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Transmission Electron Microscope

Characterization of Materials

Dr M Israr Qadir

TEM is most versatile tool for microstructural investigation


TEM is widely used in industry and academia

Primary objective to investigate the microstructure and


composition of semicondrs, alloys, and biological samples

At very high magnification 50x 150,000x and more

A resolution of 1 Angstrum can be optimized under


optimum conditions

1.

Alignment of electro-optical system


Stability in accelerating voltage
Cleanness of the microscope

2.
3.

History

In 1924, A French scientist de Broglie cleared the path

Electrons can behaves like waves

First TEM was built in 1931 by a German Ernst Ruska.

Principle

Working principle of TEM is similar to Optical microscope

Having slight differences such as


Photons are replaced by electrons
The light source is an electron gun instead of light bulb
The lenses are magnetic as opposed to glass

1.
2.
3.

Principle

A ray of electrons is generated by a filament

Focused by a illumination lens system on the specimen

Electrons penetrate the specimen

imaging lens systems are responsible to generate the


images

Pre-requisites

Pressure should be very low to reduce the interference

Sample must be very thin, so that the electrons can


penetrate the sample

Nanoparticles can be imaged as it is, however, we need


cutting, etching and polishing for bulk materials

Price of the microscope is on the order of 1-4M US $

Spherical aberration

Spherical aberration means it defocuses the electrons which are


scatter with different angles from source

Unfortunately this is inherent problem of electro-optical lens

New microscopes are equipped with SA corrector

With per piece cost of 1 M and is complicated in operation

Operator change the focus where the resolution is best

Chromatic aberration

Reflects the inability of a single lens to focus

Reason lies with difference in energy of the scattered


electron results in variation in energy

The result is an image with slight defocusing.

In early years, chromatic was most damaging aberration