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  • 1 Guaiacol 220 NM 0 .5 % Triethy Lam Ine and 0 .5 % Phosphoric Acid - Acetonitrile (10 0:18) 98.6 7% 1.0 M L/M

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    Ezzati Aziz
    16 vistas4 páginas
    This literature review examines several studies that used HPLC to analyze guaiacol and phenol. 1. Six studies analyzed guaiacol using wavelengths of 220-240 nm, mobile phases containing phosphoric acid or triethylamine, and columns at temperatures of 20-30°C. Recovery rates for guaiacol were reported between 98.67-108.54%. 2. One study analyzed 4-vinyl guaiacol and phenol using wavelengths of 225 and 280 nm respectively, with mobile phases containing acetic acid, water, methanol, acetonitrile or isopropanol. 3. HPLC was used to simultaneously determine phenolic compounds and alpha-toc

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    This literature review examines several studies that used HPLC to analyze guaiacol and phenol. 1. Six studies analyzed guaiacol using wavelengths of 220-240 nm, mobile phases containing phosphoric acid or triethylamine, and columns at temperatures of 20-30°C. Recovery rates for guaiacol were reported between 98.67-108.54%. 2. One study analyzed 4-vinyl guaiacol and phenol using wavelengths of 225 and 280 nm respectively, with mobile phases containing acetic acid, water, methanol, acetonitrile or isopropanol. 3. HPLC was used to simultaneously determine phenolic compounds and alpha-toc

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    © All Rights Reserved
    Descargue como DOCX, PDF, TXT o lea en línea desde Scribd
    Marcar por contenido inapropiado
    16 vistas4 páginas

    1 Guaiacol 220 NM 0 .5 % Triethy Lam Ine and 0 .5 % Phosphoric Acid - Acetonitrile (10 0:18) 98.6 7% 1.0 M L/M

    Cargado por

    Ezzati Aziz
    This literature review examines several studies that used HPLC to analyze guaiacol and phenol. 1. Six studies analyzed guaiacol using wavelengths of 220-240 nm, mobile phases containing phosphoric acid or triethylamine, and columns at temperatures of 20-30°C. Recovery rates for guaiacol were reported between 98.67-108.54%. 2. One study analyzed 4-vinyl guaiacol and phenol using wavelengths of 225 and 280 nm respectively, with mobile phases containing acetic acid, water, methanol, acetonitrile or isopropanol. 3. HPLC was used to simultaneously determine phenolic compounds and alpha-toc

    Copyright:

    © All Rights Reserved
    Descargue como DOCX, PDF, TXT o lea en línea desde Scribd
    Marcar por contenido inapropiado
    de 4

    LITERATURE REVIEW ON HPLC WAVELENGHT OF GUAIACOL AND PHENOL

    GUAIACOL

    NO JOURNAL TITLE SAMPLE WAV MOBILE PHASE RECOVERY COLUMN FLOWRATE REFERENCES
    E- RATE TEMP
    LEN
    GHT
    1 Determination of Guaiacol 220 0 .5 % triethy lam 98.6 7% 1.0 m l/m HU ANG Wei,ZHAO
    Guaiacol in nm ine and 0 .5 % Chen ( Lianyungang
    Qutanling Oral phosphoric acid— Institute for Drug
    Liquid with HPLC acetonitrile (10 0 Control,Jiangsu2 2 2 0 0
    :18) 6,China)

    2 Determination of Guaiacol 240 methanol- 99.8% (30±0.15) 1 mL·min-1 SUN Guo-xiang1,DING


    Guaiacol salicylate nm water(75∶25) ℃ Nan1,SONG Yu-
    salicylate in qing1,WANG
    Guacetisal by Zhen1,SONG Liang-
    HPLC method and wei2(1.College of
    qualitative Pharmacy,Shenyang
    identification of Pharmaceutical
    relevant University,Shenyang
    substances by 110016;2.Shangdong
    HPLC-MS Luoxin Pharmacy Stock
    Co.Ltd,Linyi Shangdong
    276017)
    3 Effects of water Guaiacol 220 0.5% 20 ℃ 1.0 mL/min CHEN Qiu-
    and ethanol- nm triethylamine and xiang1,JIANG Xiao-
    extraction of 0.5% H3PO4 huang2,LI
    bamboo on solution- Hong2(1.Changsha
    guaiacol content acetonitrile(78:22) Hospital of Chinese
    Medicine,Changsha,Hun
    an 410001,China; 2.TCM
    University of
    Hunan,Changsha,Hunan
    410007,China)

    4 Determination of Guaiacol 220 0.5% phosphoric (99.78±3.85) 1 mL·min1 ZOU Ji-hong1,SONG


    guaiacol nm acid and 0.5% % Xin-xin1,ZHAO Chun-
    concentration in triethylamine- jie1,SONG Dan2
    human plasma by acetonitrile(V∶V=1 (1.School of
    RP-HPLC 00∶50) Pharmacy,Shenyang
    Pharmaceutical
    Univercity,Shenyang
    110016,China;2.The
    forth People Hospital of
    Chinese Medicinal
    University,Shenyang
    110032,China)
    5 Determination of Guaiacol 220 0.5% phosphoric 108.54% LI Hong,JIANG Meng-
    guaiacol in nm acid- liang(Pharmaceutical
    bamboo juice acetonitrile(78:22, College,TCM University
    from different v:v) of
    kinds of bamboo Hunan,Changsha,Hunan
    with HPLC 410208,China)

    6 Formation of 4- 4-Vinyl 225 1% acetic lmL/min: H.S. LEE and S. NAGY


    Vinyl Guaiacol in guaiacol nm acid/acetonitrile 1990
    Adversely Stored (solvent A) and
    Orange Juice as 1% acetic
    Measured by an acid/water
    Improved HPLC (solvent B)
    Method
    PHENOL
    Simultaneous phenols and 280 A (2% acetic acid 20 ml. Maria Tasioula-Margari*,
    determination of a- in water), B Otu Okogeri
    phenolic tocopherol (methanol), C
    compounds and (acetonitrile) and
    tocopherols in D (isopropanol)
    virgin olive oil using
    HPLC and UV
    detection

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