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Abstract
In the mechanical characterization of powders using
the direct shear testers such as the Jenike shear cell, the
existence of a uniform or well-defined stress field in a
powder specimen is assumed. This assumption has not
been subjected to any serious scrutiny in the literature.
In this study, the normal stress variation in a silica
powder was locally determined by locating a pressuresensitive TekScan pad at the bottom section of a Jenike
shear cell. A computer simulation of the consolidation
and pre-shearing stages of the Jenike test procedure
Keywords: computer simulations, DEM, Jenike shear cell, powder testing, stress inhomogeneity
1 Introduction
The accurate measurement of the bulk properties of
powders and granular materials is critical to the proper
design of storage and processing equipment that handle
these bulk materials. In addition, the cohesive flow
properties are often used to compare the quality of
products. However, testing methods produce results that
have a large uncertainty causing repeated measurements
to differ by substantial amounts. This indicates that
something in the test method or material may be
responsible for the lack of consistency in the test results.
All too often, different testers used to measure bulk
cohesion produce values that disagree with one another
[1, 2] and do not predict the actual process behavior. If
the angle of internal friction and cohesion are true
properties of the bulk material, they should ideally be
independent of the type of the tester. The apparent
discrepancies between these test methods may indicate a
*
Fig. 1: A typical yield locus generated by direct shear measurements. The stress homogeneity is inherently assumed in the
construction of the yield locus.
DOI: 10.1002/ppsc.200400942
294
material. In the shear stress-normal stress space, this
yield locus represents the bounding curve or line that
describes the stress states that will produce failure of a
consolidated and pre-sheared bulk material. All failure
stress states for a given consolidation stress are represented by Mohr stress circles and are tangent to this yield
locus. The specific Mohr stress circle, which is both
tangent to this yield locus and passes through the origin,
represents the unconfined yield stress state. The major
principal stress associated with this circle is the unconfined yield strength, fc, of the material. There is one yield
locus for each critical consolidation stress and one
unique value of unconfined yield strength for each major
principal critical consolidation stress, s1. The strength of
a bulk solid is used to determine the ability of the
material to form cohesive arches or ratholes. Bulk
strength is also used to correlate process behavior to
material properties.
Direct shear testers measure the bulk strength of
materials by first generating the yield locus and then
constructing the unconfined Mohr circle stress state from
the data. The basic procedure in all direct shear tests is
similar. While under a certain consolidation load, the
specimen inside the cell is pre-sheared to a condition of
continual deformation without volume change (critical
state). The confining load on the specimen is then
reduced, and the specimen is re-sheared to failure. This
produces a single point on the yield locus. Repeating this
procedure generates points along the yield locus and
allows computation of the unconfined yield strength.
There are several accepted direct shear testers available
today. Jenike, Peschl, Schulze, and Uniaxial testers are all
examples of direct shear testers [3 5]. The Jenike cell is
the oldest direct shear tester used to measure the
unconfined yield properties of powder and granular
materials [6, 7].
Most bulk solid mechanics practitioners assume that the
stress state in a given tester can be represented by some
effective (or average) stress state (see e.g. [8, 9]). In fact,
the calculations used to reduce the raw data inherently
assume this. In the Jenike test, for example, the shear
stress, t, and the normal stress, s, in a powder specimen
are assumed nearly equal to the boundary tractions.
These tractions are determined from the shearing force
acting on the ring S and the normal force acting on the lid,
N, as t S/A and s N/A. Here, A is the area of the
circular specimen. When the specimen is subjected to the
boundary forces S and N, the specimen is assumed to
have a uniform shear stress and normal stress everywhere or, at least, at the shear zone. Rademacher and
Haaker [10] introduced some corrections to the above t
and s by making a static equilibrium analysis of the
system. The corrections took the weight of the lid and the
specimen (above the assumed shear plane) as well as
friction at several contacts (the specimen-ring, the ringbase, the pin-ring exterior etc.) into account. The results
indicate that the experimentally obtained corrections are
typically small and that their theoretical corrections are
much greater than the experimental ones. Moreover,
their equilibrium analysis ignores the possible spatiotemporal variation of the stress field in the specimen. It is
also worth-mentioning that a Discrete Element Method
(DEM) analysis of the Jenike cell can explain some of the
Rademacher and HaakerJs corrections inherently.
