ANSI/AWS Standard Procedures for Calibrating Magnetic Instruments to Measure the delta ferrite content of austenitic and duplex ferritic-austenitic stainless steel weld metal.
ANSI/AWS Standard Procedures for Calibrating Magnetic Instruments to Measure the delta ferrite content of austenitic and duplex ferritic-austenitic stainless steel weld metal.
ANSI/AWS Standard Procedures for Calibrating Magnetic Instruments to Measure the delta ferrite content of austenitic and duplex ferritic-austenitic stainless steel weld metal.
ANSVAWS A4.2WA4.2: 1 997 An American National Standard Standard Procedures for Calibrating Magnetic Instruments to Measure the Delta Ferrite Content of Austenitic and Duplex Ferritic-Austenitic Stainless Steel Weld Metal
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - Key Words- Instrument calibration, delta ferrite, ANSIIAWS A4.2M/A4.2:1997 stainless steel weld metal, austenitic An American National Standard stainless weld metal, duplex stainless weld metal Approved by American National Standards Institute November 6,1997 Standard Procedures for Calibrating Magnetic Instruments to Measure the Delta Ferrite Content of Austenitic and Duplex Ferritic-Austenitic Stainless Steel Weld Metal Supersedes ANSI/AWS A4.2-91 Prepared by AWS Committee on Filler Metals and The Welding Research Council Subcommittee on Welding Stainless Steels Under the Direction of AWS Technical Activities Committee Approved by AWS Board of Directors Abstract Calibration procedures are specified for a number of commercial instruments that can then provide reproducible rnea- surements of the ferrite content of austenitic stainless steel weld metals. Certain of these instruments can be further cali- brated for measurements of the ferrite content of duplex ferritic-austenitic stainless steel weld metals. Calibration with primary standards (nonmagnetic coating thickness standards from the U.S. National Institute of Standards and Technol- ogy) is the preferred method for appropriate instruments. Alternatively, these and other instruments can be calibrated with weld-metal-like secondary standards. Reproducibility of measurement after calibration is specified. Problems associated with accurate determination of ferrite content are described. American Welding Society 550 N.W. LeJeune Road, Miami, Florida 33126
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - Statement on Use of AWS Standards All standards (codes, specifications, recommended practices, methods, classifications, and guides) of the American Welding Society are voluntary consensus standards that have been developed in accordance with the r u l e s of the Ameri- can National Standards Institute. When AWS standards are either incorporated in, or made part of, documents that are included in federal or state laws and regulations, or the regulations of other governmental bodies, their provisions carry the full legal authority of the statute. In such cases, any changes in those AWS standards must be approved by the gov- ernmental body having statutory jurisdicti6n before they can become a part of those laws and regulations. In all cases, these standards carry the full legal authority of the contract or other document that invokes the AWS standards. Where this contractual relationship exists, changes in or deviations from requirements of an AWS standard must be by agree- ment between the contracting parties. International Standard Book Number: 0-87171-534-1 American Welding Society, 550 N.W. LeJ eune Road, Miami, FL 33126 O 1998 by American Welding Society. All rights reserved Printed in the United States of America Note: The primary purpose of AWS is to serve and benefit its members. To this end, AWS provides a forum for the ex- change, consideration, and discussion of ideas and proposals that are relevant to the welding industry and the consensus of which forms the basis for these standards. By providing such a forum, AWS does not assume any duties to which a user of these standards may be required to adhere. By publishing this standard, the American Welding Society does not insure anyone using the information it contains against any liability arising from that use. Publication of a standard by the American Welding Society does not carry with it any right to make, use, or sell any patented items. Users of the in- formation i n this standard should make an independent, substantiating investigation of the validity of that information for their particular use and the patent status of any item referred to herein. With regard to technical inquiries made concerning AWS standards, oral opinions on AWS standards may be rendered. However, such opinions represent only the personal opinions of the particular individuals giving them. These individuals do not speak on behalf of AWS, nor do these oral opinions constitute official or unofficial opinions or interpretations of AWS. In addition, oral opinions are informal and should not be used as a substitute for an official interpretation. This standard is subject to revision at any time by the AWS Committee on Filler Metals. It must be reviewed every five years and if not revised, it must be either reapproved or withdrawn. Comments (recommendations, additions, or dele- tions) and any pertinent data that may be of use in improving this standard are requested and should be addressed to AWS Headquarters. Such comments will receive careful consideration by the AWS Committee on Filler Metals and the author of the comments will be informed of the Committees response to the comments. Guests are invited to attend all meetings of the AWS Committee on Filler Metals to express their comments verbally. Procedures for appeal of an ad- verse decision concerning all such comments are provided in the Rules of Operation of the Technical Activities Commit- tee. A copy of these Rules can be obtained from the American Welding Society, 550 N.W. LeJ eune Road, Miami, FL 33 126. Photocopy Rights Authorization to photocopy items for internal, personal, or educational classroom use only, or the internal, personal, or educational classroom use only of specific clients, is granted by the American Welding Society (AWS) provided that the appropriate fee is paid to the Copyright Clearance Center, 222 Rosewood Drive, Danvers, MA 01923; Tel: 508-750- 8400; online: http:\\w.copyright.com
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - Personnel AWS Committee on Filler Metals R. A. LaFave, Chair Elliott Company J. I! Hunr, Ist Vice Chair Consultant D. A. Fink, 2nd Vice Chair The Lincoln Electric Company H. M. Woodward, Secretary American Welding Society B. E. Anderson AlcoTec Wire Company *R. L. Barernun Electromanufacturas S A R. S. Brown Carpenter Technology Corporation R. A. Bushey ESAB Welding and Cutting Products J. Caprurola, Jr. Consultant *L. J. Chrisrensen Consultant R. J. Christoffel Consultant D. J. Crement Precision Components Corporation D. D. Crockerr The Lincoln Electric Company R. A. Daemen Consultant D. A. DelSignore Consultant R. L. Drury III Caterpillar, Incorporated H. M! Ebert Exxon Research and Engineering Company J. G. Feldstein Foster Wheeler Energy International S. E. Ferree ESAB Welding and Cutting Products L. Flasche Haynes International, lncorporated C. E. Fuerstenau Alloy Ring Service G. A. Hallstrom, JI: Hallstrom Consultants R. B. Kadiyala Techalloy Company D. J. Kotecki The Lincoln Electric Company D. Y Ku American Bureau of Shipping N. E. Larson Compressed Gas Industries A. S. Laurenson Consultant G. H. MacShane MAC Associates U! A. Marttila Chrysler Corporation R. Menon Stoody Company J . S. Lee Chicago Bridge and Iron Company, Incorporated M. T Merlo Select Arc, Incorporated A. R. Merres Ampco Metal, Incorporated M. D. Morin ABB Power Generation C. L. Null Naval Sea Systems Command *Y Ogata Kobe Steel Limited - Welding Division J. J. Payne Consultant E. W Pickering, Jr. Consultant *H. E Reid Consultant *S. D. Reynolds, Jr. Consultant R. L. Peaslee Wall Colmonoy Corporation M. A. Quintana The Lincoln Electric Company L. E Roberts Canadian Welding Bureau Z? K. Salvesen Det Norske Veritas (DNV) *Advi sor ... 111
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - AWS Committee on Filler Metals (Continued) J. M. Suwhill, Jr. A. F? Serdler U! S. Severance *W A. Shopp M. S. Sierdzinski *R. G. Sim E. R. Stevens *R. U! Straiton R. A. Sulit R. A. Swain R. D. Thomas, JK K. I? Thornberry *R. limerman *S. Tsutsumi G. J. Qtanovych T. R. Warren H. D. Wehr *E J. Winsor K. G. Wold Newport News Shipbuilding Armco Steel Company ESAB Welding and Cutting Products Editorial Consultant ESAB Welding and Cutting Products The Lincoln Electric Company (Australia) Fisher Controls International, Incorporated Bechtel Corporation Digital Systems Research Euroweld, Limited R. D. Thomas and Company J. W. Harris Company, Incorporated Conarco SA Kobe Steel, Limited-Welding Division Mobil Technology Company lngalls Shipbuilding, Incorporated Arcos Alloys Consultant Siemens Power Corporation . AWS Subcommittee OD Stainless Steel Filler Metals D. A. DelSignore, Chair H. M. Woodward, Secretary E S. Babish R. S. Brown *R. J. Christofle1 J. G. Feldstein L. Flasche R. D. Fuchs J . A. Henning *J. f? Hunt S. Jana R. B. Kadiyala D. J. Kotecki E B. Lake G. H. MacShane M. T. Merlo E. U! Pickering, JI: *H. E Reid **S. I? Sathi R. A. Swain *R. D. Thomas, Jr. *S. Tsursumi H. D. Wehr D. U! Yonker, Jr. 'Advisor **Deceased Consultant American Welding Society Sandvik Steel Company Carpenter Technology Corporation Consultant Foster Wheeler Energy Intemational Haynes International, Incorporated Bhler Thyssen Welding Westinghouse Electric Consultant Hobart Brothers Company Techalloy Company The Lincoln Electric Company ESAB Welding and Cutting Products MAC Associates Select Arc, Incorporated Consultant Consultant Westinghouse Electric Corporation Euroweld, Limited R. D. Thomas and Company Kobe Steel, Limited-Welding Division Arcos Alloys National-Standard Company iv
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS --`,,`,,,`,,,,`,```,``,,,`,`,``-`-`,,`,,`,`,,`--- STD=AWS A' 4. 2M/ A4- 2- ENGL L997 E 07842b5 05137b5 790 111 Foreword (This Foreword is not a part of ANSIIAWS A4.2M/A4.2:1997, Standard Procedures for Calibrating Magnetic Instru- ments to Measure the Delta Ferrite Content of Austenitic and Duplex Ferritic-Austenitic Stainless Steel Weld Metal, but is included for information purposes only.) This document is a revision of the Standard Procedures for Calibrating Magnetic Instruments to Measure the Delta Ferrite Content of Austenitic Stainless Steel Weld Metal, first published in 1974 and revised in 1986 and again in 1991. This revision was by the Subcommittee on Welding Stainless Steel of the Welding Research Council and by the AWS Committee on Filler Metals. The current revision is the fi rst to use the SI system of measurement as the primary system, and updates the standard in the light of new information. A certain minimum ferrite content in most austenitic stainless steel weld metals is useful in assuring freedom from microfissures and hot cracks. Upper limits on ferrite content in austenitic stainless steel weld metals can be imposed to limit corrosion in certain media or to limit embrittlement due to transformation of ferrite to sigma phase during heat treatment or elevated temperature service. Upper limits on ferrite content in duplex ferritic-austenitic stainless steel weld metals can be imposed to help assure ductility, toughness, and corrosion resistance in the as-welded condition. Reproducible quantitative ferrite measurements in stainless steel weld metals are therefore of interest to filler metal producers, fabricators of weldments, weldment end users, regulatory authorities, and insurance companies. Comments and suggestions for the improvement of this standard are welcome. They should be sent to the Secretary, Committee on Filler Metals, American Welding Society, 550 N.W. LeJeune Road, Miami, FL 33126. Official interpretations of any of the technical requirements of this standard may be obtained by sending a request, in writing, to the Managing Director, Technical Services Division, American Welding Society. A formal reply will be issued after i t has been reviewed by the appropriate personnel following established procedures. V
