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ANALYTICAL REPORT

TestAmerica Laboratories, Inc.


TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Tel: (314)298-8566
TestAmerica Job ID: 160-2968-1
Client Project/Site: West Lake Landfill
For:
Engineering Management Support, Inc.
7220 W. Jefferson AVE
Suite 406
Lakewood, Colorado 80235
Attn: Mr. Paul Rosasco

Authorized for release by:


7/29/2013 3:20:04 PM
Rhonda Ridenhower, Customer Service Manager
rhonda.ridenhower@testamericainc.com

This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

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Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

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Page 2 of 88

TestAmerica St. Louis

7/29/2013

Case Narrative
Client: Engineering Management Support, Inc.
Project/Site: West Lake Landfill

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TestAmerica Job ID: 160-2968-1

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Job ID: 160-2968-1


Laboratory: TestAmerica St. Louis

Narrative

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CASE NARRATIVE

Client: Engineering Management Support, Inc.

Project: West Lake Landfill

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Report Number: 160-2968-1

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With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.

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TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses
performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the
application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data
have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions
to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written
approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and
disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the
client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
Per client request to report all analytical runs, analyses included in the package that were not used in the final report were re-analyzed due
to QC failures in the analytical sequence
RECEIPT
The samples were received on 07/12/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of
the 2 coolers at receipt time were 2.0 C and 2.0 C.
VOLATILE ORGANIC COMPOUNDS (GC MS)
Samples P2-113-SS (160-2968-1), P2-104-SS (160-2968-2), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), FB@P2-202-SS
(160-2968-5), P2-202-SS (160-2968-6), D-83 (160-2968-7), MW-1204 (160-2968-8), S-82 (160-2968-9), P2-116-SS (160-2968-10), D-93
(160-2968-11), I-9 (160-2968-12), P2-115-SS (160-2968-13), DUPLICATE 03 (160-2968-14) and TRIP BLANK (160-2968-15) were
analyzed for volatile organic compounds (GC MS) in accordance with EPA SW-846 Method 8260C. The samples were analyzed on
07/15/2013, 07/16/2013, 07/17/2013 and 07/18/2013.

Analytical batch 60813

Page 3 of 88

TestAmerica St. Louis

7/29/2013

Case Narrative
Client: Engineering Management Support, Inc.
Project/Site: West Lake Landfill

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TestAmerica Job ID: 160-2968-1

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Job ID: 160-2968-1 (Continued)


Laboratory: TestAmerica St. Louis (Continued)

The continuing calibration verification (CCV) for Chloroethane and Methyl acetate associated with batch 60813 recovered above the upper
control limit. These analytes were not detected above reporting limit in the affected analytes; therefore, the data have been reported.

The laboratory control sample (LCS) for batch 60813 recovered outside control limits for the following analyte: 2-Hexanone. This analyte
was biased high in the LCS and and was not present above the reporting limit in the associated samples; therefore, the data have been
reported.

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The MSD was also outside control limits for 2-Hexanone; this analyte was recovered high in the LCS but was not present above the
reporting limit in the associated samples.

Samples were analyzed at a dilution based on results of screening (due to strong sample odor). The reporting limit has been adjusted for
those analytes reported from the dilution. All other analytes are reported from undiluted analyses in a subsequent batch.

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The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 60813 were outside control limits for Chloroethane. The
associated laboratory control sample (LCS) recovery met acceptance criteria.

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Analytical batch 61806


The continuing calibration verification (CCV) for Chloroethane associated with batch 61806 recovered above the upper control limit
indicating that results for this analyte will be biased high. This analyte was not detected above the reporting limit in the associated
samples; therefore, the data have been reported.

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The laboratory control sample (LCS) for batch 61806 recovered outside control limits for the following analyte: Chloroethane. This analyte
was biased high in the LCS and was not detected above the reporting limit in the associated samples; therefore, the data have been
reported.
Sample, MW-1204 (160-2968-8), was analyzed at a dilution due to the presence of high levels of target analytes. The reporting limit has
been adjusted for those analytes reported from the dilution.
No other difficulties were encountered during the VOCs analysis.
All other quality control parameters were within the acceptance limits.
METALS (ICP)-Total and Dissolved
Samples P2-113-SS (160-2968-1), P2-104-SS (160-2968-2), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), P2-202-SS
(160-2968-6), D-83 (160-2968-7), MW-1204 (160-2968-8), S-82 (160-2968-9), P2-116-SS (160-2968-10), D-93 (160-2968-11), I-9
(160-2968-12), P2-115-SS (160-2968-13) and DUPLICATE 03 (160-2968-14) were analyzed for Metals (ICP) in accordance with EPA
SW-846 Method 6010C. The samples were prepared on 07/16/2013 and analyzed on 07/17/2013 and 07/18/2013.

Analytical batch 61388


The following samples were diluted to bring the concentration of target analytes (calcium, magnesium, and sodium) within the calibration
range. Magnesium also interferes with iron: (160-2968-6 SD), D-83 (160-2968-7), D-93 (160-2968-11), DUPLICATE 03 (160-2968-14), I-9
(160-2968-12), MW-1204 (160-2968-8), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), P2-104-SS (160-2968-2), P2-113-SS
(160-2968-1), P2-115-SS (160-2968-13), P2-202-SS (160-2968-6), P2-202-SS (160-2968-6 MS), P2-202-SS (160-2968-6 MSD), S-82
(160-2968-9). Elevated reporting limits (RLs) are provided.
Due to the high concentration of calcium and magnesium, the matrix spike / matrix spike duplicate (MS/MSD) for batch 60808 could not be
evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria.
The initial calibration verification (ICV) for prep batch 60808 was above the upper control limit for thallium. The affected samples are ND for
thallium and the data is reported with this narrative. The data have been qualified and reported.
Analytical batch 61428
The following samples were diluted to bring the concentration of target analytes (calcium) within the calibration range: D-93
(160-2968-11), I-9 (160-2968-12), MW-1204 (160-2968-8). Elevated reporting limits (RLs) are provided.

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TestAmerica St. Louis

7/29/2013

Case Narrative
Client: Engineering Management Support, Inc.
Project/Site: West Lake Landfill

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TestAmerica Job ID: 160-2968-1

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Job ID: 160-2968-1 (Continued)


Laboratory: TestAmerica St. Louis (Continued)

Analytical batch 61576


The following samples were diluted to bring the concentration of target analytes (calcium, magnesium, and sodium) within the calibration
range. Magnesium also interferes with iron: (160-2968-6 SD), D-83 (160-2968-7), D-93 (160-2968-11), DUPLICATE 03 (160-2968-14), I-9
(160-2968-12), MW-1204 (160-2968-8), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), P2-104-SS (160-2968-2), P2-113-SS
(160-2968-1), P2-115-SS (160-2968-13), P2-202-SS (160-2968-6), P2-202-SS (160-2968-6 MS), P2-202-SS (160-2968-6 MSD), S-82
(160-2968-9). Elevated reporting limits (RLs) are provided.

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No difficulties were encountered during the metals analysis.

All quality control parameters were within the acceptance limits.

DISSOLVED MERCURY
Samples P2-113-SS (160-2968-1), P2-104-SS (160-2968-2), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), P2-202-SS
(160-2968-6), D-83 (160-2968-7), MW-1204 (160-2968-8), S-82 (160-2968-9), P2-116-SS (160-2968-10), D-93 (160-2968-11), I-9
(160-2968-12), P2-115-SS (160-2968-13) and DUPLICATE 03 (160-2968-14) were analyzed for dissolved mercury (CVAA) in accordance
with EPA SW-846 Methods 7470A. The samples were prepared on 07/16/2013 and analyzed on 07/17/2013.

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No difficulties were encountered during the mercury analysis.

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All quality control parameters were within the acceptance limits.

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TOTAL MERCURY
Samples P2-113-SS (160-2968-1), P2-104-SS (160-2968-2), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), P2-202-SS
(160-2968-6), D-83 (160-2968-7), MW-1204 (160-2968-8), S-82 (160-2968-9), P2-116-SS (160-2968-10), D-93 (160-2968-11), I-9
(160-2968-12), P2-115-SS (160-2968-13) and DUPLICATE 03 (160-2968-14) were analyzed for total mercury in accordance with EPA
SW-846 Methods 7470A. The samples were prepared and analyzed on 07/16/2013.

No difficulties were encountered during the mercury analysis.


All quality control parameters were within the acceptance limits.
ANIONS
Samples P2-113-SS (160-2968-1), P2-104-SS (160-2968-2), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), P2-202-SS
(160-2968-6), D-83 (160-2968-7), MW-1204 (160-2968-8), S-82 (160-2968-9), P2-116-SS (160-2968-10), D-93 (160-2968-11), I-9
(160-2968-12), P2-115-SS (160-2968-13) and DUPLICATE 03 (160-2968-14) were analyzed for anions in accordance with EPA Method
300.0. The samples were analyzed on 07/12/2013, 07/13/2013 and 07/16/2013.

The following samples were diluted to bring the concentrations of Chloride, Bromide, and Sulfate within the calibration range in IC batch
62158: D-83 (160-2968-7), D-93 (160-2968-11), DUPLICATE 03 (160-2968-14), I-9 (160-2968-12), MW-1204 (160-2968-8), P2-101-SS
(160-2968-3), P2-104-SD (160-2968-4), P2-113-SS (160-2968-1), P2-115-SS (160-2968-13), P2-116-SS (160-2968-10), P2-202-SS
(160-2968-6), S-82 (160-2968-9). Elevated reporting limits (RLs) are provided.
The matrix spike (MS) recoveries for Bromide in IC batch 62158 were outside control limits. The associated laboratory control sample
(LCS) recovery met acceptance criteria.
No other difficulties were encountered during the anions analysis.
All other quality control parameters were within the acceptance limits.
ALKALINITY
Samples P2-113-SS (160-2968-1), P2-104-SS (160-2968-2), P2-101-SS (160-2968-3), P2-104-SD (160-2968-4), P2-202-SS
(160-2968-6), D-83 (160-2968-7), MW-1204 (160-2968-8), S-82 (160-2968-9), P2-116-SS (160-2968-10), D-93 (160-2968-11), I-9
(160-2968-12), P2-115-SS (160-2968-13) and DUPLICATE 03 (160-2968-14) were analyzed for alkalinity in accordance with EPA Method
310.1. The samples were analyzed on 07/25/2013.

Page 5 of 88

TestAmerica St. Louis

7/29/2013

Case Narrative
Client: Engineering Management Support, Inc.
Project/Site: West Lake Landfill

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TestAmerica Job ID: 160-2968-1

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Job ID: 160-2968-1 (Continued)


Laboratory: TestAmerica St. Louis (Continued)

For the analysis of the associated samples in Alkalinity batch 62899, the following samples were diluted to bring the concentration of
target analytes within the calibration range: D-93 (160-2968-11), I-9 (160-2968-12), MW-1204 (160-2968-8). Elevated reporting limits
(RLs) are provided.

No other difficulties were encountered during the alkalinity analysis.

All other quality control parameters were within the acceptance limits.

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Login Sample Receipt Checklist

Client: Engineering Management Support, Inc.

Job Number: 160-2968-1

Login Number: 2968

List Source: TestAmerica St. Louis

List Number: 1

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Creator: Daniels, Brian J


Question

Answer

Radioactivity wasn't checked or is </= background as measured by a survey


meter.

True

The cooler's custody seal, if present, is intact.

True

Sample custody seals, if present, are intact.

N/A

The cooler or samples do not appear to have been compromised or


tampered with.

True

Samples were received on ice.

True

Cooler Temperature is acceptable.

True

Cooler Temperature is recorded.

True

COC is present.

True

COC is filled out in ink and legible.

True

COC is filled out with all pertinent information.

True

Is the Field Sampler's name present on COC?

N/A

There are no discrepancies between the containers received and the COC.

True

Samples are received within Holding Time.

True

Sample containers have legible labels.

True

Containers are not broken or leaking.

True

Sample collection date/times are provided.

True

Appropriate sample containers are used.

True

Sample bottles are completely filled.

True

Sample Preservation Verified.

True

There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs

True

Containers requiring zero headspace have no headspace or bubble is


<6mm (1/4").

False

Multiphasic samples are not present.

True

Samples do not require splitting or compositing.

True

Residual Chlorine Checked.

N/A

Comment

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1 vial for D-83 and 2 vials for Trip Blank contain


headspace.

TestAmerica St. Louis

Page 9 of 88

7/29/2013

Definitions/Glossary
Client: Engineering Management Support, Inc.
Project/Site: West Lake Landfill

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TestAmerica Job ID: 160-2968-1

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Qualifiers
GC/MS VOA

Qualifier

Qualifier Description

LCS or LCSD exceeds the control limits

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

MS or MSD exceeds the control limits

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Metals
Qualifier

Qualifier Description

Result exceeded calibration range.

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC exceeds the control limits.

MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not
applicable.

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General Chemistry

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Qualifier

Qualifier Description

Compound was found in the blank and sample.

MS or MSD exceeds the control limits

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not
applicable.

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Glossary
Abbreviation

These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis

%R

Percent Recovery

CNF

Contains no Free Liquid

DER

Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN

Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC

Decision level concentration

MDA

Minimum detectable activity

EDL

Estimated Detection Limit

MDC

Minimum detectable concentration

MDL

Method Detection Limit

ML

Minimum Level (Dioxin)

NC

Not Calculated

ND

Not detected at the reporting limit (or MDL or EDL if shown)

PQL

Practical Quantitation Limit

QC

Quality Control

RER

Relative error ratio

RL

Reporting Limit or Requested Limit (Radiochemistry)

RPD

Relative Percent Difference, a measure of the relative difference between two points

TEF

Toxicity Equivalent Factor (Dioxin)

TEQ

Toxicity Equivalent Quotient (Dioxin)

TestAmerica St. Louis

Page 10 of 88

7/29/2013

Method Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Method

Method Description

Protocol

Laboratory

8260C

Volatile Organic Compounds by GC/MS

SW846

TAL SL

6010C

Metals (ICP)

SW846

TAL SL

7470A

Mercury (CVAA)

SW846

TAL SL

300.0

Anions, Ion Chromatography

MCAWW

TAL SL

310.1

Alkalinity

MCAWW

TAL SL

Protocol References:

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MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

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Laboratory References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566

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TestAmerica St. Louis

Page 11 of 88

7/29/2013

Sample Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Lab Sample ID

Client Sample ID

Matrix

Collected

Received

160-2968-1

P2-113-SS

Water

07/11/13 08:50

07/12/13 08:15

160-2968-2

P2-104-SS

Water

07/11/13 09:37

07/12/13 08:15

160-2968-3

P2-101-SS

Water

07/11/13 09:40

07/12/13 08:15

160-2968-4

P2-104-SD

Water

07/11/13 10:29

07/12/13 08:15

160-2968-5

FB@P2-202-SS

Water

07/11/13 12:00

07/12/13 08:15

160-2968-6

P2-202-SS

Water

07/11/13 12:32

07/12/13 08:15

160-2968-7

D-83

Water

07/11/13 13:05

07/12/13 08:15

160-2968-8

MW-1204

Water

07/11/13 14:12

07/12/13 08:15

160-2968-9

S-82

Water

07/11/13 14:32

07/12/13 08:15

160-2968-10

P2-116-SS

Water

07/11/13 15:05

07/12/13 08:15

160-2968-11

D-93

Water

07/11/13 15:40

07/12/13 08:15

160-2968-12

I-9

Water

07/11/13 16:26

07/12/13 08:15

160-2968-13

P2-115-SS

Water

07/11/13 16:36

07/12/13 08:15

160-2968-14

DUPLICATE 03

Water

07/11/13 00:00

07/12/13 08:15

160-2968-15

TRIP BLANK

Water

07/11/13 00:00

07/12/13 08:15

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TestAmerica St. Louis

Page 12 of 88

7/29/2013

Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-113-SS


Analyte

Acetone
Methylene Chloride
Aluminum

Lab Sample ID: 160-2968-1


Result Qualifier

12 J
2.5 J
8500

RL

MDL Unit

20

6.7 ug/L

Dil Fac D Method

8260C

Prep Type

Total/NA

5.0

1.7 ug/L

8260C

Total/NA

200

80 ug/L

6010C

Total/NA

Antimony

4.4 J

10

4.0 ug/L

6010C

Total/NA

Arsenic

7.2 J

10

2.0 ug/L

6010C

Total/NA

Barium

220

50

4.0 ug/L

6010C

Total/NA

Calcium

140000 E

1000

110 ug/L

6010C

Total/NA

Calcium

150000

10000

1100 ug/L

10

6010C

Total/NA

Chromium

24

10

3.1 ug/L

6010C

Total/NA

Cobalt

4.5 J

50

4.0 ug/L

6010C

Total/NA

Iron

7400

100

28 ug/L

6010C

Total/NA

Iron

7600

1000

280 ug/L

10

6010C

Total/NA

Lead

4.6 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

61000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

61000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

100

15

3.3 ug/L

6010C

Total/NA

Nickel
Potassium
Sodium
Vanadium
Zinc

40

13 ug/L

6010C

Total/NA

5400

21 J

5000

1700 ug/L

6010C

Total/NA

23000

1000

320 ug/L

6010C

Total/NA

27 J

50

4.1 ug/L

6010C

Total/NA

48

20

5.2 ug/L

6010C

Total/NA

Barium

180

50

4.0 ug/L

6010C

Dissolved

Calcium

55000 E

1000

110 ug/L

6010C

Dissolved

Calcium

55000

5000

530 ug/L

6010C

Dissolved

100

28 ug/L

6010C

Dissolved

Iron

54 J

Magnesium

31000

1000

130 ug/L

6010C

Dissolved

Manganese

26

15

3.3 ug/L

6010C

Dissolved

Potassium

1800 J

5000

1700 ug/L

6010C

Dissolved

1000

320 ug/L

6010C

Dissolved

20

5.2 ug/L

6010C

Dissolved

0.50

0.050 mg/L

300.0

Total/NA

Sodium

21000

Zinc

6.4 J

Sulfate

20

Alkalinity

270 B

5.0

0.54 mg/L

310.1

Total/NA

Chloride - DL

9.7

4.0

0.40 mg/L

20

300.0

Total/NA

Client Sample ID: P2-104-SS


Analyte

Lab Sample ID: 160-2968-2


RL

MDL Unit

1,4-Dichlorobenzene

7.0

5.0

0.35 ug/L

8260C

Total/NA

2-Hexanone

87

20

0.59 ug/L

8260C

Total/NA

250 J

400

6.6 ug/L

8260C

Total/NA

16 J

20

6.7 ug/L

8260C

Total/NA

100

5.0 ug/L

8260C

Total/NA

4-Methyl-2-pentanone (MIBK)
Acetone
Benzene

Result Qualifier

1800

Dil Fac D Method

Prep Type

Chloroethane

5.5 J *

10

0.38 ug/L

8260C

Total/NA

Ethylbenzene

25

5.0

0.30 ug/L

8260C

Total/NA

Isopropylbenzene

2.6 J

5.0

0.26 ug/L

8260C

Total/NA

Methyl tert-butyl ether

6.3

5.0

0.40 ug/L

8260C

Total/NA

m-Xylene & p-Xylene

44

5.0

0.57 ug/L

8260C

Total/NA

o-Xylene

21

5.0

0.32 ug/L

8260C

Total/NA

Styrene

1.3 J

5.0

0.35 ug/L

8260C

Total/NA

Toluene

140

5.0

1.0 ug/L

8260C

Total/NA

This Detection Summary does not include radiochemical test results.

TestAmerica St. Louis

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-104-SS (Continued)


Analyte

Result Qualifier

Lab Sample ID: 160-2968-2


RL

MDL Unit

Xylenes, Total

65

10

0.85 ug/L

8260C

Total/NA

Antimony

4.0 J

10

4.0 ug/L

6010C

Total/NA

Arsenic

2.6 J

10

2.0 ug/L

6010C

Total/NA

Barium

100

Calcium

89000 E

Calcium

97000

Dil Fac D Method

Prep Type

50

4.0 ug/L

6010C

Total/NA

1000

110 ug/L

6010C

Total/NA

10000

1100 ug/L

10

6010C

Total/NA

Iron

1800

100

28 ug/L

6010C

Total/NA

Iron

1800

1000

280 ug/L

10

6010C

Total/NA

Lead

1.7 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

53000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

54000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

40

15

3.3 ug/L

6010C

Total/NA

5000

1700 ug/L

6010C

Total/NA

1000

320 ug/L

6010C

Total/NA

Potassium
Sodium

2200 J
12000

Arsenic

2.2 J

10

2.0 ug/L

6010C

Dissolved

Barium

100

50

4.0 ug/L

6010C

Dissolved

Calcium

85000 E

1000

110 ug/L

6010C

Dissolved

Calcium

89000

5000

530 ug/L

6010C

Dissolved

Chromium

10

3.1 ug/L

6010C

Dissolved

1800

100

28 ug/L

6010C

Dissolved

Magnesium

49000

1000

130 ug/L

6010C

Dissolved

Manganese

39

15

3.3 ug/L

6010C

Dissolved

Potassium

2200 J

5000

1700 ug/L

6010C

Dissolved

Iron

3.2 J

Sodium

12000

1000

320 ug/L

6010C

Dissolved

Mercury

0.064 J

0.20

0.060 ug/L

7470A

Dissolved

Chloride

4.8

0.20

0.020 mg/L

300.0

Total/NA

Sulfate

1.0

0.50

0.050 mg/L

300.0

Total/NA

Alkalinity

440 B

5.0

0.54 mg/L

310.1

Total/NA

Client Sample ID: P2-101-SS


Analyte

Lab Sample ID: 160-2968-3


RL

MDL Unit

0.52 J

5.0

0.35 ug/L

8260C

Total/NA

Acetone

34

20

6.7 ug/L

8260C

Total/NA

Benzene

0.92 J

5.0

0.25 ug/L

8260C

Total/NA

3.3 J

5.0

0.38 ug/L

8260C

Total/NA

0.51 J

5.0

0.40 ug/L

8260C

Total/NA

Arsenic

3.4 J

10

2.0 ug/L

6010C

Total/NA

Barium

530

50

4.0 ug/L

6010C

Total/NA

Calcium

150000 E

1000

110 ug/L

6010C

Total/NA

Calcium

160000

10000

1100 ug/L

10

6010C

Total/NA

10

3.1 ug/L

6010C

Total/NA

100

28 ug/L

6010C

Total/NA

1,4-Dichlorobenzene

Chlorobenzene
Methyl tert-butyl ether

Result Qualifier

Dil Fac D Method

Prep Type

Chromium

4.8 J

Iron

590

Iron

580 J

1000

280 ug/L

10

6010C

Total/NA

Lead

2.5 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

98000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

97000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

48

15

3.3 ug/L

6010C

Total/NA

Nickel

15 J

40

13 ug/L

6010C

Total/NA

5000

1700 ug/L

6010C

Total/NA

Potassium

16000

This Detection Summary does not include radiochemical test results.

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-101-SS (Continued)


Analyte

Sodium
Sodium

Result Qualifier

110000 E

RL

MDL Unit

1000

320 ug/L

Dil Fac D Method

6010C

Prep Type

Total/NA

10000

3200 ug/L

10

6010C

Total/NA

8.6 J

20

5.2 ug/L

6010C

Total/NA

Arsenic

3.2 J

10

2.0 ug/L

6010C

Dissolved

Barium

480

50

4.0 ug/L

6010C

Dissolved

Beryllium

5.7

5.0

0.61 ug/L

6010C

Dissolved

Calcium

130000 E

1000

110 ug/L

6010C

Dissolved

Calcium

150000

5000

530 ug/L

6010C

Dissolved

Zinc

99000

Lab Sample ID: 160-2968-3

Chromium

3.5 J

10

3.1 ug/L

6010C

Dissolved

Iron

78 J

100

28 ug/L

6010C

Dissolved

Lead

2.1 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

86000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

90000

5000

660 ug/L

6010C

Dissolved

Manganese

68

15

3.3 ug/L

6010C

Dissolved

Nickel

40

13 ug/L

6010C

Dissolved

Potassium

15000

5000

1700 ug/L

6010C

Dissolved

Sodium

92000

1000

320 ug/L

6010C

Dissolved

50

4.1 ug/L

6010C

Dissolved

Vanadium
Zinc
Mercury
Nitrate as N

15 J

10 J
16 J

20

5.2 ug/L

6010C

Dissolved

0.17 J

0.20

0.060 ug/L

7470A

Dissolved

0.030

0.020

0.0040 mg/L

300.0

Total/NA

Bromide

1.5

0.25

0.025 mg/L

300.0

Total/NA

Sulfate

6.0

0.50

0.050 mg/L

300.0

Total/NA

Iodide

1.0

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity

760 B

5.0

0.54 mg/L

310.1

Total/NA

Chloride - DL2

160

20

2.0 mg/L

100

300.0

Total/NA

Client Sample ID: P2-104-SD


Analyte

Lab Sample ID: 160-2968-4


RL

MDL Unit

11

5.0

0.35 ug/L

8260C

Total/NA

3200

500

9.8 ug/L

8260C

Total/NA

42

20

0.59 ug/L

8260C

Total/NA

110

20

0.33 ug/L

8260C

Total/NA

Acetone

3800

500

170 ug/L

8260C

Total/NA

Benzene

800

25

1.3 ug/L

8260C

Total/NA

Chlorobenzene

4.6 J

5.0

0.38 ug/L

8260C

Total/NA

Chloroethane

4.4 J *

10

0.38 ug/L

8260C

Total/NA

Ethylbenzene

49

5.0

0.30 ug/L

8260C

Total/NA

Isopropylbenzene

5.9

5.0

0.26 ug/L

8260C

Total/NA

Methyl tert-butyl ether

3.8 J

5.0

0.40 ug/L

8260C

Total/NA

m-Xylene & p-Xylene

100

5.0

0.57 ug/L

8260C

Total/NA

o-Xylene

42

5.0

0.32 ug/L

8260C

Total/NA

Styrene

2.4 J

5.0

0.35 ug/L

8260C

Total/NA

Toluene

430

25

5.0 ug/L

8260C

Total/NA

Xylenes, Total

140

10

0.85 ug/L

8260C

Total/NA

Antimony

4.4 J

10

4.0 ug/L

6010C

Total/NA

Arsenic

12

10

2.0 ug/L

6010C

Total/NA

Barium

800

50

4.0 ug/L

6010C

Total/NA

Calcium

110000 E

1000

110 ug/L

6010C

Total/NA

1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)

Result Qualifier

Dil Fac D Method

Prep Type

This Detection Summary does not include radiochemical test results.

TestAmerica St. Louis

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-104-SD (Continued)


Analyte

RL

MDL Unit

130000

10000

1100 ug/L

10

6010C

Total/NA

Chromium

16

10

3.1 ug/L

6010C

Total/NA

Cobalt

5.0 J

50

4.0 ug/L

6010C

Total/NA

Calcium

Result Qualifier

Lab Sample ID: 160-2968-4


Dil Fac D Method

Prep Type

Iron

8900

100

28 ug/L

6010C

Total/NA

Iron

9000

1000

280 ug/L

10

6010C

Total/NA

10

1.5 ug/L

6010C

Total/NA

Lead

2.0 J

Magnesium

66000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

66000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

160

15

3.3 ug/L

6010C

Total/NA

40

13 ug/L

6010C

Total/NA

5000

1700 ug/L

6010C

Total/NA

1000

320 ug/L

6010C

Total/NA

Nickel
Potassium

31 J
20000

Sodium

130000 E

Sodium

120000

10000

3200 ug/L

10

6010C

Total/NA

11 J

50

4.1 ug/L

6010C

Total/NA

Zinc

8.9 J

20

5.2 ug/L

6010C

Total/NA

Arsenic

14

10

2.0 ug/L

6010C

Dissolved

Vanadium

Barium

1000

50

4.0 ug/L

6010C

Dissolved

Calcium

110000 E

1000

110 ug/L

6010C

Dissolved

Calcium

140000

5000

530 ug/L

6010C

Dissolved

19

10

3.1 ug/L

6010C

Dissolved

Chromium
Cobalt

50

4.0 ug/L

6010C

Dissolved

Iron

13000

100

28 ug/L

6010C

Dissolved

Iron

14000

500

140 ug/L

6010C

Dissolved

1.6 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

66000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

71000

5000

660 ug/L

6010C

Dissolved

Manganese

160

15

3.3 ug/L

6010C

Dissolved

40

13 ug/L

6010C

Dissolved

5000

1700 ug/L

6010C

Dissolved

Lead

Nickel
Potassium

5.8 J

36 J
23000

Sodium

160000 E

1000

320 ug/L

6010C

Dissolved

Sodium

170000

5000

1600 ug/L

6010C

Dissolved

16 J

50

4.1 ug/L

6010C

Dissolved

Mercury

0.16 J

0.20

0.060 ug/L

7470A

Dissolved

Bromide

0.64

0.25

0.025 mg/L

300.0

Total/NA

Iodide

0.45 J

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity

580 B

5.0

0.54 mg/L

310.1

Total/NA

39

10

1.0 mg/L

20

300.0

Total/NA

180

20

2.0 mg/L

100

300.0

Total/NA

Vanadium

Sulfate - DL
Chloride - DL2

Client Sample ID: FB@P2-202-SS


Analyte

Acetone

Lab Sample ID: 160-2968-5


Result Qualifier

12 J

RL

MDL Unit

20

6.7 ug/L

Client Sample ID: P2-202-SS


Analyte

Dil Fac D Method

8260C

Prep Type

Total/NA

Lab Sample ID: 160-2968-6


RL

MDL Unit

1,1,2-Trichloroethane

Result Qualifier

37

5.0

0.57 ug/L

Dil Fac D Method

8260C

Prep Type

Total/NA

Acetone

30

20

6.7 ug/L

8260C

Total/NA

Benzene

34

5.0

0.25 ug/L

8260C

Total/NA

This Detection Summary does not include radiochemical test results.

