Documentos de Académico
Documentos de Profesional
Documentos de Cultura
doi: 10.1111/ffe.12365
A B S T R A C T The recently increased interest in very high cycle fatigue properties of materials has led to
extended use and further development of the ultrasonic fatigue testing technique. Specimens
are stimulated to resonance vibrations at ultrasonic frequency, where the high frequency allows collecting lifetime data of up to 1010 cycles and measuring crack propagation rates down
to 1012 m per cycle within reasonable testing times. New capabilities and methods of ultrasonic testing and outstanding results obtained since the year 1999 are reviewed. Ultrasonic
tests at load ratios other than R = 1, variable amplitude tests, cyclic torsion tests and
methods for in situ observation of fatigue damage are described. Advances in testing at very
high temperatures or in corrosive environments and experiments with other than bulk metallic materials are summarized. Fundamental studies with copper and duplex steel became
possible and allowed new insights into the process of very high cycle fatigue damage. Higher
cyclic strength of mild steels measured at ultrasonic frequency because of plastic strain rate
effects are described. High-strength steels and high-alloy steels are less prone to frequency
inuences. Environmental effects that can lead to prolonged lifetimes in some aluminium
alloys and possible frequency effects in titanium and nickel and their alloys are reviewed.
Keywords
NOMENCLATURE
A1
A2
c
pl
N
R
=
=
=
=
=
=
=
=
=
=
ABBREVIATION
VA = variable amplitude
CA = constant amplitude
INTRODUCTION
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Fig. 2 Load train used to perform ultrasonic fatigue tests with preloads (load ratio R 1): Mechanical components, strain and displacement
amplitudes along the load train are shown; for testing at load ratio R = 1, both Mounting 1 and Mounting 2 are omitted.
description of the electrical components and of the computer system may be found in Ref. [26].
Fatigue data measured at different load ratios
Ultrasonic fatigue tests with superimposed mean load
are used to study the inuences of load ratio on fatigue
lifetimes, fatigue crack initiation and crack propagation.
Karsch et al.27 investigated fatigue lifetimes of highcarbon chromium bearing steel 100Cr6 (52100) in
bainitic condition (tensile strength 2480 MPa) and in
tempered martensitic condition (tensile strength
2150 MPa). Experiments were performed at load ratio
R = 1 and R = 0.1 in the HCF and VHCF regimes.
The VHCF strength in martensitic condition was about
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2015 Wiley Publishing Ltd. Fatigue Fract Engng Mater Struct, 2016, 39, 329
(a)
(c)
(b)
(d)
Fig. 6 Fatigue crack growth at load ratios R = 1, R = 0.05 and R = 0.5 in 2024-T3 in vacuum (a), in 7075-OA in vacuum (b), in 2024-T3 in
ambient air (c) and in 7075-OA in ambient air (d). Solid symbols refer to servo-hydraulic experiments at 20 Hz, and open symbols refer to ultrasonic experiments at 20 kHz cycling frequency.45
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Testing principle
The concept of ultrasonic CA and VA tests is illustrated
in Fig. 7.
In CA tests, the vibration amplitude of successive
pulses is kept constant. If experiments are performed
with mean loads (load ratios other than R = 1), the
superimposed force is adjusted at the servo-hydraulic or
electromechanical load frame prior to the test and stays
constant throughout the experiment (Fig. 7a).
In VA tests without mean loads (at load ratio R = 1)
or with a constant mean load, the vibration amplitude
of successive pulses is adjusted according to a predetermined repeat sequence (Fig. 7b). Computer control
is needed to determine the load sequence and to measure,
classify and store all load amplitudes during the test.
In VA tests at constant load ratio, the vibration amplitude of successive pulses as well as the preload is adjusted
according to a pre-determined repeat sequence (Fig. 7c).
During a pulse, both the nominal vibration amplitude
and the preload are kept constant, whereas both change
in successive pulses. For this purpose, computer control
is needed, which performs the following procedure illustrated in Fig. 7c.
1 The load frame is set to the corresponding preload calculated from the ultrasonic amplitude of the upcoming
pulse, the load ratio and the specimens cross-sectional
area, in a ramped movement within a pre-congured
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(a)
(b)
(c)
Fig. 7 Principle of pulsepause loading in an ultrasonic constant amplitude test (a), in a variable amplitude test with constant mean stress (b)
and in a variable amplitude test at constant load ratio (c).