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS --`,,`,,,`,,,,`,```,``,,,`,`,``-`-`,,`,,`,`,,`--- STD-AWS A4*2M/A4*2-ENGL L777 07842b5 05137bb b27 m Table of Contents Page No . ... Personnel .................................................................................................................................................................... 111 Foreword ................................................................................................................................................................... V List of Tables v11 List of Figures ............................................................................................................................................................ vii .. .............................................................................................................................................................. I . 2 . 3 . 4 . 5 . 6 . 7 . 8 . 9 . scope ..................................................................................................................................................................... 1 Definitions ............................................................................................................................................................. 1 2.1 Delta Ferrite .................................................................................................................................................. 1 2.2 Draw Filing ................................................................................................................................................... 1 2.3 Ferrite Number (FN) ..................................................................................................................................... 3 2.4 Primary Standards ......................................................................................................................................... 3 2.5 Weld-Metal-Like Secondary Standards ........................................................................................................ 3 Calibration Methods ............................................................................................................................................. 3 3.1 Primary Standards ......................................................................................................................................... 3 3.2 Secondary Standards ..................................................................................................................................... 4 3.3 Range of Calibration for All Calibration Methods ....................................................................................... 4 Calibration of Magne-Gage-Type Instruments ..................................................................................................... 4 4.1 Calibration by Means of Primary Standards ................................................................................................. 4 4.2 Calibration by Means of Weld-Metal-Like Secondary Standards ................................................................ 8 Calibration of FeritscopeslFerritescopes ............................................................................................................. 8 5.1 Calibration of Ferritescopes Model FE8-KF by Means of Primary Standards ............................................. 8 5.2 Calibration by Means of Weld-Metal-Like Secondary Standards ................................................................ 9 Calibration of Inspector Gages ............................................................................................................................. 9 6.1 Calibration by Means of Primary Standards ................................................................................................. 9 6.2 Calibration by Means of Weld-Metal-Like Secondary Standards ................................................................ 9 Calibration of Other Instruments ........................................................................................................................ 10 7.1 Calibration by Means of Primary Standards ............................................................................................... 10 7.2 Calibration by Means of Weld-Metal-Like Secondary Standards .............................................................. 10 Use of Calibrated Instruments ............................................................................................................................ 11 8.2 Variations in Measurements ........................................................................................................................ 11 Significant Figures i n Reporting Measurement Results ...................................................................................... 12 9.1 Calibration Data ........................................................................................................................................... 12 9.2 Measurement Data ...................................................................................................................................... 12 8.1 Maintaining Calibration ............................................................................................................................... 11 Annex Al . Acknowledgment .............................................................................................................................................. 13 A2 . Ways of Expressing Ferrite Content ................................................................................................................. 13 A3 . Cautions on the Use of Ferrite Number ............................................................................................................ 14 A4 . Standards for Instrument Calibration ................................................................................................................ 15 A5 . Effect of Ferrite Size, Shape and Orientation ................................................................................................... 15 A6 . Instruments ........................................................................................................................................................ 16 A7 . Use of Calibrated Instruments ......................................................................................................................... 20 AWS Filler Metal Specifications by Material and Welding Process .......................................................................... 23 A WS Filler Metal Specifications and Related Documents ......................................................................................... 25 vi
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS --`,,`,,,`,,,,`,```,``,,,`,`,``-`-`,,`,,`,`,,`--- List of Tables Table 1 2 3 4 5 6 7 8 9 10 11 Al Page No . Ferrite Numbers (FN) for Primary Standards Calibration of Instruments Using a Magne-Gage No . 3 Magnet or Equivalent ........................................................................................................................... 2 Ferrite Numbers (FN) for Primary Standards for Inspector Gage Calibration .............................................. 4 Maximum Allowable Deviation, Calibration Point to Calibration Curve, for Instruments being Calibrated with Weld-Metal-Like Secondary Standards ...................................................................... 5 Tolerance' on the Position of Calibration Points Using Primary Standards ................................................... 8 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Feritscoped Ferritescopes .................................................................................................................................................. 9 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Inspector Gages ............ 10 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Magne-Gage-Type Instruments ................................................................................................................................................... 11 Expected Range of Variation in Measurements with Calibrated Magne-Gage-Type Instruments .............. 11 Expected Range of Variation in Measurements with Calibrated FeritscopesFerritesopes ........................ 12 Expected Range of Variation in Measurements with Calibrated Inspector Gages ...................................... 12 Current NIST Coating Thickness Standards (Nominal Thicknesses) with Approximate Corresponding Ferrite Numbers ........................................................................................................................................... 16 Ferrite Numbers (FN) for Primary Standards for Ferritescope Model FE8-KF Calibration ......................... 3 List of Figures Figure Page No . 2 A l A2 A3 A4 A5 Example of Calibration Lines for Two Magne-Gage Instruments. Each with a No . 3 Magnet for Measuring the Delta Ferrite Content of Weld Metals up to 26 FN .......................................................... 6 Example of Calibration Lines for a Magne-Gage Instrument with a No . 3 Magnet for Measuring the Delta Ferrite Content of Weld Metals up to 77 FN .................................................................................. 7 Magne-Gage-Type Instruments .................................................................................................................... 17 Ferritescope Model FES-KF ........................................................................................................................ 19 Inspector Gage ............................................................................................................................................. 19 Ferrite Indicator (Severn Gage) ................................................................................................................... 20 Foerster Ferrite Content Meter ..................................................................................................................... 21
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - Standard Procedures for Calibrating Magnetic Instruments to Measure the Delta Ferrite Content of Austenitic and Duplex Ferritic-Austenitic Stainless Steel Weld Metal 1. Scope 1.1 This standard prescribes procedures for the calibra- tion and maintenance of calibration of instruments for measuring, by magnetic attraction or permeability, the delta ferrite content of an austenitic or duplex ferritic- austenitic stainless steel weld metal in terms of its Ferrite Number (FN). 1.2 A thorough review of the Annex is recommended be- fore any instrument is calibrated or used. The Annex pre- sents background information which is essential to understanding the many problems and pitfalls in deter- mining and specifying the ferrite content of weld metals. 1.3 Calibration can be accomplished with the use of the National Institute of Standards and Technology (NIST, formerly National Bureau of Standards) primary standards or weld-metal-like secondary standards. At the present time, onl y three instruments (Magne-Gage [including a torsion balance using essentially a Magne- Gage No. 3 magnet, hereinafter referred to as a Magne- Gage-type instrument), Ferritescope Model FE8-KF1, and Inspector Gage)2 can be calibrated by the use of 1. This is a pre-1980 instrument. Post-1980 models and the cur- rent models, now identified as Feritscopes, cannot be easily cal- ibrated with the NET primary standards and the tables in this document. See Section 5. 2. These instruments were selected for testing from several similar instruments by the Welding Research Council's Sub- committee on Stainless Steel Welding. Each instrument was extensively tested to develop the data shown i n Tables 1, 2, and 3. This standard contains those data and instructions for their use. For information or requests regarding the ability of other instruments to becalibrated to NIST Primary Standards, contact the Welding Research Council, 345 East 47th Street, New York. NY 10017. NIST primary standards and the values in Tables 1, 2, or 3 in this document. The range of possible calibration de- pends upon the particular instrument. This is not an en- dorsement of any particular instrument (see 3.1). 1.4 Some manufacturers may not calibrate their instru- ments to A4.2. Therefore, if calibration to A4.2 is required, it is the responsibility of the user of the instru- ment that this calibration be performed. 2. Definitions3 2.1 Delta Ferrite. The ferrite which remains at room temperature from that which was formed from the mol- ten state upon freezing. Much of the original ferrite that formed upon freezing transforms to austenite during cooling. 2.2 Draw Filing. This weld pad surface preparation technique is suitable for subsequent ferrite measurements up to about 20 FN (see 8.2). A sharp, clean 350-mm [14-in.] mill bastard file, which has not been contami- nated by ferromagnetic materials, held parallel to the base metal and perpendicular to the long axis of the weld metal sample, is stroked smoothly with a firm, down- ward pressure, in the forward (cutting) direction onl y, along the weld length. No cross-filing is done. The fi n- ished surface is flat with at least a 3-mm [1/8-in.] width where all weld ripples are removed. 3. For AWS terms and definitions, refer to the latest edition of ANSIJAWS A3.0, Standard Welding Terms and Definitions. Please notethat someof the terms and definitions used in this publication are not included in AWS A3.0. They are either new terms defined after the latest revision of A3.0 or they are used specific to this publication.
