Documentos de Académico
Documentos de Profesional
Documentos de Cultura
56
~i Standard Method of
5 3 The maxlmurn load m pounds force (W) shall bc reported as the breaklng strength
mandrel
61
SCOPE
or sol~db~rumrnousmatmals at
1.1 Thrs method appl~esro the samplrng of lrqurd. sern~.sol~d,
the pornt of manufacture. supply terrnrnal. or at the pomt of sh~pmentdellvery
12 Samples may be taken from tanks. stockpila. vehtclcs. or contamen u d for the storage or
shlpprng of brtum~nousmatenals
2.
PURPOSE
23.1
2.2.2
3. S U E OF SAMPLES
Tlre sample srze of I~quidmaterials shall be as follows
3.1
3.1.l For rounne l a b t o r y exammanon not less than 1 qt (1 Itter) (ernuls~ons.1 gal or 4
fmrs)
3.1.2 From bulk storage, 1 q t (1 h e r ) for each samphng valve.
3.13 From barrek or drums. 1 qt ( I I~ter)
33 Tbe sample sue of sern~sohdor mhd matenals shall be as foIIows
33.1 From barrels. drums. or cakes. 2 to 3 Ib ( l kg).
333
Types o f C o n t r ~ n c n
Contatncrs for lrquld brtumtnous matenal s m p h . except emulsrons. shall be double
4.1.1
fnct~on-topcans,square cans wtth screw tops, orsmall mouth cans w ~ t hscrew caps.
4.13 Contatncn for anlontc emulsrficd asphalt s m p i a shall be wtdcmouth jars or bottles
made of glass or plrstv.
4.1 3 Contarnen lor cat~ontcemuis~fikdasphalt sarnplm shall be w~demouthIan or bottles made
dplasttc or a~dcmouthcans wrth sncr* caps.
4.1
NCm I
46
43.1
SIXC of Contamers
The sltc of the contmncr shall correspond to the rcqu~redamount of sample
5.l Sample contamen s h d l be new They shall not be washed or mrrd, or mptd wath o ~ l pcloth
If they contatn ev~dtnceofsolder flux. or rf they arc not clean and dry, they shdl not be used. Top and
rontatner shall fit togaher tightly.
6.1.1
NOTS2 -During samplm~by any of the rnethodr descnbcd 111 fill~ngrnleu and dwharge outlets of the a n k shakt bc dacd
Samples shall beobtatned by one of the thmfollowmg methods
6.1.1.l
Tank Top Method-Usmg valves or taps at top, middle, and lower lacatrons of the tank
draw a I qt to I gal (I lo 4 I~terslsample from each after cleanng by drawtng and dtscatdtng a
minimum of 1 gal (4 Itten) of thcmaterral
6.1.1.2 Thtef Sampler Method (nor surrnbh for asphalt cemrnrs) - Samples shall be taken at
top. middle. and lower levels of the tank by lowenng a T h ~ e bampler
t
Into the matenal. A satrsfactory
type wlth Instructtons for use a shown tn Ftg. 1
F w I-Thd
Norr-Thn
t m ramder
Sampler
Ir l e w d lnro the rank w t h #he b l r o m valve oven l t h m s no loo clmuret Whtn ihc dalrcd drprh rr
6.1.1 3 Throw-away Concaner Method -Samples shall be taken at top, rnrddle. and lower
levels of the tank by lowenng a surtable we~ghtcdholding device Into the material. A sat~sfactorytype
with ~nstructtonsfor use IS shown In f i g 2 The essenbal feature of the method IS to use a clean
contalner each tlme a sample IS taken from the tank, pourmg the sample tnto another clean contamer
and ihrowrng away the contarner used in samplsng
6.1.1.4 The three samples from bulk storage tanks may be tested separately for consrstency to
detect strattficatton. or they may be combtncd. thoroughly mtxed and a I qt to I gal (1 to 4 Irtersl
sample taken for other tests as may be requrrd for determmng average charactertstrcs of the matenal
6.1.2 From Bulk Storage Tanks Equrppcd wath Mechantmi Agrrntom -When the tank ts
equ~ppcdwrth operatmg mechantcal agrtators w h ~ h . by observation through the sampltng or
observat~onhatch, are performtng adequate mrxrng of the tank contents, a single sample taken by
methdsdcscrrbed !n 6 1 1 1.6 1 1 2. or 4 1 1 3 wrll be sattstactory to use tor test purposa
7.1 Each delwery vehrcle or dtstrtbutor shall be q u ~ p p e dwrth a samplrng valve srrn~lorIn destgn to thoseshown tn fig 3 It shall be tnstalled at least one h o t (0 3 m) from the shell and shall be
clearly labeled as a "Sampltng Valve" Before the sample is taken from the sample valve a mjntmum
of I gal (4 Ilters) shall be drawn from the sample valve and dtscarded.