TestAmerica St. Louis

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-202-SS (Continued)


Analyte

RL

MDL Unit

4.3 J

5.0

0.40 ug/L

8260C

Total/NA

Aluminum

98 J

200

80 ug/L

6010C

Total/NA

Arsenic

7.4 J

10

2.0 ug/L

6010C

Total/NA

Methyl tert-butyl ether

Result Qualifier

Lab Sample ID: 160-2968-6

Barium

580

Calcium

180000 E

Calcium

200000

Cobalt

Prep Type

50

4.0 ug/L

6010C

Total/NA

1000

110 ug/L

6010C

Total/NA

10000

1100 ug/L

10

6010C

Total/NA

50

4.0 ug/L

6010C

Total/NA

Iron

4900

100

28 ug/L

6010C

Total/NA

Iron

5000

1000

280 ug/L

10

6010C

Total/NA

10

1.5 ug/L

6010C

Total/NA

Lead

6.9 J

Dil Fac D Method

2.1 J

Magnesium

78000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

79000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

940

Nickel
Potassium
Sodium

15

3.3 ug/L

6010C

Total/NA

21 J

40

13 ug/L

6010C

Total/NA

3100 J

5000

1700 ug/L

6010C

Total/NA

1000

320 ug/L

6010C

Total/NA

14000

Zinc

7.0 J

20

5.2 ug/L

6010C

Total/NA

Arsenic

6.8 J

10

2.0 ug/L

6010C

Dissolved

Barium

550

50

4.0 ug/L

6010C

Dissolved

Calcium

160000 E

1000

110 ug/L

6010C

Dissolved

Calcium

200000

5000

530 ug/L

6010C

Dissolved

50

4.0 ug/L

6010C

Dissolved

Cobalt

6.3 J

Iron

4600

100

28 ug/L

6010C

Dissolved

Iron

4900

500

140 ug/L

6010C

Dissolved

2.9 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

71000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

76000

5000

660 ug/L

6010C

Dissolved

Manganese

870

15

3.3 ug/L

6010C

Dissolved

20 J

40

13 ug/L

6010C

Dissolved

3100 J

5000

1700 ug/L

6010C

Dissolved

1000

320 ug/L

6010C

Dissolved

6.1 J

20

5.2 ug/L

6010C

Dissolved

Mercury

0.14 J

0.20

0.060 ug/L

7470A

Total/NA

Mercury

0.20

0.20

0.060 ug/L

7470A

Dissolved

Bromide

0.51

0.25

0.025 mg/L

300.0

Total/NA

Iodide

0.14 J

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity

610 B

5.0

0.54 mg/L

310.1

Total/NA

Lead

Nickel
Potassium
Sodium
Zinc

13000

Sulfate - DL

58

10

1.0 mg/L

20

300.0

Total/NA

Chloride - DL2

84

20

2.0 mg/L

100

300.0

Total/NA

Client Sample ID: D-83


Analyte

Lab Sample ID: 160-2968-7


RL

MDL Unit

2.0 J

5.0

0.38 ug/L

8260C

Total/NA

0.68 J

5.0

0.40 ug/L

8260C

Total/NA

Antimony

5.0 J

10

4.0 ug/L

6010C

Total/NA

Arsenic

2.8 J

10

2.0 ug/L

6010C

Total/NA

50

4.0 ug/L

6010C

Total/NA

1000

110 ug/L

6010C

Total/NA

10000

1100 ug/L

10

6010C

Total/NA

Chlorobenzene
Methyl tert-butyl ether

Result Qualifier

Barium

1800

Calcium

110000 E

Calcium

120000

Dil Fac D Method

Prep Type

This Detection Summary does not include radiochemical test results.

TestAmerica St. Louis

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-83 (Continued)

Lab Sample ID: 160-2968-7

Analyte

Result Qualifier

Iron

17000

Lead
Magnesium
Manganese

2.8 J
42000

RL

MDL Unit

100

28 ug/L

Dil Fac D Method

6010C

Prep Type

Total/NA

10

1.5 ug/L

6010C

Total/NA

1000

130 ug/L

6010C

Total/NA

410

15

3.3 ug/L

6010C

Total/NA

Potassium

45000

5000

1700 ug/L

6010C

Total/NA

Sodium

57000

1000

320 ug/L

6010C

Total/NA

20

5.2 ug/L

6010C

Total/NA

50

4.0 ug/L

6010C

Dissolved

Zinc
Barium
Calcium
Calcium
Iron
Lead

5.4 J
1700

1000

110 ug/L

6010C

Dissolved

110000

98000 E

5000

530 ug/L

6010C

Dissolved

16000

100

28 ug/L

6010C

Dissolved

10

1.5 ug/L

6010C

Dissolved

2.9 J

Magnesium

38000

1000

130 ug/L

6010C

Dissolved

Manganese

390

15

3.3 ug/L

6010C

Dissolved

Potassium

44000

5000

1700 ug/L

6010C

Dissolved

Sodium

53000

1000

320 ug/L

6010C

Dissolved

Mercury

0.099 J

0.20

0.060 ug/L

7470A

Total/NA

Mercury

0.29

0.20

0.060 ug/L

7470A

Dissolved

Bromide

0.88

0.25

0.025 mg/L

300.0

Total/NA

Sulfate

8.2

0.50

0.050 mg/L

300.0

Total/NA

Alkalinity

690 B

5.0

0.54 mg/L

310.1

Total/NA

4.0

0.40 mg/L

20

300.0

Total/NA

Chloride - DL

54

Client Sample ID: MW-1204


Analyte

2-Butanone (MEK)

Lab Sample ID: 160-2968-8


Result Qualifier

1900

RL

MDL Unit

200

3.9 ug/L

Dil Fac D Method

8260C

Prep Type

Total/NA

2-Hexanone

8.5 J

20

0.59 ug/L

8260C

Total/NA

4-Methyl-2-pentanone (MIBK)

22

20

0.33 ug/L

8260C

Total/NA

3300

1000

330 ug/L

8260C

Total/NA

Acetone
Benzene

1.1 J

5.0

0.25 ug/L

8260C

Total/NA

Methyl tert-butyl ether

1.9 J

5.0

0.40 ug/L

8260C

Total/NA

50

10 ug/L

8260C

Total/NA

Toluene

1700

Aluminum

160 J

200

80 ug/L

6010C

Total/NA

Arsenic

5.9 J

10

2.0 ug/L

6010C

Total/NA

50

4.0 ug/L

6010C

Total/NA

1000

110 ug/L

6010C

Total/NA

Barium

1300

Calcium

260000 E

Calcium

330000

10000

1100 ug/L

10

6010C

Total/NA

40

10

3.1 ug/L

6010C

Total/NA

Iron

12000

100

28 ug/L

6010C

Total/NA

Iron

13000

1000

280 ug/L

10

6010C

Total/NA

2.4 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

150000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

150000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

120

15

3.3 ug/L

6010C

Total/NA

Potassium

7300

5000

1700 ug/L

6010C

Total/NA

Sodium

120000 E

1000

320 ug/L

6010C

Total/NA

Sodium

120000

10000

3200 ug/L

10

6010C

Total/NA

Chromium

Lead

Vanadium

7.0 J

50

4.1 ug/L

6010C

Total/NA

Zinc

14 J

20

5.2 ug/L

6010C

Total/NA

This Detection Summary does not include radiochemical test results.

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: MW-1204 (Continued)


Analyte

Aluminum
Arsenic

Result Qualifier

Lab Sample ID: 160-2968-8


RL

MDL Unit

95 J

200

80 ug/L

Dil Fac D Method

6010C

Prep Type

Dissolved

4.6 J

10

2.0 ug/L

6010C

Dissolved

50

4.0 ug/L

6010C

Dissolved

Barium

1100

Calcium

230000 E

1000

110 ug/L

6010C

Dissolved

Calcium

290000 E

5000

530 ug/L

6010C

Dissolved

Calcium

300000

10000

1100 ug/L

10

6010C

Dissolved

Chromium

32

10

3.1 ug/L

6010C

Dissolved

Iron

11000

100

28 ug/L

6010C

Dissolved

Iron

12000

500

140 ug/L

6010C

Dissolved

2.4 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

130000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

130000

5000

660 ug/L

6010C

Dissolved

Lead

Manganese

110

15

3.3 ug/L

6010C

Dissolved

6100

5000

1700 ug/L

6010C

Dissolved

Sodium

100000 E

1000

320 ug/L

6010C

Dissolved

Sodium

100000

5000

1600 ug/L

6010C

Dissolved

Potassium

Vanadium

6.6 J

50

4.1 ug/L

6010C

Dissolved

Mercury

0.11 J

0.20

0.060 ug/L

7470A

Total/NA

Mercury

0.31

0.20

0.060 ug/L

7470A

Dissolved

Bromide

1.0

0.25

0.025 mg/L

300.0

Total/NA

6.1

Sulfate

0.50

0.050 mg/L

300.0

Total/NA

Iodide

0.20 J

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity - DL

1100 B

10

1.1 mg/L

310.1

Total/NA

40

4.0 mg/L

200

300.0

Total/NA

Chloride - DL2

280

Client Sample ID: S-82


Analyte

Lab Sample ID: 160-2968-9


RL

MDL Unit

2-Butanone (MEK)

7.8 J

20

0.39 ug/L

8260C

Total/NA

Acetone

23

20

6.7 ug/L

8260C

Total/NA

Chlorobenzene

1.0 J

5.0

0.38 ug/L

8260C

Total/NA

0.42 J

5.0

0.16 ug/L

8260C

Total/NA

Antimony

4.8 J

10

4.0 ug/L

6010C

Total/NA

Arsenic

200

10

2.0 ug/L

6010C

Total/NA

Barium

790

50

4.0 ug/L

6010C

Total/NA

Calcium

160000 E

1000

110 ug/L

6010C

Total/NA

Calcium

190000

10000

1100 ug/L

10

6010C

Total/NA

50

4.0 ug/L

6010C

Total/NA

cis-1,2-Dichloroethene

Cobalt

Result Qualifier

11 J

Dil Fac D Method

Prep Type

Iron

35000

100

28 ug/L

6010C

Total/NA

Iron

36000

1000

280 ug/L

10

6010C

Total/NA

5.3 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

81000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

83000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

2200

15

3.3 ug/L

6010C

Total/NA

40

13 ug/L

6010C

Total/NA

5000

1700 ug/L

6010C

Total/NA

2.7 J

15

2.7 ug/L

6010C

Total/NA

Sodium

230000 E

1000

320 ug/L

6010C

Total/NA

Sodium

220000

10000

3200 ug/L

10

6010C

Total/NA

20

5.2 ug/L

6010C

Total/NA

Lead

Nickel
Potassium
Selenium

Zinc

26 J
12000

7.1 J

This Detection Summary does not include radiochemical test results.

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: S-82 (Continued)


Analyte

Arsenic

Lab Sample ID: 160-2968-9


Result Qualifier

210

RL

MDL Unit

10

2.0 ug/L

Dil Fac D Method

6010C

Prep Type

Dissolved

Barium

790

50

4.0 ug/L

6010C

Dissolved

Calcium

160000 E

1000

110 ug/L

6010C

Dissolved

Calcium

200000

5000

530 ug/L

6010C

Dissolved

50

4.0 ug/L

6010C

Dissolved

Cobalt

9.9 J

Iron

35000

100

28 ug/L

6010C

Dissolved

Iron

37000

500

140 ug/L

6010C

Dissolved

3.3 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

77000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

81000

5000

660 ug/L

6010C

Dissolved

Manganese

2100

15

3.3 ug/L

6010C

Dissolved

40

13 ug/L

6010C

Dissolved

Lead

Nickel
Potassium

25 J

5000

1700 ug/L

6010C

Dissolved

Sodium

220000 E

1000

320 ug/L

6010C

Dissolved

Sodium

230000

5000

1600 ug/L

6010C

Dissolved

0.20

0.060 ug/L

7470A

Total/NA

Mercury
Mercury

12000

0.065 J
0.23

0.20

0.060 ug/L

7470A

Dissolved

0.0072 J

0.020

0.0040 mg/L

300.0

Total/NA

Bromide

2.9

0.25

0.025 mg/L

300.0

Total/NA

Sulfate

15

0.50

0.050 mg/L

300.0

Total/NA

Iodide

0.30 J

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity

960 B

5.0

0.54 mg/L

310.1

Total/NA

Chloride - DL2

220

40

4.0 mg/L

200

300.0

Total/NA

Nitrate as N

Client Sample ID: P2-116-SS


Analyte

Barium
Calcium

Lab Sample ID: 160-2968-10


Result Qualifier

RL

MDL Unit

73

50

4.0 ug/L

Dil Fac D Method

6010C

Prep Type

Total/NA

43000

1000

110 ug/L

6010C

Total/NA

Copper

5.3 J

25

4.6 ug/L

6010C

Total/NA

Lead

1.6 J

10

1.5 ug/L

6010C

Total/NA

1000

130 ug/L

6010C

Total/NA

3.8 J

15

3.3 ug/L

6010C

Total/NA

3800 J

5000

1700 ug/L

6010C

Total/NA

53000

1000

320 ug/L

6010C

Total/NA

Zinc

24

20

5.2 ug/L

6010C

Total/NA

Barium

69

50

4.0 ug/L

6010C

Dissolved

Calcium

40000

1000

110 ug/L

6010C

Dissolved

Magnesium

29000

1000

130 ug/L

6010C

Dissolved

5000

1700 ug/L

6010C

Dissolved

49000

1000

320 ug/L

6010C

Dissolved

24

20

5.2 ug/L

6010C

Dissolved

Magnesium
Manganese
Potassium
Sodium

Potassium
Sodium
Zinc

31000

3600 J

Mercury

0.13 J

0.20

0.060 ug/L

7470A

Total/NA

Mercury

0.19 J

0.20

0.060 ug/L

7470A

Dissolved

Nitrate as N

0.17

0.020

0.0040 mg/L

300.0

Total/NA

Chloride

3.5

0.20

0.020 mg/L

300.0

Total/NA

Alkalinity

300 B

5.0

0.54 mg/L

310.1

Total/NA

10

1.0 mg/L

20

300.0

Total/NA

Sulfate - DL

34

Client Sample ID: D-93

Lab Sample ID: 160-2968-11

This Detection Summary does not include radiochemical test results.

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-93 (Continued)


Analyte

Lab Sample ID: 160-2968-11


RL

MDL Unit

1,1-Dichloroethane

3.5 J

5.0

0.39 ug/L

8260C

Total/NA

Benzene

1.9 J

5.0

0.25 ug/L

8260C

Total/NA

cis-1,2-Dichloroethene

29

5.0

0.16 ug/L

8260C

Total/NA

Vinyl chloride

Result Qualifier

Dil Fac D Method

Prep Type

30

5.0

0.43 ug/L

8260C

Total/NA

Aluminum

200

200

80 ug/L

6010C

Total/NA

Antimony

4.3 J

10

4.0 ug/L

6010C

Total/NA

2.3 J

10

2.0 ug/L

6010C

Total/NA

50

4.0 ug/L

6010C

Total/NA

Arsenic
Barium

1400

Calcium

240000 E

Calcium

290000

1000

110 ug/L

6010C

Total/NA

10000

1100 ug/L

10

6010C

Total/NA

Iron

21000

100

28 ug/L

6010C

Total/NA

Iron

21000

1000

280 ug/L

10

6010C

Total/NA

Lead

3.7 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

80000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

81000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

420

15

3.3 ug/L

6010C

Total/NA

17000

5000

1700 ug/L

6010C

Total/NA

1000

320 ug/L

6010C

Total/NA

10000

3200 ug/L

10

6010C

Total/NA

10

2.0 ug/L

6010C

Dissolved

Potassium
Sodium

210000 E

Sodium

200000

Arsenic

2.8 J

Barium

1300

50

4.0 ug/L

6010C

Dissolved

Calcium

230000 E

1000

110 ug/L

6010C

Dissolved

Calcium

280000 E

5000

530 ug/L

6010C

Dissolved

Calcium

290000

10000

1100 ug/L

10

6010C

Dissolved

Iron

20000

100

28 ug/L

6010C

Dissolved

Iron

20000

500

140 ug/L

6010C

Dissolved

2.5 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

76000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

75000

5000

660 ug/L

6010C

Dissolved

Manganese

400

15

3.3 ug/L

6010C

Dissolved

17000

5000

1700 ug/L

6010C

Dissolved

Lead

Potassium
Sodium

200000 E

1000

320 ug/L

6010C

Dissolved

Sodium

190000

5000

1600 ug/L

6010C

Dissolved

5.4 J

20

5.2 ug/L

6010C

Dissolved

Mercury

0.12 J

0.20

0.060 ug/L

7470A

Total/NA

Mercury

0.19 J

0.20

0.060 ug/L

7470A

Dissolved

0.0072 J

0.020

0.0040 mg/L

300.0

Total/NA

Bromide

4.1

0.25

0.025 mg/L

300.0

Total/NA

Sulfate

12

0.50

0.050 mg/L

300.0

Total/NA

Iodide

0.36 J

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity - DL

1000 B

10

1.1 mg/L

310.1

Total/NA

40

4.0 mg/L

200

300.0

Total/NA

Zinc

Nitrate as N

Chloride - DL2

330

Client Sample ID: I-9


Analyte

Lab Sample ID: 160-2968-12


RL

MDL Unit

Acetone

Result Qualifier

18 J

20

6.7 ug/L

Dil Fac D Method

8260C

Prep Type

Total/NA

Vinyl chloride

2.5 J

5.0

0.43 ug/L

8260C

Total/NA

Aluminum

190 J

200

80 ug/L

6010C

Total/NA

Antimony

5.6 J

10

4.0 ug/L

6010C

Total/NA

This Detection Summary does not include radiochemical test results.

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: I-9 (Continued)


Analyte

Arsenic

Lab Sample ID: 160-2968-12


Result Qualifier

26

Barium

1500

Calcium

220000 E

Calcium

RL

MDL Unit

10

2.0 ug/L

Dil Fac D Method

6010C

Prep Type

Total/NA

50

4.0 ug/L

6010C

Total/NA

1000

110 ug/L

6010C

Total/NA

270000

10000

1100 ug/L

10

6010C

Total/NA

Iron

35000

100

28 ug/L

6010C

Total/NA

Iron

36000

1000

280 ug/L

10

6010C

Total/NA

Lead

4.1 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

73000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

74000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

1300

15

3.3 ug/L

6010C

Total/NA

40

13 ug/L

6010C

Total/NA

5000

1700 ug/L

6010C

Total/NA

Nickel
Potassium

14 J
21000

Sodium

230000 E

Sodium

220000

1000

320 ug/L

6010C

Total/NA

10000

3200 ug/L

10

6010C

Total/NA

Zinc

6.2 J

20

5.2 ug/L

6010C

Total/NA

Antimony

4.2 J

10

4.0 ug/L

6010C

Dissolved

Arsenic

24

10

2.0 ug/L

6010C

Dissolved

Barium

1500

50

4.0 ug/L

6010C

Dissolved

Calcium

210000 E

1000

110 ug/L

6010C

Dissolved

Calcium

260000 E

5000

530 ug/L

6010C

Dissolved

Calcium

270000

10000

1100 ug/L

10

6010C

Dissolved

Iron

33000

100

28 ug/L

6010C

Dissolved

Iron

34000

500

140 ug/L

6010C

Dissolved

2.9 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

68000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

69000

5000

660 ug/L

6010C

Dissolved

Manganese

1200

15

3.3 ug/L

6010C

Dissolved

40

13 ug/L

6010C

Dissolved

5000

1700 ug/L

6010C

Dissolved

Lead

Nickel
Potassium

13 J
21000

Sodium

220000 E

1000

320 ug/L

6010C

Dissolved

Sodium

220000

5000

1600 ug/L

6010C

Dissolved

5.4 J

20

5.2 ug/L

6010C

Dissolved

Mercury

0.10 J

0.20

0.060 ug/L

7470A

Total/NA

Mercury

0.18 J

0.20

0.060 ug/L

7470A

Dissolved

0.0080 J

0.020

0.0040 mg/L

300.0

Total/NA

3.5

0.25

0.025 mg/L

300.0

Total/NA

Sulfate

0.58

0.50

0.050 mg/L

300.0

Total/NA

Iodide

0.36 J

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity - DL

1100 B

10

1.1 mg/L

310.1

Total/NA

40

4.0 mg/L

200

300.0

Total/NA

Zinc

Nitrate as N
Bromide

Chloride - DL2

300

Client Sample ID: P2-115-SS


Analyte

Lab Sample ID: 160-2968-13


RL

MDL Unit

Acetone

Result Qualifier

16 J

20

6.7 ug/L

Dil Fac D Method

8260C

Prep Type

Total/NA

Antimony

4.3 J

10

4.0 ug/L

6010C

Total/NA

Arsenic

6.0 J

10

2.0 ug/L

6010C

Total/NA

Barium

330

50

4.0 ug/L

6010C

Total/NA

Calcium

160000 E

1000

110 ug/L

6010C

Total/NA

Calcium

180000

10000

1100 ug/L

10

6010C

Total/NA

This Detection Summary does not include radiochemical test results.

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Page 22 of 88

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-115-SS (Continued)


Analyte

Cobalt

Result Qualifier

15 J

Lab Sample ID: 160-2968-13


RL

MDL Unit

50

4.0 ug/L

Dil Fac D Method

Prep Type

6010C

Total/NA

Iron

1500

100

28 ug/L

6010C

Total/NA

Iron

1500

1000

280 ug/L

10

6010C

Total/NA

Lead

2.8 J

10

1.5 ug/L

6010C

Total/NA

Magnesium

82000 E

1000

130 ug/L

6010C

Total/NA

Magnesium

84000

10000

1300 ug/L

10

6010C

Total/NA

Manganese

52

15

3.3 ug/L

6010C

Total/NA

Nickel

43

40

13 ug/L

6010C

Total/NA

5000

1700 ug/L

6010C

Total/NA

1000

320 ug/L

6010C

Total/NA

Potassium
Sodium

2800 J
62000

Zinc

7.1 J

20

5.2 ug/L

6010C

Total/NA

Arsenic

5.1 J

10

2.0 ug/L

6010C

Dissolved

Barium

320

50

4.0 ug/L

6010C

Dissolved

Calcium

160000 E

1000

110 ug/L

6010C

Dissolved

Calcium

180000

5000

530 ug/L

6010C

Dissolved

50

4.0 ug/L

6010C

Dissolved

Cobalt

20 J

Iron

1500

100

28 ug/L

6010C

Dissolved

Iron

1600

500

140 ug/L

6010C

Dissolved

Lead

1.8 J

10

1.5 ug/L

6010C

Dissolved

Magnesium

78000 E

1000

130 ug/L

6010C

Dissolved

Magnesium

79000

5000

660 ug/L

6010C

Dissolved

Manganese

51

15

3.3 ug/L

6010C

Dissolved

Nickel

44

40

13 ug/L

6010C

Dissolved

5000

1700 ug/L

6010C

Dissolved

Potassium

3000 J

Sodium

60000

1000

320 ug/L

6010C

Dissolved

Mercury

0.083 J

0.20

0.060 ug/L

7470A

Total/NA

Mercury

0.16 J

0.20

0.060 ug/L

7470A

Dissolved

Bromide

1.2

0.25

0.025 mg/L

300.0

Total/NA

Sulfate

17

0.50

0.050 mg/L

300.0

Total/NA

Iodide

0.13 J

1.0

0.10 mg/L

300.0

Total/NA

Alkalinity

560 B

5.0

0.54 mg/L

310.1

Total/NA

Chloride - DL2

220

20

2.0 mg/L

100

300.0

Total/NA

Client Sample ID: DUPLICATE 03


Analyte

Lab Sample ID: 160-2968-14


RL

MDL Unit

Acetone

9.7 J

20

6.7 ug/L

8260C

Total/NA

Chlorobenzene

2.0 J

5.0

0.38 ug/L

8260C

Total/NA

0.71 J

5.0

0.40 ug/L

8260C

Total/NA

Antimony

4.5 J

10

4.0 ug/L

6010C

Total/NA

Arsenic

3.2 J

10

2.0 ug/L

6010C

Total/NA

50

4.0 ug/L

6010C

Total/NA

1000

110 ug/L

6010C

Total/NA

Methyl tert-butyl ether

Result Qualifier

Dil Fac D Method

Prep Type

Barium

1700

Calcium

100000 E

Calcium

110000

10000

1100 ug/L

10

6010C

Total/NA

16000

100

28 ug/L

6010C

Total/NA

10

1.5 ug/L

6010C

Total/NA

Iron
Lead

2.4 J

Magnesium

41000

1000

130 ug/L

6010C

Total/NA

Manganese

400

15

3.3 ug/L

6010C

Total/NA

Potassium

43000

5000

1700 ug/L

6010C

Total/NA

Sodium

54000

1000

320 ug/L

6010C

Total/NA

This Detection Summary does not include radiochemical test results.

TestAmerica St. Louis

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Detection Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: DUPLICATE 03 (Continued)


Analyte

Arsenic
Barium
Calcium
Calcium
Iron
Lead

Result Qualifier

2.2 J
1700

Lab Sample ID: 160-2968-14


RL

MDL Unit

10

2.0 ug/L

Dil Fac D Method

6010C

Prep Type

Dissolved

50

4.0 ug/L

6010C

Dissolved

1000

110 ug/L

6010C

Dissolved

110000

5000

530 ug/L

6010C

Dissolved

16000

100

28 ug/L

6010C

Dissolved

10

1.5 ug/L

6010C

Dissolved

99000 E

2.4 J

Magnesium

38000

1000

130 ug/L

6010C

Dissolved

Manganese

380

15

3.3 ug/L

6010C

Dissolved

Potassium

44000

5000

1700 ug/L

6010C

Dissolved

Sodium

52000

1000

320 ug/L

6010C

Dissolved

Zinc
Mercury
Mercury
Nitrate as N
Bromide

6.4 J

20

5.2 ug/L

6010C

Dissolved

0.075 J

0.20

0.060 ug/L

7470A

Total/NA

0.13 J

0.20

0.060 ug/L

7470A

Dissolved

0.0040 J

0.020

0.0040 mg/L

300.0

Total/NA

0.87

0.25

0.025 mg/L

300.0

Total/NA

Sulfate

8.2

0.50

0.050 mg/L

300.0

Total/NA

Alkalinity

710 B

5.0

0.54 mg/L

310.1

Total/NA

4.0

0.40 mg/L

20

300.0

Total/NA

Chloride - DL

55

Client Sample ID: TRIP BLANK


Analyte

Acetone

Lab Sample ID: 160-2968-15


Result Qualifier

8.0 J

RL

MDL Unit

20

6.7 ug/L

Dil Fac D Method

8260C

Prep Type

Total/NA

This Detection Summary does not include radiochemical test results.