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD-AWS A q - ZH/ ? A 4=2- ENGL 1997 0784265 05137b9 33b A4.2WA4.2:I 997 E v) 3 E E - E v)
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E E E I _. " 2
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - Table 2 Ferrite Numbers (FN) for Primary Standards for Ferritescope Model FE8-KF Calibration (See 5.1 .i) Coating Thickness Coating Thickness mm mils FN mils 2.00 1.90 1.80 1.70 1.60 1 so 1.45 1.40 1.35 1.30 1.25 1.20 1.15 1.10 1 .os 1 .o0 0.95 0.90 0.85 0.80 0.78 0.76 0.74 78.74 74.80 70.87 66.93 62.99 59.06 57.09 55.12 53.15 51.18 49.21 47.24 45.28 43.31 41.34 39.37 37.40 35.43 33.46 31.50 30.71 29.92 29.13 1.9 2.1 2.3 2.6 2.8 3.1 3.3 3.5 3.7 3.8 4.0 4.3 4.5 4.7 5 .o 5.3 5.6 5.9 6.2 6.6 6.8 7.0 7.1 0.72 0.70 0.68 0.66 0.64 0.62 0.60 0.58 0.56 0.54 0.52 0.50 0.49 0.48 0.47 0.46 0.45 0.44 0.43 0.42 0.41 0.40 0.39 28.35 27.56 26.77 25.98 25.20 24.41 23.62 22.83 22.05 2 1.26 20.47 19.69 19.29 18.90 18.50 18.11 17.72 17.32 16.93 16.54 16.14 15.75 15.35 7.3 7.5 7.7 8.0 8.2 8.4 8.7 9.0 9.3 9.6 9.9 10.3 10.4 10.6 10.8 11.1 11.3 11.5 11.7 12.0 12.3 12.5 12.8 2.3 Ferrite Number (FN). An arbitrary, standardized value designating the ferrite content of austenitic and du- plex ferritic-austenitic stainless steel weld metal (see Annex A2). 2.4 Primary Standards. Specimens with accurate thick- ness of nonmagnetic material on carbon steel base plate containing 0.25 percent carbon maximum. Each primary standard is assigned an FN of an equivalent magnetic weld metal, this assigned value being specific to a partic- ular make (and model, if applicable) of measuring instru- ment (i.e., Magne-Gage, Ferritescope, or Inspector Gage) (see Annex A3.1). The primary standards upon which the standard pro- cedures are based are the NISTs sets of coating thi ck- ness standards, consisting of a very uniform layer of electroplated copper covered with a hard chromium flash over a carbon steel base (see Annex A4.1). 2.5 Weld-Metal-Like Secondary Standards. Speci- mens made of weld metal or material with weld-metal- like microstructure certified for FN in a manner traceable to these standard procedures (see Annex A4.2). Coating Thickness mm mils FN 0.38 0.37 0.36 0.35 0.34 0.33 0.32 0.3 1 0.30 0.29 0.28 0.27 0.26 0.25 0.24 0.23 0.22 0.21 0.20 0.19 0.18 14.96 14.57 14.17 13.78 13.39 12.99 12.60 12.20 11.81 11.42 11 .o2 10.63 10.24 9.84 9.45 9.06 8.66 8.27 7.87 7.48 7.09 13.1 13.4 13.8 14.1 14.5 14.9 15.3 15.7 16.2 16.7 17.2 17.8 18.4 19.1 19.8 20.5 21.4 22.3 23.3 24.4 25.6 3. Calibration Methods 3.1 Primary Standards. Since each type of ferrite mea- suring instrument responds differently to the primary standards, it is not possible to specify a generic calibra- tion procedure; rather, it is necessary to tailor a calibra- tion procedure to a particular instrument. As of the two previous revisions of this standard, three types of instru- ments had been subjected to extensive testing, and de- tailed procedures and appropriate tables and values were contained in the standard to provide for their calibration to primary standards. These instruments are the Magne- Gage-type instruments, Ferritescope Model FE&KF, and Inspector Gage. At the time of publication of ANSI/AWS A4.2-86, however, the probe of the Ferritescope was changed so that the Ferritescope calibration table does not apply to newer instruments, now identified as Ferit- scopes. This situation continues. Since that time, the range of calibration by primary standards of Magne- Gage-type instruments has been expanded to include FNs appropriate to duplex ferritic-austenitic stainless steel weld metals. 3
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD=AWS A4*2M/A4-2-ENGL 3997 07842b5 0533773 T9 4 Table 3 Ferrite Numbers (FN) for Primary Standards for Inspector Gage Calibration* Coating Thickness mm mils FN 2.00 78.74 3.9 1.95 76.77 4.1 1.90 74.80 4.3 1.85 72.83 4.5 1.80 70.87 4.7 1.75 68.90 4.9 1.70 66.93 5.2 1.65 64.96 5.4 1.60 62.99 5.6 1.55 61 .O2 5.9 1 .so 59.06 6.1 1.45 57.09 6.4 1.40 55.12 6.7 1.35 53.15 7.0 1.30 51.18 7.3 1.25 49.21 7.7 1.20 47.24 8.0 1.15 45.28 8.4 1.10 43.3 1 8.9 1 .O5 41.34 9.3 1 .o0 39.37 9.8 0.98 38.58 10.0 0.96 37.80 10.3 0.94 37.01 10.5 0.92 36.22 10.7 0.90 35.43 11.0 - Coating Thickness mm mils FN 0.88 34.65 11.2 0.86 33.86 11.5 0.84 33.07 11.7 0.82 32.28 12.0 0.80 31.50 12.3 0.78 30.71 12.6 0.76 29.92 13.0 0.74 29.13 13.3 0.72 28.35 13.7 0.70 27.56 14.0 0.69 27.17 14.2 0.68 26.77 14.4 0.67 26.38 14.6 0.66 25.98 14.8 0.65 25.59 15.0 0.64 25.20 15.3 0.63 24.80 15.5 0.62 24.41 15.7 0.61 24.02 15.9 0.60 23.62 16.2 0.59 23.23 16.4 0.58 22.83 16.7 0.57 22.44 16.9 0.56 22.05 17.2 0.55 21.65 17.5 0.54 21.26 17.8 Coating Thickness mm mils FN 0.53 20.87 18.1 0.52 20.47 18.4 0.51 20.08 18.7 0.50 19.69 19.0 0.49 19.29 19.3 0.48 18.90 19.7 0.47 18.50 20.0 0.46 18.11 20.4 0.45 17.72 20.8 0.44 17.32 21.2 0.43 16.93 21.6 0.42 16.54 22.0 0.41 16.14 22.4 0.40 15.75 22.9 0.39 15.35 23.3 0.38 14.96 23.8 0.37 14.57 24.3 0.36 14.17 24.8 0.35 13.78 25.4 0.34 13.39 25.9 0.33 12.99 26.5 0.32 12.60 27.1 0.31 12.20 27.8 0.30 11.81 28.4 0.29 11.42 29.1 0.28 11 .o2 29.9 *Thi s tabl e shal l be used onl y for cal i brati ng Inspector Gage Model Number 11 1 wi t h 6F or 7F scale for measuri ng the del ta ferri te content o f as-welded austenitic stainless steel wel d metals. 3.2 Secondary Standards 33.1 Calibration by means of primary standards is the preferred method of maintaining calibration of appropri- ate instruments. But the need for frequent in-process checks is recognized along with the fact that primary standards are not necessarily durable for frequent use outside of a laboratory environment. Therefore, i t is rec- ommended that a set of secondary standards be used for frequent in-process checks (see Annex 4.2). 3.22 When secondary standards are used, the average reading on each standard shall be within the maximum allowable deviation from the calibration curve as speci- fied in Table 4. If a maximum allowable deviation is ex- ceeded, the instrument cannot be considered calibrated. Calibration with primary standards or instrument repair is then necessary. 3.23 Instruments for which there is not a detailed cal- ibration procedure in this standard utilizing primary stan- dards can only be calibrated using secondary standards. Refer to Section 7, Calibration of Other Instruments, for proper calibration instructions. 3.3 Range of Calibration for All Calibration Meth- ods. For all calibration methods and instruments, the range of calibration is defined by the interval of FNs be- tween and including the lowest F N standard and the highest FN standard used i n developing the calibration according to the corresponding procedure. 4. Calibration of Magne-GageQpe4 Instruments 4.1 Calibration by Means of Primary Standards. All Magne-Gage-type instruments can be calibrated by the 4. Tradename of Magne-GageSales and Service (see Annex A6.1). 4
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD*AWS A v - Zf l / A q =Z- ENGL L917 Table 4 Maximum Allowable Deviation, Calibration Point to Calibration Curve, for Instruments being Calibrated with Weld-Metal-Like Secondary Standards Maximum Allowable Ferrite Number Range Deviation Ot o5 FN 20.30 over 5 to IO 50.30 over 10 to 15 FN 20.40 over 15 to 25 FN 20.50 over 25 to 50 FN 25% of assigned FN over 50 to 90 FN +8% of assigned FN following procedure. Torsion balances other than a Magne-Gage may not require use of counterweights, so that statements regarding ranges of calibration may not apply. However, the requirements for the number of stan- dards for calibration over a specific FN range shall apply to all Magne-Gage-type instruments (see Annex A6.1). 4.1.1 The FNs shall be assigned from Table 1 to each of the available primary standards (coating thickness standards) as defined i n 2.3. For thicknesses between those given in the table, the FNs shall be interpolated as closely as possible. Alternatively, FN may be calculated directly from one of the two following formulas: For thickness (T) in mm: In(FN) =1.8059 - 1.11886 In(T) - 0.17740 [In(T)I2 - 0.03502 [ln(T)I3 - 0.00367 [ln(T)I4 For thickness (T) i n 0.001-inch increments (mils): ln(FN) =4.5891 - 0.50495 In(T) - 0.08918 [ln(T)]* t 0.01917 [In(T)l3 - 0.00371 [ln(T)I4 See Section 9, Significant Figures in Reporting Measure- ment Results, for information on the precision of the measurements. 4.1.2 Magne-Gage-type instruments are sensitive to premature magnet detachment from a standard or from a sample due to very small vibrations. The Magne-Gage minimizes, but does not eliminate, this effect as com- pared to other torsion balances. Repetitive measurements at a given point will yield a range of FN values due to this effect, and the range increases with increasing FN. With a Magne-Gage, above 20 FN, i t is necessary to make several measurements at any given point of a stan- dard or sample, and to accept only the highest FN as the correct value for that point. With other Magne-Gage-type = 07842b5 05L3772 920 A4.2M/A4.2:1997 instruments (torsion balances), this practice is necessary for all levels of FN. 4.13 A Magne-Gage can be used for measurements over a range of about 30 FN with a single calibration. The exact range to be used at any given time is deter- mined by the specific standards used, and the choice of a counterweight, if any, added to the balance beam of the instrument at a hole provided for this purpose. The hole is located about 38 mm[1.5 in.] from the fulcrum oppo- site from the point of suspension of the magnet (see Fig- ure Al). Care should be taken that the counterweight, if used, is free to swing without touching any other part of the instrument when the magnet is i n contact with specimen or standards. Without a counterweight, a Magne-Gage will cover from O to about 30 FN. With a counterweight of about seven grams, a Magne-Gage can cover from about 25 to 55 FN; with a counterweight of about 15 grams, the measurement range can be about 50 to 80 FN; with a counterweight of about 18 grams, the measurement range can be about 69 to 99 FN. These counterweights and ranges correspond to available coat- ing thickness standards at present, see Table Al . Exact ranges will depend upon the precise weight of the coun- terweight and upon the strength of the magnet in use. A separate calibration is required for each counterweight, and recalibration is required whenever the magnet is changed. 