73 When pcrm~tted by the purchaser. the followrng methods may be used to obtatn
npmmtattve samples
73.1 Samples of Ilqutd rnsterrals and matenals made ltqurd by heattng may be taken by the dtp
method usrng a clean small-mouth or ffrtctton-ton can rn a sultable hotder as shown m Frg 4 A clean
contamer must be used to take each sumpie. and the mntenal sampled shall then be transferred to
another new and ckan container for rctentlon or sample testrng
713 A detachable fittrng, s r m h r tn d c s ~ g nto the oneshown In Fig 5 shall b e tnscrterl tn the
drscharge hne Before the sample IS taken 1 gal (4 Irterd shall be drawn from thrs samplrng valve and
d~scardcd
9.1 When tankers and barges are bang toaded or unloaded samples may conveniently be taken
from the ptpe Itne through whtch the materral 1s flowrng by msertron of a sampltng devrce (Fig 5)Into a
rrstng section of the ptpe lrne on the discharge srde of the pump o r In a completely filled Irne m whlch
gravlty creates the matenals flow The samplrng devrce should be turned to face the flow of the Itquid
This devtce shall be provtdKi wtth a vaive or plug cock and shall dmcharge tnto a sample rccerver At
least three 1 gal (4 Irter) samples shall be taken at untform rntervals throughout the enttrc IoPdtng ar
unloadtng At the completion of the loadtng or unloading, the rndrvrdual1 gal (4 lrted sampln shall be
mmbrned. thoroughly mtxed wtthout altenng rts charactenstrcs. and a 1 gal (4 Irter) sample taken
therefrom
9 1 When sampl~ngtankers and barges 25,000 bbi ,or less, capoetty, at least five 1 gal (4 ltterl
samples shall be taken at untform intervals throughout the enrrre loading or unloading (25.000 bbl or
larger. capacity q u l m at least ten 1 gai (4 ltterl samples) At completton of the loadrng or untoadrng
the ~ndtvtdual1 gal (4 Itter) samples shall be combtned, thoroughty m~xcdIn a manner dcsrgmd to not
alter tts characterrst~cs,and a 1 gal (4 Ilter) sample taken therefrom
Pulled hole to
-
Valve Inlet P i p e to
be not less than l2Ii-/,
from any tankstifface./
FIG. 4.-Dip
10.
T40
Sampler.
10.l After thorough mlxlng, samples of Ilquld blturnlnous materral from barrels or drums shall
bc secured by Tube or Thref Samplmg by taking 1 qt (1 hter) of matenaI from packages selcctcd at
random accord~ngto Sampllng Sem~soltdor Uncrushcd Solrd Materrais
1 1.
11.1 Drums. Barn&, Cartom. and Bags-Where the lot of matmal to be sampled IS obv~ously
horn a single run or batch of the producer, oncpackagc shall be selected at random and sampled as
described below Where the lot of matenal to be sampled a not obvrouzly from a srngle run or batch of
the praducer, or where the s~nglesample selected as described above fads on test to conform to the
rcqulrements of the spec~flcat~ons,
a number of packages shall be selected at random q u ~ v a l e nto
t the
cube root of the total number of packaga m the lot The followmg table a gtven showmg the number
of samples to be selected for sh~pmentsof vanous srzes
Samples shall be taken from at least 3 In (76 mm) below the surface and at feast 3 In (76 mm) from the
s ~ d cof the contamer A clean hatchet may be used d the mater~als hard enough to shatter and a
broad. s t ~ f putty
f
kn~fed the matenal IS soft When more than one package tn a tot IS sampled each
----
r40
rndivtdual sample shall be not less than 1/4 Ib (1 15 gl In we~ght.When the lot of mater~alrs obviously
from a s~nglerun or batch of the ptoducer, d samples from the lot shall be melted and thoroughly
rn~xed,and an avmgc I gal (4 ltter)sampte taken from the combined matenal tor examma@;onIn case
more than a s~nglerun or batch of the pmdum IS present and the batches can be clearly differentiated.
a composite 1 gal (4 liter) sample shdl be prop& for examination from each batch. Where it IS not
porstble to d~ffcmnt~ate
between the various batches. each sampk shall be examined separately
12.
...-
4
Preformed Exp.nsion Jaht PWer for Concrete
346
abswptron computed
3.
Bxmnmws
a,
5.1 In the case of cork, sponge rubber and cork rubber. explmKn jomt flll only fbw
m e n for a shall be cut fro. each -do. Each test spsccmen h.U be Imhly
cut
u d L i v
<,
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