TestAmerica St. Louis

Page 24 of 88

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-113-SS

Lab Sample ID: 160-2968-1

Date Collected: 07/11/13 08:50


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/15/13 20:07

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/15/13 20:07

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/15/13 20:07

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/15/13 20:07

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/15/13 20:07

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/15/13 20:07

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/15/13 20:07

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/15/13 20:07

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/15/13 20:07

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/15/13 20:07

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/15/13 20:07

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/15/13 20:07

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/15/13 20:07

2-Butanone (MEK)

ND

20

0.39 ug/L

07/15/13 20:07

2-Hexanone

ND *

20

0.59 ug/L

07/15/13 20:07

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/15/13 20:07

Acetone

12 J

20

6.7 ug/L

07/15/13 20:07

Benzene

ND

5.0

0.25 ug/L

07/15/13 20:07

Bromodichloromethane

ND

5.0

0.25 ug/L

07/15/13 20:07

Bromoform

ND

5.0

0.37 ug/L

07/15/13 20:07

Bromomethane

ND

10

0.40 ug/L

07/15/13 20:07

Carbon disulfide

ND

5.0

0.37 ug/L

07/15/13 20:07

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/15/13 20:07

Chlorobenzene

ND

5.0

0.38 ug/L

07/15/13 20:07

Chloroethane

ND

10

0.38 ug/L

07/15/13 20:07

Chloroform

ND

5.0

0.15 ug/L

07/15/13 20:07

Chloromethane

ND

10

0.55 ug/L

07/15/13 20:07

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/15/13 20:07

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/15/13 20:07

Cyclohexane

ND

10

0.36 ug/L

07/15/13 20:07

Dibromochloromethane

ND

5.0

0.33 ug/L

07/15/13 20:07

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/15/13 20:07

Ethylbenzene

ND

5.0

0.30 ug/L

07/15/13 20:07

Isopropylbenzene

ND

5.0

0.26 ug/L

07/15/13 20:07

Methyl acetate

ND

25

2.3 ug/L

07/15/13 20:07

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/15/13 20:07

Methylcyclohexane

ND

10

0.26 ug/L

07/15/13 20:07

Methylene Chloride

2.5 J

5.0

1.7 ug/L

07/15/13 20:07

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/15/13 20:07

o-Xylene

ND

5.0

0.32 ug/L

07/15/13 20:07

Styrene

ND

5.0

0.35 ug/L

07/15/13 20:07

Tetrachloroethene

ND

5.0

0.28 ug/L

07/15/13 20:07

Toluene

ND

5.0

1.0 ug/L

07/15/13 20:07

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/15/13 20:07

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/15/13 20:07

Trichloroethene

ND

5.0

0.29 ug/L

07/15/13 20:07

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/15/13 20:07

Vinyl chloride

ND

5.0

0.43 ug/L

07/15/13 20:07

Xylenes, Total

ND

10

0.85 ug/L

07/15/13 20:07

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-113-SS

Lab Sample ID: 160-2968-1

Date Collected: 07/11/13 08:50


Date Received: 07/12/13 08:15
Surrogate

Matrix: Water

3
4

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

115

82 - 132

07/15/13 20:07

4-Bromofluorobenzene (Surr)

100

82 - 121

07/15/13 20:07

Dibromofluoromethane (Surr)

106

85 - 119

07/15/13 20:07

Toluene-d8 (Surr)

103

85 - 115

07/15/13 20:07

5
6
7

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 15:34

4.4 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 15:34

Arsenic

7.2 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 15:34

Barium

220

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:34

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 15:34

Aluminum

8500

Antimony

Cadmium

ND

Calcium

140000 E

Calcium

Dil Fac

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 15:34

1000

110 ug/L

07/16/13 14:20

07/18/13 15:34

150000

10000

1100 ug/L

07/16/13 14:20

07/18/13 16:42

10

24

10

3.1 ug/L

07/16/13 14:20

07/18/13 15:34

Cobalt

4.5 J

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:34

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 15:34

Iron

7400

100

28 ug/L

07/16/13 14:20

07/18/13 15:34

Iron

7600

Chromium

1000

280 ug/L

07/16/13 14:20

07/18/13 16:42

10

4.6 J

10

1.5 ug/L

07/16/13 14:20

07/18/13 15:34

Magnesium

61000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 15:34

Magnesium

61000

10000

1300 ug/L

07/16/13 14:20

07/18/13 16:42

10

Manganese

100

15

3.3 ug/L

07/16/13 14:20

07/18/13 15:34

40

13 ug/L

07/16/13 14:20

07/18/13 15:34

5400

5000

1700 ug/L

07/16/13 14:20

07/18/13 15:34

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 15:34

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 15:34

Sodium

23000

1000

320 ug/L

07/16/13 14:20

07/18/13 15:34

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 15:34

Vanadium

27 J

50

4.1 ug/L

07/16/13 14:20

07/18/13 15:34

Zinc

48

20

5.2 ug/L

07/16/13 14:20

07/18/13 15:34

Lead

Nickel
Potassium

21 J

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 18:58

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 18:58

Arsenic

ND

10

2.0 ug/L

07/16/13 14:16

07/17/13 18:58

Barium

180

50

4.0 ug/L

07/16/13 14:16

07/17/13 18:58

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 18:58

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 18:58

Calcium

55000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 18:58

Calcium

55000

5000

530 ug/L

07/16/13 14:16

07/17/13 20:12

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 18:58

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 18:58

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 18:58

Iron

54 J

100

28 ug/L

07/16/13 14:16

07/17/13 18:58

Lead

ND

10

1.5 ug/L

07/16/13 14:16

07/17/13 18:58

31000

1000

130 ug/L

07/16/13 14:16

07/17/13 18:58

26

15

3.3 ug/L

07/16/13 14:16

07/17/13 18:58

Magnesium
Manganese

Result Qualifier

Dil Fac

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-113-SS

Lab Sample ID: 160-2968-1

Date Collected: 07/11/13 08:50


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved (Continued)


Analyte

Nickel

Potassium
Selenium
Silver

Sodium

Result Qualifier

ND

1800 J
ND

RL

MDL Unit

Prepared

Analyzed

40

13 ug/L

07/16/13 14:16

07/17/13 18:58

Dil Fac

5000

1700 ug/L

07/16/13 14:16

07/17/13 18:58

15

2.7 ug/L

07/16/13 14:16

07/17/13 18:58

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 18:58

21000

1000

320 ug/L

07/16/13 14:16

07/17/13 18:58

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 18:58

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 18:58

Zinc

6.4 J

20

5.2 ug/L

07/16/13 14:16

07/17/13 18:58

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

ND

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:25

Dil Fac

Mercury

Result Qualifier

ND

RL

MDL Unit

0.20

0.060 ug/L

RL

MDL Unit

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:14

Prepared

Analyzed

Dil Fac

Dil Fac

ND

0.020

0.0040 mg/L

07/12/13 13:33

Bromide

ND

0.25

0.025 mg/L

07/12/13 13:33

Sulfate

20

0.50

0.050 mg/L

07/12/13 13:33

Iodide

ND

1.0

0.10 mg/L

07/16/13 17:19

Alkalinity

270 B

5.0

0.54 mg/L

07/25/13 12:49

RL

MDL Unit

4.0

0.40 mg/L

General Chemistry - DL
Chloride

Result Qualifier

9.7

Prepared

Analyzed

Dil Fac

07/12/13 13:48

Client Sample ID: P2-104-SS

20

Lab Sample ID: 160-2968-2

Date Collected: 07/11/13 09:37


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

07/18/13 03:13

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/18/13 03:13

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/18/13 03:13

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/18/13 03:13

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/18/13 03:13

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/18/13 03:13

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/18/13 03:13

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/18/13 03:13

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/18/13 03:13

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/18/13 03:13

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/18/13 03:13

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/18/13 03:13

1,4-Dichlorobenzene

7.0

5.0

0.35 ug/L

07/18/13 03:13

2-Butanone (MEK)

ND

20

0.39 ug/L

07/18/13 03:13

2-Hexanone

87

20

0.59 ug/L

07/18/13 03:13

400

6.6 ug/L

07/15/13 20:34

4-Methyl-2-pentanone (MIBK)

7
8
9
10
12
13

Result Qualifier

Nitrate as N

Analyte

11

General Chemistry
Analyte

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Result Qualifier

250 J

Prepared

Analyzed

Dil Fac

TestAmerica St. Louis

Page 27 of 88

7/29/2013

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-104-SS

Lab Sample ID: 160-2968-2

Date Collected: 07/11/13 09:37


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

Acetone

Result Qualifier

16 J

RL

MDL Unit

20

6.7 ug/L

Prepared

07/18/13 03:13

Analyzed

Dil Fac

1800

100

5.0 ug/L

07/15/13 20:34

Bromodichloromethane

ND

5.0

0.25 ug/L

07/18/13 03:13

Bromoform

ND

5.0

0.37 ug/L

07/18/13 03:13

Bromomethane

ND

10

0.40 ug/L

07/18/13 03:13

Carbon disulfide

ND

5.0

0.37 ug/L

07/18/13 03:13

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/18/13 03:13

Chlorobenzene

ND

5.0

0.38 ug/L

07/18/13 03:13

Chloroethane

5.5 J *

10

0.38 ug/L

07/18/13 03:13

Chloroform

ND

5.0

0.15 ug/L

07/18/13 03:13

Chloromethane

ND

10

0.55 ug/L

07/18/13 03:13

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/18/13 03:13

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/18/13 03:13

Cyclohexane

ND

10

0.36 ug/L

07/18/13 03:13

Dibromochloromethane

ND

5.0

0.33 ug/L

07/18/13 03:13

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/18/13 03:13

Ethylbenzene

25

5.0

0.30 ug/L

07/18/13 03:13

Isopropylbenzene

2.6 J

5.0

0.26 ug/L

07/18/13 03:13

Methyl acetate

ND

25

2.3 ug/L

07/18/13 03:13

Methyl tert-butyl ether

6.3

5.0

0.40 ug/L

07/18/13 03:13

Methylcyclohexane

ND

10

0.26 ug/L

07/18/13 03:13

Methylene Chloride

ND

5.0

1.7 ug/L

07/18/13 03:13

m-Xylene & p-Xylene

44

5.0

0.57 ug/L

07/18/13 03:13

o-Xylene

21

5.0

0.32 ug/L

07/18/13 03:13

Styrene

1.3 J

5.0

0.35 ug/L

07/18/13 03:13

Tetrachloroethene

ND

5.0

0.28 ug/L

07/18/13 03:13

Toluene

140

5.0

1.0 ug/L

07/18/13 03:13

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/18/13 03:13

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/18/13 03:13

Trichloroethene

ND

5.0

0.29 ug/L

07/18/13 03:13

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/18/13 03:13

Vinyl chloride

ND

5.0

0.43 ug/L

07/18/13 03:13

Xylenes, Total

65

10

0.85 ug/L

07/18/13 03:13

Benzene

Surrogate

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

108

82 - 132

07/15/13 20:34

1,2-Dichloroethane-d4 (Surr)

94

82 - 132

07/18/13 03:13

4-Bromofluorobenzene (Surr)

98

82 - 121

07/15/13 20:34

4-Bromofluorobenzene (Surr)

89

82 - 121

07/18/13 03:13

Dibromofluoromethane (Surr)

99

85 - 119

07/15/13 20:34

Dibromofluoromethane (Surr)

95

85 - 119

07/18/13 03:13

Toluene-d8 (Surr)

97

85 - 115

07/15/13 20:34

Toluene-d8 (Surr)

96

85 - 115

07/18/13 03:13

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 15:37

4.0 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 15:37

Arsenic

2.6 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 15:37

Barium

100

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:37

Aluminum

ND

Antimony

Dil Fac

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-104-SS

Lab Sample ID: 160-2968-2

Date Collected: 07/11/13 09:37


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) (Continued)


Analyte

Beryllium

Result Qualifier

ND

Cadmium

ND

Calcium

89000 E

Calcium

RL

MDL Unit

Prepared

Analyzed

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 15:37

Dil Fac

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 15:37

1000

110 ug/L

07/16/13 14:20

07/18/13 15:37

97000

10000

1100 ug/L

07/16/13 14:20

07/18/13 16:46

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 15:37

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:37

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 15:37

Iron

1800

100

28 ug/L

07/16/13 14:20

07/18/13 15:37

Iron

1800

1000

280 ug/L

07/16/13 14:20

07/18/13 16:46

10
1

Lead
Magnesium

1.7 J

10

1.5 ug/L

07/16/13 14:20

07/18/13 15:37

53000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 15:37

1300 ug/L

07/16/13 14:20

07/18/13 16:46

10

54000

10000

Manganese

40

15

3.3 ug/L

07/16/13 14:20

07/18/13 15:37

Nickel

ND

40

13 ug/L

07/16/13 14:20

07/18/13 15:37

5000

1700 ug/L

07/16/13 14:20

07/18/13 15:37

15

2.7 ug/L

07/16/13 14:20

07/18/13 15:37

Magnesium

Potassium
Selenium
Silver

2200 J
ND
ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 15:37

Sodium

12000

1000

320 ug/L

07/16/13 14:20

07/18/13 15:37

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 15:37

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 15:37

Zinc

ND

20

5.2 ug/L

07/16/13 14:20

07/18/13 15:37

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:02

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:02

Arsenic

2.2 J

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:02

Barium

100

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:02

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:02

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:02

Calcium

85000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:02

Calcium

89000

5000

530 ug/L

07/16/13 14:16

07/17/13 20:16

Result Qualifier

Dil Fac

Chromium

3.2 J

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:02

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:02

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:02

Iron

1800

100

28 ug/L

07/16/13 14:16

07/17/13 19:02

Lead

ND

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:02

Magnesium

49000

1000

130 ug/L

07/16/13 14:16

07/17/13 19:02

Manganese

39

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:02

Nickel

ND

40

13 ug/L

07/16/13 14:16

07/17/13 19:02

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:02

Potassium

2200 J

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:02

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:02

12000

1000

320 ug/L

07/16/13 14:16

07/17/13 19:02

Sodium

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:02

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:02

Zinc

ND

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:02

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-104-SS

Lab Sample ID: 160-2968-2

Date Collected: 07/11/13 09:37


Date Received: 07/12/13 08:15

Matrix: Water

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

ND

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:26

Dil Fac

Mercury

Result Qualifier

0.064 J

6
RL

MDL Unit

0.20

0.060 ug/L

RL

MDL Unit

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:16

Prepared

Analyzed

Dil Fac

Result Qualifier

Dil Fac

Nitrate as N

ND

0.020

0.0040 mg/L

07/12/13 14:02

Chloride

4.8

0.20

0.020 mg/L

07/12/13 14:02

Bromide

ND

0.25

0.025 mg/L

07/12/13 14:02

Sulfate

1.0

0.50

0.050 mg/L

07/12/13 14:02

Iodide

ND

1.0

0.10 mg/L

07/16/13 17:34

Alkalinity

440 B

5.0

0.54 mg/L

07/25/13 12:49

Client Sample ID: P2-101-SS

Lab Sample ID: 160-2968-3

Date Collected: 07/11/13 09:40


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

07/15/13 21:00

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/15/13 21:00

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/15/13 21:00

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/15/13 21:00

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/15/13 21:00

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/15/13 21:00

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/15/13 21:00

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/15/13 21:00

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/15/13 21:00

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/15/13 21:00

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/15/13 21:00

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/15/13 21:00

5.0

0.35 ug/L

07/15/13 21:00

1,4-Dichlorobenzene

7
8

General Chemistry
Analyte

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Result Qualifier

0.52 J

Prepared

Analyzed

Dil Fac

2-Butanone (MEK)

ND

20

0.39 ug/L

07/15/13 21:00

2-Hexanone

ND *

20

0.59 ug/L

07/15/13 21:00

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/15/13 21:00

Acetone

34

20

6.7 ug/L

07/15/13 21:00

Benzene

0.92 J

5.0

0.25 ug/L

07/15/13 21:00

Bromodichloromethane

ND

5.0

0.25 ug/L

07/15/13 21:00

Bromoform

ND

5.0

0.37 ug/L

07/15/13 21:00

Bromomethane

ND

10

0.40 ug/L

07/15/13 21:00

Carbon disulfide

ND

5.0

0.37 ug/L

07/15/13 21:00

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/15/13 21:00

Chlorobenzene

3.3 J

5.0

0.38 ug/L

07/15/13 21:00

Chloroethane

ND

10

0.38 ug/L

07/15/13 21:00

Chloroform

ND

5.0

0.15 ug/L

07/15/13 21:00

Chloromethane

ND

10

0.55 ug/L

07/15/13 21:00

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/15/13 21:00

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/15/13 21:00

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-101-SS

Lab Sample ID: 160-2968-3

Date Collected: 07/11/13 09:40


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

RL

MDL Unit

Cyclohexane

ND

10

0.36 ug/L

07/15/13 21:00

Dibromochloromethane

ND

5.0

0.33 ug/L

07/15/13 21:00

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/15/13 21:00

Ethylbenzene

ND

5.0

0.30 ug/L

07/15/13 21:00

Isopropylbenzene

ND

5.0

0.26 ug/L

07/15/13 21:00

Methyl acetate

Methyl tert-butyl ether

Result Qualifier

ND

0.51 J

Prepared

Analyzed

Dil Fac

25

2.3 ug/L

07/15/13 21:00

5.0

0.40 ug/L

07/15/13 21:00

Methylcyclohexane

ND

10

0.26 ug/L

07/15/13 21:00

Methylene Chloride

ND

5.0

1.7 ug/L

07/15/13 21:00

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/15/13 21:00

o-Xylene

ND

5.0

0.32 ug/L

07/15/13 21:00

Styrene

ND

5.0

0.35 ug/L

07/15/13 21:00

Tetrachloroethene

ND

5.0

0.28 ug/L

07/15/13 21:00

Toluene

ND

5.0

1.0 ug/L

07/15/13 21:00

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/15/13 21:00

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/15/13 21:00

Trichloroethene

ND

5.0

0.29 ug/L

07/15/13 21:00

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/15/13 21:00

Vinyl chloride

ND

5.0

0.43 ug/L

07/15/13 21:00

Xylenes, Total

ND

10

0.85 ug/L

07/15/13 21:00

Surrogate

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

109

82 - 132

07/15/13 21:00

4-Bromofluorobenzene (Surr)

103

82 - 121

07/15/13 21:00

Dibromofluoromethane (Surr)

101

85 - 119

07/15/13 21:00

Toluene-d8 (Surr)

100

85 - 115

07/15/13 21:00

Method: 6010C - Metals (ICP)


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:20

07/18/13 15:41

Antimony

ND

10

4.0 ug/L

07/16/13 14:20

07/18/13 15:41

Arsenic

3.4 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 15:41

Barium

530

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:41

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 15:41

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 15:41

Calcium

150000 E

1000

110 ug/L

07/16/13 14:20

07/18/13 15:41

Calcium

160000

10000

1100 ug/L

07/16/13 14:20

07/18/13 16:58

10

Result Qualifier

Dil Fac

Chromium

4.8 J

10

3.1 ug/L

07/16/13 14:20

07/18/13 15:41

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:41

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 15:41

Iron

590

100

28 ug/L

07/16/13 14:20

07/18/13 15:41

Iron

580 J

1000

280 ug/L

07/16/13 14:20

07/18/13 16:58

10
1

2.5 J

10

1.5 ug/L

07/16/13 14:20

07/18/13 15:41

Magnesium

98000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 15:41

Magnesium

97000

10000

1300 ug/L

07/16/13 14:20

07/18/13 16:58

10

Manganese

48

15

3.3 ug/L

07/16/13 14:20

07/18/13 15:41

Nickel

15 J

40

13 ug/L

07/16/13 14:20

07/18/13 15:41

16000

5000

1700 ug/L

07/16/13 14:20

07/18/13 15:41

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 15:41

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 15:41

Lead

Potassium

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-101-SS

Lab Sample ID: 160-2968-3

Date Collected: 07/11/13 09:40


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) (Continued)


Analyte

Sodium

Result Qualifier

110000 E

RL

MDL Unit

Prepared

Analyzed

1000

320 ug/L

07/16/13 14:20

07/18/13 15:41

Dil Fac

Sodium

99000

10000

3200 ug/L

07/16/13 14:20

07/18/13 16:58

10

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 15:41

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 15:41

Zinc

8.6 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 15:41

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:13

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:13

Arsenic

3.2 J

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:13

Barium

480

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:13

Beryllium

5.7

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:13

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:13

Calcium

130000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:13

Calcium

150000

5000

530 ug/L

07/16/13 14:16

07/17/13 20:20

Result Qualifier

Dil Fac

Chromium

3.5 J

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:13

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:13

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:13

Iron

78 J

100

28 ug/L

07/16/13 14:16

07/17/13 19:13

Iron

ND

500

140 ug/L

07/16/13 14:16

07/17/13 20:20

Lead

2.1 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:13

Magnesium

86000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 19:13

Magnesium

90000

5000

660 ug/L

07/16/13 14:16

07/17/13 20:20

Manganese

68

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:13

Nickel

15 J

40

13 ug/L

07/16/13 14:16

07/17/13 19:13

15000

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:13

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:13

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:13

92000

1000

320 ug/L

07/16/13 14:16

07/17/13 19:13

Potassium

Sodium
Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:13

Vanadium

10 J

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:13

Zinc

16 J

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:13

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

ND

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:28

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.17 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:17

Dil Fac

General Chemistry
Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

0.030

0.020

0.0040 mg/L

07/12/13 14:31

Bromide

1.5

0.25

0.025 mg/L

07/12/13 14:31

Sulfate

6.0

0.50

0.050 mg/L

07/12/13 14:31

Iodide

1.0

1.0

0.10 mg/L

07/16/13 17:49

Alkalinity

760 B

5.0

0.54 mg/L

07/25/13 12:49

Nitrate as N

5
6
7
8

Method: 6010C - Metals (ICP) - Dissolved


Analyte

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-101-SS

Lab Sample ID: 160-2968-3

Date Collected: 07/11/13 09:40


Date Received: 07/12/13 08:15

Matrix: Water

General Chemistry - DL2


Analyte

Chloride

Result Qualifier

160

RL

20

MDL Unit

Prepared

2.0 mg/L

Analyzed

Dil Fac

07/12/13 15:00

Client Sample ID: P2-104-SD

Matrix: Water

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

07/18/13 03:38

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/18/13 03:38

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/18/13 03:38

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/18/13 03:38

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/18/13 03:38

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/18/13 03:38

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/18/13 03:38

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/18/13 03:38

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/18/13 03:38

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/18/13 03:38

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/18/13 03:38

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/18/13 03:38

11

5.0

0.35 ug/L

07/18/13 03:38

3200

500

9.8 ug/L

07/16/13 03:31

42

20

0.59 ug/L

07/18/13 03:38

110

20

0.33 ug/L

07/18/13 03:38

Acetone

3800

500

170 ug/L

07/16/13 03:31

Benzene

800

25

1.3 ug/L

07/15/13 21:26

Bromodichloromethane

ND

5.0

0.25 ug/L

07/18/13 03:38

Bromoform

ND

5.0

0.37 ug/L

07/18/13 03:38

Bromomethane

ND

10

0.40 ug/L

07/18/13 03:38

Carbon disulfide

ND

5.0

0.37 ug/L

07/18/13 03:38

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/18/13 03:38

Chlorobenzene

4.6 J

5.0

0.38 ug/L

07/18/13 03:38

Chloroethane

4.4 J *

10

0.38 ug/L

07/18/13 03:38

Chloroform

ND

5.0

0.15 ug/L

07/18/13 03:38

Chloromethane

ND

10

0.55 ug/L

07/18/13 03:38

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/18/13 03:38

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/18/13 03:38

Cyclohexane

ND

10

0.36 ug/L

07/18/13 03:38

Dibromochloromethane

ND

5.0

0.33 ug/L

07/18/13 03:38

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/18/13 03:38

Ethylbenzene

49

5.0

0.30 ug/L

07/18/13 03:38

Isopropylbenzene

5.9

5.0

0.26 ug/L

07/18/13 03:38

Methyl acetate

ND

25

2.3 ug/L

07/18/13 03:38

Methyl tert-butyl ether

3.8 J

5.0

0.40 ug/L

07/18/13 03:38

Methylcyclohexane

ND

10

0.26 ug/L

07/18/13 03:38

Methylene Chloride

ND

5.0

1.7 ug/L

07/18/13 03:38

m-Xylene & p-Xylene

100

5.0

0.57 ug/L

07/18/13 03:38

o-Xylene

42

5.0

0.32 ug/L

07/18/13 03:38

Styrene

2.4 J

5.0

0.35 ug/L

07/18/13 03:38

Tetrachloroethene

ND

5.0

0.28 ug/L

07/18/13 03:38

1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)

6
7
8

Method: 8260C - Volatile Organic Compounds by GC/MS


Result Qualifier

100

Lab Sample ID: 160-2968-4

Date Collected: 07/11/13 10:29


Date Received: 07/12/13 08:15

Analyte

Prepared

Analyzed

Dil Fac

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-104-SD

Lab Sample ID: 160-2968-4

Date Collected: 07/11/13 10:29


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

RL

MDL Unit

Toluene

430

25

5.0 ug/L

07/15/13 21:26

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/18/13 03:38

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/18/13 03:38

Trichloroethene

ND

5.0

0.29 ug/L

07/18/13 03:38

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/18/13 03:38

Vinyl chloride

ND

5.0

0.43 ug/L

07/18/13 03:38

Xylenes, Total

140

10

0.85 ug/L

07/18/13 03:38

Surrogate

Result Qualifier

%Recovery Qualifier

Limits

Prepared

Prepared

Analyzed

Analyzed

Dil Fac

Dil Fac

1,2-Dichloroethane-d4 (Surr)

110

82 - 132

07/15/13 21:26

1,2-Dichloroethane-d4 (Surr)

118

82 - 132

07/16/13 03:31

1,2-Dichloroethane-d4 (Surr)

98

82 - 132

07/18/13 03:38

4-Bromofluorobenzene (Surr)

105

82 - 121

07/15/13 21:26

4-Bromofluorobenzene (Surr)

102

82 - 121

07/16/13 03:31

4-Bromofluorobenzene (Surr)

94

82 - 121

07/18/13 03:38

Dibromofluoromethane (Surr)

102

85 - 119

07/15/13 21:26

Dibromofluoromethane (Surr)

102

85 - 119

07/16/13 03:31

Dibromofluoromethane (Surr)

98

85 - 119

07/18/13 03:38

Toluene-d8 (Surr)

103

85 - 115

07/15/13 21:26

Toluene-d8 (Surr)

101

85 - 115

07/16/13 03:31

Toluene-d8 (Surr)

101

85 - 115

07/18/13 03:38

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 15:45

4.4 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 15:45

Arsenic

12

10

2.0 ug/L

07/16/13 14:20

07/18/13 15:45

Barium

800

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:45

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 15:45

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 15:45

Calcium

110000 E

1000

110 ug/L

07/16/13 14:20

07/18/13 15:45

Calcium

130000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:02

10

Chromium

16

10

3.1 ug/L

07/16/13 14:20

07/18/13 15:45

Cobalt

5.0 J

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:45

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 15:45

Iron

8900

100

28 ug/L

07/16/13 14:20

07/18/13 15:45

Iron

9000

1000

280 ug/L

07/16/13 14:20

07/18/13 17:02

10
1

Aluminum

ND

Antimony

Lead
Magnesium

Dil Fac

2.0 J

10

1.5 ug/L

07/16/13 14:20

07/18/13 15:45

66000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 15:45

1300 ug/L

07/16/13 14:20

07/18/13 17:02

10

Magnesium

66000

10000

Manganese

160

15

3.3 ug/L

07/16/13 14:20

07/18/13 15:45

40

13 ug/L

07/16/13 14:20

07/18/13 15:45

20000

5000

1700 ug/L

07/16/13 14:20

07/18/13 15:45

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 15:45

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 15:45

1000

320 ug/L

07/16/13 14:20

07/18/13 15:45

Nickel
Potassium

31 J

Sodium

130000 E

Sodium

120000

10000

3200 ug/L

07/16/13 14:20

07/18/13 17:02

10

Thallium

ND

Vanadium
Zinc

20

4.0 ug/L

07/16/13 14:20

07/18/13 15:45

11 J

50

4.1 ug/L

07/16/13 14:20

07/18/13 15:45

8.9 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 15:45

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-104-SD

Lab Sample ID: 160-2968-4

Date Collected: 07/11/13 10:29


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:17

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:17

Arsenic

14

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:17

Barium

1000

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:17

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:17

Beryllium

Result Qualifier

Dil Fac

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:17

Calcium

110000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:17

Calcium

140000

5000

530 ug/L

07/16/13 14:16

07/17/13 20:24

19

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:17

Cobalt

5.8 J

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:17

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:17

Iron

13000

100

28 ug/L

07/16/13 14:16

07/17/13 19:17

Iron

14000

500

140 ug/L

07/16/13 14:16

07/17/13 20:24

1.5 ug/L

07/16/13 14:16

07/17/13 19:17

Chromium

1.6 J

10

Magnesium

66000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 19:17

Magnesium

71000

5000

660 ug/L

07/16/13 14:16

07/17/13 20:24

Manganese

160

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:17

40

13 ug/L

07/16/13 14:16

07/17/13 19:17

Lead

Nickel

36 J
23000

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:17

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:17

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:17

Potassium

Sodium

160000 E

1000

320 ug/L

07/16/13 14:16

07/17/13 19:17

Sodium

170000

5000

1600 ug/L

07/16/13 14:16

07/17/13 20:24

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:17

Vanadium

16 J

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:17

Zinc

ND

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:17

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

ND

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:30

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.16 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:19

Dil Fac

General Chemistry
Analyte

Nitrate as N

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

ND

0.020

0.0040 mg/L

07/12/13 15:43

Bromide

0.64

0.25

0.025 mg/L

07/12/13 15:43

Iodide

0.45 J

1.0

0.10 mg/L

07/16/13 18:04

Alkalinity

580 B

5.0

0.54 mg/L

07/25/13 12:49

RL

MDL Unit

General Chemistry - DL
Analyte

Sulfate

Result Qualifier

39

10

Prepared

1.0 mg/L

Analyzed

Dil Fac

07/12/13 15:58

20

General Chemistry - DL2


Analyte

Chloride

Result Qualifier

180

RL

20

MDL Unit

2.0 mg/L

Prepared

Analyzed

Dil Fac

07/12/13 16:12

100

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: FB@P2-202-SS

Lab Sample ID: 160-2968-5

Date Collected: 07/11/13 12:00


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/16/13 04:23

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 04:23

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/16/13 04:23

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/16/13 04:23

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 04:23

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 04:23

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 04:23

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 04:23

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 04:23

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 04:23

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 04:23

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 04:23

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 04:23

2-Butanone (MEK)