4.1.4 Without a counterweight, eight or more primary standards shall be used, with nominal thicknesses that provide corresponding Ferrite Numbers well distributed over the range O to 30 FN. With the No. 3 magnet in place, the zero point (the white dial reading at which the magnet lifts free from a completely nonmagnetic mate- rial) shall be determined. I f a counterweight is used, three or more primary standards, similarly well distrib- uted, shall be used, and the slope of the calibration line (FN per white dial reading or FN per gram) shall be ex- amined for consistency with the slope of the calibration for O to 30 FN (see 4.1.5). With a counterweight, no zero point can be determined for a Magne-Gage. I n either case, the white dial reading for each of the available pri- mary standards covering the FN range of interest shall then be determined (see Annex A4.1). 4.1.5 The white dial readings shall be plotted on Car- tesian coordinates paper versus the FNs as illustrated in Figure 1. I f no counterweight is used, the zero point read- ing (white dial reading when the magnet just barely lifts from a nonmagnetic material) on the dial of the gage can be included as O FN. When a counterweight is used, the plot of white dial readings versus FNs shall be superim- posed on the calibration plot made without a counter- weight, so that consistency of slope of the calibration lines can be examined as required by 4.1.4 (see Figure 2). 5
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD-AWS A' I=Zt ' l /Aq=Z-ENGL L977 0 7 B Wb 5 0533773 Bb 7 A4.2M/A4.2:1997 4 U s O 4 8 12 16 20 24 FERRITE NUMBER NOTE: A different set of coating thickness standards was used for each instrument, although the sets included the same standard numbers. Data for the Curves NlST Coating Gage #2 Calibration Gage #1 Calibration Thickness Standard White Dial FN mm mils White Dial FN mm mils 1312 1313 8.2 132.0 0.0 111.5 114.8 0.0 Zero Point 3.6 1.537 60.5 99.0 3.4 107.3 5.2 1.600 63.0 1319 1.156 45.5 92.0 5.5 93.5 8.0 0.775 1 .o92 43.0 30.5 1318 &.O 7.8 0.792 31.2 84.1 10.1 0.617 24.3 76.0 10.0 1317 74.0 12.3 0.500 0.622 24.5 19.7 68.0 1316 12.6 57.0 15.6 0.381 15.0 0.488 19.2 1315 53.0 15.9 27.0 22.2 0.249 0.373 9.8 14.7 1314 28.0 13.2 25.5 21.5 0.259 10.2 0.208 Figure 1-Examples of Calibration Lines for W o Magne-Gage Instruments, Each with a No. 3 Magnet for Measuring the Delta Ferrite Content of Weld Metal up to 26 FN 6
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD-AWS Aq*2M/A4*2-ENGL 1797 E 07842b5 0513774 7T3 M A4.2M/A4.2:1997 Coating Thickness NlST SRM White Di al FN Counterweight, g 0.001 in. I mm 117.5 1362a 0.040 1.58 1362a 74.5 68.9 15.002 0.048 1 .W 1359 142.5 16.5 82.5 34.0 7.001 0.141 5.55 37.0 76.8 3.10 0.079 50.7 Figure %Example of Calibration Lines for a Magne-Gage Instrument with a No. 3 Magnet for Measuring the Delta Ferrite Content of Weld Metals up to 77 FN 7
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS --`,,`,,,`,,,,`,```,``,,,`,`,``-`-`,,`,,`,`,,`--- STDOAWS A4*2M/A4-2-ENGL 3997 07842b5 0533775 b3T If the calibration lines are not essentially parallel, the data shall be restudied for errors. 4.1.6 A best fit straight line shall be drawn through the points plotted in accordance with 4.1.5. Alternatively, a regression equation shall be fit to the data collected as described in 4.1.4. Magne-Gages tested to date have pro- duced a straight line up to at least 10 FN. Most yield a straight line through all points, but some have shown a slight bend. An example of each is shown in Figure 1. For acceptable calibration, all points must fall within the maximum allowable deviations shown in Table 5. If any of the calibration points fall outside of the allowed varia- tions, the data shall be restudied, or the manufacturer of the instrument shall be consulted, or both. 4.1.7 Two common sources of discrepant readings during calibration (as well as during measurement) are mechanical vibrations and dirt (usually magnetic parti- cles) clinging to the magnet. Either factor tends to pro- duce premature detachment of the magnet from the sample, with a correspondingly low FN determination (high white dial reading). A vibration-free environment is essential for accurate FN determination, especially above 15 FN. Wiping the magnet end with a clean lint- free cloth is suggested when dirt is encountered. I n case of doubt, examination of the magnet end under a micro- scope is appropriate. 4.1.8 The graph plotted as in 4.1.6, or a regression equation fit to it, may now be used to determine the FNs of stainless steel weld metals from the white dial read- ings of the instrument obtained on those weld metals with the same No. 3 magnet and counterweight, if used. 4.2 Calibration by Means of Weld-Metal-Like Sec- ondary Standards 4.2.1 Calibration by primary standards is the recom- mended method, as previously mentioned, but calibra- Table 5 Tolerance on the Position of Calibration Points Using Primary Standards Maximum Allowable Ferrite Number Range Deviation o to 5 *Oo.40 over 5 to 10 ?OS0 over 10 to 15 *.70 over 15 to 20 20.90 over 20 to 30 21 .o0 over 30 to 90 55% of assigned FN tion utilizing secondary standards is acceptable? Four or more such standards are required for calibration Lurves for O to 15 FN; and four or more are required for any range of approximately 30 FN above 15 FN. In all cases, the Ferrite Numbers of the standards shall be well dis- tributed over the range of interest (see Annex A4.2). 4.2.2 I t should be recognized that weld-metal-like secondary standards are unlikely to provide readings from point to point that are as uniform as those from pri- mary standards. Care must therefore be exercised to take readings on secondary standards in precisely those loca- tions used in assigning the original FNs to the standards. I n case of doubt, the producer of the secondary standards should be consulted. 4.2.3 Other than the departures noted in 4.2.1 and 4.2.2, the remainder of the calibration procedure with secondary standards shall be the same as that used with primary standards as given in 4.1.2 through 4.1.8. 5. Calibration of Feritscopes6/ Ferritescopes 5.1 Calibration of Ferritescopes Model FES-KF by Means of Primary Standards 5.1.1This instrument is calibrated to the FN scale by the manufacturer, but calibration should be verified by the user. The only Ferritescope which can be calibrated with pri- mary standards according to Table 2 is the pre-1980 Model FE8-KF with analog readout and dual-contact normal- ized probe. No tables for calibration with primary stan- dards are available for post-1980 instruments (those with digital readouts or single-pole probes). Other Ferritescopes and the current models identified as Ferritescope may be calibrated by weld-metal-like secondary standards as de- scribed in Section 7, Calibration of Other Instruments. 5.1.2 The manufacturers instructions with regard to the use of the instrument and the adjustments of the scale shall befollowed. 5.13 The FNs shall be assigned from Table 2 to each of the available primary standards as defined in 2.3. For thicknesses between those given in the table, the FNs shall beinterpolated as closely as possible. Eight or more thickness standards shall be used, with nominal thickness corresponding to Ferrite Numbers well distributed in the range O to 25 FN (see Annex A4.1). The instrument read- ing for each of the available primary standards shall then bedetermined. 5. Weld-metal-like secondary standards are commercially sold by The Welding Institute, Abington Hall, Abington, Cam- bridge, CBl 6AL, UK. 6. Trademark of Helmut Fischer GmbH and Company 8
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS --`,,`,,,`,,,,`,```,``,,,`,`,``-`-`,,`,,`,`,,`--- 5.1.4 The instrument readings shall be plotted on Carte- sian coordinates paper versus the FN assigned from Table 2 for each primary standard. A best fit line shall be drawn through the data. Alternatively, a regression equa- tion shall be fit to the data collected as described in 5.1.3. 5.1.5 For approved calibration, all readings shall fall within the maximum allowable deviations shown in Table 6 from the best fit line. If any of the calibration readings fall outside of these allowed variations, the data shall be restudied, or the manufacturer of the instrument shall be consulted, or both. 5.1.6 The graph plotted as in 5.1.4, or a regression equation fit to it, may now be used to determine the FNs of stainless steel weld metals from the instrument reading. 5.2 Calibration by Means of Weld-Metal-Like Sec- ondary Standards 5.2.1 As previously mentioned, calibration to primary standards is the preferred method for suitable instru- ments, but calibration to weld-metal-like secondary stan- dards is acceptable. Calibration to weld-metal-like secondary standards is necessary for other Feritscopes/ Ferritescopes. 5.2.2 Section 7.2 should be referred to for instructions to calibrate the Feritscope/Ferritescope to weld-metal- like secondary standards. 6. Calibration of Inspector Gages 6.1 Calibration by Means of Primary Standards 6.1.1 This instrument is the Inspector Gage Model Number 1 1 1 with either a 6F (%-ferrite) or a 7F (FN) 7. Trademark of Elcometer instruments Ltd. (see Annex A6.3) W 078q2b5 051377b 575 E A4.2MlA4.2:1997 scale. The latter is preferable becausL it has smaller divi- sions (see Annex A6.3). 6.1.2 The manufacturers instructions with regard to the use of the instrument and adjustments of the scale shall be followed. 6.13 The FNs shall be assigned from Table 3 to each of the available primary thickness standards as defined in 2.3. For thicknesses between those given in the table, the FNs shall be interpolated as closely as possible. Seven or more thickness standards shall be used, with nominal thicknesses corresponding to Ferrite Numbers well dis- tributed in the range O to 30 FN (see Annex A4.1). The instrument reading for each of the available primary standards shall then be determined. 