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Fig. 8 Fatigue lifetimes of DISPAL S232-T6x measured in constant amplitude (CA, squares) and variable amplitude (VA, circles)
tests, respectively. The solid lines approximate measured data; the
dashed line shows the predicted lifetimes with Miner calculation assuming fracture at damage sum S = 1.61
Fig. 9 Fatigue lifetimes of DISPAL S232-T6x under variable amplitude loading conditions: The solid line approximates all measured
data; the dashed line shows the predicted mean lifetimes for all specimens using a fracture mechanics model assuming a defect with
1/2
areaCI = 45 m; the dash-dotted line shows the predicted lifetime
1/2
for a specimen with a large interior defect with areaCI = 91 m.61
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Test method
Fig. 10 Variable amplitude fatigue data of Al 2024-T351 for load ratio R = 1 (squares), R = 0.1 (circles) and R = 0.5 (triangles), respectively: The dashed lines show the predicted lifetimes with Miner
calculation assuming fracture at damage sum S = 1.56
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The ultrasonic torsion fatigue testing method has been developed at the authors institute.24,64 First experiments
were performed with 2024-T3 aluminium alloy.64 In a second work, the cyclic properties of zirkonia were tested.24
The ceramic tubes were fatigued under cyclic torsion loading in one series and with static compression stress
superimposed to cyclic torsion in another test series.
The working principle of the ultrasonic torsion fatigue testing equipment employed is as follows: An ultrasonic torsion converter generates twist oscillations and
couples torsion waves into one end of the load train. All
components of the load train must be designed appropriately to allow the formation of a standing wave at 20 kHz,
which is the resonance frequency of the ultrasonic torsion converter. Besides the ultrasonic converter, the load
train consists of a mounting part, an ultrasonic horn and
the specimen. The mounting part is an approximately
cylindrical component, where the vibration node in its
centre serves to mount the whole load train. The ultrasonic torsion horn serves to magnify the rotational oscillation. The specimen is hourglass shaped to increase the
cyclic shear strain amplitude to a magnitude high enough
to initiate cracks and to propagate them to fracture.
Design principles for the components of the load train
are based on the propagation of shear waves along the bars
of different polar momentum. The lengths of all components of an ultrasonic torsion load train are signicantly
smaller than in a cyclic tensioncompression or cyclic tension load train, because shear waves are shorter and more
sensitive to changes of cross section than longitudinal waves.
The design method and a layout capable of performing ultrasonic torsion fatigue tests are described in Refs. [64,65].
Control of vibration amplitude and resonance frequency and the way to perform tests in pulsepause mode
are similar in ultrasonic torsion and ultrasonic axial loading fatigue tests. The same test generator and ultrasonic
ampliers are used. However, different vibration gauges
are necessary for measuring rotational and axial
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Experimental results
Akiniwa et al.66 performed ultrasonic torsion fatigue tests
with an oil-tempered SiCr spring steel (JIS G3561,
SWOSC-V). Fatigue data were measured in the regime
between 105 and 109 load cycles and were compared to
cyclic tensioncompression data. The ratio of fatigue
strength under torsional and axial loading at the same
number of cycles was about 0.68 and was similar in the
HCF and VHCF regimes. Cracks were initiated
solely at the surface and were initially growing in mode II
(i.e. in maximum shear direction, either parallel or perpendicular to the specimens length axis). At greater lengths,
cracks propagated in mode I (i.e. 45 to the specimens
length axis, perpendicular to the maximum tensile stress).
No internal inclusion-induced failure was observed. This
was attributed to the very small maximum inclusion size
in the investigated steel. Additionally, the specimens had
been electropolished to remove surface residual stresses,
which facilitated surface crack initiation.