ND

20

0.39 ug/L

07/16/13 04:23

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 04:23

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/16/13 04:23

Acetone

12 J

20

6.7 ug/L

07/16/13 04:23

Benzene

ND

5.0

0.25 ug/L

07/16/13 04:23

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 04:23

Bromoform

ND

5.0

0.37 ug/L

07/16/13 04:23

Bromomethane

ND

10

0.40 ug/L

07/16/13 04:23

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 04:23

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 04:23

Chlorobenzene

ND

5.0

0.38 ug/L

07/16/13 04:23

Chloroethane

ND

10

0.38 ug/L

07/16/13 04:23

Chloroform

ND

5.0

0.15 ug/L

07/16/13 04:23

Chloromethane

ND

10

0.55 ug/L

07/16/13 04:23

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/16/13 04:23

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/16/13 04:23

Cyclohexane

ND

10

0.36 ug/L

07/16/13 04:23

Dibromochloromethane

ND

5.0

0.33 ug/L

07/16/13 04:23

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/16/13 04:23

Ethylbenzene

ND

5.0

0.30 ug/L

07/16/13 04:23

Isopropylbenzene

ND

5.0

0.26 ug/L

07/16/13 04:23

Methyl acetate

ND

25

2.3 ug/L

07/16/13 04:23

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/16/13 04:23

Methylcyclohexane

ND

10

0.26 ug/L

07/16/13 04:23

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 04:23

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 04:23

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 04:23

Styrene

ND

5.0

0.35 ug/L

07/16/13 04:23

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 04:23

Toluene

ND

5.0

1.0 ug/L

07/16/13 04:23

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 04:23

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 04:23

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 04:23

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 04:23

Vinyl chloride

ND

5.0

0.43 ug/L

07/16/13 04:23

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 04:23

TestAmerica St. Louis

Page 36 of 88

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: FB@P2-202-SS

Lab Sample ID: 160-2968-5

Date Collected: 07/11/13 12:00


Date Received: 07/12/13 08:15
Surrogate

Matrix: Water

4
%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

109

82 - 132

07/16/13 04:23

4-Bromofluorobenzene (Surr)

102

82 - 121

07/16/13 04:23

Dibromofluoromethane (Surr)

98

85 - 119

07/16/13 04:23

101

85 - 115

07/16/13 04:23

Toluene-d8 (Surr)

Client Sample ID: P2-202-SS

Lab Sample ID: 160-2968-6

Date Collected: 07/11/13 12:32


Date Received: 07/12/13 08:15

Matrix: Water

Result Qualifier

5
6
7
8
9

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

Prepared

07/15/13 22:18

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/15/13 22:18

1,1,2-Trichloroethane

37

5.0

0.57 ug/L

07/15/13 22:18

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/15/13 22:18

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/15/13 22:18

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/15/13 22:18

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/15/13 22:18

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/15/13 22:18

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/15/13 22:18

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/15/13 22:18

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/15/13 22:18

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/15/13 22:18

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/15/13 22:18

2-Butanone (MEK)

ND

20

0.39 ug/L

07/15/13 22:18

2-Hexanone

ND *

20

0.59 ug/L

07/15/13 22:18

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/15/13 22:18

Acetone

30

20

6.7 ug/L

07/15/13 22:18

Benzene

34

5.0

0.25 ug/L

07/15/13 22:18

Bromodichloromethane

ND

5.0

0.25 ug/L

07/15/13 22:18

Bromoform

ND

5.0

0.37 ug/L

07/15/13 22:18

Bromomethane

ND

10

0.40 ug/L

07/15/13 22:18

Carbon disulfide

ND

5.0

0.37 ug/L

07/15/13 22:18

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/15/13 22:18

Chlorobenzene

ND

5.0

0.38 ug/L

07/15/13 22:18

Chloroethane

ND

10

0.38 ug/L

07/15/13 22:18

Chloroform

ND

5.0

0.15 ug/L

07/15/13 22:18

Chloromethane

ND

10

0.55 ug/L

07/15/13 22:18

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/15/13 22:18

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/15/13 22:18

Cyclohexane

ND

10

0.36 ug/L

07/15/13 22:18

Dibromochloromethane

ND

5.0

0.33 ug/L

07/15/13 22:18

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/15/13 22:18

Ethylbenzene

ND

5.0

0.30 ug/L

07/15/13 22:18

Isopropylbenzene

ND

5.0

0.26 ug/L

07/15/13 22:18

Methyl acetate

ND

25

2.3 ug/L

07/15/13 22:18

Methyl tert-butyl ether

4.3 J

5.0

0.40 ug/L

07/15/13 22:18

Methylcyclohexane

ND

10

0.26 ug/L

07/15/13 22:18

Methylene Chloride

ND

5.0

1.7 ug/L

07/15/13 22:18

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/15/13 22:18

TestAmerica St. Louis

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13

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-202-SS

Lab Sample ID: 160-2968-6

Date Collected: 07/11/13 12:32


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

RL

MDL Unit

o-Xylene

ND

5.0

0.32 ug/L

07/15/13 22:18

Styrene

ND

5.0

0.35 ug/L

07/15/13 22:18

Tetrachloroethene

ND

5.0

0.28 ug/L

07/15/13 22:18

Toluene

ND

5.0

1.0 ug/L

07/15/13 22:18

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/15/13 22:18

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/15/13 22:18

Trichloroethene

ND

5.0

0.29 ug/L

07/15/13 22:18

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/15/13 22:18

Vinyl chloride

ND

5.0

0.43 ug/L

07/15/13 22:18

Xylenes, Total

ND

10

0.85 ug/L

07/15/13 22:18

Surrogate

Result Qualifier

%Recovery Qualifier

Limits

Prepared

Prepared

Analyzed

Analyzed

Dil Fac

5
6
7
8
9
10

Dil Fac

1,2-Dichloroethane-d4 (Surr)

118

82 - 132

07/15/13 22:18

4-Bromofluorobenzene (Surr)

110

82 - 121

07/15/13 22:18

Dibromofluoromethane (Surr)

109

85 - 119

07/15/13 22:18

Toluene-d8 (Surr)

107

85 - 115

07/15/13 22:18

11
12
13

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 15:49

ND

10

4.0 ug/L

07/16/13 14:20

07/18/13 15:49

7.4 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 15:49

Barium

580

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:49

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 15:49

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 15:49

Calcium

180000 E

1000

110 ug/L

07/16/13 14:20

07/18/13 15:49

Calcium

200000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:05

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 15:49

Cobalt

6.9 J

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:49

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 15:49

Iron

4900

100

28 ug/L

07/16/13 14:20

07/18/13 15:49

Iron

5000

1000

280 ug/L

07/16/13 14:20

07/18/13 17:05

10
1

Aluminum

98 J

Antimony

Arsenic

Dil Fac

2.1 J

10

1.5 ug/L

07/16/13 14:20

07/18/13 15:49

Magnesium

78000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 15:49

Magnesium

79000

10000

1300 ug/L

07/16/13 14:20

07/18/13 17:05

10

Manganese

940

Lead

Nickel
Potassium

15

3.3 ug/L

07/16/13 14:20

07/18/13 15:49

21 J

40

13 ug/L

07/16/13 14:20

07/18/13 15:49

3100 J

5000

1700 ug/L

07/16/13 14:20

07/18/13 15:49

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 15:49

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 15:49

Sodium

14000

1000

320 ug/L

07/16/13 14:20

07/18/13 15:49

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 15:49

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 15:49

Zinc

7.0 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 15:49

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

Result Qualifier

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:21

Dil Fac

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:21

Arsenic

6.8 J

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:21

TestAmerica St. Louis

Page 38 of 88

7/29/2013

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-202-SS

Lab Sample ID: 160-2968-6

Date Collected: 07/11/13 12:32


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved (Continued)


Analyte

RL

MDL Unit

Prepared

Analyzed

Barium

550

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:21

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:21

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:21

Calcium

160000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:21

Calcium

200000

5000

530 ug/L

07/16/13 14:16

07/17/13 20:27

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:21

Cobalt

6.3 J

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:21

Copper

Result Qualifier

Dil Fac

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:21

Iron

4600

100

28 ug/L

07/16/13 14:16

07/17/13 19:21

Iron

4900

500

140 ug/L

07/16/13 14:16

07/17/13 20:27

2.9 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:21

Magnesium

71000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 19:21

Magnesium

76000

5000

660 ug/L

07/16/13 14:16

07/17/13 20:27

870

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:21

Lead

Manganese
Nickel
Potassium

20 J

40

13 ug/L

07/16/13 14:16

07/17/13 19:21

3100 J

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:21

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:21

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:21

13000

1000

320 ug/L

07/16/13 14:16

07/17/13 19:21

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:21

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:21

Zinc

6.1 J

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:21

Sodium

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.14 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:31

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.20

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:24

Dil Fac

General Chemistry
Analyte

Nitrate as N

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

ND

0.020

0.0040 mg/L

07/12/13 16:26

Bromide

0.51

0.25

0.025 mg/L

07/12/13 16:26

Iodide

0.14 J

1.0

0.10 mg/L

07/16/13 18:34

Alkalinity

610 B

5.0

0.54 mg/L

07/25/13 12:49

RL

MDL Unit

General Chemistry - DL
Analyte

Sulfate

Result Qualifier

58

10

Prepared

1.0 mg/L

Analyzed

Dil Fac

07/12/13 16:41

20

General Chemistry - DL2


Analyte

Chloride

Result Qualifier

84

RL

20

MDL Unit

2.0 mg/L

Prepared

Analyzed

Dil Fac

07/12/13 16:55

100

TestAmerica St. Louis

Page 39 of 88

7/29/2013

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-83

Lab Sample ID: 160-2968-7

Date Collected: 07/11/13 13:05


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

07/16/13 00:02

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 00:02

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/16/13 00:02

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/16/13 00:02

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 00:02

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 00:02

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 00:02

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 00:02

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 00:02

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 00:02

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 00:02

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 00:02

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 00:02

2-Butanone (MEK)

ND

20

0.39 ug/L

07/16/13 00:02

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 00:02

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/16/13 00:02

Acetone

ND

20

6.7 ug/L

07/16/13 00:02

Benzene

ND

5.0

0.25 ug/L

07/16/13 00:02

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 00:02

Bromoform

ND

5.0

0.37 ug/L

07/16/13 00:02

Bromomethane

ND

10

0.40 ug/L

07/16/13 00:02

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 00:02

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 00:02

Chlorobenzene

2.0 J

5.0

0.38 ug/L

07/16/13 00:02

Chloroethane

ND

10

0.38 ug/L

07/16/13 00:02

Chloroform

ND

5.0

0.15 ug/L

07/16/13 00:02

Chloromethane

ND

10

0.55 ug/L

07/16/13 00:02

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/16/13 00:02

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/16/13 00:02

Cyclohexane

ND

10

0.36 ug/L

07/16/13 00:02

Dibromochloromethane

ND

5.0

0.33 ug/L

07/16/13 00:02

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/16/13 00:02

Ethylbenzene

ND

5.0

0.30 ug/L

07/16/13 00:02

Isopropylbenzene

ND

5.0

0.26 ug/L

07/16/13 00:02

Methyl acetate

ND

25

2.3 ug/L

07/16/13 00:02

5.0

0.40 ug/L

07/16/13 00:02

Methyl tert-butyl ether

Result Qualifier

0.68 J

Prepared

Analyzed

Dil Fac

Methylcyclohexane

ND

10

0.26 ug/L

07/16/13 00:02

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 00:02

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 00:02

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 00:02

Styrene

ND

5.0

0.35 ug/L

07/16/13 00:02

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 00:02

Toluene

ND

5.0

1.0 ug/L

07/16/13 00:02

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 00:02

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 00:02

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 00:02

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 00:02

Vinyl chloride

ND

5.0

0.43 ug/L

07/16/13 00:02

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 00:02

TestAmerica St. Louis

Page 40 of 88

7/29/2013

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-83

Lab Sample ID: 160-2968-7

Date Collected: 07/11/13 13:05


Date Received: 07/12/13 08:15
Surrogate

Matrix: Water

3
4

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

119

82 - 132

07/16/13 00:02

4-Bromofluorobenzene (Surr)

107

82 - 121

07/16/13 00:02

Dibromofluoromethane (Surr)

104

85 - 119

07/16/13 00:02

Toluene-d8 (Surr)

101

85 - 115

07/16/13 00:02

5
6
7

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 16:11

5.0 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:11

2.8 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:11

Aluminum

ND

Antimony
Arsenic
Barium
Beryllium

Dil Fac

1800

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:11

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:11

Cadmium

ND

Calcium

110000 E

Calcium

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:11

1000

110 ug/L

07/16/13 14:20

07/18/13 16:11

120000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:20

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:11

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:11

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:11

17000

100

28 ug/L

07/16/13 14:20

07/18/13 16:11

Iron

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:11

Magnesium

42000

1000

130 ug/L

07/16/13 14:20

07/18/13 16:11

Manganese

410

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:11

Nickel

ND

40

13 ug/L

07/16/13 14:20

07/18/13 16:11

45000

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:11

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:11

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:11

Sodium

57000

1000

320 ug/L

07/16/13 14:20

07/18/13 16:11

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:11

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:11

Zinc

5.4 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 16:11

Lead

2.8 J

Potassium

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:35

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:35

Arsenic

ND

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:35

Barium

1700

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:35

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:35

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:35

Calcium

98000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:35

110000

5000

530 ug/L

07/16/13 14:16

07/17/13 20:49

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:35

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:35

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:35

16000

100

28 ug/L

07/16/13 14:16

07/17/13 19:35

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:35

Calcium

Iron
Lead

Result Qualifier

2.9 J

Dil Fac

Magnesium

38000

1000

130 ug/L

07/16/13 14:16

07/17/13 19:35

Manganese

390

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:35

Nickel

ND

40

13 ug/L

07/16/13 14:16

07/17/13 19:35

44000

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:35

Potassium

TestAmerica St. Louis

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7/29/2013

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-83

Lab Sample ID: 160-2968-7

Date Collected: 07/11/13 13:05


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved (Continued)


Analyte

Selenium
Silver

Sodium

Result Qualifier

ND

RL

MDL Unit

Prepared

Analyzed

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:35

Dil Fac

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:35

53000

1000

320 ug/L

07/16/13 14:16

07/17/13 19:35

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:35

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:35

Zinc

ND

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:35

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.099 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:42

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.29

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:31

Dil Fac

Nitrate as N

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

ND

0.020

0.0040 mg/L

07/12/13 19:05

0.88

0.25

0.025 mg/L

07/12/13 19:05

Sulfate

8.2

0.50

0.050 mg/L

07/12/13 19:05

Iodide

ND

1.0

0.10 mg/L

07/16/13 19:48

Alkalinity

690 B

5.0

0.54 mg/L

07/25/13 12:49

RL

MDL Unit

4.0

0.40 mg/L

Bromide

General Chemistry - DL
Analyte

Chloride

Result Qualifier

54

Prepared

Analyzed

Dil Fac

07/12/13 19:19

Client Sample ID: MW-1204

20

Lab Sample ID: 160-2968-8

Date Collected: 07/11/13 14:12


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

07/18/13 04:02

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/18/13 04:02

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/18/13 04:02

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/18/13 04:02

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/18/13 04:02

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/18/13 04:02

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/18/13 04:02

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/18/13 04:02

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/18/13 04:02

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/18/13 04:02

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/18/13 04:02

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/18/13 04:02

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/18/13 04:02

1900

200

3.9 ug/L

07/16/13 00:28

2-Butanone (MEK)

Result Qualifier

Prepared

Analyzed

Dil Fac

2-Hexanone

8.5 J

20

0.59 ug/L

07/18/13 04:02

4-Methyl-2-pentanone (MIBK)

22

20

0.33 ug/L

07/18/13 04:02

3300

1000

330 ug/L

07/17/13 19:48

5.0

0.25 ug/L

07/18/13 04:02

Acetone
Benzene

5
6
7
8
9
10
11
12

General Chemistry
Analyte

1.1 J

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: MW-1204

Lab Sample ID: 160-2968-8

Date Collected: 07/11/13 14:12


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

RL

MDL Unit

Bromodichloromethane

ND

5.0

0.25 ug/L

07/18/13 04:02

Bromoform

ND

5.0

0.37 ug/L

07/18/13 04:02

Bromomethane

ND

10

0.40 ug/L

07/18/13 04:02

Carbon disulfide

ND

5.0

0.37 ug/L

07/18/13 04:02

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/18/13 04:02

Chlorobenzene

ND

5.0

0.38 ug/L

07/18/13 04:02

Chloroethane

ND *

10

0.38 ug/L

07/18/13 04:02

Chloroform

ND

5.0

0.15 ug/L

07/18/13 04:02

Chloromethane

ND

10

0.55 ug/L

07/18/13 04:02

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/18/13 04:02

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/18/13 04:02

Cyclohexane

ND

10

0.36 ug/L

07/18/13 04:02

Dibromochloromethane

ND

5.0

0.33 ug/L

07/18/13 04:02

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/18/13 04:02

Ethylbenzene

ND

5.0

0.30 ug/L

07/18/13 04:02

Isopropylbenzene

ND

5.0

0.26 ug/L

07/18/13 04:02

Methyl acetate

ND

25

2.3 ug/L

07/18/13 04:02

Methyl tert-butyl ether

1.9 J

5.0

0.40 ug/L

07/18/13 04:02

Methylcyclohexane

ND

10

0.26 ug/L

07/18/13 04:02

Methylene Chloride

ND

5.0

1.7 ug/L

07/18/13 04:02

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/18/13 04:02

o-Xylene

ND

5.0

0.32 ug/L

07/18/13 04:02

Styrene

ND

5.0

0.35 ug/L

07/18/13 04:02

Tetrachloroethene

ND

5.0

0.28 ug/L

07/18/13 04:02

1700

50

10 ug/L

07/16/13 00:28

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/18/13 04:02

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/18/13 04:02

Trichloroethene

ND

5.0

0.29 ug/L

07/18/13 04:02

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/18/13 04:02

Vinyl chloride

ND

5.0

0.43 ug/L

07/18/13 04:02

Xylenes, Total

ND

10

0.85 ug/L

07/18/13 04:02

Toluene

Surrogate

Result Qualifier

%Recovery Qualifier

Limits

Prepared

Prepared

Analyzed

Analyzed

Dil Fac

Dil Fac

1,2-Dichloroethane-d4 (Surr)

109

82 - 132

07/16/13 00:28

1,2-Dichloroethane-d4 (Surr)

94

82 - 132

07/17/13 19:48

1,2-Dichloroethane-d4 (Surr)

97

82 - 132

07/18/13 04:02

4-Bromofluorobenzene (Surr)

98

82 - 121

07/16/13 00:28

4-Bromofluorobenzene (Surr)

83

82 - 121

07/17/13 19:48

4-Bromofluorobenzene (Surr)

95

82 - 121

07/18/13 04:02

Dibromofluoromethane (Surr)

98

85 - 119

07/16/13 00:28

Dibromofluoromethane (Surr)

92

85 - 119

07/17/13 19:48

Dibromofluoromethane (Surr)

98

85 - 119

07/18/13 04:02

Toluene-d8 (Surr)

98

85 - 115

07/16/13 00:28

Toluene-d8 (Surr)

96

85 - 115

07/17/13 19:48

Toluene-d8 (Surr)

100

85 - 115

07/18/13 04:02

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

Aluminum

160 J

Antimony

ND

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 16:15

Dil Fac

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:15

TestAmerica St. Louis

Page 43 of 88

7/29/2013

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: MW-1204

Lab Sample ID: 160-2968-8

Date Collected: 07/11/13 14:12


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) (Continued)


Analyte

Result Qualifier

Arsenic

5.9 J

Barium
Beryllium

RL

MDL Unit

Prepared

Analyzed

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:15

Dil Fac

1300

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:15

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:15

Cadmium

ND

Calcium

260000 E

Calcium

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:15

1000

110 ug/L

07/16/13 14:20

07/18/13 16:15

330000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:24

10

Chromium

40

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:15

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:15

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:15

Iron

12000

100

28 ug/L

07/16/13 14:20

07/18/13 16:15

Iron

13000

1000

280 ug/L

07/16/13 14:20

07/18/13 17:24

10

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:15

Lead
Magnesium

2.4 J
150000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 16:15

1300 ug/L

07/16/13 14:20

07/18/13 17:24

10

Magnesium

150000

10000

Manganese

120

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:15

Nickel

ND

40

13 ug/L

07/16/13 14:20

07/18/13 16:15

7300

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:15

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:15

1
1

Potassium
Selenium
Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:15

1000

320 ug/L

07/16/13 14:20

07/18/13 16:15

120000

10000

3200 ug/L

07/16/13 14:20

07/18/13 17:24

10

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:15

Vanadium

7.0 J

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:15

Zinc

14 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 16:15

Sodium

120000 E

Sodium

Method: 6010C - Metals (ICP) - Dissolved


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:16

07/17/13 19:38

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:38

4.6 J

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:38

1100

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:38

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:38

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:38

Calcium

230000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:38

Calcium

290000 E

5000

530 ug/L

07/16/13 14:16

07/17/13 20:53

1100 ug/L

07/16/13 14:16

07/18/13 11:00

10

Aluminum

95 J

Antimony

Arsenic
Barium

Dil Fac

300000

10000

Chromium

32

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:38

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:38

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:38

Iron

11000

100

28 ug/L

07/16/13 14:16

07/17/13 19:38

Iron

12000

500

140 ug/L

07/16/13 14:16

07/17/13 20:53

2.4 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:38

Magnesium

130000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 19:38

Magnesium

130000

5000

660 ug/L

07/16/13 14:16

07/17/13 20:53

Manganese

110

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:38

Nickel

ND

40

13 ug/L

07/16/13 14:16

07/17/13 19:38

6100

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:38

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:38

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:38

1000

320 ug/L

07/16/13 14:16

07/17/13 19:38

Calcium

Lead

Potassium

Sodium

100000 E

TestAmerica St. Louis

Page 44 of 88

7/29/2013

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13

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: MW-1204

Lab Sample ID: 160-2968-8

Date Collected: 07/11/13 14:12


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved (Continued)


Analyte

Sodium

Result Qualifier

100000

RL

MDL Unit

Prepared

Analyzed

5000

1600 ug/L

07/16/13 14:16

07/17/13 20:53

Dil Fac

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:38

Vanadium

6.6 J

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:38

Zinc

ND

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:38

RL

MDL Unit

Prepared

Analyzed

0.20

0.060 ug/L

07/16/13 12:14

07/16/13 16:43

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.11 J

Dil Fac

5
6
7
8
9

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.31

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:32

Dil Fac

11

General Chemistry
Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

Nitrate as N

ND

0.020

0.0040 mg/L

07/12/13 19:48

Bromide

1.0

0.25

0.025 mg/L

07/12/13 19:48

Sulfate

6.1

0.50

0.050 mg/L

07/12/13 19:48

1.0

0.10 mg/L

07/16/13 20:03

RL

MDL Unit

Iodide

0.20 J

General Chemistry - DL
Analyte

Alkalinity

Result Qualifier

1100 B

10

Prepared

1.1 mg/L

Analyzed

Dil Fac

07/25/13 12:49

General Chemistry - DL2


Analyte

Chloride

Result Qualifier

280

RL

40

MDL Unit

Prepared

4.0 mg/L

Analyzed

Dil Fac

07/12/13 20:17

Client Sample ID: S-82

200

Lab Sample ID: 160-2968-9

Date Collected: 07/11/13 14:32


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

10

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/16/13 00:55

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 00:55

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/16/13 00:55

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/16/13 00:55

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 00:55

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 00:55

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 00:55

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 00:55

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 00:55

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 00:55

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 00:55

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 00:55

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 00:55

2-Butanone (MEK)

7.8 J

20

0.39 ug/L

07/16/13 00:55

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 00:55

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/16/13 00:55

Acetone

23

20

6.7 ug/L

07/16/13 00:55

TestAmerica St. Louis

Page 45 of 88

7/29/2013

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13

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: S-82

Lab Sample ID: 160-2968-9

Date Collected: 07/11/13 14:32


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

RL

MDL Unit

Benzene

ND

5.0

0.25 ug/L

07/16/13 00:55

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 00:55

Bromoform

ND

5.0

0.37 ug/L

07/16/13 00:55

Bromomethane

ND

10

0.40 ug/L

07/16/13 00:55

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 00:55

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 00:55

Chlorobenzene

1.0 J

5.0

0.38 ug/L

07/16/13 00:55

Chloroethane

ND

10

0.38 ug/L

07/16/13 00:55

Chloroform

ND

5.0

0.15 ug/L

07/16/13 00:55

Chloromethane

cis-1,2-Dichloroethene

Result Qualifier

ND

0.42 J

Prepared

Analyzed

Dil Fac

10

0.55 ug/L

07/16/13 00:55

5.0

0.16 ug/L

07/16/13 00:55

5.0

0.34 ug/L

07/16/13 00:55

cis-1,3-Dichloropropene

ND

Cyclohexane

ND

10

0.36 ug/L

07/16/13 00:55

Dibromochloromethane

ND

5.0

0.33 ug/L

07/16/13 00:55

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/16/13 00:55

Ethylbenzene

ND

5.0

0.30 ug/L

07/16/13 00:55

Isopropylbenzene

ND

5.0

0.26 ug/L

07/16/13 00:55

Methyl acetate

ND

25

2.3 ug/L

07/16/13 00:55

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/16/13 00:55

Methylcyclohexane

ND

10

0.26 ug/L

07/16/13 00:55

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 00:55

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 00:55

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 00:55

Styrene

ND

5.0

0.35 ug/L

07/16/13 00:55

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 00:55

Toluene

ND

5.0

1.0 ug/L

07/16/13 00:55

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 00:55

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 00:55

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 00:55

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 00:55

Vinyl chloride

ND

5.0

0.43 ug/L

07/16/13 00:55

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 00:55

Surrogate

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

111

82 - 132

07/16/13 00:55

4-Bromofluorobenzene (Surr)

103

82 - 121

07/16/13 00:55

Dibromofluoromethane (Surr)

99

85 - 119

07/16/13 00:55

101

85 - 115

07/16/13 00:55

Toluene-d8 (Surr)

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 16:19

4.8 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:19

Arsenic

200

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:19

Barium

790

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:19

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:19

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:19

Calcium

160000 E

1000

110 ug/L

07/16/13 14:20

07/18/13 16:19

Calcium

190000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:28

10

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:19

Aluminum

ND

Antimony

Chromium

Dil Fac

TestAmerica St. Louis

Page 46 of 88

7/29/2013

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: S-82

Lab Sample ID: 160-2968-9

Date Collected: 07/11/13 14:32


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) (Continued)


Analyte

Result Qualifier

Cobalt

11 J

Copper

RL

MDL Unit

Prepared

Analyzed

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:19

Dil Fac

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:19

Iron

35000

100

28 ug/L

07/16/13 14:20

07/18/13 16:19

Iron

36000

1000

280 ug/L

07/16/13 14:20

07/18/13 17:28

10

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:19

Lead

5.3 J

Magnesium

81000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 16:19

Magnesium

83000

10000

1300 ug/L

07/16/13 14:20

07/18/13 17:28

10

Manganese

2200

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:19

40

13 ug/L

07/16/13 14:20

07/18/13 16:19

Nickel

26 J

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:19

Selenium

2.7 J

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:19

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:19

Potassium

Sodium

12000

230000 E

1000

320 ug/L

07/16/13 14:20

07/18/13 16:19

3200 ug/L

07/16/13 14:20

07/18/13 17:28

10

Sodium

220000

10000

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:19

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:19

Zinc

7.1 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 16:19

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:42

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:42

Arsenic

210

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:42

Barium

790

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:42

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:42

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:42

Calcium

160000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:42

Calcium

200000

5000

530 ug/L

07/16/13 14:16

07/17/13 20:57

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:42

Cobalt

9.9 J

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:42

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:42

Iron

35000

100

28 ug/L

07/16/13 14:16

07/17/13 19:42

Iron

37000

500

140 ug/L

07/16/13 14:16

07/17/13 20:57

3.3 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:42

77000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 19:42

81000

5000

660 ug/L

07/16/13 14:16

07/17/13 20:57

2100

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:42

40

13 ug/L

07/16/13 14:16

07/17/13 19:42

12000

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:42

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:42

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:42

Lead
Magnesium
Magnesium
Manganese
Nickel
Potassium

Result Qualifier

25 J

Dil Fac

Sodium

220000 E

1000

320 ug/L

07/16/13 14:16

07/17/13 19:42

Sodium

230000

5000

1600 ug/L

07/16/13 14:16

07/17/13 20:57

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:42

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:42

Zinc

ND

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:42

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.065 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:45

Dil Fac

TestAmerica St. Louis

Page 47 of 88

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: S-82

Lab Sample ID: 160-2968-9

Date Collected: 07/11/13 14:32


Date Received: 07/12/13 08:15

Matrix: Water

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.23

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:34

Dil Fac

Analyte

Result Qualifier

Nitrate as N

0.0072 J

0.020

0.0040 mg/L

07/12/13 21:00

Bromide

2.9

0.25

0.025 mg/L

07/12/13 21:00

Sulfate

15

0.50

0.050 mg/L

07/12/13 21:00

Iodide

0.30 J

1.0

0.10 mg/L

07/16/13 20:33

Alkalinity

960 B

5.0

0.54 mg/L

07/25/13 12:49

RL

MDL Unit

Prepared

Analyzed

Dil Fac

RL

MDL Unit

General Chemistry - DL2


Chloride

Result Qualifier

220

40

Prepared

4.0 mg/L

Analyzed

Dil Fac

07/12/13 21:29

Client Sample ID: P2-116-SS

200

Lab Sample ID: 160-2968-10

Date Collected: 07/11/13 15:05


Date Received: 07/12/13 08:15

Matrix: Water

7
8
9
10
11
12
13

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

General Chemistry

Analyte

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/16/13 01:21

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 01:21

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/16/13 01:21

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/16/13 01:21

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 01:21

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 01:21

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 01:21

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 01:21

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 01:21

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 01:21

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 01:21

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 01:21

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 01:21

2-Butanone (MEK)