6.1.4 The instrument readings shall be plotted on Car- tesian coordinates paper versus the FN assigned from Table 3 for each primary standard. A best fit line shall be drawn through the data. Alternatively, a regression equation shall be fit to the data collected as described in 6.1.3. 6.1.5 For approved calibration, all readings shall fall within the maximum allowable deviations shown in Table 7 from the best fit line. I f any of the calibration readings fall outside of these allowed variations, the data shall be restudied, or the manufacturer of the instrument shall be consulted, or both. 6.1.6 The graph plotted as in 6.1.4, or a regression equation f i t to it, may now be used to determine the FNs of stainless steel weld metals from the instrument reading. 6.2 Calibration by Means of Weld-Metal-Like Sec- ondary Standards 6.2.1 As previously mentioned, calibration to primary standards is the preferred method, but calibration to weld-metal-like secondary standards is acceptable. Table 6 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Feritscopes/Ferritescopes Maxi mum Allowable Deviation of the Periodic Ferrite Number Check From the Ferrite Number From the Ferrite Number From the Ferrite Number Value Assigned to the Value Assigned to the Value First Assigned to the Primary Standard Secondary Standard Secondary Standard Ferrite Number Range in Table 2 by the Seller by the User o to 5 over 5 to 10 over 10 to 15 over 15 20.40 20.40 20.70 21.0 20.40 20.40 20.70 21.0 20.20 20.20 20.20 20.30 9
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - ~ Table 7 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Inspector Gages Maximum Allowable Deviation of the Periodic Ferrite Number Check From the Ferrite Number From the Ferrite Number From the Ferrite Number Value Assigned to the Value Assigned to the Value First Assigned to the Primary Standard Secondary Standard Secondary Standard Ferrite Number Range in Table3 by the Seller by theUser o to 5 20.40 S. 40 20.20 over 5 to 10 20.40 50.40 50.20 over 10 to 15 20.70 50.70 50.20 over 15 21.0 f l . O 20.30 6.2.2 Section 7.2 should be referred to for instructions to calibrate the Inspector Gage to weld-metal-like sec- ondary standards. 7. Calibration of Other Instruments 7.1 Calibration by Means of Primary Standards. As of this revision of this standard (see 3.1) only Magne- Gage-type instruments, Ferritescopes Model FE8-KF with normalized probes, and Inspector Gages, can be cal- ibrated to this standard by means of primary standards. All other instruments must be calibrated by means of weld-metal-like secondary standards (see Annex A6.4). 7.2 Calibration by Means of Weld-Metal-Like Sec- ondary Standards 7.2.1 Other instruments can be calibrated by weld- metal-like secondary standards to produce a satisfactory correlation between the instrument readout and weld metal FN. While it may be desirable that the instrument readout be precisely the calibrated value of FN it is not essential, provided a unique correlation between the in- strument readout and weld metal FN, can be determined. Such instruments may be used if they have been cali- brated using secondary weld metal standards to which FNs were assigned by an instrument with primary stan- dard calibration. 7.2.2 Four or more such secondary standards are re- quired for calibration curves covering O to 15 FN; eight or more such secondary standards are required for cali- bration from O to 30 FN; and four or more such second- ary standards are required for calibration of any interval of approximately 30 FN above 15 FN. Some Feritscopes accept only a smaller number of secondary standards in setting a calibration. For example, the Model MP-3 can only accept three secondary standards for setting the cal- ibration over any given range, while four calibration ranges are possible. Then for checking the calibration over a given range against the requirements of Table 4, there must be at least four secondary standards, as re- quired above, within the given calibration range, and check measurements on all of them must satisfy the requirements of Table 4 for acceptable calibration over that range. In all cases, the Ferrite Numbers of the sec- ondary standards shall be well distributed over the range of interest. 7.2.3 Instrument readings shall be determined for each of the available secondary standards and, if possi- ble, for a zero point. When taking readings on secondary standards, the same precaution noted in 4.2.2 should be taken. 7.2.4 Instrument readings shall be plotted against as- signed secondary standard FN values on Cartesian coor- dinate paper, and the zero point can be included i f applicable. 7.2.5 A best fit smooth line, or a regression equa- tion line, shall be drawn through the points plotted in 7.2.4. For acceptable calibration, no data point may vary from the curve any more than the allowable deviations shown in Table 4. If any point falls outside of the appro- priate allowed deviation, the data shall be restudied, or the manufacturer of the instrument shall be consulted, or both. 7.2.6 The graph plotted as in 7.2.4, or a regression equation fit to it, may now be used to determine the FNs of stainless steel weld metals over the calibration range. 7.2.7 It is the responsibility of the user to ensure that the instrument is properly calibrate& .e., such that the results obtained with weld-metal-like secondary stan- dards in the FN range(s) of use are within the expected range of variations shown in Table 4. 10
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD-AUS A' I =ZM/ Aq. 2- ENGL 3797 E 078'Y2b5 0533778 349 II 8. Use of Calibrated Instruments 8.1 Maintaining Calibration. Instruments must be checked periodically on a regular basis against primary or secondary standards to ensure and verify the mainte- nance of the original calibration. Records of such checks shall be maintained. It is the responsibility of the user to check at a frequency which is adequate to maintain cali- bration. For frequently used instruments, a weekly cali- bration check is recommended. For infrequently used instruments, a calibration check before each use is rec- ommended. Two standards, one near each extreme of the calibration range being checked, shall be used for each of the ranges shown in Tables 4, 6, 7, or 8, as appropriate, for which the instrument is used. When the instrument no longer produces values within the maximum deviation specified in the relevant table, it shall be removed from service and the manufacturer shall be consulted (see Annex A3.2). A calibration curve may be made for an individual in- strument using reference material other than the stan- dards used for the original calibration. This calibration curve may be used for verifying the original calibration. When the instrument can no longer produce readings on this curve within the maximum deviations of Tables 4,5, 6, 7, or 8, i t must be :ecalibrated in accordance with this document. 8.2 Variations in Measurements. Based upon round- robin tests within the Welding Research Council Sub- committee on Welding Stainless Steels, the FNs deter- mined by these instruments are expected to fall within the limits shown in Table 9, 10, or 11 as compared to the overall average FN values of stainless steel weld metals checked on other instruments of the same type calibrated to this standard. When measurements are made with a variety of calibrated instrument types, somewhat larger variation in measurements than those indicated i n Table 9, 10, or 11 might be expected, but the magnitude of the variation has not been determined. Weld ripples and other surface perturbations must be removed because surface finish affects measurement ac- curacy. Up to about 20 FN, the practice known as draw filing produces acceptable accuracy (see 2.2). For accu- rate and reproducible ferrite measurements, above 20 FN, a Magne-Gage No. 3 magnet or equivalent requires a flat surface at least 3 mm[1/8-in.] in diameter finished no coarser than with a 600-grit abrasive (about 0.2 mi- crons/8 microinches RMS). Rougher surfaces or convex Table 8 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Magne-Gage-Type Instruments Maximum Allowable Deviation of the Periodic Ferrite Number Check Fromthe Ferrite Number Fromthe Ferrite Number Fromthe Ferrite Number Value Assigned to the Value Assigned to the Value First Assigned to the Primary Standard Secondary Standard Secondary Standard Ferrite Number Range i n Table1 by the Seller by the User o to 5 20.50 20.50 20.20 over 5 to 10 20.50 20.50 20.20 over 10 to 15 20.60 20.60 20.30 over 15 to 25 20.80 20.80 20.40 over 25 to 90 25% of assigned FN value 25% of assigned FN value 23% of assigned FN value Table 9 Expected Range of Variation in Measurements with Calibrated Magne-Gage-Type Instruments* Ferrite Number Range 67% of the Instruments 95% of the Instruments o to 10 20.30 FN 20.60 FN over 10 to 18 20.35 FN 20.70 FN over 18 to 25 20.45 FN 20.90 FN over 25 to 90 55% of mean FN value 210% of mean FN value *Based upon WRC round-robin tests. 11
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - . - Table 10 Expected Range of Variation in Measurements with Calibrated Feritscopes/Ferritescopes* Ferrite Number Range 67% of the Instruments 95% of the lnstruments o to 10 over 10 to 18 over 18 to 25 over 25 to 80 20.20 FN k0.40 FN 20.50 FN 5% of mean FN value S.40 FN S.80 FN 21.0 FN 510% of mean FN value +Based upon WRC round-robin tests. Table 11 Expected Range of Variation in Measurements with Calibrated Inspector Gages* Ferrite Number Range 67% of the Instruments 95% of the Instruments o to 10 20.20 FN 20.40 FN over 10 to 18 20.40 FN *.80 FN over 18 to 30 +OS0 FN 21 .O FN 'Based upon WRC round-robin tests. surfaces will result in artificially low FN values and shall be avoided. Other instruments may respond differently to rough, convex, or narrow surfaces and should be evalu- ated fully before use. At all ferrite levels, surface prepa- ration must be accomplished without contamination by ferromagnetic materials. 9. Significant Figures in Reporting Measurement Results 9.1 Calibration Data. For purposes of developing cali- bration data or demonstrating compliance of an instru- ment with calibration requirements, the number of significant figures shown in the relevant table herein shall be used. 9.2 Measurement Data. For purposes of reporting mea- surement data on weld metal test samples or demonstrat- ing compliance with the requirements of a specification other than this specification, the precision implied by the number of significant figures in the tables herein is gen- erally inappropriate. For ferrite measurements of 25 FN or higher, rounding-off to the nearest whole number con- veys appropriate precision. For ferrite measurement of 5 to 25 FN, rounding-off to the nearest 0.5 FN conveys ap- propriate precision. For ferrite measurements less than5 FN, rounding-off to the nearest 0.1 FN conveys appropri- ate precision. 12