Considering the granular nature of the material, wall
friction effects, and the operatorJs style of specimen
preparation, the stress homogeneity assumption becomes questionable. However, this assumption has not
been questioned thoroughly in the open literature. The
motivation behind our research is that the stress-strain
inhomogeneity may be the origin of the aforementioned
problems associated with the testers and that a fundamental understanding of the stress inhomogeneity may
enable us to improve these testers.
The goal of this paper is to provide evidence for the
existence of stress inhomogeneity in a powder specimen
tested in the Jenike shear cell via experiments and
discrete element simulations. Very recently, Thornton
and Zhang [11] performed discrete element simulations
of a direct shear tester and presented the average shear to
normal stress ratio. Their investigation disregarded the
possibility of stress inhomogeneity (gradient) in the
specimen. Similarly, the corrections introduced by Rademacher and Haaker [10] disregarded this possibility, as
mentioned previously. However, the stress inhomogeneity cannot be ruled out in a real direct shear tester,
which is the main concern of the present investigation.
Our experiments and discrete element simulations show
that the powder specimen actually develops a complex
inhomogeneous stress field, thus invalidating the commonly accepted stress homogeneity assumption.
2 Experimental
The Jenike cell consists of a shear ring, base, and a top
cover plate or lid (Figure 2). The ring and mold ring are
positioned above the base with the ring edge offset by the
thickness of the base cylinder. Material is placed in the
ring and base and a special twisting top applied. As the
total shear in the Jenike cell is limited, the standard
testing procedure [3] suggests pre-consolidating (compacting) the material within the cell by applying a weight
onto the top of the cell and rotating the twisting top to
produce a stress state in the test cell that is close to the
desired critical state. At this point, the mold ring and
twisting top are removed, and the shearing top and
consolidation weight are placed on the material in the
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The TekScan pad is made up of smooth plastic. Consequently, to create a rough surface, sand particles of
about 800 microns were glued to the surface of the pad.
The pad was calibrated with this sand coating and found
to produce accurate and repeatable load measurements
within 10% error. Besides repeatability of the sensor
output, other issues related to the measurement are the
drift, hysteresis, and non-linearity of the sensor output.
Within the time scale of the experiment, the drift was
observed to be small, while hysteresis was not tested. The
linearity of the output was assumed for the normal loads
considered in the Jenike test and checked intermittently
for loads that were not used in the calibration.
A moderately cohesive silica powder with a mean size of
about 50 mm was placed in the Jenike cell. The specimen
was consolidated with a normal load of 2.5 kPa and
subsequently pre-sheared to a steady-state condition
(constant shear force). After that, the normal load was
reduced to 1.3 kPa and the specimen was re-sheared to a
failure condition. The TekScan pad provides the vertical
normal stress, Tzz, during the consolidation, pre-shearing, and re-shearing to failure stages while a load cell
measured the boundary shear force during the preshearing and the re-shearing stages. It should be noted
that the spatiotemporal variation of the normal stress
was measured only for the part of the specimen that is
adjacent to the bottom section of the cell (a circular
domain). The discrete element method, which will be
presented in the next section, can provide the spatiotemporal variation of the stress field not only at the
bottom section, but also within the shear zone (practically anywhere in the specimen).
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homogeneity assumption experimentally, at least, for the
bottom section of the specimen. The boundary shear
force increases with the shearing time and attains a
constant value (steady-state) at about 60 s (Figure 4(b)),
whereas the normal stress still exhibits some time-wise
variations.
Initially (t 0 s), the normal stress appears to be somewhat symmetric about the centerline of the test cell. The
normal stress generally decreases non-monotonically
from the central region toward the edges (walls) of the
cell, where the wall friction has a dominant effect. During
pre-shear, a skewed stress profile developed with the
highest stress towards the leading edge of the cell. The
shearing renders the normal load to be redistributed;
consequently, a concentration of the normal stress
toward the leading edge occurs.
The vertical normal stress Tzz shown in Figure 4(a) was
averaged to simplify the presentation of the data and to
compare the experimental findings with the slice model
in the DEM simulations. For this purpose, a rectangular
domain shown in the inset of Figure 5 was considered,
and Tzz was averaged transverse to the direction of
shearing. The width of the domain was chosen to be one
quarter of the test cell diameter (23.8 mm) and a length
equal to the tester diameter (95.3 mm). The long axis of
this averaging domain was aligned with the shearing
direction and was assumed equivalent to the x-axis in the
slice model (see Figure 3). By computing the average
value of the nine Tzz measurements along the short axis
of the domain, the transverse averaging was carried out.
This procedure produced 37 averaged Tzz values across
the tester centerline in the direction of shear (x-axis).