Cyclic torsion and cyclic tensioncompression fatigue
properties of mild steel (0.15%C, C15E, 1.1141) were investigated in the authors laboratory.60,67 SN curves under both loading conditions showed a pronounced
change of slope at about 107 cycles. Above 108 cycles,
failures are very rare, indicating the existence of a fatigue
limit. With 50% fracture probability at 109 cycles, the ratio of cyclic torsion and cyclic tensioncompression fatigue strength was 0.60. Surfaces of specimens that did
not fail in the fatigue tests were studied in a scanning
electron microscope. Figure 11 shows a fatigue crack
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Fig. 12 Mechanical setup and load train for ultrasonic cyclic torsion tests with superimposed static torsion load: (1) ultrasonic
converter, (2) upper mounting part, (3) and (6) ultrasonic horns,
(4) vibration gauge, (5) specimen and (7) rotating disc and lower
mounting part.75
Test method
A method to perform ultrasonic torsion fatigue tests at
different load ratios was developed in the authors
laboratory.75 Static torsion loads are superimposed to
the ultrasonic torsion vibration, which allows testing
up to high load ratios. The mechanical setup and the ultrasonic load train are shown in Fig. 12. An ultrasonic
converter (1) generates circumferential vibrations. All
components of the load train are designed to have resonance length for circumferential vibrations at the testing
frequency of about 20 kHz.64,65 Both ends of each component twist in opposite directions, and a vibration node
is formed in the centre. The node in the centre of the
upper mounting part (2) serves for rigid mounting of
the load train without damping the vibration. Ultrasonic
horns (3) with decreasing cross sections along their
lengths serve to increase the vibration amplitude. The
vibration amplitude at the coupling of ultrasonic horn
and specimen is measured with a vibration gauge (4),
which is an adapted induction coil. The specimen (5)
has two threads for attaching it on both sides to the
ultrasonic horns (3 and 6). The rotating disc, which is
guided by a ball bearing, and the lower mounting part
(7) serve to introduce a static torque into the load train
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Experimental results
VDSiCr spring steel in patented and oil-quenched condition (tensile strength 1980 MPa) was investigated under
ultrasonic torsion fatigue loading at load ratios R = 0.1,
R = 0.35 and R = 0.5.75 The material is, for example, used
in the form of wires for coil valve springs in engines. Very
high numbers of torsional load cycles are superimposed
to a static torsional load because of the preloading of
the spring. Specimens were tested with shot-peened
surfaces to reproduce the surface conditions of actual
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load ratio R = 0.5. Measurements of surface residual compression stresses in runout specimens showed that they
are reduced to about 60% of their initial value after
loading with R = 0.1 and R = 0.35 and to about 30% after
loading with R = 0.5. The considerably reduced compression residual stresses at R = 0.5 facilitate surface crack initiation, and specimens either fail from the surface in the
HCF regime or do not fail at all.
DAMAGE MONITORING
Fig. 13 SN data of shot-peened VDSiCr spring steel for cyclic torsion loading at load ratios R = 0.1 (black symbols), R = 0.35 (red symbols) and R = 0.5 (blue symbols), respectively. Triangles indicate
surface crack initiation, circles refer to interior crack initiation in
the matrix and open circles with arrows show runout specimens.
9
Dashed lines indicate 50% fracture probability at 5 10 cycles at
the respective load ratios.75
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Fig. 14 Interior matrix crack initiation after cyclic torsion loading at a = 572 MPa and load ratio R = 0.1, 3.6 10 cycles to failure.75
cT
;
N
(1)
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amplitude cycling at stress amplitudes close to the endurance limit of 340 MPa. Cyclic softening is observed at low
numbers of cycles, which starts the earlier the higher the
stress amplitude. After the cyclic plastic strain has reached
a maximum, cyclic hardening is observed. Cyclic hardening
may continue to up to 109 cycles at stress amplitudes below
the endurance limit. At a cyclic stress slightly above the endurance limit, the specimen failed during cyclic hardening.
Fig. 16 Fast Fourier transform-based monitoring of fatigue damage and resonance frequency.26
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(2)
19
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Fatigue testing at ultrasonic frequency allows investigating materials at numbers of cycles that are hardly accessible with conventional testing techniques because of
excessive testing times. This gave recently new insights
into the fatigue process of materials when materials are
stressed with very high numbers of low load amplitudes.