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD-AWS Aq-ZH/Aq=Z-ENGL 1777 = 07842b5 0513780 TT7 W A4.2M/A4.2:1997 Annex (This Annex is not a part of ANSIIAWS A4.2M/4.2:1997, Standard Procedures for Calibrating Magnetic Instru- ments to Measure the Delta Ferrite Content of Austenitic and Duplex Ferritic-Austenitic Stainless Steel Weld Metal, but is included for information purposes only.) Al. Acknowledgment These standard procedures are based upon the studies and recommendations made by the Subcommittee on Welding Stainless Steel of the High Alloys Committee of the Welding Research Council (WRC)8 and work within International Institute of Welding Subcommission II-C. The document on which much of this standard is based is the Calibration Procedure for Instruments to Measure the Delta Ferrite Content of Austenitic Stainless Steel Weld Metal, published by the WRC on J uly 1, 1972. Expansion of the measurement system beyond 28 FN is based upon Extension of the WRC Ferrite Number Sys- tem, D. J . Kotecki, Welding Journal, November 1982, and International Institute of Welding Documents II-C- 730-84, II-C-821-88, II-C-835-88 and 11-C-836-88. A2. Ways of Expressing Ferrite Content A2.1The methods of determining ferrite content i n stain- less steel weld metals have evolved over an extended time period. The interested reader is referred to WRC Bulletin 318 (September 1986). Only a few of the perti- nent conclusions of that Bulletin are summarized briefly i n the following paragraphs. A2.2 Measured Percent Ferrite. The percent ferrite in austenitic stainless steel weld metals i n the past has too often been regarded as a firm fixed value. Extensive round-robins have been run on sets of weld metal speci- mens, containing up to a nominal 25 percent ferrite, in the U.S. under the sponsorship of the WRC and on simi- 8. Welding Research Council, 345 East 47th St., New York, NY 10017 lar sets in Europe by the International Institute of Weld- ing (I I W). These round-robins showed that most laboratories used somewhat different calibration curves, as well as a variety of instruments. At nominal levels of up to 10 percent ferrite, which is often the most useful and pertinent range, the values obtained by participating laboratories ranged from 0.6 to 1.6-times the nominal value. The instrument calibration procedure defined in this standard is designed to overcome this problem. A similar problem existed with metallographic deter- minations due to the extreme fineness of the ferrite i n weld metals, variations in the etching media and the de- gree of etch, and to the Quantitative Television Micro- scope (QTM) settings, i f a QTM was used. Similar problems, though perhaps to a lesser degree, have been encountered with magnetic saturation, x-ray diffraction, Mossbauer studies, and with other methods of determin- ing the ferrite content of weld metals. Thus a percent ferrite figure in past literature is very dependent upon the source, and should be defined in relation to the in- strument, the laboratory using it, and the calibration source, or to the diagram if derived from a constitution diagram. I n the opinion of the WRC Subcommittee, i t has been impossible, to date, to determine accurately the true absolute ferrite content of stainless steel weld metals. A2.3 Ferrite Number. Because on a given specimen, laboratory A might rate the percent ferrite at as low as 3 percent, laboratory B at 5 percent, and laboratory C at as high as 8 percent, the WRC Subcommittee decided to use the new termFerrite Number (FN) to define the fer- rite quantity as measured by instruments calibrated with its recommended procedure. Thus, FN is an arbitrary, standardized value related to the ferrite content of an equivalently magnetic weld metal. I t is not necessarily the true absolute ferrite percentage of the weld. FNs 13
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - A4.2MlA4.2:1997 below 10 do represent an excellent average of the per- cent ferrite as determined by U.S. and world methods of measuring delta ferrite, based upon the previously dis- cussed round-robins conducted by the WRC Subcommit- tee and the IIW Subcommission II-C. FNs above 10 clearly exceed the true volume percent. Magnetic satura- tion measurements on castings of known-percent ferrite have shown that the magnetic response of a given per- cent ferrite depends upon its composition. So, any rela- tion between ferrite and FN will be influenced somewhat by composition of the ferrite. For common duplex fer- ritic-austenitic weld metals, it is not unreasonable to esti- mate that the percent ferrite is on the order of 0.7 times the FN as measured herein, but this should not be consid- ered as exact. A2.4 Ferrite Content Calculated from Constitution Diagrams. The several committees that have investi- gated and reviewed this subject recommend for most ap- plications the use of measured ferrite as opposed to the use of ferrite calculated from the weld metal analysis. The basic reason for this is that the variables involved in determining the chemical composition, and other vari- ables involved in the diagrams themselves, are very likely to have substantially greater effects than those as- sociated with the direct determination of ferrite content using instruments calibrated in accordance with this stan- dard. Nevertheless, constitution diagrams are very useful tools, even though they are less exact, because they per- mit anticipation or prediction of ferrite content for a vari- ety of situations (see WRC Bulletin 342, Stainless Steel Weld Metal: Prediction of Ferrite Content, April 1989). By taking into account dilution effects, such diagrams can also be useful for anticipating or predicting the fer- rite content of weld overlays and dissimilar metal joints. The Schaeffler diagram, developed in the late 1940s. presents its values as percent ferrite. The DeLong dia- gram, J anuary 1973 version, was the first diagram pre- sented i n terms of FN. Espy, i n 1982, proposed a modification of the Schaeffler Diagram to take into ac- count high-nitrogen, high-manganese stainless steel weld metals. More recently, Siewert, McCowan and Olson prepared the WRC-1988 Diagram, under WRC sponsor- ship (see Welding Journaf, December 1988, pp. 289-s to 298-s, or WRC Bulletin 342, April 1989). This was mod- ified slightly by Kotecki and Siewert to include the effect of copper in the nickel equivalent, as originally proposed by Lake, to produce the WRC-1992 Diagram (see Weld- ingJourna1, May 1992, pp. 171-s to 17th). The WRC- 1992 Diagram is considered, at the time of this writing, to be the best estimation tool available for most austen- itic and duplex ferritic-austenitic stainless steel weld metals, and has replaced the DeLong Diagram in Section I I I of the ASME Code with publication of the 1994 Addenda. 14 The American Welding Institute developed the per- sonal computer software package, FERRITEPREDIC- TOR, to assist i n Ferrite Number estimation. The software is available from the American Welding Soci- ety. This software permits estimation of weld metal fer- rite by the WRC-1992 Diagram, as well as by the WRC- 1988 Diagram, the Schaeffler Diagram and the DeLong Diagram. A3. Cautions on the Use of Ferrite Number A3.1 Instrument Calibration A3.1.1 Various thicknesses of nonmagnetic material over carbon steel represent a very convenient method of calibrating instruments for the measurement of ferrite in stainless steel weld metals. Useful general information on the subject can be obtained from the latest edition of The American Society for Testing and Materials (ASTM) B 499, Standard Method for Measurement of Coating Thicknesses by Magnetic Method: Nonmagnetic Coatings on Magnetic Base Met akg The response of the instrument when a nonmagnetic skin is between the measuring probe and the plate, versus its response to fer- rite in stainless steel weld metal at several levels, can be plotted and the relationship between them established. A change i n the magnet size or strength, or in the probe characteristics, changes the relationship. Thus, a calibra- tion curve or table for FN versus nonmagnetic coating thickness for a Magne-Gage-type instrument (Figure Al ) will be different for each of the magnets (Nos. 1, 2, 3, and 4) because the strengths of the magnets are different. A3.1.2 With Magne-Gage-type instruments, only cali- bration using a No. 3 magnet is considered in this stan- dard. A weaker magnet (Nos. 1 or 2), if used with the calibration points of Table 1, will on weld metal yield falsely high FN values. Conversely, a stronger magnet (No. 4), if used with the calibration points of Table 1, will on weld metal yield falsely low FN values. If the No. 3 magnet of a Magne-Gage is damaged, such as by rough handling or exposure to an alternating current field which weakened it, it will also yield false readings. Work wi thi n the WRC Subcommittee on Welding Stainless Steel, on behalf of the International Institute of Welding, Subcommission WC, has demonstrated that accurate readings on weld metal are obtained via calibration from Table 1 when the magnet strength is such that it provides 9. ASTM standards can be obtained from the American SoCi- ety for Testing and Materials, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959.
