 |
0.0086033 0.0286299 |
0.00913905 0.03776895 |
0.00769712 0.04546607 |
0.00763504 0.05310111 |
0.00799276 0.06109387 |
0.00688311 0.06797698 |
0.00796618 0.07594316 |
0.0022464 0.07818956 |
0.00889626 0.08708582 |
0.01407786 0.10116368 |
0.01097059 0.11213427 |
0.01024944 0.12238371 |
0.01761542 0.13999913 |
0.01128252 0.15128164 |
0.00986727 0.16114891 |
0.01255659 0.1737055 |
|
|
 |
ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428
|
|
Sample: Sonia quem | Sample: Sonia quem
Operator: | Operator:
Submitter: | Submitter:
File: C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
Started: 25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis Adso
Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath
Report Time:26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal Corr
Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp
Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration
Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure
Automatic DeYes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
DFT Surface Energy Reports | Dubinin Reports
|
Primary Data | 4034- Fewer than 2 points available for Dubinin calc
4073- The analysis gas (N2) does not match the mode | 4030- Preparations failed in primary data.
4074- The analysis temperature (-196.033 °C) does | 4034- Fewer than 2 points available for Dubinin calc
| 4030- Preparations failed in primary data.
|
|
 | |
Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4
| |
| |
| Sample: Sonia quem | Sample:
| Operator: | Operator:
| Submitter: | Submitter:
A\000-103.SMP | File: C:\2020\DATA\000-103.SMP | File:
| |
| |
N2 | Started: 25/01/2017 2Analysis AdsoN2 | Started:
-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C | Completed:
No | Report Time:26/01/2017 1Thermal CorrNo | Report Time:
18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass
60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s | Cold Free Spa
1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp
| Automatic DeYes | Automatic De
| |
| |
| Comments: SiC | Comments: SiC
| |
| |
| |
| |
| MP-Method Reports | Options Report
| |
available for Dubinin calc | Primary Data |
n primary data. | 4059- Fewer than 2 points available for MP-Method c |
available for Dubinin calc | 4059- Fewer than 2 points available for MP-Method c | Sample Tube
n primary data. | |
| | Warm free sp
| | Cold free spa
| Non-ideality f
| Use Isotherma
| Use Filler Rod
| Vacuum seal
|
|
| Analysis Conditions
|
|
|
| Preparation
|
| Fast evacuati
| Vacuum setpo
| Evacuation ti
| Leak test:
| Leak test dur
| Use TranSeal:
|
|
| Free Space
|
| Free-space ty
| Lower dewar
| Evacuation ti
| Outgas test:
|
|
| Po and Temperature
|
| Po and T type
| Measurement
| Ambient temp
|
|
| Dosing
|
| Use first pres
| Use maximum
| Target tolera
| Low pressure
| Dose amount
| Minimum equi
| Maximum equi
|
|
| Equilibration
|
| Equilibration
| Equilibration
| Equilibration
| Equilibration
| Equilibration
| Equilibration
| Minimum equil
|
|
| Sample Backfill
|
| Backfill at sta
| Backfill at en
| Backfill gas:
|
|
| Adsorptive Properties
|
| Adsorptive:
| Maximum mani
| Non-ideality f
| Density conve
| Therm. tran.