Stanzl-Tschegg et al.84,85 performed fundamental
investigations on the progress of fatigue damage in polycrystalline copper in the VHCF regime. Using cylindrical samples, the sinusoidal stress distribution along the
specimens length allowed studying the generation of
slip lines and persistent slip bands (PSBs) at different
cyclic strain amplitudes in one specimen. A minimum
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stress amplitude of about 63 MPa is necessary to generate PSBs in polycrystalline copper within 2 106 cycles
(in the conventional sense of PSB threshold). Continuing cyclic loading beyond 1010 cycles, it was found that
PSBs are formed already at about 50% of the conventional PSB threshold.84,85 Weidner et al.86 investigated
the fatigue damage produced by more than 1010 load cycles below the conventional PSB threshold in more detail.
They characterize the damage by lamella of localized shear
containing elongated dislocation cells, a pronounced surface roughening, the initiation of stage I cracks not only
at the surface but also in interior grains and substantial
grain boundary displacements.
Stanzl-Tschegg et al.85 also showed that the stress amplitudes necessary to rupture a specimen are much higher
than those necessary to form PSBs or to initiate cracks.
Stress amplitudes higher than 93 MPa (about 50% above
the conventional PSB threshold) are necessary for failure
of polycrystalline copper within 1010 cycles. Otherwise,
possibly initiated short cracks stop propagating, which
can be well interpreted using a Kitagawa diagram.
Zimmermann and Jones87 observed surface roughening and the evolution of intergranular as well as
transgranular microcracks in runout specimens of pure
nickel. The cracks reached a length of approximately
30 m but did not propagate to fracture within more than
109 cycles. Higher stresses are necessary to propagate a
crack to fracture than to initiate cracks in pure Ni.
Moderate weight, limited space requirements and the
capability to work without cooling circuits make it possible to set up an ultrasonic system quickly. Liu et al.32 designed a portable ultrasonic fatigue instrument, which
was installed at a high-brilliance X-ray beamline. Thin
sheets of a single crystal Ni-based superalloy were
mounted on a carrier specimen where a hole served to allow the X-radiation to pass through. A small load frame
was designed that served to introduce a static preload.
With this method, crack initiation and propagation could
be studied in situ at load ratio R = 0.1. Information regarding the inuences of microstructure, compositional segregation and strain on initiation and successive crack growth
could be acquired by in situ X-ray imaging.
Dnges et al.88 investigated crack initiation and early
crack growth in the HCF and VHCF regime in stainless
steel X2CrNiMoN22-5-3 (equal volume fraction of
50% of austenitic and ferritic phase). Plastic deformation was found to start in the austenitic phase by activating discrete slip bands. Slip can be transferred to the
harder ferrite phase if well-oriented slip planes are present, and this transition often led to microcrack initiation
in the ferrite phase. Initiation of a microcrack in the rst
grain and overcoming the rst structural barrier (grain
or phase boundary) essentially determines HCF and
VHCF lifetime.
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Mild steel
Tsutsumi et al.96 performed fatigue tests at 10 and 20 kHz
with annealed and cold worked 0.13%C steel (tensile
strength 370 MPa) containing small holes. The fatigue
limit under fully reversed loading conditions is 23 to
26% higher if measured at ultrasonic frequency rather
than at 10 Hz. Near threshold fatigue crack propagation
rates are lower, and plastic zone sizes are smaller in ultrasonic frequency tests. Crack paths show many slip bands
after cycling in the conventional test and only very
few bands after ultrasonic loading. An increase of yield
stress with increasing strain rate and reduced crack propagation rates serves to explain the higher cyclic strength
measured in the ultrasonic fatigue tests.
A comprehensive study of frequency inuences in
0.15%C steel (JIS S15C, tensile strength 441 MPa) was
performed by Guennec et al.97,98 Figure 18 shows SN
curves that were measured at four different frequencies
in the range between 0.2 and 140 Hz and at ultrasonic
frequency.97 The number of cycles to failure and the fatigue limit stress were found to increase with increasing
frequency. In the regime from 0.2 and 140 Hz, the increase of cyclic strength can be explained with an increase
of yield stress with increasing strain rate, whereas the frequency inuence on ultrasonic tests is stronger. Studies
21
Austenitic steel
Austenitic stainless steel tubes (AISI 904L, tensile
strength 657 MPa) have been studied in rotating bending
tests at 160200 Hz and in ultrasonic tests at 20 kHz by
Carstensen et al.101 In the range from 3 106 to 108 cycles, rotating bending and ultrasonic fatigue data are
available, which show no inuence of cycling frequency
on measured lifetimes. Ultrasonic data had been measured up to 1010 cycles. The slope of the SN curve
strongly changes at approximately 108 cycles, and failures
at greater numbers of cycles are very rare. This indicates
the presence of an endurance limit, which is remarkable
considering the face-centred cubic (fcc) lattice structure
of the investigated metal.