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - a tearing-off force as a function of FN of 5 FN/gram 5 0.5 FN/gram. With a torsion balance other than a Magne- Gage, compliance with this requirement is determined directly from the slope of the calibration line. With a Magne-Gage, this can be evaluated simply by suspend- ing a 5-gram iron weight from the No. 3 magnet. When the white dial of the Magne-Gage is turned to just barely lift the weight past the balance point of the instrument, the reading should correspond to 25 2 2.5 FN using the calibration line of white dial readings versus FN. A3.1.3 I t is strongly recommended that reference weld-metal-like secondary standards be used along with the calibration curves obtained from primary standards when using a Ferritescope Model FES-KF to check for compliance with Table 6, when using an Inspector Gage to check for compliance with Table 7, or when using a Magne-Gage-type instrument to check for compliance with Table 8, I f compliance cannot be obtained as re- quired by the appropriate table, the instrument is in need of recalibration or servicing by the manufacturer, or it is not suitable for calibration with primary standards. A3.2 Instrument Malfunction. Recalibration or re- checking of each instrument at periodic and sometimes frequent intervals is necessary to ensure that the instru- ment is operating properly (see 8.1). Permanent magnets may be partially demagnetized by exposure to any signif- icant alternating-current field such as that generated by a strong alternating current in a wire or by a weaker alter- nating current in a coil. The tips of such permanent mag- nets, or of the probes which are used to establish a magnetic field i n the specimen, may become worn and the response of the system may change for this reason. Bearings may become fouled with dirt and thus fail to operate freely. A4. Standards for Instrument Calibration . A4.1 Primary Standards. NIST'O coating thickness standards were developed many years ago to calibrate in- struments for the determination of coating thickness. The standards useful for the determination of delta ferrite consist of varying thicknesses of copper electroplated on a carbon steel base and protected with a hard chromium flash. NIST certifies the thickness of the total coating to within 55% of the stated thickness, but the majority will be within t2% or even 51%. Table Al lists the coating 10. Office of Standard Reference Materials, Room B311, Chemistry Building, National Institute of Standards and Tech- nology (NIST), Gaithersburg, MD 20899. A4.2MlA4.2:1997 thickness standards available from NIST at the t i m of this writing, and corresponding Ferrite Numbers for cali- braiion of various instruments. It should bc recognized that the exact coating thickness value of a particular stan- dard from NIST may not be exactly as given in Table Al , and the corresponding FN may therefore be slightly dif- ferent. The sets can be ordered from the NIST office listed in Footnote 10. A4.2 Secondary Standards A4.2.1 Weld-Metal-Like Secondary Standards. Magnetic instruments may also be calibrated by using weld-metal-like secondary standards rated by two or more instruments carefully calibrated through the use of these standard procedures. Each such standard should be provided with FN values at specific points on its test sur- face. These secondary standards can be used for the cali- bration of a suitable instrument or for maintaining calibration. They can also be used to establish the rela- tionship between other instruments and Magne-Gage- type instruments. A4.2.2 Other mpes of Secondary Standards. The use of cast specimens or powder compacts is risky be- cause the size, shape, and orientation of the magnetic particles may influence the response of the magnetic or other type probes to varying degrees, However, cast specimens or powder compacts calibrated with one in- strument traceable to this procedure can be used for cali- brating instruments of the same type and manufacture or for day-to-day verification of such instruments. A5. Effect of Ferrite Size, Shape, and Orientation I t has been established that the ferrite size, shape, and orientation can influence the relative response of the low-field-strength magnets and probes used with the measuring instruments. For this reason, a measuring in- strument may respond differently to a given volume-per- cent ferrite in a stainless steel weld metal as compared to the same volume-percent ferrite i n a cast stainless steel, or even i n a solution heat-treated stainless steel weld metal. The ferrite i n as-welded weld metal up to about 15 FN is very fine and i n the form of lacy, dendritic stringers generally perpendicular to the fusion line, and often extensively interconnected at ferrite contents over 3 or 4 FN. Above about 15 FN in as-welded weld metal, the ferrite and austenite generally form laths which are also very fine. The ferrite in castings is usually much larger and tends to be lesser in volume and more sphe- roidized than in an as-welded weld metal of the same composition because heat treatment tends to transform some ferrite to austenite and spheroidize the balance. 15
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS --`,,`,,,`,,,,`,```,``,,,`,`,``-`-`,,`,,`,`,,`--- STD.AWS A4. 2M/ A' I . Z- ENGL 1997 = 078' 42b5 O513783 7Db = A4.2MlA4.2:1997 Table A l Current NIST Coating Thickness Standards (Nominal Thicknesses) with Approximate Corresponding Ferrite Numbers Nominal Thickness Approximate Ferrite Number NIST SRM Ferritescope Set Number mm mils Magne-Gage Model FB- KF Inspector Gage 1364a 1.935 76.18 2.7 2.0 4.2 1.525 60.04 3.7 3.1 6.0 1.ooO 39.37 6.1 5.3 9.8 0.800 31.50 7.7 6.6 12.3 1363a 0.635 25.00 9.8 8.2 15.4 0.505 19.88 12.2 10.2 18.8 0.385 15.16 15.5 13.0 23.6 0.255 10.04 21.7 18.7 off-scale 1362a 0.205 8.07 25.8 22.8 off-scale 0.140 5.51 34.2 off-scale off-scale 0.080 3.15 50.2 off-scale off-scale 0.040 1.57 77.0 off-scale off-scale 1361a 0.048 1.89 69.1 off-scale off-scale 0.025 0.98 99.2 off-scale off-scale 0.01 2 0.47 off-scale off-scale off-scale 0.006 0.24 off-sale off-scale off-scale 1359 0.800 31 S O 7.7 6.6 12.3 0.505 19.88 12.2 10.2 18.8 0.140 5.5 1 34.2 off-scale off-scale 0.048 1.89 69.1 off-scale off-scale 1358 1 .o00 39.37 6.1 5.3 9.8 0.225 8.86 24.0 20.9 off-scale 0.080 3.15 50.2 off-scale off-scale 1357 0.048 1.89 69.1 off-scale off-scale 0.020 0.79 110.5 off-scale off-sale 0.006 0.24 off-scale off-scale off-scale Since the volume-percent of ferrite in castings is i n close agreement when measured by either magnetic response or by metallographic point count, the ferrite content of castings is expressed as a percentage and not by the arbi- trary FN, as noted in ASTM Practice A800. A6. Instruments A6.1 Magne-Gage and Magne-Gage-Qpe Instruments A6.1.1The Magne-Gage" (Figure Al ) is usable only in the flat position on relatively small specimens. The 11. Manufactured by Magne-Gage Sales & Service, 629 Packer St., Avoca, PA 18641. probe is a long, thin magnet hung on a spiral spring. The spring is wound by means of turning a knob with a corre- sponding reading on a dial. When the magnet is pulled free of a specimen, the white dial reading used in con- junction with the calibration curve establishes the FN of the specimen. A6.1.2 Returning the Magne-Gage periodically to the factory for maintenance is desirable. With frequent use, one year is a reasonable time; with occasional use, two years. A6.1.3 A Magne-Gage No. 3 Magnet or equivalent can be used with a variety of torsion balances to obtain the same results as are obtained with a Magne-Gage. A complete example of such a Magne-Gage-type instru- ment is given in Extension of rhe WRC Ferrite Number 16
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - (A) STANDARD MAGNE-GAGE (B) MAGNE-GAGE FROM REAR, COUNTERWEIGHT ADDED TO LEFT SIDE OF BALANCE BEAM Figure Al-Magne-Gage-Type Instruments 17
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS --`,,`,,,`,,,,`,```,``,,,`,`,``-`-`,,`,,`,`,,`--- STD-AWS A 4. 2H/ Aq. Z-ENGL 1777 0781.12b5 0513785 587 W A4.2M/A4.2:199? (C) TORSION BALANCE WITH MAGNE-GAGE NO. 3 MAGNET Figure Al (Continued)-Magne-Gage-Qpe Instruments System, referenced in Section Al . Numerous other con- figurations could also be conceived. This is outside the scope of this standard. A6.2 Feritscope/Ferritescope-. These instruments, which consist of a probe connected by a cable to an elec- tronics package (Figure A2), are usable in any position. Several models and a variety of probes are available. Only one model and probe (Model FE8-KF) has been shown to be able to be calibrated with primary standards as given in Table 2 (see 5.1.1). All others must be cali- brated with weld-metal-like secondary standards as no standard tables have been developed for calibration with primary standards. Models are available in either battery- powered or alternating current versions. At least one model can be calibrated with secondary standards up to 80 FN or more. A63 Inspector Gage.13 This instrument (Figure A3), is usable in any position. It is a hand-held magnetic instru- 12. Manufactured by Fischer Technology, 750 Marshall Phelps Road, Windsor, CT 06095. 13. Manufactured by Elcorneter, Inc., 1893 Rochester Industrial Drive, Rochester Hills, MI 48309. ment with thumb-actuated spring tension. The instrument gives direct readings in FN if it is a new model designed to do so. Older models can be rebuilt by the manufacturer to give acceptable readings on weld metal in terms of FN. At the time of this printing, the ability of Inspector Gages to determine ferrite above 30 FN is unknown. A6.4 Other Instruments A6.4.1 The following instruments at the time of the writing of this revision are not capable of being cali- brated to primary standards. They can, however, be cali- brated to weld-metal-like secondary standards and produce acceptable consistent results. Again, it is the re- sponsibility of the user to ensure that instrument calibra- tion is maintained and to have the instrument repaired by the manufacturer if consistent readings on the weld- metal-like secondary standards cannot be obtained. At the time of this printing, the ability of these instruments to determine ferrite above 30 FN is unknown. A6.4.1.1 Ferrite Indicator (more commonly called a Severn Guge).14 This instrument (Figure A4) is 14. Manufactured by Severn Engineering Co., Inc., 98 Edge- wood Street, Annapolis, MD 21401. 18