ND

20

0.39 ug/L

07/16/13 01:21

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 01:21

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/16/13 01:21

Acetone

ND

20

6.7 ug/L

07/16/13 01:21

Benzene

ND

5.0

0.25 ug/L

07/16/13 01:21

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 01:21

Bromoform

ND

5.0

0.37 ug/L

07/16/13 01:21

Bromomethane

ND

10

0.40 ug/L

07/16/13 01:21

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 01:21

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 01:21

Chlorobenzene

ND

5.0

0.38 ug/L

07/16/13 01:21

Chloroethane

ND

10

0.38 ug/L

07/16/13 01:21

Chloroform

ND

5.0

0.15 ug/L

07/16/13 01:21

Chloromethane

ND

10

0.55 ug/L

07/16/13 01:21

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/16/13 01:21

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/16/13 01:21

Cyclohexane

ND

10

0.36 ug/L

07/16/13 01:21

TestAmerica St. Louis

Page 48 of 88

7/29/2013

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-116-SS

Lab Sample ID: 160-2968-10

Date Collected: 07/11/13 15:05


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

Result Qualifier

RL

MDL Unit

5.0

0.33 ug/L

07/16/13 01:21

10

0.45 ug/L

07/16/13 01:21

5.0

0.30 ug/L

07/16/13 01:21

5.0

0.26 ug/L

07/16/13 01:21

25

2.3 ug/L

07/16/13 01:21

ND

5.0

0.40 ug/L

07/16/13 01:21

ND

10

0.26 ug/L

07/16/13 01:21

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 01:21

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 01:21

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 01:21

Styrene

ND

5.0

0.35 ug/L

07/16/13 01:21

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 01:21

Toluene

ND

5.0

1.0 ug/L

07/16/13 01:21

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 01:21

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 01:21

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 01:21

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 01:21

Vinyl chloride

ND

5.0

0.43 ug/L

07/16/13 01:21

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 01:21

Dibromochloromethane

ND

Dichlorodifluoromethane

ND

Ethylbenzene

ND

Isopropylbenzene

ND

Methyl acetate

ND

Methyl tert-butyl ether


Methylcyclohexane

Surrogate

%Recovery Qualifier

Limits

Prepared

Prepared

Analyzed

Analyzed

Dil Fac

Dil Fac

1,2-Dichloroethane-d4 (Surr)

121

82 - 132

07/16/13 01:21

4-Bromofluorobenzene (Surr)

110

82 - 121

07/16/13 01:21

Dibromofluoromethane (Surr)

107

85 - 119

07/16/13 01:21

Toluene-d8 (Surr)

110

85 - 115

07/16/13 01:21

Method: 6010C - Metals (ICP)


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:20

07/18/13 16:23

Antimony

ND

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:23

Arsenic

ND

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:23

Barium

73

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:23

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:23

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:23

Calcium

43000

1000

110 ug/L

07/16/13 14:20

07/18/13 16:23

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:23

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:23

Copper

5.3 J

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:23

Iron

ND

100

28 ug/L

07/16/13 14:20

07/18/13 16:23

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:23

1000

130 ug/L

07/16/13 14:20

07/18/13 16:23

Lead
Magnesium

Result Qualifier

1.6 J
31000

Dil Fac

Manganese

3.8 J

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:23

Nickel

ND

40

13 ug/L

07/16/13 14:20

07/18/13 16:23

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:23

Potassium

3800 J

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:23

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:23

Sodium

53000

1000

320 ug/L

07/16/13 14:20

07/18/13 16:23

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:23

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:23

Zinc

24

20

5.2 ug/L

07/16/13 14:20

07/18/13 16:23

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-116-SS

Lab Sample ID: 160-2968-10

Date Collected: 07/11/13 15:05


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:46

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:46

Arsenic

ND

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:46

Result Qualifier

Dil Fac

Barium

69

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:46

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:46

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:46

Calcium

40000

1000

110 ug/L

07/16/13 14:16

07/17/13 19:46

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:46

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:46

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:46

Iron

ND

100

28 ug/L

07/16/13 14:16

07/17/13 19:46

Lead

ND

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:46

29000

1000

130 ug/L

07/16/13 14:16

07/17/13 19:46

ND

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:46

Magnesium
Manganese
Nickel

Potassium

ND

3600 J

40

13 ug/L

07/16/13 14:16

07/17/13 19:46

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:46

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:46

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:46

49000

1000

320 ug/L

07/16/13 14:16

07/17/13 19:46

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:46

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:46

Zinc

24

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:46

Sodium

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.13 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:46

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.19 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:36

Dil Fac

General Chemistry
Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

0.17

0.020

0.0040 mg/L

07/12/13 21:44

Chloride

3.5

0.20

0.020 mg/L

07/12/13 21:44

Bromide

ND

0.25

0.025 mg/L

07/12/13 21:44

Iodide

ND

1.0

0.10 mg/L

07/16/13 20:48

Alkalinity

300 B

5.0

0.54 mg/L

07/25/13 12:49

RL

MDL Unit

Nitrate as N

General Chemistry - DL
Analyte

Sulfate

Result Qualifier

34

10

Prepared

1.0 mg/L

Analyzed

Dil Fac

07/12/13 21:58

Client Sample ID: D-93

20

Lab Sample ID: 160-2968-11

Date Collected: 07/11/13 15:40


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/16/13 01:47

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 01:47

TestAmerica St. Louis

Page 50 of 88

7/29/2013

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-93

Lab Sample ID: 160-2968-11

Date Collected: 07/11/13 15:40


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

RL

MDL Unit

ND

5.0

0.57 ug/L

07/16/13 01:47

1,1-Dichloroethane

3.5 J

5.0

0.39 ug/L

07/16/13 01:47

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 01:47

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 01:47

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 01:47

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 01:47

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 01:47

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 01:47

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 01:47

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 01:47

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 01:47

2-Butanone (MEK)

ND

20

0.39 ug/L

07/16/13 01:47

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 01:47

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/16/13 01:47

Acetone

ND

20

6.7 ug/L

07/16/13 01:47

Benzene

1.9 J

5.0

0.25 ug/L

07/16/13 01:47

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 01:47

Bromoform

ND

5.0

0.37 ug/L

07/16/13 01:47

Bromomethane

ND

10

0.40 ug/L

07/16/13 01:47

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 01:47

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 01:47

Chlorobenzene

ND

5.0

0.38 ug/L

07/16/13 01:47

Chloroethane

ND

10

0.38 ug/L

07/16/13 01:47

Chloroform

ND

5.0

0.15 ug/L

07/16/13 01:47

Chloromethane

ND

10

0.55 ug/L

07/16/13 01:47

cis-1,2-Dichloroethene

29

5.0

0.16 ug/L

07/16/13 01:47

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/16/13 01:47

Cyclohexane

ND

10

0.36 ug/L

07/16/13 01:47

Dibromochloromethane

ND

5.0

0.33 ug/L

07/16/13 01:47

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/16/13 01:47

Ethylbenzene

ND

5.0

0.30 ug/L

07/16/13 01:47

Isopropylbenzene

ND

5.0

0.26 ug/L

07/16/13 01:47

Methyl acetate

ND

25

2.3 ug/L

07/16/13 01:47

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/16/13 01:47

Methylcyclohexane

ND

10

0.26 ug/L

07/16/13 01:47

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 01:47

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 01:47

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 01:47

Styrene

ND

5.0

0.35 ug/L

07/16/13 01:47

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 01:47

Toluene

ND

5.0

1.0 ug/L

07/16/13 01:47

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 01:47

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 01:47

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 01:47

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 01:47

Vinyl chloride

30

5.0

0.43 ug/L

07/16/13 01:47

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 01:47

1,1,2-Trichloroethane

Surrogate

1,2-Dichloroethane-d4 (Surr)

Result Qualifier

%Recovery Qualifier

113

Limits

82 - 132

Prepared

Prepared

Analyzed

Analyzed

Dil Fac

Dil Fac

07/16/13 01:47

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-93

Lab Sample ID: 160-2968-11

Date Collected: 07/11/13 15:40


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Surrogate

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

4-Bromofluorobenzene (Surr)

103

82 - 121

07/16/13 01:47

Dibromofluoromethane (Surr)

101

85 - 119

07/16/13 01:47

Toluene-d8 (Surr)

102

85 - 115

07/16/13 01:47

5
6
7

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 16:27

4.3 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:27

2.3 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:27

Aluminum

200

Antimony
Arsenic
Barium
Beryllium

Dil Fac

1400

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:27

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:27

Cadmium

ND

Calcium

240000 E

Calcium

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:27

1000

110 ug/L

07/16/13 14:20

07/18/13 16:27

290000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:44

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:27

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:27

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:27

Iron

21000

100

28 ug/L

07/16/13 14:20

07/18/13 16:27

Iron

21000

1000

280 ug/L

07/16/13 14:20

07/18/13 17:44

10

3.7 J

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:27

Magnesium

80000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 16:27

Magnesium

81000

10000

1300 ug/L

07/16/13 14:20

07/18/13 17:44

10

Manganese

420

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:27

Nickel

ND

40

13 ug/L

07/16/13 14:20

07/18/13 16:27

17000

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:27

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:27

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:27

1000

320 ug/L

07/16/13 14:20

07/18/13 16:27

Lead

Potassium

Sodium

210000 E

Sodium

200000

10000

3200 ug/L

07/16/13 14:20

07/18/13 17:44

10

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:27

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:27

Zinc

ND

20

5.2 ug/L

07/16/13 14:20

07/18/13 16:27

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 19:57

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 19:57

Arsenic

2.8 J

10

2.0 ug/L

07/16/13 14:16

07/17/13 19:57

1300

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:57

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 19:57

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 19:57

Calcium

230000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 19:57

Calcium

280000 E

5000

530 ug/L

07/16/13 14:16

07/17/13 21:04

Calcium

290000

10000

1100 ug/L

07/16/13 14:16

07/18/13 11:04

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 19:57

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 19:57

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 19:57

20000

100

28 ug/L

07/16/13 14:16

07/17/13 19:57

20000

500

140 ug/L

07/16/13 14:16

07/17/13 21:04

Barium

Iron
Iron

Result Qualifier

Dil Fac

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: D-93

Lab Sample ID: 160-2968-11

Date Collected: 07/11/13 15:40


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved (Continued)


Analyte

RL

MDL Unit

Prepared

Analyzed

2.5 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 19:57

Magnesium

76000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 19:57

Magnesium

75000

5000

660 ug/L

07/16/13 14:16

07/17/13 21:04

Manganese

400

15

3.3 ug/L

07/16/13 14:16

07/17/13 19:57

Nickel

ND

40

13 ug/L

07/16/13 14:16

07/17/13 19:57

17000

5000

1700 ug/L

07/16/13 14:16

07/17/13 19:57

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 19:57

Lead

Potassium
Selenium
Silver

Result Qualifier

ND

Dil Fac

10

6.0 ug/L

07/16/13 14:16

07/17/13 19:57

Sodium

200000 E

1000

320 ug/L

07/16/13 14:16

07/17/13 19:57

Sodium

190000

5000

1600 ug/L

07/16/13 14:16

07/17/13 21:04

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 19:57

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 19:57

Zinc

5.4 J

20

5.2 ug/L

07/16/13 14:16

07/17/13 19:57

RL

MDL Unit

Prepared

Analyzed

0.20

0.060 ug/L

07/16/13 12:14

07/16/13 16:48

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.12 J

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.19 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:37

Dil Fac

General Chemistry
Analyte

Result Qualifier

Nitrate as N

0.0072 J

0.020

0.0040 mg/L

07/12/13 22:41

4.1

0.25

0.025 mg/L

07/12/13 22:41

12

0.50

0.050 mg/L

07/12/13 22:41

0.36 J

1.0

0.10 mg/L

07/16/13 21:03

RL

MDL Unit

Bromide
Sulfate
Iodide

RL

MDL Unit

Prepared

Analyzed

Dil Fac

General Chemistry - DL
Analyte

Alkalinity

Result Qualifier

1000 B

10

Prepared

1.1 mg/L

Analyzed

Dil Fac

07/25/13 12:49

General Chemistry - DL2


Analyte

Chloride

Result Qualifier

330

RL

40

MDL Unit

Prepared

4.0 mg/L

Analyzed

Dil Fac

07/12/13 23:10

Client Sample ID: I-9

200

Lab Sample ID: 160-2968-12

Date Collected: 07/11/13 16:26


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/16/13 02:13

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 02:13

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/16/13 02:13

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/16/13 02:13

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 02:13

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 02:13

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 02:13

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 02:13

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: I-9

Lab Sample ID: 160-2968-12

Date Collected: 07/11/13 16:26


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

RL

MDL Unit

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 02:13

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 02:13

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 02:13

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 02:13

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 02:13

2-Butanone (MEK)

ND

20

0.39 ug/L

07/16/13 02:13

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 02:13

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/16/13 02:13

Acetone

18 J

20

6.7 ug/L

07/16/13 02:13

Benzene

ND

5.0

0.25 ug/L

07/16/13 02:13

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 02:13

Bromoform

ND

5.0

0.37 ug/L

07/16/13 02:13

Bromomethane

ND

10

0.40 ug/L

07/16/13 02:13

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 02:13

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 02:13

Chlorobenzene

ND

5.0

0.38 ug/L

07/16/13 02:13

Chloroethane

ND

10

0.38 ug/L

07/16/13 02:13

Chloroform

ND

5.0

0.15 ug/L

07/16/13 02:13

Chloromethane

ND

10

0.55 ug/L

07/16/13 02:13

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/16/13 02:13

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/16/13 02:13

Cyclohexane

ND

10

0.36 ug/L

07/16/13 02:13

Dibromochloromethane

ND

5.0

0.33 ug/L

07/16/13 02:13

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/16/13 02:13

Ethylbenzene

ND

5.0

0.30 ug/L

07/16/13 02:13

Isopropylbenzene

ND

5.0

0.26 ug/L

07/16/13 02:13

Methyl acetate

ND

25

2.3 ug/L

07/16/13 02:13

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/16/13 02:13

Methylcyclohexane

ND

10

0.26 ug/L

07/16/13 02:13

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 02:13

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 02:13

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 02:13

Styrene

ND

5.0

0.35 ug/L

07/16/13 02:13

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 02:13

Toluene

ND

5.0

1.0 ug/L

07/16/13 02:13

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 02:13

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 02:13

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 02:13

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 02:13

Vinyl chloride

2.5 J

5.0

0.43 ug/L

07/16/13 02:13

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 02:13

Surrogate

Result Qualifier

%Recovery Qualifier

Limits

Prepared

Prepared

Analyzed

Analyzed

Dil Fac

Dil Fac

1,2-Dichloroethane-d4 (Surr)

114

82 - 132

07/16/13 02:13

4-Bromofluorobenzene (Surr)

101

82 - 121

07/16/13 02:13

Dibromofluoromethane (Surr)

104

85 - 119

07/16/13 02:13

99

85 - 115

07/16/13 02:13

Toluene-d8 (Surr)

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: I-9

Lab Sample ID: 160-2968-12

Date Collected: 07/11/13 16:26


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP)


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

190 J

200

80 ug/L

07/16/13 14:20

07/18/13 16:31

Antimony

5.6 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:31

Arsenic

26

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:31

Barium

Result Qualifier

1500

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:31

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:31

Beryllium
Cadmium

ND

Calcium

220000 E

Calcium

Dil Fac

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:31

1000

110 ug/L

07/16/13 14:20

07/18/13 16:31

270000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:47

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:31

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:31

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:31

Iron

35000

100

28 ug/L

07/16/13 14:20

07/18/13 16:31

Iron

36000

1000

280 ug/L

07/16/13 14:20

07/18/13 17:47

10

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:31

Lead

4.1 J

Magnesium

73000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 16:31

Magnesium

74000

10000

1300 ug/L

07/16/13 14:20

07/18/13 17:47

10

Manganese

1300

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:31

40

13 ug/L

07/16/13 14:20

07/18/13 16:31

Nickel

14 J
21000

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:31

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:31

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:31

1000

320 ug/L

07/16/13 14:20

07/18/13 16:31

Potassium

Sodium

230000 E

Sodium

220000

10000

3200 ug/L

07/16/13 14:20

07/18/13 17:47

10

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:31

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:31

Zinc

6.2 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 16:31

Method: 6010C - Metals (ICP) - Dissolved


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:16

07/17/13 20:01

4.2 J

10

4.0 ug/L

07/16/13 14:16

07/17/13 20:01

Arsenic

24

10

2.0 ug/L

07/16/13 14:16

07/17/13 20:01

Barium

1500

50

4.0 ug/L

07/16/13 14:16

07/17/13 20:01

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 20:01

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 20:01

210000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 20:01

Calcium

260000 E

5000

530 ug/L

07/16/13 14:16

07/17/13 21:08

Calcium

270000

10000

1100 ug/L

07/16/13 14:16

07/18/13 11:08

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 20:01

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 20:01

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 20:01

Iron

33000

100

28 ug/L

07/16/13 14:16

07/17/13 20:01

Iron

34000

500

140 ug/L

07/16/13 14:16

07/17/13 21:08

2.9 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 20:01

Magnesium

68000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 20:01

Magnesium

69000

5000

660 ug/L

07/16/13 14:16

07/17/13 21:08

Manganese

1200

15

3.3 ug/L

07/16/13 14:16

07/17/13 20:01

40

13 ug/L

07/16/13 14:16

07/17/13 20:01

21000

5000

1700 ug/L

07/16/13 14:16

07/17/13 20:01

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 20:01

Aluminum

ND

Antimony

Calcium

Lead

Nickel
Potassium
Selenium

13 J

Dil Fac

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: I-9

Lab Sample ID: 160-2968-12

Date Collected: 07/11/13 16:26


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) - Dissolved (Continued)


Analyte

Silver

Result Qualifier

ND

RL

MDL Unit

Prepared

Analyzed

10

6.0 ug/L

07/16/13 14:16

07/17/13 20:01

Dil Fac

Sodium

220000 E

1000

320 ug/L

07/16/13 14:16

07/17/13 20:01

Sodium

220000

5000

1600 ug/L

07/16/13 14:16

07/17/13 21:08

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 20:01

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 20:01

Zinc

5.4 J

20

5.2 ug/L

07/16/13 14:16

07/17/13 20:01

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.10 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:50

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.18 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:39

Dil Fac

Analyte

Result Qualifier

Nitrate as N

0.0080 J

0.020

0.0040 mg/L

07/12/13 23:53

3.5

0.25

0.025 mg/L

07/12/13 23:53

Sulfate

0.58

0.50

0.050 mg/L

07/12/13 23:53

Iodide

0.36 J

1.0

0.10 mg/L

07/16/13 21:18

RL

MDL Unit

Prepared

Analyzed

Dil Fac

RL

MDL Unit

General Chemistry - DL
Analyte

Alkalinity

Result Qualifier

1100 B

10

Prepared

1.1 mg/L

Analyzed

Dil Fac

07/25/13 12:51

General Chemistry - DL2


Analyte

Chloride

Result Qualifier

300

RL

40

MDL Unit

Prepared

4.0 mg/L

Analyzed

Dil Fac

07/13/13 00:22

Client Sample ID: P2-115-SS

200

Lab Sample ID: 160-2968-13

Date Collected: 07/11/13 16:36


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

5
6
7
8
9
10
11
12

General Chemistry

Bromide

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/16/13 02:39

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 02:39

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/16/13 02:39

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/16/13 02:39

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 02:39

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 02:39

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 02:39

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 02:39

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 02:39

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 02:39

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 02:39

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 02:39

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 02:39

2-Butanone (MEK)

ND

20

0.39 ug/L

07/16/13 02:39

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 02:39

TestAmerica St. Louis

Page 56 of 88

7/29/2013

13

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-115-SS

Lab Sample ID: 160-2968-13

Date Collected: 07/11/13 16:36


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

4-Methyl-2-pentanone (MIBK)

Result Qualifier

ND

RL

MDL Unit

20

0.33 ug/L

Prepared

07/16/13 02:39

Analyzed

Dil Fac

Acetone

16 J

20

6.7 ug/L

07/16/13 02:39

Benzene

ND

5.0

0.25 ug/L

07/16/13 02:39

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 02:39

Bromoform

ND

5.0

0.37 ug/L

07/16/13 02:39

Bromomethane

ND

10

0.40 ug/L

07/16/13 02:39

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 02:39

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 02:39

Chlorobenzene

ND

5.0

0.38 ug/L

07/16/13 02:39

Chloroethane

ND

10

0.38 ug/L

07/16/13 02:39

Chloroform

ND

5.0

0.15 ug/L

07/16/13 02:39

Chloromethane

ND

10

0.55 ug/L

07/16/13 02:39

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/16/13 02:39

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/16/13 02:39

Cyclohexane

ND

10

0.36 ug/L

07/16/13 02:39

Dibromochloromethane

ND

5.0

0.33 ug/L

07/16/13 02:39

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/16/13 02:39

Ethylbenzene

ND

5.0

0.30 ug/L

07/16/13 02:39

Isopropylbenzene

ND

5.0

0.26 ug/L

07/16/13 02:39

Methyl acetate

ND

25

2.3 ug/L

07/16/13 02:39

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/16/13 02:39

Methylcyclohexane

ND

10

0.26 ug/L

07/16/13 02:39

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 02:39

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 02:39

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 02:39

Styrene

ND

5.0

0.35 ug/L

07/16/13 02:39

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 02:39

Toluene

ND

5.0

1.0 ug/L

07/16/13 02:39

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 02:39

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 02:39

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 02:39

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 02:39

Vinyl chloride

ND

5.0

0.43 ug/L

07/16/13 02:39

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 02:39

Surrogate

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

113

82 - 132

07/16/13 02:39

4-Bromofluorobenzene (Surr)

104

82 - 121

07/16/13 02:39

Dibromofluoromethane (Surr)

103

85 - 119

07/16/13 02:39

Toluene-d8 (Surr)

104

85 - 115

07/16/13 02:39

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 16:35

4.3 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:35

Arsenic

6.0 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:35

Barium

330

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:35

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:35

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:35

Calcium

160000 E

1000

110 ug/L

07/16/13 14:20

07/18/13 16:35

Aluminum

ND

Antimony

Dil Fac

TestAmerica St. Louis

Page 57 of 88

7/29/2013

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13

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-115-SS

Lab Sample ID: 160-2968-13

Date Collected: 07/11/13 16:36


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) (Continued)


Analyte

RL

MDL Unit

Prepared

Analyzed

180000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:51

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:35

Cobalt

15 J

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:35

Calcium

Result Qualifier

Copper

Dil Fac

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:35

Iron

1500

100

28 ug/L

07/16/13 14:20

07/18/13 16:35

Iron

1500

1000

280 ug/L

07/16/13 14:20

07/18/13 17:51

10

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:35

Lead

2.8 J

Magnesium

82000 E

1000

130 ug/L

07/16/13 14:20

07/18/13 16:35

Magnesium

84000

10000

1300 ug/L

07/16/13 14:20

07/18/13 17:51

10

Manganese

52

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:35

Nickel

43

40

13 ug/L

07/16/13 14:20

07/18/13 16:35

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:35

Potassium

2800 J

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:35

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:35

Sodium

62000

1000

320 ug/L

07/16/13 14:20

07/18/13 16:35

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:35

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:35

Zinc

7.1 J

20

5.2 ug/L

07/16/13 14:20

07/18/13 16:35

Method: 6010C - Metals (ICP) - Dissolved


Analyte

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 20:05

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 20:05

Arsenic

5.1 J

10

2.0 ug/L

07/16/13 14:16

07/17/13 20:05

Barium

320

50

4.0 ug/L

07/16/13 14:16

07/17/13 20:05

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 20:05

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 20:05

Calcium

160000 E

1000

110 ug/L

07/16/13 14:16

07/17/13 20:05

Calcium

180000

5000

530 ug/L

07/16/13 14:16

07/17/13 21:12

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 20:05

Cobalt

20 J

50

4.0 ug/L

07/16/13 14:16

07/17/13 20:05

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 20:05

Iron

1500

100

28 ug/L

07/16/13 14:16

07/17/13 20:05

Iron

1600

500

140 ug/L

07/16/13 14:16

07/17/13 21:12

1.8 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 20:05

78000 E

1000

130 ug/L

07/16/13 14:16

07/17/13 20:05

Magnesium

79000

5000

660 ug/L

07/16/13 14:16

07/17/13 21:12

Manganese

51

15

3.3 ug/L

07/16/13 14:16

07/17/13 20:05

Nickel

44

40

13 ug/L

07/16/13 14:16

07/17/13 20:05

5000

1700 ug/L

07/16/13 14:16

07/17/13 20:05

Lead
Magnesium

Potassium

Result Qualifier

3000 J

Dil Fac

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 20:05

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 20:05

60000

1000

320 ug/L

07/16/13 14:16

07/17/13 20:05

Sodium
Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 20:05

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 20:05

Zinc

ND

20

5.2 ug/L

07/16/13 14:16

07/17/13 20:05

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.083 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:51

Dil Fac

TestAmerica St. Louis

Page 58 of 88

7/29/2013

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6
7
8
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13

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: P2-115-SS

Lab Sample ID: 160-2968-13

Date Collected: 07/11/13 16:36


Date Received: 07/12/13 08:15

Matrix: Water

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.16 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:44

Dil Fac

6
Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

Nitrate as N

ND

0.020

0.0040 mg/L

07/13/13 00:37

Bromide

1.2

0.25

0.025 mg/L

07/13/13 00:37

Sulfate

17

0.50

0.050 mg/L

07/13/13 00:37

Iodide

0.13 J

1.0

0.10 mg/L

07/16/13 21:33

Alkalinity

560 B

5.0

0.54 mg/L

07/25/13 12:51

RL

MDL Unit

General Chemistry - DL2


Analyte

Chloride

Result Qualifier

220

20

Prepared

2.0 mg/L

Analyzed

Dil Fac

07/13/13 01:06

Client Sample ID: DUPLICATE 03

100

Lab Sample ID: 160-2968-14

Date Collected: 07/11/13 00:00


Date Received: 07/12/13 08:15

Matrix: Water

7
8
9
10
11
12
13

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

General Chemistry
Analyte

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/16/13 03:05

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/16/13 03:05

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/16/13 03:05

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/16/13 03:05

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/16/13 03:05

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/16/13 03:05

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/16/13 03:05

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/16/13 03:05

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/16/13 03:05

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/16/13 03:05

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/16/13 03:05

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/16/13 03:05

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/16/13 03:05

2-Butanone (MEK)

ND

20

0.39 ug/L

07/16/13 03:05

2-Hexanone

ND *

20

0.59 ug/L

07/16/13 03:05

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/16/13 03:05

Acetone

9.7 J

20

6.7 ug/L

07/16/13 03:05

Benzene

ND

5.0

0.25 ug/L

07/16/13 03:05

Bromodichloromethane

ND

5.0

0.25 ug/L

07/16/13 03:05

Bromoform

ND

5.0

0.37 ug/L

07/16/13 03:05

Bromomethane

ND

10

0.40 ug/L

07/16/13 03:05

Carbon disulfide

ND

5.0

0.37 ug/L

07/16/13 03:05

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/16/13 03:05

Chlorobenzene

2.0 J

5.0

0.38 ug/L

07/16/13 03:05

Chloroethane

ND

10

0.38 ug/L

07/16/13 03:05

Chloroform

ND

5.0

0.15 ug/L

07/16/13 03:05

Chloromethane

ND

10

0.55 ug/L

07/16/13 03:05

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/16/13 03:05

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/16/13 03:05

Cyclohexane

ND

10

0.36 ug/L

07/16/13 03:05

TestAmerica St. Louis

Page 59 of 88

7/29/2013

Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: DUPLICATE 03

Lab Sample ID: 160-2968-14

Date Collected: 07/11/13 00:00


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Analyte

Result Qualifier

Dibromochloromethane

ND

Dichlorodifluoromethane

ND

Ethylbenzene

ND

Isopropylbenzene

ND

Methyl acetate

ND

RL

MDL Unit

5.0

0.33 ug/L

Prepared

07/16/13 03:05

Analyzed

Dil Fac

10

0.45 ug/L

07/16/13 03:05

5.0

0.30 ug/L

07/16/13 03:05

5.0

0.26 ug/L

07/16/13 03:05

25

2.3 ug/L

07/16/13 03:05

5.0

0.40 ug/L

07/16/13 03:05

Methylcyclohexane

ND

10

0.26 ug/L

07/16/13 03:05

Methylene Chloride

ND

5.0

1.7 ug/L

07/16/13 03:05

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/16/13 03:05

o-Xylene

ND

5.0

0.32 ug/L

07/16/13 03:05

Styrene

ND

5.0

0.35 ug/L

07/16/13 03:05

Tetrachloroethene

ND

5.0

0.28 ug/L

07/16/13 03:05

Toluene

ND

5.0

1.0 ug/L

07/16/13 03:05

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/16/13 03:05

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/16/13 03:05

Trichloroethene

ND

5.0

0.29 ug/L

07/16/13 03:05

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/16/13 03:05

Vinyl chloride

ND

5.0

0.43 ug/L

07/16/13 03:05

Xylenes, Total

ND

10

0.85 ug/L

07/16/13 03:05

Methyl tert-butyl ether

Surrogate

0.71 J

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

117

82 - 132

07/16/13 03:05

4-Bromofluorobenzene (Surr)

98

82 - 121

07/16/13 03:05

Dibromofluoromethane (Surr)

101

85 - 119

07/16/13 03:05

95

85 - 115

07/16/13 03:05

Toluene-d8 (Surr)

Method: 6010C - Metals (ICP)


Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

200

80 ug/L

07/16/13 14:20

07/18/13 16:39

4.5 J

10

4.0 ug/L

07/16/13 14:20

07/18/13 16:39

3.2 J

10

2.0 ug/L

07/16/13 14:20

07/18/13 16:39

1700

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:39

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 16:39

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 16:39

Calcium

100000 E

1000

110 ug/L

07/16/13 14:20

07/18/13 16:39

Calcium

110000

10000

1100 ug/L

07/16/13 14:20

07/18/13 17:55

10

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 16:39

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 16:39

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 16:39

16000

100

28 ug/L

07/16/13 14:20

07/18/13 16:39

10

1.5 ug/L

07/16/13 14:20

07/18/13 16:39

Aluminum

ND

Antimony
Arsenic
Barium

Iron
Lead

2.4 J

Dil Fac

Magnesium

41000

1000

130 ug/L

07/16/13 14:20

07/18/13 16:39

Manganese

400

15

3.3 ug/L

07/16/13 14:20

07/18/13 16:39

Nickel

ND

40

13 ug/L

07/16/13 14:20

07/18/13 16:39

43000

5000

1700 ug/L

07/16/13 14:20

07/18/13 16:39

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 16:39

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 16:39

Sodium

54000

1000

320 ug/L

07/16/13 14:20

07/18/13 16:39

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 16:39

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 16:39

Potassium

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: DUPLICATE 03

Lab Sample ID: 160-2968-14

Date Collected: 07/11/13 00:00


Date Received: 07/12/13 08:15

Matrix: Water

Method: 6010C - Metals (ICP) (Continued)


Analyte

Result Qualifier

Zinc

ND

RL

MDL Unit

20

5.2 ug/L

Prepared

Analyzed

07/16/13 14:20

07/18/13 16:39

Dil Fac

6
RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 20:09

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 20:09

Arsenic

2.2 J

10

2.0 ug/L

07/16/13 14:16

07/17/13 20:09

Result Qualifier

Dil Fac

1700

50

4.0 ug/L

07/16/13 14:16

07/17/13 20:09

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 20:09

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 20:09

Barium

1000

110 ug/L

07/16/13 14:16

07/17/13 20:09

110000

5000

530 ug/L

07/16/13 14:16

07/17/13 21:15

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 20:09

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 20:09

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 20:09

16000

100

28 ug/L

07/16/13 14:16

07/17/13 20:09

Calcium
Calcium

Copper

Iron
Lead

99000 E

2.4 J

10

1.5 ug/L

07/16/13 14:16

07/17/13 20:09

130 ug/L

07/16/13 14:16

07/17/13 20:09

Magnesium

38000

1000

Manganese

380

15

3.3 ug/L

07/16/13 14:16

07/17/13 20:09

Nickel

ND

40

13 ug/L

07/16/13 14:16

07/17/13 20:09

44000

5000

1700 ug/L

07/16/13 14:16

07/17/13 20:09

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 20:09

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 20:09

52000

1000

320 ug/L

07/16/13 14:16

07/17/13 20:09

Potassium

Sodium
Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 20:09

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 20:09

Zinc

6.4 J

20

5.2 ug/L

07/16/13 14:16

07/17/13 20:09

Method: 7470A - Mercury (CVAA)


Analyte

Mercury

Result Qualifier

0.075 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:53

Dil Fac

Method: 7470A - Mercury (CVAA) - Dissolved


Analyte

Mercury

Result Qualifier

0.13 J

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:45

Dil Fac

General Chemistry
Analyte

Result Qualifier

Nitrate as N

0.0040 J

0.020

0.0040 mg/L

07/13/13 01:20

0.87

0.25

0.025 mg/L

07/13/13 01:20

Sulfate

8.2

0.50

0.050 mg/L

07/13/13 01:20

Iodide

ND

1.0

0.10 mg/L

07/16/13 21:48

Alkalinity

710 B

5.0

0.54 mg/L

07/25/13 12:51

RL

MDL Unit

4.0

0.40 mg/L

Bromide

RL

MDL Unit

Prepared

Analyzed

Dil Fac

General Chemistry - DL
Analyte

Chloride

Method: 6010C - Metals (ICP) - Dissolved


Analyte

Result Qualifier

55

Prepared

Analyzed

Dil Fac

07/13/13 01:34

20

TestAmerica St. Louis

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Client Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

Client Sample ID: TRIP BLANK

Lab Sample ID: 160-2968-15

Date Collected: 07/11/13 00:00


Date Received: 07/12/13 08:15

Matrix: Water

Method: 8260C - Volatile Organic Compounds by GC/MS


Analyte

RL

MDL Unit

1,1,1-Trichloroethane

Result Qualifier

ND

5.0

0.29 ug/L

Prepared

07/15/13 19:41

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/15/13 19:41

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/15/13 19:41

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/15/13 19:41

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/15/13 19:41

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/15/13 19:41

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/15/13 19:41

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/15/13 19:41

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/15/13 19:41

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/15/13 19:41

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/15/13 19:41

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/15/13 19:41

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/15/13 19:41

2-Butanone (MEK)

ND

20

0.39 ug/L

07/15/13 19:41

2-Hexanone

ND *

20

0.59 ug/L

07/15/13 19:41

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/15/13 19:41

Acetone

8.0 J

20

6.7 ug/L

07/15/13 19:41

Benzene

ND

5.0

0.25 ug/L

07/15/13 19:41

Bromodichloromethane

ND

5.0

0.25 ug/L

07/15/13 19:41

Bromoform

ND

5.0

0.37 ug/L

07/15/13 19:41

Bromomethane

ND

10

0.40 ug/L

07/15/13 19:41

Carbon disulfide

ND

5.0

0.37 ug/L

07/15/13 19:41

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/15/13 19:41

Chlorobenzene

ND

5.0

0.38 ug/L

07/15/13 19:41

Chloroethane

ND

10

0.38 ug/L

07/15/13 19:41

Chloroform

ND

5.0

0.15 ug/L

07/15/13 19:41

Chloromethane

ND

10

0.55 ug/L

07/15/13 19:41

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/15/13 19:41

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/15/13 19:41

Cyclohexane

ND

10

0.36 ug/L

07/15/13 19:41

Dibromochloromethane

ND

5.0

0.33 ug/L

07/15/13 19:41

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/15/13 19:41

Ethylbenzene

ND

5.0

0.30 ug/L

07/15/13 19:41

Isopropylbenzene

ND

5.0

0.26 ug/L

07/15/13 19:41

Methyl acetate

ND

25

2.3 ug/L

07/15/13 19:41

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/15/13 19:41

Methylcyclohexane

ND

10

0.26 ug/L

07/15/13 19:41

Methylene Chloride

ND

5.0

1.7 ug/L

07/15/13 19:41

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/15/13 19:41

o-Xylene

ND

5.0

0.32 ug/L

07/15/13 19:41

Styrene

ND

5.0

0.35 ug/L

07/15/13 19:41

Tetrachloroethene

ND

5.0

0.28 ug/L

07/15/13 19:41

Toluene

ND

5.0

1.0 ug/L

07/15/13 19:41

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/15/13 19:41

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/15/13 19:41

Trichloroethene

ND

5.0

0.29 ug/L

07/15/13 19:41

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/15/13 19:41

Vinyl chloride

ND

5.0

0.43 ug/L

07/15/13 19:41

Xylenes, Total

ND

10

0.85 ug/L

07/15/13 19:41

TestAmerica St. Louis

Page 62 of 88

7/29/2013

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Client Sample Results


Client: Engineering Management Support, Inc.
Project/Site: West Lake Landfill

1
TestAmerica Job ID: 160-2968-1

Client Sample ID: TRIP BLANK

Lab Sample ID: 160-2968-15

Date Collected: 07/11/13 00:00


Date Received: 07/12/13 08:15
Surrogate

Matrix: Water

3
4

%Recovery Qualifier

Limits

Prepared

Analyzed

Dil Fac

1,2-Dichloroethane-d4 (Surr)

106

82 - 132

07/15/13 19:41

4-Bromofluorobenzene (Surr)

98

82 - 121

07/15/13 19:41

Dibromofluoromethane (Surr)

99

85 - 119

07/15/13 19:41

Toluene-d8 (Surr)

99

85 - 115

07/15/13 19:41

5
6
7
8
9
10
11
12
13

TestAmerica St. Louis

Page 63 of 88

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS


Lab Sample ID: MB 160-60813/3-A
Matrix: Water
Analysis Batch: 60813

Client Sample ID: Method Blank


Prep Type: Total/NA

MB MB
Analyte

Result Qualifier

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

Prepared

07/15/13 18:23

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/15/13 18:23

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/15/13 18:23

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/15/13 18:23

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/15/13 18:23

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/15/13 18:23

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/15/13 18:23

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/15/13 18:23

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/15/13 18:23

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/15/13 18:23

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/15/13 18:23

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/15/13 18:23

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/15/13 18:23

2-Butanone (MEK)

ND

20

0.39 ug/L

07/15/13 18:23

2-Hexanone

ND

20

0.59 ug/L

07/15/13 18:23

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/15/13 18:23

Acetone

ND

20

6.7 ug/L

07/15/13 18:23

Benzene

ND

5.0

0.25 ug/L

07/15/13 18:23

Bromodichloromethane

ND

5.0

0.25 ug/L

07/15/13 18:23

Bromoform

ND

5.0

0.37 ug/L

07/15/13 18:23

Bromomethane

ND

10

0.40 ug/L

07/15/13 18:23

Carbon disulfide

ND

5.0

0.37 ug/L

07/15/13 18:23

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/15/13 18:23

Chlorobenzene

ND

5.0

0.38 ug/L

07/15/13 18:23

Chloroethane

ND

10

0.38 ug/L

07/15/13 18:23

Chloroform

ND

5.0

0.15 ug/L

07/15/13 18:23

Chloromethane

ND

10

0.55 ug/L

07/15/13 18:23

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/15/13 18:23

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/15/13 18:23

Cyclohexane

ND

10

0.36 ug/L

07/15/13 18:23

Dibromochloromethane

ND

5.0

0.33 ug/L

07/15/13 18:23

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/15/13 18:23

Ethylbenzene

ND

5.0

0.30 ug/L

07/15/13 18:23

Isopropylbenzene

ND

5.0

0.26 ug/L

07/15/13 18:23

Methyl acetate

ND

25

2.3 ug/L

07/15/13 18:23

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/15/13 18:23

Methylcyclohexane

ND

10

0.26 ug/L

07/15/13 18:23

Methylene Chloride

ND

5.0

1.7 ug/L

07/15/13 18:23

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/15/13 18:23

o-Xylene

ND

5.0

0.32 ug/L

07/15/13 18:23

Styrene

ND

5.0

0.35 ug/L

07/15/13 18:23

Tetrachloroethene

ND

5.0

0.28 ug/L

07/15/13 18:23

Toluene

ND

5.0

1.0 ug/L

07/15/13 18:23

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/15/13 18:23

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/15/13 18:23

Trichloroethene

ND

5.0

0.29 ug/L

07/15/13 18:23

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/15/13 18:23

Vinyl chloride

ND

5.0

0.43 ug/L

07/15/13 18:23

TestAmerica St. Louis

Page 64 of 88

7/29/2013

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QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Lab Sample ID: MB 160-60813/3-A
Matrix: Water
Analysis Batch: 60813

Client Sample ID: Method Blank


Prep Type: Total/NA

MB MB
Analyte

Xylenes, Total

Result Qualifier

ND

RL

MDL Unit

10

0.85 ug/L

Prepared

Analyzed

Dil Fac

Dil Fac

07/15/13 18:23

MB MB
Surrogate

%Recovery Qualifier

Limits

Prepared

Analyzed

1,2-Dichloroethane-d4 (Surr)

106

82 - 132

07/15/13 18:23

4-Bromofluorobenzene (Surr)

99

82 - 121

07/15/13 18:23

Dibromofluoromethane (Surr)

103

85 - 119

07/15/13 18:23

Toluene-d8 (Surr)

104

85 - 115

07/15/13 18:23

Lab Sample ID: LCS 160-60813/4-A


Matrix: Water
Analysis Batch: 60813

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Spike

Analyte

Added

LCS LCS
Result Qualifier

Unit

%Rec

Limits

50.0

51.6

ug/L

103

85 - 115

1,1,2,2-Tetrachloroethane

50.0

54.6

ug/L

109

84 - 115

1,1,2-Trichloroethane

50.0

51.8

ug/L

104

85 - 115

1,1-Dichloroethane

50.0

50.4

ug/L

101

85 - 115

1,1-Dichloroethene

50.0

49.7

ug/L

99

85 - 118

1,2,4-Trichlorobenzene

50.0

52.4

ug/L

105

75 - 124

1,2-Dibromo-3-Chloropropane

50.0

54.5

ug/L

109

71 - 123

1,2-Dibromoethane (EDB)

50.0

51.4

ug/L

103

85 - 115

1,2-Dichlorobenzene

50.0

52.9

ug/L

106

85 - 115

1,2-Dichloroethane

50.0

53.0

ug/L

106

79 - 122

1,2-Dichloropropane

50.0

49.9

ug/L

100

85 - 115

1,3-Dichlorobenzene

50.0

51.5

ug/L

103

85 - 115

1,4-Dichlorobenzene

50.0

49.2

ug/L

98

85 - 115

2-Butanone (MEK)

50.0

58.4

ug/L

117

71 - 123

2-Hexanone

50.0

61.9 *

ug/L

124

66 - 121

4-Methyl-2-pentanone (MIBK)

50.0

60.5

ug/L

121

74 - 123

Acetone

50.0

62.2

ug/L

124

51 - 140

Benzene

50.0

49.2

ug/L

98

85 - 115

Bromodichloromethane

50.0

53.1

ug/L

106

85 - 117

Bromoform

50.0

54.0

ug/L

108

85 - 115

Bromomethane

50.0

56.0

ug/L

112

70 - 135

Carbon disulfide

50.0

50.6

ug/L

101

85 - 123

Carbon tetrachloride

50.0

51.3

ug/L

103

85 - 118

Chlorobenzene

50.0

49.6

ug/L

99

85 - 115

Chloroethane

50.0

59.0

ug/L

118

75 - 125

Chloroform

50.0

50.2

ug/L

100

85 - 115

Chloromethane

50.0

50.3

ug/L

101

73 - 132

cis-1,2-Dichloroethene

50.0

48.7

ug/L

97

85 - 115

cis-1,3-Dichloropropene

50.0

50.8

ug/L

102

85 - 127

Cyclohexane

50.0

50.8

ug/L

102

73 - 115

Dibromochloromethane

50.0

50.5

ug/L

101

85 - 115

Dichlorodifluoromethane

50.0

54.4

ug/L

109

62 - 115

Ethylbenzene

50.0

51.5

ug/L

103

85 - 115

Isopropylbenzene

50.0

52.8

ug/L

106

85 - 124

Methyl acetate

250

269

ug/L

108

73 - 135

10
12
13

TestAmerica St. Louis

Page 65 of 88

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%Rec.

1,1,1-Trichloroethane

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Lab Sample ID: LCS 160-60813/4-A
Matrix: Water
Analysis Batch: 60813

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Spike

Analyte

Added

LCS LCS
Result Qualifier

%Rec.
Unit

%Rec

Limits

Methyl tert-butyl ether

50.0

54.7

ug/L

109

73 - 115

Methylcyclohexane

50.0

52.8

ug/L

106

85 - 134

Methylene Chloride

50.0

50.0

ug/L

100

84 - 115

m-Xylene & p-Xylene

50.0

51.3

ug/L

103

85 - 115

o-Xylene

50.0

49.8

ug/L

100

85 - 115

Styrene

50.0

51.4

ug/L

103

85 - 115

Tetrachloroethene

50.0

50.6

ug/L

101

85 - 115

Toluene

50.0

49.3

ug/L

99

85 - 115

trans-1,2-Dichloroethene

50.0

47.2

ug/L

94

85 - 115

trans-1,3-Dichloropropene

50.0

50.0

ug/L

100

85 - 123

Trichloroethene

50.0

49.0

ug/L

98

85 - 115

Trichlorofluoromethane

50.0

53.9

ug/L

108

85 - 116

Vinyl chloride

50.0

48.5

ug/L

97

68 - 133

Xylenes, Total

100

101

ug/L

101

70 - 130

6
7
8
9
10
11
12
13

LCS LCS
Surrogate

%Recovery Qualifier

Limits

1,2-Dichloroethane-d4 (Surr)

107

82 - 132

4-Bromofluorobenzene (Surr)

100

82 - 121

Dibromofluoromethane (Surr)

99

85 - 119

Toluene-d8 (Surr)

99

85 - 115

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 60813

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

Result Qualifier

Spike
Added

MS MS
Result Qualifier

%Rec.
Unit

%Rec

Limits

1,1,1-Trichloroethane

ND

50.0

53.3

ug/L

107

85 - 118

1,1,2,2-Tetrachloroethane

ND

50.0

53.9

ug/L

108

85 - 116

37

50.0

90.8

ug/L

108

85 - 115

1,1-Dichloroethane

ND

50.0

51.2

ug/L

102

85 - 115

1,1-Dichloroethene

ND

50.0

51.8

ug/L

104

85 - 118

1,2,4-Trichlorobenzene

ND

50.0

51.7

ug/L

103

75 - 124

1,2-Dibromo-3-Chloropropane

ND

50.0

55.5

ug/L

111

71 - 123

1,2-Dibromoethane (EDB)

ND

50.0

52.0

ug/L

104

85 - 115

1,2-Dichlorobenzene

ND

50.0

52.5

ug/L

105

84 - 115

1,2-Dichloroethane

ND

50.0

56.7

ug/L

113

80 - 125

1,2-Dichloropropane

ND

50.0

52.6

ug/L

105

85 - 117

1,3-Dichlorobenzene

ND

50.0

51.9

ug/L

104

84 - 115

1,4-Dichlorobenzene

ND

50.0

50.6

ug/L

101

85 - 115

2-Butanone (MEK)

ND

50.0

54.7

ug/L

109

73 - 133

2-Hexanone

ND *

50.0

56.6

ug/L

113

66 - 121

4-Methyl-2-pentanone (MIBK)

ND

50.0

54.9

ug/L

110

77 - 134

Acetone

30

50.0

86.4

ug/L

112

38 - 150

Benzene

34

50.0

83.6

ug/L

100

85 - 115

Bromodichloromethane

ND

50.0

52.3

ug/L

105

56 - 119

Bromoform

ND

50.0

54.2

ug/L

108

84 - 116

Bromomethane

ND

50.0

57.6

ug/L

115

70 - 135

Carbon disulfide

ND

50.0

53.4

ug/L

107

85 - 127

1,1,2-Trichloroethane

TestAmerica St. Louis

Page 66 of 88

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Lab Sample ID: 160-2968-6 MS
Matrix: Water
Analysis Batch: 60813

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

Result Qualifier

Spike
Added

MS MS
Result Qualifier

%Rec.
Unit

%Rec

Limits

Carbon tetrachloride

ND

50.0

53.4

ug/L

107

85 - 121

Chlorobenzene

ND

50.0

51.9

ug/L

104

85 - 115

Chloroethane

ND

50.0

63.6 F

ug/L

127

73 - 123

Chloroform

ND

50.0

50.8

ug/L

102

85 - 115

Chloromethane

ND

50.0

55.1

ug/L

110

67 - 130

cis-1,2-Dichloroethene

ND

50.0

50.6

ug/L

101

80 - 116

cis-1,3-Dichloropropene

ND

50.0

50.5

ug/L

101

85 - 124

Cyclohexane

ND

50.0

51.7

ug/L

103

73 - 115

Dibromochloromethane

ND

50.0

51.3

ug/L

103

85 - 115

Dichlorodifluoromethane

ND

50.0

57.5

ug/L

115

85 - 119

Ethylbenzene

ND

50.0

54.2

ug/L

108

85 - 115

Isopropylbenzene

ND

50.0

52.9

ug/L

106

85 - 124

Methyl acetate

ND

250

288

ug/L

115

49 - 150

Methyl tert-butyl ether

4.3 J

50.0

60.8

ug/L

113

75 - 115

Methylcyclohexane

ND

50.0

53.8

ug/L

108

85 - 137

Methylene Chloride

ND

50.0

50.7

ug/L

101

85 - 115

m-Xylene & p-Xylene

ND

50.0

52.9

ug/L

106

85 - 115

o-Xylene

ND

50.0

51.3

ug/L

103

85 - 118

Styrene

ND

50.0

52.8

ug/L

106

85 - 115

Tetrachloroethene

ND

50.0

49.8

ug/L

100

85 - 118

Toluene

ND

50.0

50.8

ug/L

102

85 - 118

trans-1,2-Dichloroethene

ND

50.0

48.7

ug/L

97

84 - 115

trans-1,3-Dichloropropene

ND

50.0

50.9

ug/L

102

85 - 127

Trichloroethene

ND

50.0

48.7

ug/L

97

85 - 115

Trichlorofluoromethane

ND

50.0

57.4

ug/L

115

85 - 115

Vinyl chloride

ND

50.0

55.5

ug/L

111

63 - 129

Xylenes, Total

ND

100

104

ug/L

104

70 - 130

6
7
8
9
10
11
12
13

MS MS
Surrogate

%Recovery Qualifier

Limits

1,2-Dichloroethane-d4 (Surr)

110

82 - 132

4-Bromofluorobenzene (Surr)

102

82 - 121

Dibromofluoromethane (Surr)

100

85 - 119

Toluene-d8 (Surr)

101

85 - 115

Lab Sample ID: 160-2968-6 MSD


Matrix: Water
Analysis Batch: 60813

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

Result Qualifier

Spike
Added

MSD MSD
Result Qualifier

%Rec.
Unit

%Rec

Limits

RPD
RPD

Limit

1,1,1-Trichloroethane

ND

50.0

53.5

ug/L

107

85 - 118

20

1,1,2,2-Tetrachloroethane

ND

50.0

54.2

ug/L

108

85 - 116

20

37

50.0

88.8

ug/L

104

85 - 115

20

1,1-Dichloroethane

ND

50.0

52.7

ug/L

105

85 - 115

20

1,1-Dichloroethene

ND

50.0

51.6

ug/L

103

85 - 118

20

1,2,4-Trichlorobenzene

ND

50.0

48.7

ug/L

97

75 - 124

20

1,2-Dibromo-3-Chloropropane

ND

50.0

56.7

ug/L

113

71 - 123

20

1,2-Dibromoethane (EDB)

ND

50.0

52.3

ug/L

105

85 - 115

20

1,2-Dichlorobenzene

ND

50.0

52.6

ug/L

105

84 - 115

20

1,1,2-Trichloroethane

TestAmerica St. Louis

Page 67 of 88

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Lab Sample ID: 160-2968-6 MSD
Matrix: Water
Analysis Batch: 60813

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

Result Qualifier

Spike
Added

MSD MSD
Result Qualifier

%Rec.
Unit

%Rec

Limits

RPD
RPD

Limit

1,2-Dichloroethane

ND

50.0

57.0

ug/L

114

80 - 125

20

1,2-Dichloropropane

ND

50.0

52.0

ug/L

104

85 - 117

20

1,3-Dichlorobenzene

ND

50.0

51.0

ug/L

102

84 - 115

20

1,4-Dichlorobenzene

ND

50.0

50.3

ug/L

101

85 - 115

20

2-Butanone (MEK)

ND

50.0

56.3

ug/L

113

73 - 133

20

2-Hexanone

ND *

50.0

62.3 F

ug/L

125

66 - 121

10

20

4-Methyl-2-pentanone (MIBK)

ND

50.0

60.5

ug/L

121

77 - 134

10

20

30

50.0

95.0

ug/L

129

38 - 150

10

20

Acetone
Benzene

34

50.0

85.1

ug/L

103

85 - 115

20

Bromodichloromethane

ND

50.0

54.3

ug/L

109

56 - 119

20

Bromoform

ND

50.0

53.0

ug/L

106

84 - 116

20

Bromomethane

ND

50.0

62.5

ug/L

125

70 - 135

20

Carbon disulfide

ND

50.0

52.3

ug/L

105

85 - 127

20

Carbon tetrachloride

ND

50.0

52.7

ug/L

105

85 - 121

20

Chlorobenzene

ND

50.0

50.8

ug/L

102

85 - 115

20

Chloroethane

ND

50.0

65.5 F

ug/L

131

73 - 123

20

Chloroform

ND

50.0

53.7

ug/L

107

85 - 115

20

Chloromethane

ND

50.0

55.1

ug/L

110

67 - 130

20

cis-1,2-Dichloroethene

ND

50.0

50.4

ug/L

101

80 - 116

20

cis-1,3-Dichloropropene

ND

50.0

52.1

ug/L

104

85 - 124

20

Cyclohexane

ND

50.0

51.9

ug/L

104

73 - 115

20

Dibromochloromethane

ND

50.0

49.8

ug/L

100

85 - 115

20

Dichlorodifluoromethane

ND

50.0

59.3

ug/L

119

85 - 119

20

Ethylbenzene

ND

50.0

52.7

ug/L

105

85 - 115

20

Isopropylbenzene

ND

50.0

52.6

ug/L

105

85 - 124

20

Methyl acetate

ND

250

294

ug/L

118

49 - 150

20

Methyl tert-butyl ether

4.3 J

50.0

60.7

ug/L

113

75 - 115

20

Methylcyclohexane

ND

50.0

53.1

ug/L

106

85 - 137

20

Methylene Chloride

ND

50.0

52.8

ug/L

106

85 - 115

20

m-Xylene & p-Xylene

ND

50.0

51.6

ug/L

103

85 - 115

20

o-Xylene

ND

50.0

51.6

ug/L

103

85 - 118

20

Styrene

ND

50.0

52.9

ug/L

106

85 - 115

20

Tetrachloroethene

ND

50.0

49.4

ug/L

99

85 - 118

20

Toluene

ND

50.0

49.0

ug/L

98

85 - 118

20

trans-1,2-Dichloroethene

ND

50.0

49.1

ug/L

98

84 - 115

20

trans-1,3-Dichloropropene

ND

50.0

49.2

ug/L

98

85 - 127

20

Trichloroethene

ND

50.0

49.1

ug/L

98

85 - 115

20

Trichlorofluoromethane

ND

50.0

57.7

ug/L

115

85 - 115

20

Vinyl chloride

ND

50.0

55.1

ug/L

110

63 - 129

20

Xylenes, Total

ND

100

103

ug/L

103

70 - 130

20

MSD MSD
Surrogate

%Recovery Qualifier

Limits

1,2-Dichloroethane-d4 (Surr)

112

82 - 132

4-Bromofluorobenzene (Surr)

102

82 - 121

Dibromofluoromethane (Surr)

105

85 - 119

Toluene-d8 (Surr)

100

85 - 115

TestAmerica St. Louis

Page 68 of 88

7/29/2013

4
5
6
7
8
9
10
11
12
13

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Lab Sample ID: MB 160-61806/3-A
Matrix: Water
Analysis Batch: 61806

Client Sample ID: Method Blank


Prep Type: Total/NA

MB MB
Analyte

Result Qualifier

RL

MDL Unit

1,1,1-Trichloroethane

ND

5.0

0.29 ug/L

Prepared

07/17/13 18:59

Analyzed

Dil Fac

1,1,2,2-Tetrachloroethane

ND

5.0

0.43 ug/L

07/17/13 18:59

1,1,2-Trichloroethane

ND

5.0

0.57 ug/L

07/17/13 18:59

1,1-Dichloroethane

ND

5.0

0.39 ug/L

07/17/13 18:59

1,1-Dichloroethene

ND

5.0

0.37 ug/L

07/17/13 18:59

1,2,4-Trichlorobenzene

ND

5.0

0.55 ug/L

07/17/13 18:59

1,2-Dibromo-3-Chloropropane

ND

10

1.2 ug/L

07/17/13 18:59

1,2-Dibromoethane (EDB)

ND

5.0

0.44 ug/L

07/17/13 18:59

1,2-Dichlorobenzene

ND

5.0

0.28 ug/L

07/17/13 18:59

1,2-Dichloroethane

ND

5.0

0.37 ug/L

07/17/13 18:59

1,2-Dichloropropane

ND

5.0

0.32 ug/L

07/17/13 18:59

1,3-Dichlorobenzene

ND

5.0

0.23 ug/L

07/17/13 18:59

1,4-Dichlorobenzene

ND

5.0

0.35 ug/L

07/17/13 18:59

2-Butanone (MEK)

ND

20

0.39 ug/L

07/17/13 18:59

2-Hexanone

ND

20

0.59 ug/L

07/17/13 18:59

4-Methyl-2-pentanone (MIBK)