High-strength steel
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Furuya et al.102 investigated fatigue lifetimes of a lowalloy high-strength steel (JIS SNCM439, tensile strength
1960 MPa) at 100 Hz, 600 Hz and 20 kHz at load ratio
R = 1. Fatigue properties were found to be independent
of cycling frequency. Fatigue crack initiation was mainly
found at interior inclusions. Fine granular areas were
found at the crack initiation locations, and their sizes
were independent of cycling frequency. A spring steel
(JIS-SUP7, tensile strength 1730 MPa) was tested by
Furuya et al.103 at 30 and 100 Hz under rotating bending,
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solely showed surface failures. An explanation for the frequency inuence is proposed in terms of dislocation
movement, with shorter travelling distances and smaller
accumulated damage at higher loading frequencies.
Cast iron
Wang and Bathias109 investigated fatigue lifetimes of
spheroidal graphite cast iron (tensile strength 510 MPa)
at load ratios R = 1 and R = 0 at cycling frequencies of
25 Hz and 20 kHz. No fatigue limit was observed, but
specimens continued to fail above 107 cycles. Crack initiation in the VHCF regime was preferentially at interior
microshrinkage cavities. They concluded that a very
good agreement was found between ultrasonic and conventional fatigue test data.
The inuence of cycling frequency on fatigue lifetimes of high-strength austempered ductile iron (tensile
strength 1140 MPa) was investigated by Zhang et al.110
Fatigue tests were performed at load ratio R = 1 with a
resonance testing equipment working at 90 Hz and with
ultrasonic equipment at 20 kHz. In the HCF regime,
similar SN curves were measured at low and ultrasonic
frequency. Similar crack initiation locations at graphite
nodules or at shrinkage cavities were found for both
frequencies, indicating no inuence of cycling frequency
on fatigue damage in this material.
Summary on steels
Based on the investigations described earlier, it can be
concluded that fatigue properties of low-carbon and
medium-carbon steels are sensitive to cycling frequency.
Higher cyclic strengths are measured at ultrasonic rather
than conventional frequency. Mild steel contains ferrite
and pearlite, and cyclic plastic deformation in the HCF
regime takes place in the softer ferrite. Cyclic plastic deformation is smaller because of the increase of yield
strength at high strain rates in ultrasonic tests. The dislocation structure in the ferrite grains as well as the crack
initiation is affected by frequency. Surface crack initiation
occurs in the ferrite grains at low frequency and preferentially at grain boundaries at ultrasonic frequency.
Laird and Charsley111 have very well predicted these
strong inuences of cycling frequency on fatigue damage
in body-centred cubic metals. Shape changes of grains
due to asymmetric gliding of screw dislocations in tension and compression, which promotes intergranular
crack initiation and cleavage crack planes on fracture
surfaces, are the consequences of the high strain rates in
ultrasonic testing. In contrast, cyclic deformation of fcc
metals, crack initiation and propagation and the associated fatigue lifetime is assumed to be only weakly dependent on the strain rate.111 Consequently, measured
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growth measurements performed at 50 Hz and load ratios R = 0.1, R = 0.5 and R = 0.8 are available. Threshold
stress intensities at a limiting crack propagation rate of
10-10 m per cycle were comparable at low and ultrasonic
frequency for the three load ratios. At growth rates in
the range of 10-9 to 10-8 m per cycle; however, fatigue
cracks grow by mean by a factor 3 faster in ultrasonic experiments than in tests at 50 Hz. The smaller crack
length evaluated in ultrasonic experiments as well as differences in the experimental procedure leading to load
history effects is possible explanations for the differences.
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temperature. Further increase to 800 C had a strong inuence and a pronounced decrease of cyclic strength resulted,
more pronounced for the overaged condition. This was
attributed to the formation of brittle oxide layers and
microcracks at the grain boundaries.
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