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - Figure A.2-Ferritescope Model FE&KF Figure &Inspector Gage usable in any position. It is a go-no-go-type gage which determines whether the ferrite content of the weld under test is above or below that of each of a number of inserts of various magnetic strengths which come with the in- strument. At least one unthreaded test insert must be available for use i n conjunction with one of the threaded inserts with specified FN values. The purpose of the un- threaded inserts is to assure that the magnet has not lost strength. Details may be obtained from the manufacturer for conversion of percent-ferrite values on earlier model Severn gages to FN. Severn gages calibrated directly in terms of FN are now available. Older model gages can be converted to the FN scale by the manufacturer. Calibra- tion of a Severn gage with secondary standards can only be approximate because the Severn gage does not pro- vide a discrete FN test value, only a range of possible FN values for the sample under test. A6.4.1.2 Foerster Ferrite Content Meter. This is a light, portable, battery-powered instrument (Figure 15. Marketed by Foerstet Instrument, Inc., 140 Industry Drive, RIOC Park West, Pittsburgh, PA 15275. 19
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD*AWS A4*2M/A4.2-ENGL 1997 07842b5 0513787 351 M A4.2MlA4.2 : 1 997 Figure A4 - Ferrite Indicator (Severn Gage) M) usable in any position. It closely resembles the Ferit- scope i n its operation except that it has a single contact- point probe which allows ferrite determination in very localized regions. On older models, the meter output in- dicates ferrite content as a percentage, which can be ef- fectively converted to FN values by the use of suitable weld-metal-like secondary standards to produce a satis- factory calibration curve. Newer models are now avail- able on which the meter reads directly in FN values. A6.4.2 A number of other magnetic measuring instru- ments are available for various purposes. Many are re- garded as not suitable in their present form because of limitations such as range, problems in calibration, or vary- ing response due to the position of use or to their relation to the north-to-south magnetic field lines of the earth. Instruments which are suitable in other respects must still be calibrated to the FN scale in a manner traceable to this standard. This can be accomplished by the use of a set of weld-metal-like secondary standards, as specified i n Section 7, Calibration of Other Instruments. The es- tablishment of an adequate correlation is the responsibil- base metal may be increased by varying degrees on each instrument depending on the distance of the magnet or probe from the base metal, on the ferrite content, and on the permeability of the base metal. Hence, to limit the in- crease in FN values to 0.2 FN maximum due to the effect of a ferromagnetic carbon steel base metal, the carbon steel base plate should be approximately 8 mm [0.3 in.] or more away from a Magne-Gage magnet or Inspector Gage magnet, 25 mm[1.0 in.] from a Ferrite Indicator (Severn Gage), and 5 mm[0.2 in.] from a Feritscope or Foerster Ferrite Content Meter probe. For other instru- ments, a safe distance can be obtained by experimenta- tion or by contacting the instrument manufacturer. If it is not possible to obtain the above minimum distances from ferromagnetic material in a production situation, FN measurements can still be meaningful if the effect of the proximity of the ferromagnetic material can be taken into account. One way to do this is by comparing FN mea- sured with ferromagnetic material i n place to FN mea- sured with ferromagnetic material removed using laboratory samples. ity of the user. A73 Wrought Stainless Steels. It is not intended that the determination of FN be extended to wrought stainless steels. Wrought steels are beyond the scope of this standard. A7.1 Distance from Ferromagnetic Material. The FN A7.3 Cast Stainless Steels. The FNs are not used for values of stainless steel weld deposits on ferromagnetic cast stainless steels. The same measurement scales used A7. Use of Calibrated Instruments 20
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - 21
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STD-AWS A4.2M/A4=2-ENGL L777 07842b5 0533789 124 A4.2MIA4.2: 1997 AWS Filler Metal Specifications by Material and Welding Process ESW EGW Brazing A5.25 A5.26 A5.8, A5.31 A525 A5.26 M. 8, M. 31 A59 A5.9 A5.8, A5.31 23 Previous page is blank
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - - STDeAWS A4=ZH/Aq.Z-ENGL L997 0784Zb5 0533770 74b W A4.2MlA4.2:1997 AWS Filler Metal Specifications and Related Documents AWS Desienatioa Title FMC Filler Metal Comparison Charts A4.2M/A4.2 Standard Procedures for Calibrating Magnetic Instruments to MeasuretheDeltaFerriteContent of Austenitic and Duolex Austenitic-Ferritic Stainless Steel Weld Metal A4.3 Standard Methods for Determination of the Diffusible Hydrogen Content of Martensitic, Bainitic, and Ferritic Steel Weld Metal Produced by Arc Welding A5.01 Filler Metal Procurement Guidelines A5.1 Specification for Carbon Steel Electrodes for Shielded Metal Arc Welding A.5.2 Specification for Carbon and Low-Alloy Steel Rods for Oxyfuel Gas Welding ~ ~ A5.3 ~ ~~ Specificationfor Aluminum and Aluminum Alloy Electrodes for Shielded Metal Arc Welding ~~~ ~~ A5.4 Specification for Stainless Steel Welding Electrodes for Shielded Metal Arc Welding A5.5 Soecification for Low-Allov Steel Electrodes for Shielded Metal Arc Weldine A5.6 Specification for Covered Copper and Copper Alloy Arc Welding Electrodes A5.7 Specification for Copper and Copper Alloy Bare Welding Rods and Electrodes A5.8 Specification for Filler Metals for Brazing and Braze Welding ~~ ~~ ~ A5.9 Specification for Bare Stainless Steel Welding Electrodes and Rods A5.10 Specification for Bare Aluminumand AluminumAlloy Welding Electrodes and Rods A5.11/A5.11M Specification for Nickel and Nickel-Alloy Welding Electrodes for Shielded Metal Arc Welding A5.12/A5.12M Specification for Tungsten and Tungsten Alloy Electrodes for Arc Welding and Cutting A513 Specification for Solid Surfacing Welding Rods and Electrodes A5.14/A5.14M Specification for Nickel and Nickel-Alloy BareWelding Electrodes and Rods A5.15 Specification for Welding Electrodes and Rods for Cast Iron A5.16 Specification for Titaniumand TitaniumAlloy Welding Electrodes and Rods ~~ ~ A5.17/A5.17M Specification for Carbon Steel Electrodes and Fluxes for Submerged Arc Welding A5.18 Specification for Carbon Steel Electrodes and Rods for Gas Shielded Arc Welding A5.19 Specification for Magnesium Alloy Welding Electrodes and Rods A5.20 Soecification for Carbon Steel Electrodes for Flux Cored Arc Weldine A5.21 Specification for Composite Surfacing Welding Rods and Electrodes A5.22 Specification for Stainless Steel Electrodes for Flux Cored Arc Welding and Stainless Steel Flux Cored Rods for Gas Tungsten Arc Welding A5.23/A5.23M SDecification for Low-Allov Steel Electrodes and Fluxes for Submereed Arc Weldine AS.24 Specification for Zirconiumand ZirconiumAlloy Welding Electrodes and Rods A5.25/A5.25M Specification for Carbon and Low-Alloy Steel Electrodes and Fluxes for Electroslag Welding Ph5.26/A5.26M Specification for Carbon and Low-Alloy Steel Electrodes for Electrogas Welding A5.28 Specification for Low-Alloy Steel Electrodes and Rods for Gas Shielded Arc Welding A5.29 Specification for Low-Alloy Steel Electrodes for Flux Cored Arc Welding A530 Specification for Consumable Inserts A5.3 1 Specification for Fluxes for Brazing and Braze Welding ~ _ _ _ _ _ A5.32/A5.32M Specification for Welding Shielding Gases ~~ ~ For ordering information, contact the AWS Order Department, American Welding Society, 550 N.W. LeJ eune Road, Miami, FL 33126. Telephones: (800) 334-9353, (305) 443-9353, ext. 280; FAX (305) 443-7559. 25 Previous page is blank
Copyright American Welding Society Provided by IHS under license with AWS Licensee=Loc 25-27Venezuela/Parlaguan,Puerto la Cr,San Die/5919206111, User=hern Not for Resale, 09/27/2005 07:22:29 MDT No reproduction or networking permitted without license from IHS - - ` , , ` , , , ` , , , , ` , ` ` ` , ` ` , , , ` , ` , ` ` - ` - ` , , ` , , ` , ` , , ` - - -