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Similar to Figure 4(a), Figure 5 illustrates the inhomogeneous nature of the vertical normal stress Tzz that was
transversely averaged in the rectangular domain, as
mentioned above. Upon shearing, the normal load is
transferred from the shearing edge toward the leading
edge, which is clearly marked in the averaging domain.
The normal stress decreases from the mid-section of the
cell toward the cell walls; however, the decrease is not
monotonic. Figure 5 clearly reveals the presence of
strong spatial fluctuations although the averaging domain was chosen to be relatively large (95.3 mm
23.8 mm). Therefore, the normal stress redistribution
upon shearing and the presence of stress fluctuations are
some qualitative features that should be predicted by the
DEM. The stress inhomogeneity depicted in Figures 4(a)
and 5 could originate from the wall friction and roughness, initial asymmetry of the ring with respect to the
base, asymmetric normal loading on the top lid, and the
discrete or discontinuous nature of the powder specimen.
The mean value of the normal stress Tzz, i.e., the
x-averaged normal stress was determined from the
profiles in Figure 5. The mean values are 1.93, 1.55, and
1.92 kPa for shearing times of 0, 25, and 50 s, respectively,
which are smaller than the boundary traction applied to
the lid (2.50 kPa). This can be partly explained by the
walls taking part of the normal load through friction but
mainly attributed to the transverse averaging in the
rectangular domain as well as the measurement errors
(see Section 2). Repeat measurements were made for the
steady state and failure at the given consolidation stress
and failure stress. All of the repeats showed similar
skewed Tzz patterns in which the loads concentrate
toward the leading edge of the cell. The maximum
difference between identical steady states was about
15% and occurred with steady states that were obtained
from the normally consolidated specimen and the overconsolidated specimen.
The TekScan pad also measured the vertical normal
stress Tzz at the failure of the specimen after the
reduction of the normal load from 2.5 kPa (at the
steady-state) to 1.3 kPa. The whole stress profile at the
bottom of the cell (a circular domain) is illustrated in
Figure 6(a), while Figure 6(b) shows the x-variation of
the transversely averaged normal stress. The normal
stress decreased across the cell when the normal load was
decreased from 2.5 kPa to 1.3 kPa at the failure. It is clear
that the stress inhomogeneity persists during the failure
stage of the Jenike test.
The measurements in the tester are confined to only the
normal stress at the bottom of the cell. Without measuring additional shear and normal stresses, there is no way
of experimentally confirming the stress state acting in the
material. There are three possible reasons for variations
in the measured normal stress. One possibility is that the
sin d;
s 1 1 sin d
s1 s3
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300
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5 Conclusions
The Jenike shear cell is an established powder tester,
which is widely and successfully used in process design,
particularly in the design of storage bins. As new
techniques are developed, it is possible to understand
and resolve some of the problems that have arisen in the
past. In particular, it is still necessary to use a standardized procedure with this tester [3], and the clear
identification of a unique steady state shear has always
been elusive. The measurements and simulations of the
complex stress patterns, which may arise, imply that the
achievement of steady state is dependent not only upon
the dilation of the powder but also upon the development
of the stress profile in the direction of the shear.
The measurements and simulations presented here can
be used to explain why different pre-shear preparation
techniques lead to varying results even though the same
apparent steady state is achieved during shear. The
results of this study also emphasize the need for
development of shear cells in which the strain of the
powder is more closely controlled. When used for
process design, the average values of stress that are
recorded by the Jenike cell, as well as other direct shear
testers, reflect the average value for a sample of the size
of the cell. If this size is small compared to the equipment
to be designed, then those average values represent a
conservative value that can be used in the design.
A more detailed measurement of the stress-strain
behavior of the powder is necessary when the objective
is product design. In this case, it is the size of the particles
relative to the cell, which is critical, and wide variations
of stress within the cell make the average values
insensitive to variations in the powders tested. We
postulate with fine cohesive powders that the large
variation in stress leads to a similar variation in strain.
Macroscopically, this may exhibit itself as stick-slip
behavior.
6 Acknowledgements
The authors would like to acknowledge the financial
support of the Particle Engineering Research Center
(PERC) at the University of Florida, the National
Science Foundation (NSF) grant #EEC-94-0289, and
the Industrial Partners of the PERC. The thanks are
extended to the referees whose comments and suggestions helped us to enhance the quality of the paper. The
first author (E. B.) is especially grateful to the referee,
who pointed out the paper by F. J. C. Rademacher and G.
Haaker.
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