ND

20

0.33 ug/L

07/17/13 18:59

Acetone

ND

20

6.7 ug/L

07/17/13 18:59

Benzene

ND

5.0

0.25 ug/L

07/17/13 18:59

Bromodichloromethane

ND

5.0

0.25 ug/L

07/17/13 18:59

Bromoform

ND

5.0

0.37 ug/L

07/17/13 18:59

Bromomethane

ND

10

0.40 ug/L

07/17/13 18:59

Carbon disulfide

ND

5.0

0.37 ug/L

07/17/13 18:59

Carbon tetrachloride

ND

5.0

0.36 ug/L

07/17/13 18:59

Chlorobenzene

ND

5.0

0.38 ug/L

07/17/13 18:59

Chloroethane

ND

10

0.38 ug/L

07/17/13 18:59

Chloroform

ND

5.0

0.15 ug/L

07/17/13 18:59

Chloromethane

ND

10

0.55 ug/L

07/17/13 18:59

cis-1,2-Dichloroethene

ND

5.0

0.16 ug/L

07/17/13 18:59

cis-1,3-Dichloropropene

ND

5.0

0.34 ug/L

07/17/13 18:59

Cyclohexane

ND

10

0.36 ug/L

07/17/13 18:59

Dibromochloromethane

ND

5.0

0.33 ug/L

07/17/13 18:59

Dichlorodifluoromethane

ND

10

0.45 ug/L

07/17/13 18:59

Ethylbenzene

ND

5.0

0.30 ug/L

07/17/13 18:59

Isopropylbenzene

ND

5.0

0.26 ug/L

07/17/13 18:59

Methyl acetate

ND

25

2.3 ug/L

07/17/13 18:59

Methyl tert-butyl ether

ND

5.0

0.40 ug/L

07/17/13 18:59

Methylcyclohexane

ND

10

0.26 ug/L

07/17/13 18:59

Methylene Chloride

ND

5.0

1.7 ug/L

07/17/13 18:59

m-Xylene & p-Xylene

ND

5.0

0.57 ug/L

07/17/13 18:59

o-Xylene

ND

5.0

0.32 ug/L

07/17/13 18:59

Styrene

ND

5.0

0.35 ug/L

07/17/13 18:59

Tetrachloroethene

ND

5.0

0.28 ug/L

07/17/13 18:59

Toluene

ND

5.0

1.0 ug/L

07/17/13 18:59

trans-1,2-Dichloroethene

ND

5.0

0.18 ug/L

07/17/13 18:59

trans-1,3-Dichloropropene

ND

5.0

0.35 ug/L

07/17/13 18:59

Trichloroethene

ND

5.0

0.29 ug/L

07/17/13 18:59

Trichlorofluoromethane

ND

5.0

0.22 ug/L

07/17/13 18:59

Vinyl chloride

ND

5.0

0.43 ug/L

07/17/13 18:59

TestAmerica St. Louis

Page 69 of 88

7/29/2013

6
7
8
9
10
11
12
13

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Lab Sample ID: MB 160-61806/3-A
Matrix: Water
Analysis Batch: 61806

Client Sample ID: Method Blank


Prep Type: Total/NA

MB MB
Analyte

Xylenes, Total

Result Qualifier

ND

RL

MDL Unit

10

0.85 ug/L

Prepared

Analyzed

Dil Fac

Dil Fac

07/17/13 18:59

MB MB
Surrogate

%Recovery Qualifier

Limits

Prepared

Analyzed

1,2-Dichloroethane-d4 (Surr)

100

82 - 132

07/17/13 18:59

4-Bromofluorobenzene (Surr)

87

82 - 121

07/17/13 18:59

97

85 - 119

07/17/13 18:59

100

85 - 115

07/17/13 18:59

Dibromofluoromethane (Surr)
Toluene-d8 (Surr)

Lab Sample ID: LCS 160-61806/4-A


Matrix: Water
Analysis Batch: 61806

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Spike

Analyte

Added

LCS LCS
Result Qualifier

Unit

%Rec

Limits

50.0

45.5

ug/L

91

85 - 115

1,1,2,2-Tetrachloroethane

50.0

50.7

ug/L

101

84 - 115

1,1,2-Trichloroethane

50.0

52.3

ug/L

105

85 - 115

1,1-Dichloroethane

50.0

51.9

ug/L

104

85 - 115

1,1-Dichloroethene

50.0

46.0

ug/L

92

85 - 118

1,2,4-Trichlorobenzene

50.0

44.4

ug/L

89

75 - 124

1,2-Dibromo-3-Chloropropane

50.0

52.0

ug/L

104

71 - 123

1,2-Dibromoethane (EDB)

50.0

49.9

ug/L

100

85 - 115

1,2-Dichlorobenzene

50.0

50.1

ug/L

100

85 - 115

1,2-Dichloroethane

50.0

47.1

ug/L

94

79 - 122

1,2-Dichloropropane

50.0

52.8

ug/L

106

85 - 115

1,3-Dichlorobenzene

50.0

50.8

ug/L

102

85 - 115

1,4-Dichlorobenzene

50.0

51.0

ug/L

102

85 - 115

2-Butanone (MEK)

50.0

52.6

ug/L

105

71 - 123

2-Hexanone

50.0

52.9

ug/L

106

66 - 121

4-Methyl-2-pentanone (MIBK)

50.0

51.9

ug/L

104

74 - 123

Acetone

50.0

47.5

ug/L

95

51 - 140

Benzene

50.0

50.2

ug/L

100

85 - 115

Bromodichloromethane

50.0

48.2

ug/L

96

85 - 117

Bromoform

50.0

43.5

ug/L

87

85 - 115

Bromomethane

50.0

56.2

ug/L

112

70 - 135

Carbon disulfide

50.0

47.4

ug/L

95

85 - 123

Carbon tetrachloride

50.0

46.9

ug/L

94

85 - 118

Chlorobenzene

50.0

52.6

ug/L

105

85 - 115

Chloroethane

50.0

75.0 *

ug/L

150

75 - 125

Chloroform

50.0

46.6

ug/L

93

85 - 115

Chloromethane

50.0

50.1

ug/L

100

73 - 132

cis-1,2-Dichloroethene

50.0

48.1

ug/L

96

85 - 115

cis-1,3-Dichloropropene

50.0

54.0

ug/L

108

85 - 127

Cyclohexane

50.0

49.5

ug/L

99

73 - 115

Dibromochloromethane

50.0

48.4

ug/L

97

85 - 115

Dichlorodifluoromethane

50.0

44.1

ug/L

88

62 - 115

Ethylbenzene

50.0

47.3

ug/L

95

85 - 115

Isopropylbenzene

50.0

51.4

ug/L

103

85 - 124

Methyl acetate

250

256

ug/L

103

73 - 135

10
12
13

TestAmerica St. Louis

Page 70 of 88

9
11

%Rec.

1,1,1-Trichloroethane

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


Lab Sample ID: LCS 160-61806/4-A
Matrix: Water
Analysis Batch: 61806

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Spike

Analyte

LCS LCS

Added

Result Qualifier

%Rec.
Unit

%Rec

Limits

Methyl tert-butyl ether

50.0

48.2

ug/L

96

73 - 115

Methylcyclohexane

50.0

51.5

ug/L

103

85 - 134

Methylene Chloride

50.0

47.3

ug/L

95

84 - 115

m-Xylene & p-Xylene

50.0

51.4

ug/L

103

85 - 115

o-Xylene

50.0

51.0

ug/L

102

85 - 115

Styrene

50.0

51.4

ug/L

103

85 - 115

Tetrachloroethene

50.0

50.8

ug/L

102

85 - 115

Toluene

50.0

52.0

ug/L

104

85 - 115

trans-1,2-Dichloroethene

50.0

47.3

ug/L

95

85 - 115

trans-1,3-Dichloropropene

50.0

56.1

ug/L

112

85 - 123

Trichloroethene

50.0

49.4

ug/L

99

85 - 115

Trichlorofluoromethane

50.0

45.5

ug/L

91

85 - 116

Vinyl chloride

50.0

54.0

ug/L

108

68 - 133

Xylenes, Total

100

102

ug/L

102

70 - 130

6
7
8
9
10
11
12
13

LCS LCS
Surrogate

%Recovery Qualifier

Limits

1,2-Dichloroethane-d4 (Surr)

92

82 - 132

4-Bromofluorobenzene (Surr)

92

82 - 121

Dibromofluoromethane (Surr)

92

85 - 119

Toluene-d8 (Surr)

99

85 - 115

Method: 6010C - Metals (ICP)


Lab Sample ID: MB 160-60808/1-A
Matrix: Water
Analysis Batch: 61388

Client Sample ID: Method Blank


Prep Type: Total/NA
Prep Batch: 60808
MB MB

Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:16

07/17/13 18:51

Dil Fac

Antimony

ND

10

4.0 ug/L

07/16/13 14:16

07/17/13 18:51

Arsenic

ND

10

2.0 ug/L

07/16/13 14:16

07/17/13 18:51

Barium

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 18:51

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:16

07/17/13 18:51

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:16

07/17/13 18:51

Calcium

ND

1000

110 ug/L

07/16/13 14:16

07/17/13 18:51

Chromium

ND

10

3.1 ug/L

07/16/13 14:16

07/17/13 18:51

Cobalt

ND

50

4.0 ug/L

07/16/13 14:16

07/17/13 18:51

Copper

ND

25

4.6 ug/L

07/16/13 14:16

07/17/13 18:51

Iron

ND

100

28 ug/L

07/16/13 14:16

07/17/13 18:51

Lead

ND

10

1.5 ug/L

07/16/13 14:16

07/17/13 18:51

Magnesium

ND

1000

130 ug/L

07/16/13 14:16

07/17/13 18:51

Manganese

ND

15

3.3 ug/L

07/16/13 14:16

07/17/13 18:51

Nickel

ND

40

13 ug/L

07/16/13 14:16

07/17/13 18:51

Potassium

ND

5000

1700 ug/L

07/16/13 14:16

07/17/13 18:51

Selenium

ND

15

2.7 ug/L

07/16/13 14:16

07/17/13 18:51

Silver

ND

10

6.0 ug/L

07/16/13 14:16

07/17/13 18:51

Sodium

ND

1000

320 ug/L

07/16/13 14:16

07/17/13 18:51

Thallium

ND ^

20

4.0 ug/L

07/16/13 14:16

07/17/13 18:51

TestAmerica St. Louis

Page 71 of 88

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 6010C - Metals (ICP) (Continued)


Lab Sample ID: MB 160-60808/1-A
Matrix: Water
Analysis Batch: 61388

Client Sample ID: Method Blank


Prep Type: Total/NA
Prep Batch: 60808
MB MB

Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

Vanadium

ND

50

4.1 ug/L

07/16/13 14:16

07/17/13 18:51

Zinc

ND

20

5.2 ug/L

07/16/13 14:16

07/17/13 18:51

Lab Sample ID: LCS 160-60808/2-A


Matrix: Water
Analysis Batch: 61388

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Prep Batch: 60808
Spike

LCS LCS

Added

Aluminum

10000

9660

ug/L

97

80 - 120

Antimony

500

518

ug/L

104

80 - 120

Arsenic

1000

1040

ug/L

104

80 - 120

Barium

1000

1020

ug/L

102

80 - 120

Beryllium

1000

994

ug/L

99

80 - 120

Cadmium

Result Qualifier

%Rec.

Analyte

Unit

%Rec

1000

1040

ug/L

104

80 - 120

10100

ug/L

101

80 - 120

Chromium

1000

1070

ug/L

107

80 - 120

Cobalt

1000

1070

ug/L

107

80 - 120

Copper

1000

1040

ug/L

104

80 - 120

Iron

10000

10300

ug/L

103

80 - 120

Lead

1000

1110

ug/L

111

80 - 120

Magnesium

10000

9920

ug/L

99

80 - 120

Manganese

1000

1010

ug/L

101

80 - 120

Nickel

1000

1080

ug/L

108

80 - 120

Potassium

10000

10300

ug/L

103

80 - 120

Selenium

1000

1050

ug/L

105

80 - 120

100

88.8

ug/L

89

80 - 120

10000

9610

80 - 120

Silver
Sodium
Thallium

200

ug/L

96

226 ^

ug/L

113

80 - 120

Vanadium

1000

959

ug/L

96

80 - 120

Zinc

1000

1050

ug/L

105

80 - 120

Lab Sample ID: MB 160-60810/1-A


Matrix: Water
Analysis Batch: 61576
D

12
13

RL

MDL Unit

Prepared

Analyzed

Aluminum

ND

200

80 ug/L

07/16/13 14:20

07/18/13 15:26

Antimony

ND

10

4.0 ug/L

07/16/13 14:20

07/18/13 15:26

Arsenic

ND

10

2.0 ug/L

07/16/13 14:20

07/18/13 15:26

Barium

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:26

Beryllium

ND

5.0

0.61 ug/L

07/16/13 14:20

07/18/13 15:26

Cadmium

ND

5.0

0.91 ug/L

07/16/13 14:20

07/18/13 15:26

Calcium

ND

1000

110 ug/L

07/16/13 14:20

07/18/13 15:26

Chromium

ND

10

3.1 ug/L

07/16/13 14:20

07/18/13 15:26

Cobalt

ND

50

4.0 ug/L

07/16/13 14:20

07/18/13 15:26

Copper

ND

25

4.6 ug/L

07/16/13 14:20

07/18/13 15:26

Iron

ND

100

28 ug/L

07/16/13 14:20

07/18/13 15:26

Lead

ND

10

1.5 ug/L

07/16/13 14:20

07/18/13 15:26

Magnesium

ND

1000

130 ug/L

07/16/13 14:20

07/18/13 15:26

Dil Fac

TestAmerica St. Louis

Page 72 of 88

11

Client Sample ID: Method Blank


Prep Type: Total/NA
Prep Batch: 60810
Result Qualifier

10

MB MB
Analyte

Limits

10000

Calcium

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 6010C - Metals (ICP) (Continued)


Lab Sample ID: MB 160-60810/1-A
Matrix: Water
Analysis Batch: 61576

Client Sample ID: Method Blank


Prep Type: Total/NA
Prep Batch: 60810
MB MB

Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

Manganese

ND

15

3.3 ug/L

07/16/13 14:20

07/18/13 15:26

Nickel

ND

40

13 ug/L

07/16/13 14:20

07/18/13 15:26

Potassium

ND

5000

1700 ug/L

07/16/13 14:20

07/18/13 15:26

Selenium

ND

15

2.7 ug/L

07/16/13 14:20

07/18/13 15:26

Silver

ND

10

6.0 ug/L

07/16/13 14:20

07/18/13 15:26

Sodium

ND

1000

320 ug/L

07/16/13 14:20

07/18/13 15:26

Thallium

ND

20

4.0 ug/L

07/16/13 14:20

07/18/13 15:26

Vanadium

ND

50

4.1 ug/L

07/16/13 14:20

07/18/13 15:26

Zinc

ND

20

5.2 ug/L

07/16/13 14:20

07/18/13 15:26

Lab Sample ID: LCS 160-60810/2-A


Matrix: Water
Analysis Batch: 61576

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Prep Batch: 60810
Spike

LCS LCS

%Rec.

Analyte

Added

Result Qualifier

Unit

Aluminum

10000

10300

ug/L

103

80 - 120

Antimony

500

532

ug/L

106

80 - 120

Arsenic

1000

1050

ug/L

105

80 - 120

Barium

1000

1070

ug/L

107

80 - 120

Beryllium

1000

1070

ug/L

107

80 - 120

Cadmium

1000

1070

ug/L

107

80 - 120

10000

10900

ug/L

109

80 - 120

Chromium

1000

1090

ug/L

109

80 - 120

Cobalt

1000

1110

ug/L

111

80 - 120

Copper

1000

1070

ug/L

107

80 - 120

Iron

10000

10700

ug/L

107

80 - 120

Lead

1000

1110

ug/L

111

80 - 120

Magnesium

10000

10700

ug/L

107

80 - 120

Manganese

1000

1080

ug/L

108

80 - 120

Nickel

1000

1110

ug/L

111

80 - 120

Potassium

10000

10400

ug/L

104

80 - 120

Selenium

1000

1060

ug/L

106

80 - 120

100

91.2

ug/L

91

80 - 120

10000

10400

ug/L

104

80 - 120

200

238

ug/L

119

80 - 120

Vanadium

1000

1060

ug/L

106

80 - 120

Zinc

1000

1070

ug/L

107

80 - 120

Calcium

Silver
Sodium
Thallium

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 61576

Aluminum

Result Qualifier

98 J

Spike

MS MS
%Rec

Added

Result Qualifier

Unit

10000

10700

ug/L

106

75 - 125

Limits

Antimony

ND

500

541

ug/L

108

75 - 125

Arsenic

7.4 J

1000

1080

ug/L

107

75 - 125

Barium

580

1000

1650

ug/L

107

75 - 125

Beryllium

ND

1000

1080

ug/L

108

75 - 125

Cadmium

ND

1000

1070

ug/L

107

75 - 125

TestAmerica St. Louis

Page 73 of 88

6
7
8
9
10
11
12
13

%Rec.
D

Limits

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60810
Sample Sample

Analyte

%Rec

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 6010C - Metals (ICP) (Continued)


Lab Sample ID: 160-2968-6 MS
Matrix: Water
Analysis Batch: 61576

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60810
Sample Sample

Analyte

Calcium

Result Qualifier

Spike
Added

MS MS
Result Qualifier

%Rec

Limits

180000 E

10000

ug/L

121

75 - 125

ND

1000

1070

ug/L

107

75 - 125

Cobalt

6.9 J

1000

1060

ug/L

106

75 - 125

Copper

ND

1000

1060

ug/L

106

75 - 125

4900

Chromium

Iron

187000 E 4

%Rec.
Unit

10000

15500

ug/L

106

75 - 125

2.1 J

1000

1060

ug/L

106

75 - 125

Magnesium

78000 E

10000

Manganese

940

1000

Lead

Nickel

90100 E 4

ug/L

118

75 - 125

2000

ug/L

106

75 - 125

21 J

1000

1070

ug/L

105

75 - 125

Potassium

3100 J

10000

13900

ug/L

108

75 - 125

Selenium

ND

1000

1070

ug/L

107

75 - 125

Silver

ND

100

91.1

ug/L

91

75 - 125

Sodium

14000

10000

24600

ug/L

107

75 - 125

Thallium

ND

200

222

ug/L

111

75 - 125

Vanadium

ND

1000

1050

ug/L

105

75 - 125

Zinc

7.0 J

1000

1080

ug/L

107

75 - 125

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 61576

Calcium
Iron
Magnesium

Result Qualifier

Spike
Added

200000

10000

5000

10000

79000

10000

MS MS
Result Qualifier

211000 4

8
9
10
11
12
13

Limits

90

75 - 125

15800

ug/L

108

75 - 125

89500 4

ug/L

103

75 - 125

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60810
Sample Sample

Aluminum

%Rec

ug/L

Lab Sample ID: 160-2968-6 MSD


Matrix: Water
Analysis Batch: 61576
Analyte

%Rec.
Unit

Result Qualifier

98 J

Spike

MSD MSD

%Rec.

Added

Result Qualifier

Unit

%Rec

10000

10800

ug/L

107

500

526

ug/L

105

Limits

RPD
RPD

Limit

75 - 125

20

75 - 125

20

Antimony

ND

Arsenic

7.4 J

1000

1050

ug/L

104

75 - 125

20

Barium

580

1000

1660

ug/L

108

75 - 125

20

Beryllium

ND

1000

1080

ug/L

108

75 - 125

20

Cadmium

ND

1000

1040

ug/L

104

75 - 125

20

180000 E

10000

ug/L

46

75 - 125

20

Chromium

ND

1000

1040

ug/L

104

75 - 125

20

Cobalt

6.9 J

1000

1030

ug/L

102

75 - 125

20

Copper

ND

1000

1030

ug/L

103

75 - 125

20

4900

10000

15500

ug/L

106

75 - 125

20

2.1 J

1000

1030

ug/L

103

75 - 125

20

Magnesium

78000 E

10000

ug/L

107

75 - 125

20

Manganese

940

1000

2000

ug/L

106

75 - 125

20

21 J

1000

1040

ug/L

102

75 - 125

20

Potassium

3100 J

10000

14000

ug/L

108

75 - 125

20

Selenium

ND

1000

1050

ug/L

105

75 - 125

20

Silver

ND

100

89.4

ug/L

89

75 - 125

20

Calcium

Iron
Lead

Nickel

180000 E 4

88900 E 4

TestAmerica St. Louis

Page 74 of 88

5
6

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60810
Sample Sample

Analyte

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 6010C - Metals (ICP) (Continued)


Lab Sample ID: 160-2968-6 MSD
Matrix: Water
Analysis Batch: 61576

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60810
Sample Sample

Spike

MSD MSD

%Rec.

Analyte

Result Qualifier

Added

Result Qualifier

Unit

Sodium

%Rec

Limits

RPD
RPD

Limit

14000

10000

24700

ug/L

108

75 - 125

20

Thallium

ND

200

217

ug/L

108

75 - 125

20

Vanadium

ND

1000

1050

ug/L

105

75 - 125

20

Zinc

7.0 J

1000

1050

ug/L

104

75 - 125

20

Lab Sample ID: 160-2968-6 MSD


Matrix: Water
Analysis Batch: 61576

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60810
Sample Sample

Analyte

Calcium
Iron
Magnesium

Result Qualifier

Spike
Added

MSD MSD
Result Qualifier

214000 4

%Rec.
Unit

Limits

10000

ug/L

123

75 - 125

20

10000

15900

ug/L

109

75 - 125

20

79000

10000

89900 4

ug/L

106

75 - 125

20

Client Sample ID: P2-202-SS


Prep Type: Dissolved
Prep Batch: 60808
Result Qualifier

Aluminum

ND

Antimony

ND

Arsenic

6.8 J

Barium

550

Beryllium
Cadmium

Spike
Added

%Rec.
Unit

%Rec

Limits

ug/L

100

75 - 125

500

522

ug/L

104

75 - 125

1000

1050

ug/L

104

75 - 125

1000

1620

ug/L

107

75 - 125

ND

1000

1020

ug/L

102

75 - 125

ND

1000

1030

ug/L

103

75 - 125

160000 E

10000

ug/L

147

75 - 125

Chromium

ND

1000

1040

ug/L

104

75 - 125

Cobalt

6.3 J

1000

1020

ug/L

101

75 - 125

Copper

ND

1000

1020

ug/L

102

75 - 125

4600

10000

15100

ug/L

105

75 - 125

2.9 J

1000

1040

ug/L

104

75 - 125

Magnesium

71000 E

10000

ug/L

127

75 - 125

Manganese

870

1000

1920

ug/L

105

75 - 125

20 J

1000

1030

ug/L

101

75 - 125

Potassium

3100 J

10000

13800

ug/L

107

75 - 125

Selenium

ND

1000

1060

ug/L

106

75 - 125

Silver

ND

100

89.6

ug/L

90

75 - 125

13000

10000

23400

75 - 125

Lead

Nickel

Sodium
Thallium

ND ^

Vanadium

ND

Zinc

6.1 J

10000

MS MS
Result Qualifier

9960

Iron

176000 E 4

84000 E 4

ug/L

105

209 ^

ug/L

104

75 - 125

1000

973

ug/L

97

75 - 125

1000

1040

ug/L

103

75 - 125

200

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 61388

Client Sample ID: P2-202-SS


Prep Type: Dissolved
Prep Batch: 60808
Sample Sample

Analyte

Calcium
Iron

Limit

5000

Sample Sample

Calcium

RPD
RPD

200000

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 61388
Analyte

%Rec

Result Qualifier

Spike
Added

200000

10000

4900

10000

MS MS
Result Qualifier

194000 4
14900

%Rec.
Unit

%Rec

Limits

ug/L

-49

75 - 125

ug/L

100

75 - 125

TestAmerica St. Louis

Page 75 of 88

7/29/2013

4
5
6
7
8
9
10
11
12
13

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 6010C - Metals (ICP) (Continued)


Lab Sample ID: 160-2968-6 MS
Matrix: Water
Analysis Batch: 61388

Client Sample ID: P2-202-SS


Prep Type: Dissolved
Prep Batch: 60808
Sample Sample

Spike

MS MS

%Rec.

Analyte

Result Qualifier

Added

Result Qualifier

Unit

Magnesium

76000

10000

82000 4

ug/L

60

Lab Sample ID: 160-2968-6 MSD


Matrix: Water
Analysis Batch: 61388

Limits

Result Qualifier

Spike

MSD MSD

RPD

Limit

ug/L

94

75 - 125

20

500

495

ug/L

99

75 - 125

20

1000

996

ug/L

99

75 - 125

20

1000

1530

ug/L

98

75 - 125

20

1000

961

ug/L

96

75 - 125

20

ND

1000

977

ug/L

98

75 - 125

20

160000 E

10000

ug/L

81

75 - 125

20

ND

1000

983

ug/L

98

75 - 125

20

Cobalt

6.3 J

1000

965

ug/L

96

75 - 125

20

Copper

ND

1000

960

ug/L

96

75 - 125

20

4600

Antimony

ND

Arsenic

6.8 J

Barium

550

Beryllium

ND

Cadmium
Calcium
Chromium

Iron

Result Qualifier

169000 E 4

Unit

%Rec

RPD

9430

ND

Added

%Rec.

10000

Aluminum

Limits

10000

14200

ug/L

96

75 - 125

20

2.9 J

1000

992

ug/L

99

75 - 125

20

Magnesium

71000 E

10000

ug/L

83

75 - 125

20

Manganese

870

1000

1820

ug/L

94

75 - 125

20

20 J

1000

983

ug/L

96

75 - 125

20

Potassium

3100 J

10000

13100

ug/L

100

75 - 125

20

Selenium

ND

1000

1000

ug/L

100

75 - 125

20

Silver

ND

100

85.1

ug/L

85

75 - 125

20

13000

10000

22200

ug/L

93

75 - 125

20

199 ^

ug/L

100

75 - 125

20

Lead

Nickel

Sodium

79700 E 4

200

Thallium

ND ^

Vanadium

ND

1000

923

ug/L

92

75 - 125

20

Zinc

6.1 J

1000

984

ug/L

98

75 - 125

20

Lab Sample ID: 160-2968-6 MSD


Matrix: Water
Analysis Batch: 61388

Client Sample ID: P2-202-SS


Prep Type: Dissolved
Prep Batch: 60808
Sample Sample

Analyte

Calcium

Result Qualifier

MSD MSD
Result Qualifier

201000 4

%Rec.
Unit

%Rec

RPD

Limits

RPD

Limit

200000

10000

ug/L

22

75 - 125

20

4900

10000

15100

ug/L

102

75 - 125

20

76000

10000

83100 4

ug/L

71

75 - 125

20

Iron
Magnesium

Spike
Added

Method: 7470A - Mercury (CVAA)


Lab Sample ID: MB 160-60787/1-A
Matrix: Water
Analysis Batch: 60965

Client Sample ID: Method Blank


Prep Type: Total/NA
Prep Batch: 60787
MB MB

Analyte

Mercury

Result Qualifier

ND

RL

MDL Unit

0.20

0.060 ug/L

Prepared

Analyzed

07/16/13 12:14

07/16/13 16:21

Dil Fac

TestAmerica St. Louis

Page 76 of 88

5
6

75 - 125

Client Sample ID: P2-202-SS


Prep Type: Dissolved
Prep Batch: 60808
Sample Sample

Analyte

%Rec

7/29/2013

7
8
9
10
11
12
13

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 7470A - Mercury (CVAA) (Continued)


Lab Sample ID: LCS 160-60787/2-A
Matrix: Water
Analysis Batch: 60965

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Prep Batch: 60787
Spike

Analyte

Added

Mercury

5.00

LCS LCS
Result Qualifier

5.90

%Rec.
Unit

ug/L

118

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 60965

Mercury

Result Qualifier

0.14 J

Spike

MS MS

Added

Result Qualifier

5.00

5.28

Mercury

Unit

ug/L

%Rec

103

Result Qualifier

0.14 J

Spike

MSD MSD

Added

Result Qualifier

5.00

5.48

%Rec.
Unit

ug/L

%Rec

107

Lab Sample ID: MB 160-60792/1-A


Matrix: Water
Analysis Batch: 61008

RPD

Limits

RPD

Limit

20

80 - 120

Client Sample ID: Method Blank


Prep Type: Total/NA
Prep Batch: 60792
MB MB

Analyte

Result Qualifier

Mercury

ND

RL

MDL Unit

0.20

0.060 ug/L

Lab Sample ID: LCS 160-60792/2-A


Matrix: Water
Analysis Batch: 61008

Prepared

Analyzed

07/16/13 12:21

07/17/13 11:11

Spike
Added

Mercury

5.00

LCS LCS
Result Qualifier

5.46

ug/L

109

Result Qualifier

0.20

Spike
Added

5.00

MS MS
Result Qualifier

5.46

ug/L

%Rec

105

Limits

80 - 120

Client Sample ID: P2-202-SS


Prep Type: Dissolved
Prep Batch: 60792
Sample Sample

Mercury

Limits

80 - 120

%Rec.
Unit

Lab Sample ID: 160-2968-6 MSD


Matrix: Water
Analysis Batch: 61008
Analyte

%Rec

Client Sample ID: P2-202-SS


Prep Type: Dissolved
Prep Batch: 60792
Sample Sample

Mercury

%Rec.
Unit

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 61008
Analyte

Dil Fac

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Prep Batch: 60792

Analyte

Result Qualifier

0.20

Spike
Added

5.00

MSD MSD
Result Qualifier

5.39

%Rec.
Unit

ug/L

%Rec

104

Limits

80 - 120

RPD
RPD

Limit

20

TestAmerica St. Louis

Page 77 of 88

7
8
9

Limits

80 - 120

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60787
Sample Sample

%Rec.