| Molecular cro
|
|
| Inside diamet
|
|
 |
Unit 1 Serial #: 428 Page 1 | ASAP 2020 V4Unit 1 Serial #: 428 Page 1
|
|
Sonia quem | Sample: Sonia quem
| Operator:
| Submitter:
C:\2020\DATA\000-103.SMP | File: C:\2020\DATA\000-103.SMP
|
|
25/01/2017 2Analysis AdsoN2 | Started: 25/01/2017 2Analysis AdsoN2
26/01/2017 8Analysis Bath-196.033 °C | Completed: 26/01/2017 8Analysis Bath-196.033 °C
26/01/2017 1Thermal CorrNo | Report Time:26/01/2017 1Thermal CorrNo
1.0344 g Warm Free Sp18.6504 cm³ | Sample Mass1.0344 g Warm Free Sp18.6504 cm³
56.8154 cm³ Equilibration 60 s | Cold Free Spa56.8154 cm³ Equilibration 60 s
22.00 °C Low Pressure 1.000 cm³/g | Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g
Yes | Automatic DeYes
|
|
Comments: SiC | Comments: SiC
|
|
|
|
Options Report | Sample Log Report
|
| Date Time Message
| 25/01/2017 11:51:43 Degas operation started on
Sample Tube | 25/01/2017 11:51:43 Started evacuation at
| 25/01/2017 12:59:15 Started temperature ramp a
1.0000 cm³ | 25/01/2017 13:15:21 Started temperature hold a
1.0000 cm³ | 25/01/2017 19:15:23 Started cool-down wait.
0.0000620 | 25/01/2017 19:27:51 Degas operation done.
Yes | 25/01/2017 19:33:26 Analysis started.
Yes | 25/01/2017 19:39:39 6240- Leak test failed. An
Seal Frit | 25/01/2017 19:40:09 Analysis Canceled.
| 25/01/2017 19:40:15 Analysis Skipped.
| 25/01/2017 19:40:42 Analysis Skipped.
Analysis Conditions | 25/01/2017 19:40:58 Analysis Skipped.
| 25/01/2017 19:41:36 Analysis Skipped.
| 25/01/2017 19:41:45 Analysis Skipped.
| 25/01/2017 19:42:01 Analysis done.
| 25/01/2017 20:16:28 Analysis started.
 |
Yes |
50 µmHg |
0.10 h |
Yes |
120 s |
No |
|
|
|
|
Measured |
Yes |
0.10 h |
No |
|
|
Po and Temperature |
|
Measure Po at intervals during analysis |
120 min |
22.00 °C |
|
|
|
|
No |
No |
5.0% or 5.000 mmHg |
Yes |
1.0000 cm³/g STP |
0.00 h |
999.00 h |
|
|
|
|
60 s |
60 s |
60 s |
60 s |
60 s |
60 s |
 600 s |
|
|
Sample Backfill |
|
Yes |
Yes |
N2 |
|
|
Adsorptive Properties |
|
Nitrogen |
925.00 mmHg |
0.0000620 |
0.0015468 |
3.860 Å |
0.162 nm² |
|
|
9.53 mm |
|
|
|
| ASAP 2020 V4Unit 1 Serial #: 428 Page 1
|
|
| Sample: Sonia quem
| Operator:
| Submitter:
| File: C:\2020\DATA\000-103.SMP
|
|
| Started: 25/01/2017 2Analysis AdsoN2
| Completed: 26/01/2017 8Analysis Bath-196.033 °C
| Report Time:26/01/2017 1Thermal CorrNo
| Sample Mass1.0344 g Warm Free Sp18.6504 cm³ Measured
| Cold Free Spa56.8154 cm³ Equilibration 60 s
| Ambient Temp 22.00 °C Low Pressure 1.000 cm³/g STP
| Automatic DeYes
|
|
| Comments: SiC
|
|
|
|
| Validation Report
|
|
|
| Isotherm Reports
|
| Free Space: Passed
|
|
| Po: Passed
|
|
| Pressure/Vol Equilibration interval may not be
| sufficient. Increase the equilibration interval.
|
| Desorption: Not within limits. Increase the sample mass, increase
| the equilibration interval, or check the free space.
|
|
|
|
| BET Reports
|
| C Value: C value is low. Select a new range, removing
| some of the higher pressure points.
|
| Correlation Co
Review the BET plot and see if the correct
| range has been selected for calculating surface area.
|
| Surface area:Passed
|
|
| Pressure RanThe selected BET relative pressure range is outside the
| recommended values of 0.05 to 0.30.
|
|
|
|