Lab Sample ID: 160-2968-6 MSD


Matrix: Water
Analysis Batch: 60965
Analyte

Limits

80 - 120

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Prep Batch: 60787
Sample Sample

Analyte

%Rec

7/29/2013

10
11
12
13

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 300.0 - Anions, Ion Chromatography


Lab Sample ID: MB 160-61027/9
Matrix: Water
Analysis Batch: 61027

Client Sample ID: Method Blank


Prep Type: Total/NA

MB MB
Analyte

Result Qualifier

Iodide

ND

RL

MDL Unit

1.0

0.10 mg/L

Prepared

LCS LCS

Added

Iodide

Result Qualifier

4.00

4.02

Unit

mg/L

101

Result Qualifier

0.14 J

Spike

MS MS

Added

Result Qualifier

4.00

3.98

mg/L

96

Result Qualifier

ND

Spike

MS MS

Added

Result Qualifier

4.00

3.85

mg/L

Iodide

%Rec

96

Limits

90 - 110

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

DU DU

Result Qualifier

Result Qualifier

0.14 J

0.134 J

RPD
Unit

RPD

Limit

20

mg/L

Lab Sample ID: MB 160-62158/3


Matrix: Water
Analysis Batch: 62158

Client Sample ID: Method Blank


Prep Type: Total/NA
MB MB

Analyte

Result Qualifier

RL

MDL Unit

Prepared

Analyzed

Dil Fac

Nitrate as N

ND

0.020

0.0040 mg/L

07/12/13 13:05

Chloride

ND

0.20

0.020 mg/L

07/12/13 13:05

Bromide

ND

0.25

0.025 mg/L

07/12/13 13:05

Sulfate

ND

0.50

0.050 mg/L

07/12/13 13:05

Lab Sample ID: LCS 160-62158/4


Matrix: Water
Analysis Batch: 62158

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Spike

Analyte

Nitrate as N

Added

LCS LCS
Result Qualifier

%Rec.
Unit

0.400

0.412

mg/L

Chloride

2.00

1.97

Bromide

2.00

2.01

Sulfate

8.00

7.74

%Rec

Limits

103

90 - 110

mg/L

98

90 - 110

mg/L

101

90 - 110

mg/L

97

90 - 110

TestAmerica St. Louis

Page 78 of 88

7
8
10
11
12

Limits

90 - 110

%Rec.
Unit

Lab Sample ID: 160-2968-6 DU


Matrix: Water
Analysis Batch: 61027
Analyte

%Rec

Client Sample ID: DUPLICATE 03


Prep Type: Total/NA
Sample Sample

Limits

90 - 110

%Rec.
Unit

Lab Sample ID: 160-2968-14 MS


Matrix: Water
Analysis Batch: 61027

Iodide

%Rec

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

%Rec.

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 61027

Iodide

Dil Fac

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Spike

Analyte

Analyzed

07/16/13 16:50

Lab Sample ID: LCS 160-61027/10


Matrix: Water
Analysis Batch: 61027
Analyte

7/29/2013

13

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 300.0 - Anions, Ion Chromatography (Continued)


Lab Sample ID: 160-2968-6 MS
Matrix: Water
Analysis Batch: 62158

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

Nitrate as N
Bromide

Result Qualifier

Spike
Added

ND

0.400

0.51

2.00

MS MS
Result Qualifier

0.365
2.72 F

Limits

91

90 - 110

mg/L

111

90 - 110

Result Qualifier

Spike
Added

MS MS
Result Qualifier

%Rec

0.400

0.538

mg/L

93

90 - 110

3.5

2.00

5.56

mg/L

101

90 - 110

Bromide

ND

2.00

1.78 F

mg/L

89

90 - 110

Lab Sample ID: 160-2968-6 DU


Matrix: Water
Analysis Batch: 62158
Sample Sample

Bromide

10
11

Client Sample ID: P2-202-SS


Prep Type: Total/NA

12

RPD

13

DU DU

Result Qualifier

Result Qualifier

Unit

RPD

Limit

ND

ND

mg/L

NC

20

0.51

0.501

mg/L

20

Method: 300.0 - Anions, Ion Chromatography - DL


Lab Sample ID: 160-2968-6 MS
Matrix: Water
Analysis Batch: 62158

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

Sulfate - DL

Result Qualifier

58

Spike
Added

80.0

MS MS
Result Qualifier

138

%Rec.
Unit

mg/L

Sulfate - DL

Result Qualifier

34

Spike
Added

80.0

MS MS
Result Qualifier

112

%Rec.
Unit

mg/L

Limits

90 - 110

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Sulfate - DL

%Rec

99

Lab Sample ID: 160-2968-6 DU


Matrix: Water
Analysis Batch: 62158
Analyte

Limits

90 - 110

Client Sample ID: P2-116-SS


Prep Type: Total/NA
Sample Sample

Analyte

%Rec

100

Lab Sample ID: 160-2968-10 MS


Matrix: Water
Analysis Batch: 62158

Result Qualifier

58

DU DU
Result Qualifier

57.9

RPD
Unit

mg/L

RPD

Limit

0.3

20

TestAmerica St. Louis

Page 79 of 88

8
9

Limits

0.17

Nitrate as N

%Rec.
Unit

Chloride

Analyte

Client Sample ID: P2-116-SS


Prep Type: Total/NA
Sample Sample

Nitrate as N

%Rec

mg/L

Lab Sample ID: 160-2968-10 MS


Matrix: Water
Analysis Batch: 62158
Analyte

%Rec.
Unit

7/29/2013

QC Sample Results

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 300.0 - Anions, Ion Chromatography - DL2


Lab Sample ID: 160-2968-6 MS
Matrix: Water
Analysis Batch: 62158

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Analyte

Chloride - DL2

Result Qualifier

84

Spike

MS MS

Added

Result Qualifier

200

281

mg/L

Limits

90 - 110

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Chloride - DL2

%Rec

98

Lab Sample ID: 160-2968-6 DU


Matrix: Water
Analysis Batch: 62158
Analyte

%Rec.
Unit

DU DU

Result Qualifier

Result Qualifier

84

82.8

Unit

RPD

Limit

20

mg/L

Client Sample ID: Method Blank


Prep Type: Total/NA
MB MB
Result Qualifier

0.350 J

RL

MDL Unit

1.3

0.14 mg/L

Prepared

Spike
Added

Alkalinity

400

LCS LCS
Result Qualifier

374

mg/L

%Rec

94

Limits

90 - 110

Client Sample ID: Lab Control Sample


Prep Type: Total/NA
Spike

Analyte

Added

Alkalinity

200

LLCS LLCS
Result Qualifier

187

%Rec.
Unit

mg/L

%Rec

94

Lab Sample ID: 160-2968-6 MS


Matrix: Water
Analysis Batch: 62899

Limits

90 - 110

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample
Result Qualifier

610 B

Spike
Added

20.0

MS MS
Result Qualifier

622 4

%Rec.
Unit

mg/L

%Rec

85

Lab Sample ID: 160-2968-6 DU


Matrix: Water
Analysis Batch: 62899

Limits

80 - 120

Client Sample ID: P2-202-SS


Prep Type: Total/NA
Sample Sample

Alkalinity

%Rec.
Unit

Lab Sample ID: LLCS 160-62899/2


Matrix: Water
Analysis Batch: 62899

Analyte

Dil Fac

Client Sample ID: Lab Control Sample


Prep Type: Total/NA

Analyte

Alkalinity

Analyzed

07/25/13 12:49

Lab Sample ID: LCS 160-62899/3


Matrix: Water
Analysis Batch: 62899

Analyte

8
9
10

Lab Sample ID: MB 160-62899/1


Matrix: Water
Analysis Batch: 62899

Alkalinity

RPD

Method: 310.1 - Alkalinity

Analyte

Result Qualifier

610 B

DU DU
Result Qualifier

599

RPD
Unit

mg/L

RPD

Limit

20

TestAmerica St. Louis

Page 80 of 88

7/29/2013

11
12
13

QC Association Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

GC/MS VOA
Analysis Batch: 60813

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

8260C

160-2968-2

P2-104-SS

Total/NA

Water

8260C

160-2968-3

P2-101-SS

Total/NA

Water

8260C

160-2968-4

P2-104-SD

Total/NA

Water

8260C

160-2968-4

P2-104-SD

Total/NA

Water

8260C

160-2968-5

FB@P2-202-SS

Total/NA

Water

8260C

160-2968-6

P2-202-SS

Total/NA

Water

8260C

160-2968-6 MS

P2-202-SS

Total/NA

Water

8260C

160-2968-6 MSD

P2-202-SS

Total/NA

Water

8260C

160-2968-7

D-83

Total/NA

Water

8260C

160-2968-8

MW-1204

Total/NA

Water

8260C

160-2968-9

S-82

Total/NA

Water

8260C

160-2968-10

P2-116-SS

Total/NA

Water

8260C

160-2968-11

D-93

Total/NA

Water

8260C

160-2968-12

I-9

Total/NA

Water

8260C

160-2968-13

P2-115-SS

Total/NA

Water

8260C

160-2968-14

DUPLICATE 03

Total/NA

Water

8260C

160-2968-15

TRIP BLANK

Total/NA

Water

8260C

LCS 160-60813/4-A

Lab Control Sample

Total/NA

Water

8260C

MB 160-60813/3-A

Method Blank

Total/NA

Water

8260C

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-2

P2-104-SS

Total/NA

Water

8260C

160-2968-4

P2-104-SD

Total/NA

Water

8260C

160-2968-8

MW-1204

Total/NA

Water

8260C

160-2968-8

MW-1204

Total/NA

Water

8260C

LCS 160-61806/4-A

Lab Control Sample

Total/NA

Water

8260C

MB 160-61806/3-A

Method Blank

Total/NA

Water

8260C

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

7470A

160-2968-2

P2-104-SS

Total/NA

Water

7470A

160-2968-3

P2-101-SS

Total/NA

Water

7470A

160-2968-4

P2-104-SD

Total/NA

Water

7470A

160-2968-6

P2-202-SS

Total/NA

Water

7470A

160-2968-6 MS

P2-202-SS

Total/NA

Water

7470A

160-2968-6 MSD

P2-202-SS

Total/NA

Water

7470A

160-2968-7

D-83

Total/NA

Water

7470A

160-2968-8

MW-1204

Total/NA

Water

7470A

160-2968-9

S-82

Total/NA

Water

7470A

160-2968-10

P2-116-SS

Total/NA

Water

7470A

160-2968-11

D-93

Total/NA

Water

7470A

160-2968-12

I-9

Total/NA

Water

7470A

160-2968-13

P2-115-SS

Total/NA

Water

7470A

160-2968-14

DUPLICATE 03

Total/NA

Water

7470A

LCS 160-60787/2-A

Lab Control Sample

Total/NA

Water

7470A

Prep Batch

5
6
7
8
9
10
11
12
13

Analysis Batch: 61806


Prep Batch

Metals
Prep Batch: 60787
Prep Batch

TestAmerica St. Louis

Page 81 of 88

7/29/2013

QC Association Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Metals (Continued)
Prep Batch: 60787 (Continued)

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

MB 160-60787/1-A

Method Blank

Total/NA

Water

7470A

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Dissolved

Water

7470A

160-2968-2

P2-104-SS

Dissolved

Water

7470A

160-2968-3

P2-101-SS

Dissolved

Water

7470A

160-2968-4

P2-104-SD

Dissolved

Water

7470A

160-2968-6

P2-202-SS

Dissolved

Water

7470A

160-2968-6 MS

P2-202-SS

Dissolved

Water

7470A

160-2968-6 MSD

P2-202-SS

Dissolved

Water

7470A

160-2968-7

D-83

Dissolved

Water

7470A

160-2968-8

MW-1204

Dissolved

Water

7470A

160-2968-9

S-82

Dissolved

Water

7470A

160-2968-10

P2-116-SS

Dissolved

Water

7470A

160-2968-11

D-93

Dissolved

Water

7470A

160-2968-12

I-9

Dissolved

Water

7470A

160-2968-13

P2-115-SS

Dissolved

Water

7470A

160-2968-14

DUPLICATE 03

Dissolved

Water

7470A

LCS 160-60792/2-A

Lab Control Sample

Total/NA

Water

7470A

MB 160-60792/1-A

Method Blank

Total/NA

Water

7470A

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Dissolved

Water

3010A

160-2968-2

P2-104-SS

Dissolved

Water

3010A

160-2968-3

P2-101-SS

Dissolved

Water

3010A

160-2968-4

P2-104-SD

Dissolved

Water

3010A

160-2968-6

P2-202-SS

Dissolved

Water

3010A

160-2968-6 MS

P2-202-SS

Dissolved

Water

3010A

160-2968-6 MSD

P2-202-SS

Dissolved

Water

3010A

160-2968-7

D-83

Dissolved

Water

3010A

160-2968-8

MW-1204

Dissolved

Water

3010A

160-2968-9

S-82

Dissolved

Water

3010A

160-2968-10

P2-116-SS

Dissolved

Water

3010A

160-2968-11

D-93

Dissolved

Water

3010A

160-2968-12

I-9

Dissolved

Water

3010A

160-2968-13

P2-115-SS

Dissolved

Water

3010A

160-2968-14

DUPLICATE 03

Dissolved

Water

3010A

LCS 160-60808/2-A

Lab Control Sample

Total/NA

Water

3010A

MB 160-60808/1-A

Method Blank

Total/NA

Water

3010A

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

3010A

160-2968-2

P2-104-SS

Total/NA

Water

3010A

160-2968-3

P2-101-SS

Total/NA

Water

3010A

160-2968-4

P2-104-SD

Total/NA

Water

3010A

160-2968-6

P2-202-SS

Total/NA

Water

3010A

160-2968-6 MS

P2-202-SS

Total/NA

Water

3010A

160-2968-6 MSD

P2-202-SS

Total/NA

Water

3010A

Prep Batch

Prep Batch: 60792


Prep Batch

7
8
9
10
11
12
13

Prep Batch: 60808


Prep Batch

Prep Batch: 60810


Prep Batch

TestAmerica St. Louis

Page 82 of 88

7/29/2013

QC Association Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Metals (Continued)
Prep Batch: 60810 (Continued)

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

Prep Batch

160-2968-7

D-83

Total/NA

Water

3010A

160-2968-8

MW-1204

Total/NA

Water

3010A

160-2968-9

S-82

Total/NA

Water

3010A

160-2968-10

P2-116-SS

Total/NA

Water

3010A

160-2968-11

D-93

Total/NA

Water

3010A

160-2968-12

I-9

Total/NA

Water

3010A

160-2968-13

P2-115-SS

Total/NA

Water

3010A

160-2968-14

DUPLICATE 03

Total/NA

Water

3010A

LCS 160-60810/2-A

Lab Control Sample

Total/NA

Water

3010A

MB 160-60810/1-A

Method Blank

Total/NA

Water

3010A

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

7470A

60787

160-2968-2

P2-104-SS

Total/NA

Water

7470A

60787

160-2968-3

P2-101-SS

Total/NA

Water

7470A

60787

160-2968-4

P2-104-SD

Total/NA

Water

7470A

60787

160-2968-6

P2-202-SS

Total/NA

Water

7470A

60787

160-2968-6 MS

P2-202-SS

Total/NA

Water

7470A

60787

160-2968-6 MSD

P2-202-SS

Total/NA

Water

7470A

60787

160-2968-7

D-83

Total/NA

Water

7470A

60787

160-2968-8

MW-1204

Total/NA

Water

7470A

60787

160-2968-9

S-82

Total/NA

Water

7470A

60787

160-2968-10

P2-116-SS

Total/NA

Water

7470A

60787

160-2968-11

D-93

Total/NA

Water

7470A

60787

160-2968-12

I-9

Total/NA

Water

7470A

60787

160-2968-13

P2-115-SS

Total/NA

Water

7470A

60787

160-2968-14

DUPLICATE 03

Total/NA

Water

7470A

60787

LCS 160-60787/2-A

Lab Control Sample

Total/NA

Water

7470A

60787

MB 160-60787/1-A

Method Blank

Total/NA

Water

7470A

60787

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Dissolved

Water

7470A

60792

160-2968-2

P2-104-SS

Dissolved

Water

7470A

60792

160-2968-3

P2-101-SS

Dissolved

Water

7470A

60792

160-2968-4

P2-104-SD

Dissolved

Water

7470A

60792

160-2968-6

P2-202-SS

Dissolved

Water

7470A

60792

160-2968-6 MS

P2-202-SS

Dissolved

Water

7470A

60792

160-2968-6 MSD

P2-202-SS

Dissolved

Water

7470A

60792

160-2968-7

D-83

Dissolved

Water

7470A

60792

160-2968-8

MW-1204

Dissolved

Water

7470A

60792

160-2968-9

S-82

Dissolved

Water

7470A

60792

160-2968-10

P2-116-SS

Dissolved

Water

7470A

60792

160-2968-11

D-93

Dissolved

Water

7470A

60792

160-2968-12

I-9

Dissolved

Water

7470A

60792

160-2968-13

P2-115-SS

Dissolved

Water

7470A

60792

160-2968-14

DUPLICATE 03

Dissolved

Water

7470A

60792

LCS 160-60792/2-A

Lab Control Sample

Total/NA

Water

7470A

60792

MB 160-60792/1-A

Method Blank

Total/NA

Water

7470A

60792

5
6
7
8
9

Analysis Batch: 60965

10
Prep Batch

Analysis Batch: 61008


Prep Batch

TestAmerica St. Louis

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13

QC Association Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Metals (Continued)
Analysis Batch: 61388

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

Prep Batch

160-2968-1

P2-113-SS

Dissolved

Water

6010C

60808

160-2968-1

P2-113-SS

Dissolved

Water

6010C

60808

160-2968-2

P2-104-SS

Dissolved

Water

6010C

60808

160-2968-2

P2-104-SS

Dissolved

Water

6010C

60808

160-2968-3

P2-101-SS

Dissolved

Water

6010C

60808

160-2968-3

P2-101-SS

Dissolved

Water

6010C

60808

160-2968-4

P2-104-SD

Dissolved

Water

6010C

60808

160-2968-4

P2-104-SD

Dissolved

Water

6010C

60808

160-2968-6

P2-202-SS

Dissolved

Water

6010C

60808

160-2968-6

P2-202-SS

Dissolved

Water

6010C

60808

160-2968-6 MS

P2-202-SS

Dissolved

Water

6010C

60808

160-2968-6 MS

P2-202-SS

Dissolved

Water

6010C

60808

160-2968-6 MSD

P2-202-SS

Dissolved

Water

6010C

60808

160-2968-6 MSD

P2-202-SS

Dissolved

Water

6010C

60808

160-2968-7

D-83

Dissolved

Water

6010C

60808

160-2968-7

D-83

Dissolved

Water

6010C

60808

160-2968-8

MW-1204

Dissolved

Water

6010C

60808

160-2968-8

MW-1204

Dissolved

Water

6010C

60808

160-2968-9

S-82

Dissolved

Water

6010C

60808

160-2968-9

S-82

Dissolved

Water

6010C

60808

160-2968-10

P2-116-SS

Dissolved

Water

6010C

60808

160-2968-11

D-93

Dissolved

Water

6010C

60808

160-2968-11

D-93

Dissolved

Water

6010C

60808

160-2968-12

I-9

Dissolved

Water

6010C

60808

160-2968-12

I-9

Dissolved

Water

6010C

60808

160-2968-13

P2-115-SS

Dissolved

Water

6010C

60808

160-2968-13

P2-115-SS

Dissolved

Water

6010C

60808

160-2968-14

DUPLICATE 03

Dissolved

Water

6010C

60808

160-2968-14

DUPLICATE 03

Dissolved

Water

6010C

60808

LCS 160-60808/2-A

Lab Control Sample

Total/NA

Water

6010C

60808

MB 160-60808/1-A

Method Blank

Total/NA

Water

6010C

60808

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-8

MW-1204

Dissolved

Water

6010C

60808

160-2968-11

D-93

Dissolved

Water

6010C

60808

160-2968-12

I-9

Dissolved

Water

6010C

60808

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

6010C

60810

160-2968-1

P2-113-SS

Total/NA

Water

6010C

60810

160-2968-2

P2-104-SS

Total/NA

Water

6010C

60810

160-2968-2

P2-104-SS

Total/NA

Water

6010C

60810

160-2968-3

P2-101-SS

Total/NA

Water

6010C

60810

160-2968-3

P2-101-SS

Total/NA

Water

6010C

60810

160-2968-4

P2-104-SD

Total/NA

Water

6010C

60810

160-2968-4

P2-104-SD

Total/NA

Water

6010C

60810

160-2968-6

P2-202-SS

Total/NA

Water

6010C

60810

160-2968-6

P2-202-SS

Total/NA

Water

6010C

60810

160-2968-6 MS

P2-202-SS

Total/NA

Water

6010C

60810

Analysis Batch: 61428


Prep Batch

Analysis Batch: 61576


Prep Batch

TestAmerica St. Louis

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QC Association Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Metals (Continued)
Analysis Batch: 61576 (Continued)

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

Prep Batch

160-2968-6 MS

P2-202-SS

Total/NA

Water

6010C

60810

160-2968-6 MSD

P2-202-SS

Total/NA

Water

6010C

60810

160-2968-6 MSD

P2-202-SS

Total/NA

Water

6010C

60810

160-2968-7

D-83

Total/NA

Water

6010C

60810

160-2968-7

D-83

Total/NA

Water

6010C

60810

160-2968-8

MW-1204

Total/NA

Water

6010C

60810

160-2968-8

MW-1204

Total/NA

Water

6010C

60810

160-2968-9

S-82

Total/NA

Water

6010C

60810

160-2968-9

S-82

Total/NA

Water

6010C

60810

160-2968-10

P2-116-SS

Total/NA

Water

6010C

60810

160-2968-11

D-93

Total/NA

Water

6010C

60810

160-2968-11

D-93

Total/NA

Water

6010C

60810

160-2968-12

I-9

Total/NA

Water

6010C

60810

160-2968-12

I-9

Total/NA

Water

6010C

60810

160-2968-13

P2-115-SS

Total/NA

Water

6010C

60810

160-2968-13

P2-115-SS

Total/NA

Water

6010C

60810

160-2968-14

DUPLICATE 03

Total/NA

Water

6010C

60810

160-2968-14

DUPLICATE 03

Total/NA

Water

6010C

60810

LCS 160-60810/2-A

Lab Control Sample

Total/NA

Water

6010C

60810

MB 160-60810/1-A

Method Blank

Total/NA

Water

6010C

60810

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

300.0

160-2968-2

P2-104-SS

Total/NA

Water

300.0

160-2968-3

P2-101-SS

Total/NA

Water

300.0

160-2968-4

P2-104-SD

Total/NA

Water

300.0

160-2968-6

P2-202-SS

Total/NA

Water

300.0

160-2968-6 DU

P2-202-SS

Total/NA

Water

300.0

160-2968-6 MS

P2-202-SS

Total/NA

Water

300.0

160-2968-7

D-83

Total/NA

Water

300.0

160-2968-8

MW-1204

Total/NA

Water

300.0

160-2968-9

S-82

Total/NA

Water

300.0

160-2968-10

P2-116-SS

Total/NA

Water

300.0

160-2968-11

D-93

Total/NA

Water

300.0

160-2968-12

I-9

Total/NA

Water

300.0

160-2968-13

P2-115-SS

Total/NA

Water

300.0

160-2968-14

DUPLICATE 03

Total/NA

Water

300.0

160-2968-14 MS

DUPLICATE 03

Total/NA

Water

300.0

LCS 160-61027/10

Lab Control Sample

Total/NA

Water

300.0

MB 160-61027/9

Method Blank

Total/NA

Water

300.0

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

300.0

160-2968-1 - DL

P2-113-SS

Total/NA

Water

300.0

160-2968-2

P2-104-SS

Total/NA

Water

300.0

160-2968-3

P2-101-SS

Total/NA

Water

300.0

General Chemistry
Analysis Batch: 61027
Prep Batch

Analysis Batch: 62158


Prep Batch

TestAmerica St. Louis

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QC Association Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

General Chemistry (Continued)


Analysis Batch: 62158 (Continued)

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-3 - DL2

P2-101-SS

Total/NA

Water

300.0

160-2968-4

P2-104-SD

Total/NA

Water

300.0

160-2968-4 - DL

P2-104-SD

Total/NA

Water

300.0

160-2968-4 - DL2

P2-104-SD

Total/NA

Water

300.0

160-2968-6

P2-202-SS

Total/NA

Water

300.0

160-2968-6 - DL

P2-202-SS

Total/NA

Water

300.0

160-2968-6 - DL2

P2-202-SS

Total/NA

Water

300.0

160-2968-6 DU

P2-202-SS

Total/NA

Water

300.0

160-2968-6 DU - DL

P2-202-SS

Total/NA

Water

300.0

160-2968-6 DU - DL2

P2-202-SS

Total/NA

Water

300.0

160-2968-6 MS

P2-202-SS

Total/NA

Water

300.0

160-2968-6 MS - DL

P2-202-SS

Total/NA

Water

300.0

160-2968-6 MS - DL2

P2-202-SS

Total/NA

Water

300.0

160-2968-7

D-83

Total/NA

Water

300.0

160-2968-7 - DL

D-83

Total/NA

Water

300.0

160-2968-8

MW-1204

Total/NA

Water

300.0

160-2968-8 - DL2

MW-1204

Total/NA

Water

300.0

160-2968-9

S-82

Total/NA

Water

300.0

160-2968-9 - DL2

S-82

Total/NA

Water

300.0

160-2968-10

P2-116-SS

Total/NA

Water

300.0

160-2968-10 - DL

P2-116-SS

Total/NA

Water

300.0

160-2968-10 MS

P2-116-SS

Total/NA

Water

300.0

160-2968-10 MS - DL

P2-116-SS

Total/NA

Water

300.0

160-2968-11

D-93

Total/NA

Water

300.0

160-2968-11 - DL2

D-93

Total/NA

Water

300.0

160-2968-12

I-9

Total/NA

Water

300.0

160-2968-12 - DL2

I-9

Total/NA

Water

300.0

160-2968-13

P2-115-SS

Total/NA

Water

300.0

160-2968-13 - DL2

P2-115-SS

Total/NA

Water

300.0

160-2968-14

DUPLICATE 03

Total/NA

Water

300.0

160-2968-14 - DL

DUPLICATE 03

Total/NA

Water

300.0

LCS 160-62158/4

Lab Control Sample

Total/NA

Water

300.0

MB 160-62158/3

Method Blank

Total/NA

Water

300.0

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

160-2968-1

P2-113-SS

Total/NA

Water

310.1

160-2968-2

P2-104-SS

Total/NA

Water

310.1

160-2968-3

P2-101-SS

Total/NA

Water

310.1

160-2968-4

P2-104-SD

Total/NA

Water

310.1

160-2968-6

P2-202-SS

Total/NA

Water

310.1

160-2968-6 DU

P2-202-SS

Total/NA

Water

310.1

160-2968-6 MS

P2-202-SS

Total/NA

Water

310.1

160-2968-7

D-83

Total/NA

Water

310.1

160-2968-8 - DL

MW-1204

Total/NA

Water

310.1

160-2968-9

S-82

Total/NA

Water

310.1

160-2968-10

P2-116-SS

Total/NA

Water

310.1

160-2968-11 - DL

D-93

Total/NA

Water

310.1

160-2968-12 - DL

I-9

Total/NA

Water

310.1

160-2968-13

P2-115-SS

Total/NA

Water

310.1

160-2968-14

DUPLICATE 03

Total/NA

Water

310.1

Prep Batch

5
6
7
8
9
10
11
12
13

Analysis Batch: 62899


Prep Batch

TestAmerica St. Louis

Page 86 of 88

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QC Association Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

General Chemistry (Continued)


Analysis Batch: 62899 (Continued)

Lab Sample ID

Client Sample ID

Prep Type

Matrix

Method

LCS 160-62899/3

Lab Control Sample

Total/NA

Water

310.1

LLCS 160-62899/2

Lab Control Sample

Total/NA

Water

310.1

MB 160-62899/1

Method Blank

Total/NA

Water

310.1

Prep Batch

5
6
7
8
9
10
11
12
13

TestAmerica St. Louis

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Surrogate Summary

Client: Engineering Management Support, Inc.


Project/Site: West Lake Landfill

TestAmerica Job ID: 160-2968-1

2
3

Method: 8260C - Volatile Organic Compounds by GC/MS


Matrix: Water

Prep Type: Total/NA

Percent Surrogate Recovery (Acceptance Limits)


12DCE

BFB

DBFM

TOL

(82-132)

(82-121)

(85-119)

(85-115)

P2-113-SS

115

100

106

103

P2-104-SS

108

98

99

97

160-2968-2

P2-104-SS

94

89

95

96

160-2968-3

P2-101-SS

109

103

101

100

160-2968-4

P2-104-SD

110

105

102

103

160-2968-4

P2-104-SD

118

102

102

101

160-2968-4

P2-104-SD

98

94

98

101

160-2968-5

FB@P2-202-SS

109

102

98

101

160-2968-6

P2-202-SS

118

110

109

107

160-2968-6 MS

P2-202-SS

110

102

100

101

160-2968-6 MSD

P2-202-SS

112

102

105

100

160-2968-7

D-83

119

107

104

101

160-2968-8

MW-1204

109

98

98

98

160-2968-8

MW-1204

97

95

98

100

160-2968-8

MW-1204

94

83

92

96

160-2968-9

S-82

111

103

99

101

160-2968-10

P2-116-SS

121

110

107

110

160-2968-11

D-93

113

103

101

102

160-2968-12

I-9

114

101

104

99

160-2968-13

P2-115-SS

113

104

103

104

160-2968-14

DUPLICATE 03

117

98

101

95

160-2968-15

TRIP BLANK

106

98

99

99

LCS 160-60813/4-A

Lab Control Sample

107

100

99

99

LCS 160-61806/4-A

Lab Control Sample

92

92

92

99

MB 160-60813/3-A

Method Blank

106

99

103

104

MB 160-61806/3-A

Method Blank

100

87

97

100

Lab Sample ID

Client Sample ID

160-2968-1
160-2968-2

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6
7
8
9
10
11
12
13

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)


BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)

TestAmerica St. Louis

Page 88 of 88

7/29/2013

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